DE102013004317A1 - Lyocell-Formkörper zur selektiven Bindung von einwertigen Schwermetallionen, insbesondere von Thallium- und Caesiumionen und deren radioaktiven Isotopen - Google Patents

Lyocell-Formkörper zur selektiven Bindung von einwertigen Schwermetallionen, insbesondere von Thallium- und Caesiumionen und deren radioaktiven Isotopen Download PDF

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Publication number
DE102013004317A1
DE102013004317A1 DE102013004317A DE102013004317A DE102013004317A1 DE 102013004317 A1 DE102013004317 A1 DE 102013004317A1 DE 102013004317 A DE102013004317 A DE 102013004317A DE 102013004317 A DE102013004317 A DE 102013004317A DE 102013004317 A1 DE102013004317 A1 DE 102013004317A1
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Prior art keywords
cellulose
hexacyanoferrate
lyocell
metal ions
heavy metal
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DE102013004317A
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German (de)
English (en)
Inventor
Marcus Krieg
Martin Sellin
Michael Mooz
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Thueringisches Institut fuer Textil und Kunststoff Forschung eV
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Thueringisches Institut fuer Textil und Kunststoff Forschung eV
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Priority to DE102013004317A priority Critical patent/DE102013004317A1/de
Publication of DE102013004317A1 publication Critical patent/DE102013004317A1/de
Withdrawn legal-status Critical Current

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L26/00—Chemical aspects of, or use of materials for, wound dressings or bandages in liquid, gel or powder form
    • A61L26/0061—Use of materials characterised by their function or physical properties
    • A61L26/0066—Medicaments; Biocides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L26/00—Chemical aspects of, or use of materials for, wound dressings or bandages in liquid, gel or powder form
    • A61L26/0095—Composite materials, i.e. containing one material dispersed in a matrix of the same or different material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0225—Compounds of Fe, Ru, Os, Co, Rh, Ir, Ni, Pd, Pt
    • B01J20/0229—Compounds of Fe
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
    • B01J20/0274—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04 characterised by the type of anion
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/24—Naturally occurring macromolecular compounds, e.g. humic acids or their derivatives
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28023—Fibres or filaments
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28026—Particles within, immobilised, dispersed, entrapped in or on a matrix, e.g. a resin
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28028—Particles immobilised within fibres or filaments
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3007—Moulding, shaping or extruding
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/286—Treatment of water, waste water, or sewage by sorption using natural organic sorbents or derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/58—Treatment of water, waste water, or sewage by removing specified dissolved compounds
    • C02F1/62—Heavy metal compounds
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00—General methods for the manufacture of artificial filaments or the like
    • D01F1/02—Addition of substances to the spinning solution or to the melt
    • D01F1/10—Other agents for modifying properties
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/46—Materials comprising a mixture of inorganic and organic materials
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/48—Sorbents characterised by the starting material used for their preparation
    • B01J2220/4812—Sorbents characterised by the starting material used for their preparation the starting material being of organic character
    • B01J2220/4825—Polysaccharides or cellulose materials, e.g. starch, chitin, sawdust, wood, straw, cotton
    • B01J2220/4831—Polysaccharides or cellulose materials, e.g. starch, chitin, sawdust, wood, straw, cotton having been subjected to further processing, e.g. paper, cellulose pulp
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
    • C02F1/683—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water by addition of complex-forming compounds
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/006—Radioactive compounds
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/10—Inorganic compounds
    • C02F2101/20—Heavy metals or heavy metal compounds

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Textile Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Manufacturing & Machinery (AREA)
  • Dispersion Chemistry (AREA)
  • Composite Materials (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Water Treatment By Sorption (AREA)
DE102013004317A 2012-03-26 2013-03-13 Lyocell-Formkörper zur selektiven Bindung von einwertigen Schwermetallionen, insbesondere von Thallium- und Caesiumionen und deren radioaktiven Isotopen Withdrawn DE102013004317A1 (de)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DE102013004317A DE102013004317A1 (de) 2012-03-26 2013-03-13 Lyocell-Formkörper zur selektiven Bindung von einwertigen Schwermetallionen, insbesondere von Thallium- und Caesiumionen und deren radioaktiven Isotopen

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102012005947.7 2012-03-26
DE102012005947 2012-03-26
DE102013004317A DE102013004317A1 (de) 2012-03-26 2013-03-13 Lyocell-Formkörper zur selektiven Bindung von einwertigen Schwermetallionen, insbesondere von Thallium- und Caesiumionen und deren radioaktiven Isotopen

Publications (1)

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DE102013004317A1 true DE102013004317A1 (de) 2013-09-26

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DE102013004317A Withdrawn DE102013004317A1 (de) 2012-03-26 2013-03-13 Lyocell-Formkörper zur selektiven Bindung von einwertigen Schwermetallionen, insbesondere von Thallium- und Caesiumionen und deren radioaktiven Isotopen

Country Status (4)

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US (1) US9242023B2 (https=)
EP (1) EP2644266B1 (https=)
JP (1) JP6328373B2 (https=)
DE (1) DE102013004317A1 (https=)

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CN115286139A (zh) * 2022-08-10 2022-11-04 铜陵铜冠环保科技有限公司 一种工业废水除铊剂复合制备方法及应用

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JP6270203B2 (ja) * 2011-08-19 2018-01-31 一般財団法人生産技術研究奨励会 放射性セシウム吸着材およびその製造方法、ならびに該吸着材による環境中の放射性セシウムの除去方法
JP6237134B2 (ja) * 2013-11-08 2017-11-29 Nok株式会社 陽イオン物質分離用材料の製造方法
JP6320781B2 (ja) * 2014-02-06 2018-05-09 国立研究開発法人日本原子力研究開発機構 フェロシアン化物粒子−多糖類複合体
JP6427346B2 (ja) * 2014-07-01 2018-11-21 浩義 井上 放射性セシウム吸着材の製造方法
US10982381B2 (en) 2014-10-06 2021-04-20 Natural Fiber Welding, Inc. Methods, processes, and apparatuses for producing welded substrates
US10011931B2 (en) 2014-10-06 2018-07-03 Natural Fiber Welding, Inc. Methods, processes, and apparatuses for producing dyed and welded substrates
MX2018010421A (es) 2016-03-25 2019-05-20 Natural Fiber Welding Inc Metodos, procesos y aparatos para producir sustratos soldados.
CN109196149B (zh) 2016-05-03 2021-10-15 天然纤维焊接股份有限公司 用于生产染色的焊接基质的方法、工艺和设备
JP6439836B2 (ja) * 2017-08-24 2018-12-19 Nok株式会社 陽イオン物質の分離方法
TWI829660B (zh) 2017-11-11 2024-01-21 美商天然纖維焊接股份有限公司 紗與熔接紗
JP2019132651A (ja) * 2018-01-30 2019-08-08 日本製紙株式会社 セシウムを含む液体の処理技術
JP7648081B2 (ja) 2020-01-28 2025-03-18 旭化成株式会社 セルロースと無機系多孔性配位高分子との複合体、及びその製造方法
CN116240639A (zh) * 2022-12-30 2023-06-09 唐山三友集团兴达化纤有限公司 一种普鲁士蓝原液共混粘胶纤维及其制备方法

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EP0575612A1 (en) 1991-12-24 1993-12-29 Sovmestnoe Sovetsko-Kanadskoe Predpriyatie " Compomet Cantec" Method for obtaining composite sorbents
RU2033240C1 (ru) 1992-01-22 1995-04-20 Акционерное общество открытого типа "Научно-исследовательский институт нетканых материалов" Способ получения фильтрующего материала для очистки жидких пищевых продуктов от радионуклидов цезия
US5601722A (en) 1994-05-18 1997-02-11 Agency Of Industrial Science And Technology Method for the preparation of an ion exchanger for cesium ions and method for the regeneration thereof
DE4426966C2 (de) 1994-07-29 2001-02-22 Thueringisches Inst Textil Verfahren zur Herstellung von Cellulosefäden und Folien mit sehr hohen Anteilen von Zusatzstoffen
EP1419009A1 (fr) 2001-08-22 2004-05-19 Commissariat A L'Energie Atomique Procede de preparation d'un materiau solide composite a base d'hexacyanoferrates, et procede de fixation de polluants mineraux le mettant en oeuvre

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JP5658097B2 (ja) * 2011-06-14 2015-01-21 大日精化工業株式会社 吸着剤組成物、放射性セシウム吸着剤及びそれを用いた放射性セシウムの分離方法
JP6270203B2 (ja) * 2011-08-19 2018-01-31 一般財団法人生産技術研究奨励会 放射性セシウム吸着材およびその製造方法、ならびに該吸着材による環境中の放射性セシウムの除去方法

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3735304A1 (de) 1987-10-17 1989-05-03 Bruno Brosch Maschine zum herstellen von loechern im erdreich
EP0575612A1 (en) 1991-12-24 1993-12-29 Sovmestnoe Sovetsko-Kanadskoe Predpriyatie " Compomet Cantec" Method for obtaining composite sorbents
RU2033240C1 (ru) 1992-01-22 1995-04-20 Акционерное общество открытого типа "Научно-исследовательский институт нетканых материалов" Способ получения фильтрующего материала для очистки жидких пищевых продуктов от радионуклидов цезия
US5601722A (en) 1994-05-18 1997-02-11 Agency Of Industrial Science And Technology Method for the preparation of an ion exchanger for cesium ions and method for the regeneration thereof
DE4426966C2 (de) 1994-07-29 2001-02-22 Thueringisches Inst Textil Verfahren zur Herstellung von Cellulosefäden und Folien mit sehr hohen Anteilen von Zusatzstoffen
EP1419009A1 (fr) 2001-08-22 2004-05-19 Commissariat A L'Energie Atomique Procede de preparation d'un materiau solide composite a base d'hexacyanoferrates, et procede de fixation de polluants mineraux le mettant en oeuvre

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115286139A (zh) * 2022-08-10 2022-11-04 铜陵铜冠环保科技有限公司 一种工业废水除铊剂复合制备方法及应用

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JP2013215723A (ja) 2013-10-24
JP6328373B2 (ja) 2018-05-23
US9242023B2 (en) 2016-01-26
EP2644266A1 (de) 2013-10-02
US20130295197A1 (en) 2013-11-07
EP2644266B1 (de) 2018-05-30

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