DE1110406B - Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis - Google Patents

Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis

Info

Publication number
DE1110406B
DE1110406B DEF27499A DEF0027499A DE1110406B DE 1110406 B DE1110406 B DE 1110406B DE F27499 A DEF27499 A DE F27499A DE F0027499 A DEF0027499 A DE F0027499A DE 1110406 B DE1110406 B DE 1110406B
Authority
DE
Germany
Prior art keywords
tin
weight
parts
compounds
alcoholates
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DEF27499A
Other languages
German (de)
English (en)
Inventor
Dr Guenther Loew
Dr Rudolf Merten
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to BE587687D priority Critical patent/BE587687A/xx
Priority to NL247436D priority patent/NL247436A/xx
Priority to BE586595D priority patent/BE586595A/xx
Application filed by Bayer AG filed Critical Bayer AG
Priority to DEF27498A priority patent/DE1109878B/de
Priority to DEF27499A priority patent/DE1110406B/de
Priority to DEF27728A priority patent/DE1111377B/de
Priority to DEF27732A priority patent/DE1112285B/de
Priority to CH6160A priority patent/CH419597A/de
Priority to US1878A priority patent/US3047540A/en
Priority to US1870A priority patent/US3164557A/en
Priority to GB1603/60A priority patent/GB936395A/en
Priority to FR815711A priority patent/FR1253978A/fr
Priority to SE038160A priority patent/SE218461C1/sl
Priority claimed from CH545160A external-priority patent/CH416077A/de
Priority to FR827059A priority patent/FR1259632A/fr
Priority to GB18550/60A priority patent/GB908337A/en
Publication of DE1110406B publication Critical patent/DE1110406B/de
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/34—Chemical features in the manufacture of articles consisting of a foamed macromolecular core and a macromolecular surface layer having a higher density than the core
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/09—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture
    • C08G18/092—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture oligomerisation to isocyanurate groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/18—Catalysts containing secondary or tertiary amines or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/22—Catalysts containing metal compounds
    • C08G18/225—Catalysts containing metal compounds of alkali or alkaline earth metals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/22—Catalysts containing metal compounds
    • C08G18/24—Catalysts containing metal compounds of tin
    • C08G18/242—Catalysts containing metal compounds of tin organometallic compounds containing tin-carbon bonds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/4244—Polycondensates having carboxylic or carbonic ester groups in the main chain containing oxygen in the form of ether groups
    • C08G18/4247—Polycondensates having carboxylic or carbonic ester groups in the main chain containing oxygen in the form of ether groups derived from polyols containing at least one ether group and polycarboxylic acids
    • C08G18/425—Polycondensates having carboxylic or carbonic ester groups in the main chain containing oxygen in the form of ether groups derived from polyols containing at least one ether group and polycarboxylic acids the polyols containing one or two ether groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/4244—Polycondensates having carboxylic or carbonic ester groups in the main chain containing oxygen in the form of ether groups
    • C08G18/4247—Polycondensates having carboxylic or carbonic ester groups in the main chain containing oxygen in the form of ether groups derived from polyols containing at least one ether group and polycarboxylic acids
    • C08G18/4252—Polycondensates having carboxylic or carbonic ester groups in the main chain containing oxygen in the form of ether groups derived from polyols containing at least one ether group and polycarboxylic acids derived from polyols containing polyether groups and polycarboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
    • C08G18/4263—Polycondensates having carboxylic or carbonic ester groups in the main chain containing carboxylic acid groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4887—Polyethers containing carboxylic ester groups derived from carboxylic acids other than acids of higher fatty oils or other than resin acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/67—Unsaturated compounds having active hydrogen
    • C08G18/6795—Unsaturated polyethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/67—Unsaturated compounds having active hydrogen
    • C08G18/68—Unsaturated polyesters
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0008—Foam properties flexible
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0016—Foam properties semi-rigid
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0025—Foam properties rigid
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0033—Foam properties having integral skins
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0041—Foam properties having specified density
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2375/00—Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers
    • C08J2375/04—Polyurethanes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyurethanes Or Polyureas (AREA)
DEF27499A 1959-01-17 1959-01-17 Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis Pending DE1110406B (de)

Priority Applications (15)

Application Number Priority Date Filing Date Title
BE587687D BE587687A (en, 2012) 1959-01-17
NL247436D NL247436A (en, 2012) 1959-01-17
BE586595D BE586595A (en, 2012) 1959-01-17
DEF27498A DE1109878B (de) 1959-01-17 1959-01-17 Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis
DEF27499A DE1110406B (de) 1959-01-17 1959-01-17 Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis
DEF27728A DE1111377B (de) 1959-01-17 1959-02-18 Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis
DEF27732A DE1112285B (de) 1959-01-17 1959-02-18 Verfahren zur Herstellung von Urethangruppen aufweisenden Schaumstoffen
CH6160A CH419597A (de) 1959-01-17 1960-01-06 Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis
US1878A US3047540A (en) 1959-01-17 1960-01-12 Polyurethane plastics
US1870A US3164557A (en) 1959-01-17 1960-01-12 Polyurethane production catalyzed by an organo-tin compound, which compound containstertiary nitrogen
GB1603/60A GB936395A (en) 1959-01-17 1960-01-15 A process for the production of foamed polyurethanes
FR815711A FR1253978A (fr) 1959-01-17 1960-01-15 Procédé de préparation de matières en mousse à base d'isocyanates
SE038160A SE218461C1 (en, 2012) 1959-01-17 1960-01-15
FR827059A FR1259632A (fr) 1959-01-17 1960-05-13 Procédé de préparation de matières alvéolaires à base d'isocyanates
GB18550/60A GB908337A (en) 1959-01-17 1960-05-25 A process for the production of foam materials

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DEF27499A DE1110406B (de) 1959-01-17 1959-01-17 Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis
DEF27498A DE1109878B (de) 1959-01-17 1959-01-17 Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis
DEF27728A DE1111377B (de) 1959-01-17 1959-02-18 Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis
CH545160A CH416077A (de) 1960-05-12 1960-05-12 Verfahren zur Herstellung von Schaumstoffen

Publications (1)

Publication Number Publication Date
DE1110406B true DE1110406B (de) 1961-07-06

Family

ID=27428892

Family Applications (3)

Application Number Title Priority Date Filing Date
DEF27499A Pending DE1110406B (de) 1959-01-17 1959-01-17 Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis
DEF27498A Pending DE1109878B (de) 1959-01-17 1959-01-17 Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis
DEF27728A Pending DE1111377B (de) 1959-01-17 1959-02-18 Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis

Family Applications After (2)

Application Number Title Priority Date Filing Date
DEF27498A Pending DE1109878B (de) 1959-01-17 1959-01-17 Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis
DEF27728A Pending DE1111377B (de) 1959-01-17 1959-02-18 Verfahren zur Herstellung von Schaumstoffen auf Isocyanatbasis

Country Status (6)

Country Link
US (2) US3047540A (en, 2012)
BE (2) BE587687A (en, 2012)
CH (1) CH419597A (en, 2012)
DE (3) DE1110406B (en, 2012)
GB (2) GB936395A (en, 2012)
NL (1) NL247436A (en, 2012)

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US4405725A (en) * 1967-03-24 1983-09-20 Mobay Chemical Corporation Foamed polyisocyanurates
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US3981828A (en) * 1972-06-19 1976-09-21 Basf Wyandotte Corporation Flexible cellular polyurethane foam compositions having increased flame retardance
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US4212952A (en) * 1978-12-21 1980-07-15 Union Carbide Corporation N,N,N',N'-Tetramethyl-αω-polymethlenediamines as catalysts for the preparation of urethane foams
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US9834638B2 (en) * 2008-06-04 2017-12-05 Covestro Llc Process for preparing rigid polyisocyanurate foams using natural-oil polyols
DE102009033710A1 (de) * 2009-07-18 2011-01-20 Evonik Goldschmidt Gmbh Verwendung von Metallsalzen einer Carbonsäure bei der Herstellung von Polyurethansystemen
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US20150252138A1 (en) 2012-09-25 2015-09-10 Bayer Materialscience, Ag Polyisocyanate-polyaddition products
CN104640896B (zh) 2012-09-25 2019-03-15 科思创德国股份有限公司 多异氰酸酯加聚产物
WO2015164408A1 (en) 2014-04-21 2015-10-29 Gaco Western, LLC Foam compositions
CN109422896B (zh) * 2017-08-24 2021-04-13 山东理工大学 包含伯胺盐和丙醇胺盐的发泡剂及用于聚氨酯冰箱冰柜泡沫体材料的用途
CN114341225A (zh) * 2019-08-20 2022-04-12 巴斯夫欧洲公司 具有改进加工性能的含可选择的发泡剂的阻燃聚氨酯泡沫

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Publication number Priority date Publication date Assignee Title
GB760782A (en) * 1953-08-19 1956-11-07 Bayer Ag Process for the production of foamed products based on polyisocyanates
US2933462A (en) * 1957-07-03 1960-04-19 Aerojet General Co Method for the preparation of foamed polyurethanes
NL106889C (en, 2012) * 1957-09-25 1900-01-01

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
None *

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Publication number Publication date
GB936395A (en) 1963-09-11
GB908337A (en) 1962-10-17
BE586595A (en, 2012)
DE1109878B (de) 1961-06-29
US3047540A (en) 1962-07-31
US3164557A (en) 1965-01-05
NL247436A (en, 2012)
DE1111377B (de) 1961-07-20
CH419597A (de) 1966-08-31
BE587687A (en, 2012)

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