DE10164264A1 - Verfahren zur Herstellung von Trimethylolpropan - Google Patents

Verfahren zur Herstellung von Trimethylolpropan

Info

Publication number
DE10164264A1
DE10164264A1 DE10164264A DE10164264A DE10164264A1 DE 10164264 A1 DE10164264 A1 DE 10164264A1 DE 10164264 A DE10164264 A DE 10164264A DE 10164264 A DE10164264 A DE 10164264A DE 10164264 A1 DE10164264 A1 DE 10164264A1
Authority
DE
Germany
Prior art keywords
distillation
tmp
trimethylolpropane
columns
formaldehyde
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE10164264A
Other languages
German (de)
English (en)
Inventor
Dirk Mueller
Paul Wagner
Brian Schwegler
Ulrich Notheis
Ralph Armbrust
Hans-Detlef Heinz
Alexander Wagner
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer Chemicals AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer AG filed Critical Bayer AG
Priority to DE10164264A priority Critical patent/DE10164264A1/de
Priority to EP02028037A priority patent/EP1323698A3/de
Priority to US10/322,962 priority patent/US7211701B2/en
Priority to PL02357927A priority patent/PL357927A1/xx
Priority to JP2002373118A priority patent/JP2003192620A/ja
Priority to TW091137396A priority patent/TW200305558A/zh
Priority to KR1020020083845A priority patent/KR20030057363A/ko
Priority to CNB021598010A priority patent/CN1280245C/zh
Publication of DE10164264A1 publication Critical patent/DE10164264A1/de
Priority to HK03107455A priority patent/HK1055110A1/xx
Withdrawn legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/36—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal
    • C07C29/38—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal by reaction with aldehydes or ketones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
DE10164264A 2001-12-27 2001-12-27 Verfahren zur Herstellung von Trimethylolpropan Withdrawn DE10164264A1 (de)

Priority Applications (9)

Application Number Priority Date Filing Date Title
DE10164264A DE10164264A1 (de) 2001-12-27 2001-12-27 Verfahren zur Herstellung von Trimethylolpropan
EP02028037A EP1323698A3 (de) 2001-12-27 2002-12-16 Verfahren zur Herstellung von Trimethylolpropan
US10/322,962 US7211701B2 (en) 2001-12-27 2002-12-18 Preparation of trimethylolpropane
PL02357927A PL357927A1 (en) 2001-12-27 2002-12-20 Method of obtaining trimethylpropane
JP2002373118A JP2003192620A (ja) 2001-12-27 2002-12-24 低いａｐｈａ色数を有するトリメチロールプロパンの製造方法
TW091137396A TW200305558A (en) 2001-12-27 2002-12-26 Preparation of trimethylolpropane
KR1020020083845A KR20030057363A (ko) 2001-12-27 2002-12-26 트리메틸올프로판의 제조
CNB021598010A CN1280245C (zh) 2001-12-27 2002-12-27 三羟甲基丙烷的制备方法
HK03107455A HK1055110A1 (en) 2001-12-27 2003-10-15 Preparation of trimethylolpropane

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE10164264A DE10164264A1 (de) 2001-12-27 2001-12-27 Verfahren zur Herstellung von Trimethylolpropan

Publications (1)

Publication Number Publication Date
DE10164264A1 true DE10164264A1 (de) 2003-07-17

Family

ID=7711048

Family Applications (1)

Application Number Title Priority Date Filing Date
DE10164264A Withdrawn DE10164264A1 (de) 2001-12-27 2001-12-27 Verfahren zur Herstellung von Trimethylolpropan

Country Status (9)

Country Link
US (1) US7211701B2 (zh)
EP (1) EP1323698A3 (zh)
JP (1) JP2003192620A (zh)
KR (1) KR20030057363A (zh)
CN (1) CN1280245C (zh)
DE (1) DE10164264A1 (zh)
HK (1) HK1055110A1 (zh)
PL (1) PL357927A1 (zh)
TW (1) TW200305558A (zh)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2281794A1 (de) 2009-08-07 2011-02-09 LANXESS Deutschland GmbH Verfahren zur Farbzahlverbesserung von Trimethylolpropan

Families Citing this family (43)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100837523B1 (ko) * 2006-03-07 2008-06-12 주식회사 엘지화학 트리메틸올프로판의 제조방법
WO2008037587A1 (de) * 2006-09-28 2008-04-03 Basf Se Verfahren zur kontinuierlichen destillativen auftrennung von gemischen enthaltend morpholin (mo), monoaminodiglykol (adg), ammoniak und wasser
EP2079718B1 (de) * 2006-09-28 2010-04-07 Basf Se Verfahren zur kontinuierlichen destillativen auftrennung von gemischen enthaltend morpholin (mo), monoaminodiglykol (adg), ammoniak und wasser
WO2008091317A2 (en) 2007-01-19 2008-07-31 Exxonmobil Upstream Research Company Integrated controlled freeze zone (cfz) tower and dividing wall (dwc) for enhanced hydrocarbon recovery
US20100018248A1 (en) * 2007-01-19 2010-01-28 Eleanor R Fieler Controlled Freeze Zone Tower
DE102007013963A1 (de) * 2007-03-23 2008-09-25 Lanxess Deutschland Gmbh Verfahren zur Farbzahlverbesserung von Trimethylolpropan
DE102008038021A1 (de) * 2008-08-16 2010-02-18 Lanxess Deutschland Gmbh Verfahren zur Isolierung von Di-Trimethylolpropan
CN102355929B (zh) 2009-03-19 2014-07-30 Lg化学株式会社 用于制备高纯度丙烯酸的分隔壁蒸馏塔和使用该分隔壁蒸馏塔的分馏方法
CN102355928B (zh) * 2009-03-19 2014-03-12 Lg化学株式会社 用于制备高纯度2-乙基己醇的分隔壁蒸馏塔和采用该分隔壁蒸馏塔的分馏方法
WO2010123598A1 (en) 2009-04-20 2010-10-28 Exxonmobil Upstream Research Company Cryogenic system for removing acid gases from a hyrdrocarbon gas stream, and method of removing acid gases
JP5791609B2 (ja) 2009-09-09 2015-10-07 エクソンモービル アップストリーム リサーチ カンパニー 炭化水素ガス流から酸性ガスを除去する極低温システム
EP2607341B1 (en) * 2009-12-24 2015-11-18 Oxea Bishop LLC Trimethylolpropane color improvement
CA2786574C (en) 2010-01-22 2016-06-28 Exxonmobil Upstream Research Company Removal of acid gases from a gas stream, with co2 capture and sequestration
CA2786498C (en) 2010-02-03 2018-06-26 Exxonmobil Upstream Research Company Systems and methods for using cold liquid to remove solidifiable gas components from process gas streams
EP2598817A4 (en) 2010-07-30 2018-07-25 Exxonmobil Upstream Research Company Cryogenic systems for removing acid gases from a hydrocarbon gas stream using co-current separation devices
DE102011118953B4 (de) 2011-11-19 2014-06-05 Oxea Gmbh Destillatives Verfahren zur Gewinnung von Di-Trimethylolpropan
MY166180A (en) 2012-03-21 2018-06-07 Exxonmobil Upstream Res Co Separating carbon dioxide and ethane from mixed stream
CN102795963B (zh) * 2012-09-12 2013-07-10 江西高信有机化工有限公司 一种采用离心过滤式钙法三羟甲基丙烷制备工艺
CN102795964B (zh) * 2012-09-12 2013-05-29 江西高信有机化工有限公司 一种年产2万吨钙法三羟甲基丙烷的生产工艺
WO2014112808A1 (ko) * 2013-01-16 2014-07-24 주식회사 엘지화학 알칸올의 제조 장치
US9504934B2 (en) 2013-10-27 2016-11-29 Purdue Research Foundation Multicomponent dividing wall columns
US9869511B2 (en) 2013-12-06 2018-01-16 Exxonmobil Upstream Research Company Method and device for separating hydrocarbons and contaminants with a spray assembly
US9562719B2 (en) 2013-12-06 2017-02-07 Exxonmobil Upstream Research Company Method of removing solids by modifying a liquid level in a distillation tower
US9874395B2 (en) 2013-12-06 2018-01-23 Exxonmobil Upstream Research Company Method and system for preventing accumulation of solids in a distillation tower
US10139158B2 (en) 2013-12-06 2018-11-27 Exxonmobil Upstream Research Company Method and system for separating a feed stream with a feed stream distribution mechanism
AU2014357665B2 (en) 2013-12-06 2017-06-22 Exxonmobil Upstream Research Company Method and device for separating a feed stream using radiation detectors
US9752827B2 (en) 2013-12-06 2017-09-05 Exxonmobil Upstream Research Company Method and system of maintaining a liquid level in a distillation tower
CA2925404C (en) 2013-12-06 2018-02-06 Exxonmobil Upstream Research Company Method and system of dehydrating a feed stream processed in a distillation tower
WO2015084499A2 (en) 2013-12-06 2015-06-11 Exxonmobil Upstream Research Company Method and system of modifying a liquid level during start-up operations
AU2014357669B2 (en) 2013-12-06 2017-12-21 Exxonmobil Upstream Research Company Method and device for separating hydrocarbons and contaminants with a heating mechanism to destabilize and/or prevent adhesion of solids
CA2972796C (en) 2015-02-27 2019-08-13 Exxonmobil Upstream Research Company Reducing refrigeration and dehydration load for a feed stream entering a cryogenic distillation process
AU2016323618B2 (en) 2015-09-18 2019-06-13 Exxonmobil Upsteam Research Company Heating component to reduce solidification in a cryogenic distillation system
CA2998466C (en) 2015-09-24 2021-06-29 Exxonmobil Upstream Research Company Treatment plant for hydrocarbon gas having variable contaminant levels
CA3024545C (en) 2016-03-30 2020-08-25 Exxonmobile Upstream Research Company Self-sourced reservoir fluid for enhanced oil recovery
EP3315484B1 (de) 2016-10-25 2019-02-27 OXEA GmbH Verfahren zur koppelproduktion von polyolen in gegenwart einer anorganischen base
CN109485544B (zh) * 2017-09-11 2021-12-14 中国科学院大连化学物理研究所 一种连续制备三羟甲基丙烷的方法
KR102245932B1 (ko) 2017-10-23 2021-04-28 주식회사 엘지화학 트리메틸올프로판의 제조방법
KR102391592B1 (ko) 2018-02-01 2022-04-28 주식회사 엘지화학 디메틸올부탄알의 제조방법 및 증류 장치
WO2020005552A1 (en) 2018-06-29 2020-01-02 Exxonmobil Upstream Research Company Hybrid tray for introducing a low co2 feed stream into a distillation tower
WO2020005553A1 (en) 2018-06-29 2020-01-02 Exxonmobil Upstream Research Company (Emhc-N1.4A.607) Mixing and heat integration of melt tray liquids in a cryogenic distillation tower
JP6916366B1 (ja) * 2020-11-16 2021-08-11 株式会社日本触媒 ジオールの製造方法
CN114763403B (zh) * 2021-01-14 2024-02-02 万华化学集团股份有限公司 一种低色号tmp型多异氰酸酯组合物及其制备方法
CN114524712A (zh) * 2022-01-24 2022-05-24 南通百川新材料有限公司 一种冷冻缩合制备三羟甲基丙烷的工艺方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE45078C (de) R. landsberger, W. kaestner und L. harwitz in Berlin Selbstthätiger Schankapparat
DE287251C (zh)
US3183274A (en) * 1956-10-09 1965-05-11 Celanese Corp Trimethylolpropane
US3097245A (en) 1959-01-13 1963-07-09 Trojan Powder Co Process for the preparation of trimethylolalkane
DE1154080B (de) 1959-06-04 1963-09-12 Bayer Ag Verfahren zur kontinuierlichen Herstellung von drei- und mehrwertigen Alkoholen durch alkalische Kondensation
FR1300975A (fr) 1961-07-01 1962-08-10 Ferodo Sa Perfectionnements aux embrayages
JPS509B1 (zh) 1969-11-28 1975-01-06
DE3207746A1 (de) * 1982-03-04 1983-09-08 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von trimethylolpropan
JP4284477B2 (ja) 1998-12-25 2009-06-24 三菱瓦斯化学株式会社 高純度トリメチロールプロパンの製造法
DE19963435A1 (de) * 1999-12-28 2001-07-05 Basf Ag Verfahren zur Reinigung von durch Hydrierung hergestelltem Trimethylolpropan durch kontinuierliche Destillation

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2281794A1 (de) 2009-08-07 2011-02-09 LANXESS Deutschland GmbH Verfahren zur Farbzahlverbesserung von Trimethylolpropan
WO2011015644A2 (de) 2009-08-07 2011-02-10 Lanxess Deutschland Gmbh Verfahren zur farbzahlverbesserung von trimethylolpropan
WO2011015644A3 (de) * 2009-08-07 2011-04-21 Lanxess Deutschland Gmbh Verfahren zur farbzahlverbesserung von trimethylolpropan

Also Published As

Publication number Publication date
EP1323698A2 (de) 2003-07-02
PL357927A1 (en) 2003-06-30
HK1055110A1 (en) 2003-12-24
US7211701B2 (en) 2007-05-01
CN1280245C (zh) 2006-10-18
JP2003192620A (ja) 2003-07-09
TW200305558A (en) 2003-11-01
CN1428323A (zh) 2003-07-09
KR20030057363A (ko) 2003-07-04
US20030139631A1 (en) 2003-07-24
EP1323698A3 (de) 2003-11-26

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Legal Events

Date Code Title Description
8127 New person/name/address of the applicant

Owner name: BAYER CHEMICALS AG, 51373 LEVERKUSEN, DE

8139 Disposal/non-payment of the annual fee