DE1230001B - Verfahren zur Herstellung von Trimethylphosphit - Google Patents

Verfahren zur Herstellung von Trimethylphosphit

Info

Publication number
DE1230001B
DE1230001B DEH53713A DEH0053713A DE1230001B DE 1230001 B DE1230001 B DE 1230001B DE H53713 A DEH53713 A DE H53713A DE H0053713 A DEH0053713 A DE H0053713A DE 1230001 B DE1230001 B DE 1230001B
Authority
DE
Germany
Prior art keywords
phosphite
methanol
flask
trimethyl phosphite
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
DEH53713A
Other languages
German (de)
English (en)
Other versions
DE1230001C2 (enExample
Inventor
Charles Francis Baranauckas
Russell Leo Kenneth Carr
James John Hodan
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hooker Chemical Corp
Original Assignee
Hooker Chemical Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hooker Chemical Corp filed Critical Hooker Chemical Corp
Publication of DE1230001B publication Critical patent/DE1230001B/de
Application granted granted Critical
Publication of DE1230001C2 publication Critical patent/DE1230001C2/de
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/025—Purification; Separation; Stabilisation; Desodorisation of organo-phosphorus compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/08—Esters of oxyacids of phosphorus
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/08—Esters of oxyacids of phosphorus
    • C07F9/09—Esters of phosphoric acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/08—Esters of oxyacids of phosphorus
    • C07F9/141—Esters of phosphorous acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/08—Esters of oxyacids of phosphorus
    • C07F9/141—Esters of phosphorous acids
    • C07F9/142—Esters of phosphorous acids with hydroxyalkyl compounds without further substituents on alkyl
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
    • C07F9/165—Esters of thiophosphoric acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
    • C07F9/165—Esters of thiophosphoric acids
    • C07F9/17—Esters of thiophosphoric acids with hydroxyalkyl compounds without further substituents on alkyl
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/06—Phosphorus compounds without P—C bonds
    • C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
    • C07F9/201—Esters of thiophosphorus acids
    • C07F9/202—Esters of thiophosphorus acids with hydroxyl compounds without further substituents on alkyl
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/40—Esters thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/6564—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
    • C07F9/6571—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
    • C07F9/6574—Esters of oxyacids of phosphorus

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DEH53713A 1960-12-23 1961-12-19 Verfahren zur Herstellung von Trimethylphosphit Granted DE1230001B (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US77812A US3184495A (en) 1960-12-23 1960-12-23 Process for the preparation and recovery of trimethyl phosphite and derivatives thereof

Publications (2)

Publication Number Publication Date
DE1230001B true DE1230001B (de) 1966-12-08
DE1230001C2 DE1230001C2 (enExample) 1967-09-14

Family

ID=22140207

Family Applications (2)

Application Number Title Priority Date Filing Date
DEH53713A Granted DE1230001B (de) 1960-12-23 1961-12-19 Verfahren zur Herstellung von Trimethylphosphit
DEH44429A Granted DE1230414B (de) 1960-12-23 1961-12-19 Verfahren zur Abtrennung von Trimethylphosphit aus Reaktionsgemischen, welche bei der Herstellung von Trimethylphosphit erhalten werden

Family Applications After (1)

Application Number Title Priority Date Filing Date
DEH44429A Granted DE1230414B (de) 1960-12-23 1961-12-19 Verfahren zur Abtrennung von Trimethylphosphit aus Reaktionsgemischen, welche bei der Herstellung von Trimethylphosphit erhalten werden

Country Status (7)

Country Link
US (1) US3184495A (enExample)
BE (1) BE611708A (enExample)
CH (4) CH408893A (enExample)
DE (2) DE1230001B (enExample)
FR (1) FR1312167A (enExample)
GB (1) GB1015201A (enExample)
NL (1) NL272868A (enExample)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3451968A (en) * 1965-07-26 1969-06-24 Diamond Shamrock Corp Composition comprising urea-formaldehyde resin,triester of h3po4,and alkyl phosphite
US3972866A (en) 1972-06-09 1976-08-03 Imperial Chemical Industries Limited Polymerization process
IL51178A (en) * 1976-12-28 1981-01-30 Yeda Res & Dev Polyhydroxylated 0,0-dialkyl phosphonoacetals and process for their preparation
US4218405A (en) * 1978-04-26 1980-08-19 Olin Corporation Halogenated tertiary phosphite esters
EP0319617B1 (en) * 1987-12-02 1994-05-11 Mobil Oil Corporation Use of reaction products of trialkyl phosphites with elemental sulfur and process for making same
CN107840858A (zh) * 2017-10-28 2018-03-27 南通江山农药化工股份有限公司 亚磷酸三甲酯连续减压精馏工艺
CN112979696B (zh) * 2019-12-17 2022-05-10 张家港市国泰华荣化工新材料有限公司 一种三（2-甲基烯丙基）亚磷酸酯的合成方法
CN116514871A (zh) * 2022-01-21 2023-08-01 中国石油化工股份有限公司 一种降低有机亚磷酸酯杂质含量的方法及制备的有机亚磷酸酯和应用
CN117599596B (zh) * 2022-08-24 2026-04-21 湖北富博化工有限责任公司 一种硝基甲烷尾气的治理方法及硝基甲烷的生产方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1075584B (de) * 1960-02-18 Hooker Chemical Corporation, Niagara Falls, N. Y. (V. St. A.) Verfahren zur Herstellung von tertiären aliphatischen Estern der phosphorigen Säure
GB933029A (en) * 1958-11-26 1963-07-31 Albright & Wilson Mfg Ltd Process for the manufacture of trimethyl phosphites
US2970166A (en) * 1959-10-20 1961-01-31 Montrose Chemical Company Preparation of trimethyl phosphite and triethyl phosphite

Also Published As

Publication number Publication date
FR1312167A (fr) 1962-12-14
GB1015201A (en) 1965-12-31
NL272868A (enExample)
DE1230001C2 (enExample) 1967-09-14
CH469026A (de) 1969-02-28
CH441256A (de) 1967-08-15
DE1230414B (de) 1966-12-15
CH408893A (de) 1966-03-15
BE611708A (fr) 1962-04-16
DE1230414C2 (enExample) 1967-07-13
US3184495A (en) 1965-05-18
CH423739A (de) 1966-11-15

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