DE102004038053A1 - Verfahren zur Herstellung von 3-(Methylthio)propanal - Google Patents

Verfahren zur Herstellung von 3-(Methylthio)propanal Download PDF

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Publication number
DE102004038053A1
DE102004038053A1 DE102004038053A DE102004038053A DE102004038053A1 DE 102004038053 A1 DE102004038053 A1 DE 102004038053A1 DE 102004038053 A DE102004038053 A DE 102004038053A DE 102004038053 A DE102004038053 A DE 102004038053A DE 102004038053 A1 DE102004038053 A1 DE 102004038053A1
Authority
DE
Germany
Prior art keywords
catalyst
methylthio
acrolein
reaction medium
mmp
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
DE102004038053A
Other languages
German (de)
English (en)
Inventor
Frank Dr. Dübner
Christoph Dr. Weckbecker
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Evonik Operations GmbH
Original Assignee
Degussa GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Degussa GmbH filed Critical Degussa GmbH
Priority to DE102004038053A priority Critical patent/DE102004038053A1/de
Priority to EP15186588.8A priority patent/EP2987785B1/de
Priority to MX2007000345A priority patent/MX2007000345A/es
Priority to EP05775924.3A priority patent/EP1778631B1/de
Priority to CA002573047A priority patent/CA2573047A1/en
Priority to BRPI0513072-7A priority patent/BRPI0513072A/pt
Priority to JP2007524209A priority patent/JP4773441B2/ja
Priority to CN2005800265919A priority patent/CN101031542B/zh
Priority to RU2007108071/04A priority patent/RU2383531C2/ru
Priority to ES05775924.3T priority patent/ES2560447T3/es
Priority to CN2010101447601A priority patent/CN101812004B/zh
Priority to PCT/EP2005/007666 priority patent/WO2006015684A2/de
Priority to ES15186588.8T priority patent/ES2667220T3/es
Priority to US11/198,609 priority patent/US7119233B2/en
Publication of DE102004038053A1 publication Critical patent/DE102004038053A1/de
Priority to JP2011066503A priority patent/JP5306402B2/ja
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/20—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
    • C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
    • C07C319/18—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by addition of thiols to unsaturated compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
DE102004038053A 2004-08-05 2004-08-05 Verfahren zur Herstellung von 3-(Methylthio)propanal Ceased DE102004038053A1 (de)

Priority Applications (15)

Application Number Priority Date Filing Date Title
DE102004038053A DE102004038053A1 (de) 2004-08-05 2004-08-05 Verfahren zur Herstellung von 3-(Methylthio)propanal
CN2005800265919A CN101031542B (zh) 2004-08-05 2005-07-14 3-(甲硫基)丙醛和2-羟基-4-(甲硫基)丁腈的制备方法
RU2007108071/04A RU2383531C2 (ru) 2004-08-05 2005-07-14 Способ получения 3-(метилтио)пропаналя и 2-гидрокси-4(метилтио)бутаннитрила
EP05775924.3A EP1778631B1 (de) 2004-08-05 2005-07-14 Verfahren zur herstellung von 3-(methylthio)propanal und 2-hydroxy-4-(methylthio)butannitril
CA002573047A CA2573047A1 (en) 2004-08-05 2005-07-14 Method for the production of 3-(methylthio)propanal and 2-hydroxy-4-(methylthio)butanitrile
BRPI0513072-7A BRPI0513072A (pt) 2004-08-05 2005-07-14 método de produção de 3-(metiltio) propanal
JP2007524209A JP4773441B2 (ja) 2004-08-05 2005-07-14 ３−（メチルチオ）プロパナールの製造方法
EP15186588.8A EP2987785B1 (de) 2004-08-05 2005-07-14 Verfahren zur herstellung von 3-(methylthio)propanal
MX2007000345A MX2007000345A (es) 2004-08-05 2005-07-14 Metodo para producir 3-(metiltio)propanal y 2-hidroxi 4-(metiltio)butanonitrilo.
ES05775924.3T ES2560447T3 (es) 2004-08-05 2005-07-14 Procedimiento para la obtención de 3-(metiltio)propanal y 2-hidroxi-4-(metiltio)butanonitrilo
CN2010101447601A CN101812004B (zh) 2004-08-05 2005-07-14 3-(甲硫基)丙醛和2-羟基-4-(甲硫基)丁腈的制备方法
PCT/EP2005/007666 WO2006015684A2 (de) 2004-08-05 2005-07-14 Verfahren zur herstellung von 3-(methylthio)propanal und 2-hydroxy-4-(methylthio)butannitril
ES15186588.8T ES2667220T3 (es) 2004-08-05 2005-07-14 Procedimiento para la producción de 3-(metiltio)propanal
US11/198,609 US7119233B2 (en) 2004-08-05 2005-08-05 Method for preparing 3-(methylthio)propanal
JP2011066503A JP5306402B2 (ja) 2004-08-05 2011-03-24 ３−（メチルチオ）プロパナールの製造方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102004038053A DE102004038053A1 (de) 2004-08-05 2004-08-05 Verfahren zur Herstellung von 3-(Methylthio)propanal

Publications (1)

Publication Number Publication Date
DE102004038053A1 true DE102004038053A1 (de) 2006-04-27

Family

ID=35149290

Family Applications (1)

Application Number Title Priority Date Filing Date
DE102004038053A Ceased DE102004038053A1 (de) 2004-08-05 2004-08-05 Verfahren zur Herstellung von 3-(Methylthio)propanal

Country Status (11)

Country Link
US (1) US7119233B2 (https=)
EP (2) EP2987785B1 (https=)
JP (2) JP4773441B2 (https=)
CN (2) CN101812004B (https=)
BR (1) BRPI0513072A (https=)
CA (1) CA2573047A1 (https=)
DE (1) DE102004038053A1 (https=)
ES (2) ES2560447T3 (https=)
MX (1) MX2007000345A (https=)
RU (1) RU2383531C2 (https=)
WO (1) WO2006015684A2 (https=)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102005003990A1 (de) * 2005-01-28 2006-08-03 Degussa Ag Herstellung von 3-(Alkylthio)propanal
JP5182198B2 (ja) * 2009-04-06 2013-04-10 住友化学株式会社 ３−メチルチオプロパナールの製造方法
JP5402864B2 (ja) * 2010-07-20 2014-01-29 住友化学株式会社 ３−メチルチオプロパナールの製造方法
FR2966456B1 (fr) * 2010-10-26 2013-03-15 Adisseo France Sas Procede d'obtention d'acroleine par deshydratation catalytique de glycerol ou de glycerine
EP2468383A1 (de) * 2010-12-22 2012-06-27 Evonik Degussa GmbH Verfahren zur thermischen Nachverbrennung von Abgasen aus der Acrolein- und aus der Blausäureherstellung
WO2012113664A1 (de) * 2011-02-23 2012-08-30 Evonik Degussa Gmbh Verfahren zur herstellung von 2-hydroxy-4-(methylthio)buttersäurenitril aus 3-(methylthio)propanal und cyanwasserstoff
WO2012113665A1 (de) 2011-02-23 2012-08-30 Evonik Degussa Gmbh Lagerstabiles 2-hydroxy-4-(methylthio)buttersäurenitril
SG11201509776VA (en) 2013-06-03 2015-12-30 Evonik Degussa Gmbh Method for producing acrolein
CN107417570B (zh) * 2017-09-14 2020-04-14 哈尔滨理工大学 利用丙酮氰醇制备α-羟基腈的方法
CN111116437B (zh) 2018-11-01 2021-02-05 山东新和成氨基酸有限公司 制备2-羟基-4-甲硫基丁酸及其中间体的方法和装置
CN109651215B (zh) * 2019-02-14 2023-12-22 天宝动物营养科技股份有限公司 一种2-羟基-4-甲硫基丁腈的连续制备工艺和装置
CN121794383A (zh) 2023-07-17 2026-04-03 摩珈生物科技有限公司 通过3-甲硫基丙醛与c1来源的甲酰辅酶a缩合生产蛋氨酸
CN119912370B (zh) * 2025-04-03 2025-08-05 山东新和成氨基酸有限公司 一种2-羟基-4-甲硫基丁腈的制备方法及反应装置

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2542768A (en) * 1945-10-24 1951-02-20 Du Pont Hydroxy-methylmercaptobutyronitrile
DE2320544C2 (de) 1973-04-21 1975-06-05 Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt Verfahren zur Herstellung von 3-Methylmercaptopropionaldehyd
FR2314917A1 (fr) 1975-06-20 1977-01-14 Rhone Poulenc Ind Procede de fabrication de l'aldehyde beta-methylthiopropionique
DE2623285C3 (de) 1976-05-25 1980-10-02 Gebrueder Grau Und Co Kg Chem. Fabrik, 7070 Schwaebisch Gmuend Riechstoffkomposition
FR2460925A1 (fr) 1979-07-10 1981-01-30 Rhone Poulenc Ind Procede de preparation directe d'aldehyde beta-methylthiopropionique
FR2480925A1 (fr) 1980-04-22 1981-10-23 Electricite De France Echangeur thermique modulaire
US4440676A (en) 1981-12-24 1984-04-03 The British Petroleum Company P.L.C. Process for the production of a dipeptide, a polypeptide or a protein
JP3219544B2 (ja) * 1992-05-21 2001-10-15 ダイセル化学工業株式会社 ２−ヒドロキシ−４−メチルチオブタン酸の製造法
US5905171A (en) * 1995-06-22 1999-05-18 Novus International, Inc. Process for the preparation of 3-(methylthio)propanal
US5352837A (en) 1993-06-08 1994-10-04 Novus International, Inc. Process for the preparation of 3-(methylthio)propanal
US5663409A (en) * 1995-06-07 1997-09-02 Novus International, Inc. Process for the preparation of 3-(methylthio) propanal and 2-hydroxy-4-(methylthio) butanenitrile
AR002174A1 (es) * 1995-06-07 1998-01-07 Novus Int Inc Proceso para la preparacion de 3-(metiltio)propanal y 2-hidroxi-4-metiltio) butanonitrilo
JP3490459B2 (ja) * 1996-04-01 2004-01-26 ユニオン カーバイド ケミカルズ アンド プラスティックス テクノロジー コーポレイション メチルメルカプトプロパナールの製造方法
JP4517486B2 (ja) * 2000-09-25 2010-08-04 住友化学株式会社 ２−ヒドロキシ−４−メチルチオブタンニトリルの製造方法
EP1409131A2 (en) 2001-07-23 2004-04-21 Andrew Bruce Holmes Palladium-catalysed carbon-carbon bond forming reactions in compressed carbon dioxide
JP4186572B2 (ja) * 2002-09-27 2008-11-26 住友化学株式会社 ３−メチルチオプロパナールの製造方法

Also Published As

Publication number Publication date
EP1778631A2 (de) 2007-05-02
JP2008508330A (ja) 2008-03-21
MX2007000345A (es) 2007-03-07
CN101031542B (zh) 2010-05-12
CA2573047A1 (en) 2006-02-16
JP2011132256A (ja) 2011-07-07
RU2007108071A (ru) 2008-09-20
EP2987785A1 (de) 2016-02-24
EP1778631B1 (de) 2015-11-18
US7119233B2 (en) 2006-10-10
CN101031542A (zh) 2007-09-05
RU2383531C2 (ru) 2010-03-10
WO2006015684A3 (de) 2006-08-03
CN101812004A (zh) 2010-08-25
BRPI0513072A (pt) 2008-04-22
WO2006015684A2 (de) 2006-02-16
EP2987785B1 (de) 2018-03-14
CN101812004B (zh) 2012-09-19
JP5306402B2 (ja) 2013-10-02
JP4773441B2 (ja) 2011-09-14
US20060030739A1 (en) 2006-02-09
ES2560447T3 (es) 2016-02-19
ES2667220T3 (es) 2018-05-10

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Legal Events

Date Code Title Description
ON Later submitted papers
8127 New person/name/address of the applicant

Owner name: DEGUSSA GMBH, 40474 DUESSELDORF, DE

8127 New person/name/address of the applicant

Owner name: EVONIK DEGUSSA GMBH, 40474 DUESSELDORF, DE

R012 Request for examination validly filed
R409 Internal rectification of the legal status completed
R409 Internal rectification of the legal status completed
R074 Re-establishment allowed
R409 Internal rectification of the legal status completed
R005 Application deemed withdrawn due to failure to request examination

Effective date: 20110806

R012 Request for examination validly filed

Effective date: 20110624

R016 Response to examination communication
R002 Refusal decision in examination/registration proceedings
R003 Refusal decision now final