DE1228611B - Verfahren zur Herstellung von N, N-Di-(beta-chlor-aethyl)-aminophosphorsaeuredichlorid - Google Patents
Verfahren zur Herstellung von N, N-Di-(beta-chlor-aethyl)-aminophosphorsaeuredichloridInfo
- Publication number
- DE1228611B DE1228611B DEM64458A DEM0064458A DE1228611B DE 1228611 B DE1228611 B DE 1228611B DE M64458 A DEM64458 A DE M64458A DE M0064458 A DEM0064458 A DE M0064458A DE 1228611 B DE1228611 B DE 1228611B
- Authority
- DE
- Germany
- Prior art keywords
- chloro
- ethyl
- acid dichloride
- phosphorus oxychloride
- production
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 7
- 238000004519 manufacturing process Methods 0.000 title description 4
- CTCXOWMDEYGDJQ-UHFFFAOYSA-N ClCCN(CCCl)OP(O)(O)=O Chemical compound ClCCN(CCCl)OP(O)(O)=O CTCXOWMDEYGDJQ-UHFFFAOYSA-N 0.000 title description 3
- XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 claims description 26
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 8
- 238000006243 chemical reaction Methods 0.000 claims description 8
- 239000002253 acid Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 5
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
- -1 N, N-disubstituted aminophosphoric acid Chemical class 0.000 description 5
- 239000002826 coolant Substances 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- 230000001174 ascending effect Effects 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 125000001340 2-chloroethyl group Chemical group [H]C([H])(Cl)C([H])([H])* 0.000 description 1
- JZTPOMIFAFKKSK-UHFFFAOYSA-N O-phosphonohydroxylamine Chemical compound NOP(O)(O)=O JZTPOMIFAFKKSK-UHFFFAOYSA-N 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000006277 sulfonation reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/22—Amides of acids of phosphorus
- C07F9/26—Amides of acids of phosphorus containing P-halide groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Luminescent Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RO4767764 | 1964-03-18 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1228611B true DE1228611B (de) | 1966-11-17 |
Family
ID=20086441
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEM64458A Pending DE1228611B (de) | 1964-03-18 | 1965-03-09 | Verfahren zur Herstellung von N, N-Di-(beta-chlor-aethyl)-aminophosphorsaeuredichlorid |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE660772A (enrdf_load_stackoverflow) |
| CH (1) | CH434252A (enrdf_load_stackoverflow) |
| DE (1) | DE1228611B (enrdf_load_stackoverflow) |
| GB (1) | GB1030836A (enrdf_load_stackoverflow) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2558185C3 (de) | 1975-12-23 | 1982-03-18 | Wacker-Chemie GmbH, 8000 München | Verfahren zur Herstellung von Phosphorsäure-dimethylamid-dichlorid oder Phosphorsäure-bis-(dimethylamid)-chlorid |
-
1965
- 1965-03-05 GB GB954165A patent/GB1030836A/en not_active Expired
- 1965-03-08 BE BE660772D patent/BE660772A/xx unknown
- 1965-03-09 DE DEM64458A patent/DE1228611B/de active Pending
- 1965-03-17 CH CH375365A patent/CH434252A/fr unknown
Non-Patent Citations (1)
| Title |
|---|
| None * |
Also Published As
| Publication number | Publication date |
|---|---|
| CH434252A (fr) | 1967-04-30 |
| GB1030836A (en) | 1966-05-25 |
| BE660772A (enrdf_load_stackoverflow) | 1965-07-01 |
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