DE122474C - - Google Patents

Info

Publication number

DE122474C

DE122474C DENDAT122474D DE122474DA DE122474C DE 122474 C DE122474 C DE 122474C DE NDAT122474 D DENDAT122474 D DE NDAT122474D DE 122474D A DE122474D A DE 122474DA DE 122474 C DE122474 C DE 122474C

Authority

DE

Germany

Prior art keywords

hydrochloric acid

solution

parts

base

yellow

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Active

Links

• Espacenet
• Global Dossier
• DPMA
• Discuss

• VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical class Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 31
• WSFSSNUMVMOOMR-UHFFFAOYSA-N formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 10
• 238000007792 addition Methods 0.000 claims description 2
• 125000003118 aryl group Chemical group 0.000 claims 1
• 238000000034 method Methods 0.000 claims 1
• 150000003142 primary aromatic amines Chemical class 0.000 claims 1
• 235000011167 hydrochloric acid Nutrition 0.000 description 14
• 239000000243 solution Substances 0.000 description 11
• 239000000126 substance Substances 0.000 description 7
• 239000002253 acid Substances 0.000 description 6
• 239000000975 dye Substances 0.000 description 5
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
• BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 4
• 229920000742 Cotton Polymers 0.000 description 3
• 150000007513 acids Chemical class 0.000 description 3
• 238000001816 cooling Methods 0.000 description 3
• 229910052500 inorganic mineral Inorganic materials 0.000 description 3
• 238000002844 melting Methods 0.000 description 3
• 239000011707 mineral Substances 0.000 description 3
• 239000011780 sodium chloride Substances 0.000 description 3
• 238000003756 stirring Methods 0.000 description 3
• QSNSCYSYFYORTR-UHFFFAOYSA-N 4-Chloroaniline Chemical compound NC1=CC=C(Cl)C=C1 QSNSCYSYFYORTR-UHFFFAOYSA-N 0.000 description 2
• SXPSZIHEWFTLEQ-UHFFFAOYSA-N Tröger's base Chemical compound C12=CC=C(C)C=C2CN2C3=CC=C(C)C=C3CN1C2 SXPSZIHEWFTLEQ-UHFFFAOYSA-N 0.000 description 2
• -1 acids salts Chemical class 0.000 description 2
• PAYRUJLWNCNPSJ-UHFFFAOYSA-N aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
• 238000009835 boiling Methods 0.000 description 2
• 239000006227 byproduct Substances 0.000 description 2
• SUXCALIDMIIJCK-UHFFFAOYSA-L disodium;4-amino-3-[[4-[4-[(1-amino-4-sulfonatonaphthalen-2-yl)diazenyl]-3-methylphenyl]-2-methylphenyl]diazenyl]naphthalene-1-sulfonate Chemical compound [Na+].[Na+].C1=CC=CC2=C(N)C(N=NC3=CC=C(C=C3C)C=3C=C(C(=CC=3)N=NC=3C(=C4C=CC=CC4=C(C=3)S([O-])(=O)=O)N)C)=CC(S([O-])(=O)=O)=C21 SUXCALIDMIIJCK-UHFFFAOYSA-L 0.000 description 2
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
• 239000008098 formaldehyde solution Substances 0.000 description 2
• 238000010438 heat treatment Methods 0.000 description 2
• 239000000155 melt Substances 0.000 description 2
• BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
• 150000003839 salts Chemical class 0.000 description 2
• 150000004992 toluidines Chemical class 0.000 description 2
• ISJBQSJDQZLCSF-UHFFFAOYSA-N (4-chlorophenyl)azanium;chloride Chemical compound [Cl-].[NH3+]C1=CC=C(Cl)C=C1 ISJBQSJDQZLCSF-UHFFFAOYSA-N 0.000 description 1
• 235000005979 Citrus limon Nutrition 0.000 description 1
• 240000002268 Citrus limon Species 0.000 description 1
• 230000036826 Excretion Effects 0.000 description 1
• QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
• 150000001412 amines Chemical class 0.000 description 1
• 238000004458 analytical method Methods 0.000 description 1
• 239000007864 aqueous solution Substances 0.000 description 1
• 150000004982 aromatic amines Chemical class 0.000 description 1
• 239000011248 coating agent Substances 0.000 description 1
• 238000000576 coating method Methods 0.000 description 1
• 150000001875 compounds Chemical class 0.000 description 1
• 238000001035 drying Methods 0.000 description 1
• 238000004043 dyeing Methods 0.000 description 1
• 230000029142 excretion Effects 0.000 description 1
• JQKBUTDZZRGQDR-UHFFFAOYSA-N hydron;4-methylaniline;chloride Chemical compound Cl.CC1=CC=C(N)C=C1 JQKBUTDZZRGQDR-UHFFFAOYSA-N 0.000 description 1
• 239000007788 liquid Substances 0.000 description 1
• 229910052697 platinum Inorganic materials 0.000 description 1
• 239000000843 powder Substances 0.000 description 1
• 239000002244 precipitate Substances 0.000 description 1
• 238000001556 precipitation Methods 0.000 description 1
• 239000000047 product Substances 0.000 description 1
• 238000001953 recrystallisation Methods 0.000 description 1
• 239000011347 resin Substances 0.000 description 1
• 229920005989 resin Polymers 0.000 description 1
• 238000000926 separation method Methods 0.000 description 1
• CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
• 239000007787 solid Substances 0.000 description 1
• 239000002966 varnish Substances 0.000 description 1
• 238000005406 washing Methods 0.000 description 1