DD298403A5 - Verfahren zur herstellung von ketoximosilanen - Google Patents
Verfahren zur herstellung von ketoximosilanen Download PDFInfo
- Publication number
- DD298403A5 DD298403A5 DD89334522A DD33452289A DD298403A5 DD 298403 A5 DD298403 A5 DD 298403A5 DD 89334522 A DD89334522 A DD 89334522A DD 33452289 A DD33452289 A DD 33452289A DD 298403 A5 DD298403 A5 DD 298403A5
- Authority
- DD
- German Democratic Republic
- Prior art keywords
- ketoximosilanes
- carbon atoms
- general formula
- ketoxime
- preparation
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 10
- 238000004519 manufacturing process Methods 0.000 title claims 2
- 239000007791 liquid phase Substances 0.000 claims abstract description 5
- 238000000926 separation method Methods 0.000 claims abstract description 4
- 238000002360 preparation method Methods 0.000 claims abstract 5
- 229920001296 polysiloxane Polymers 0.000 claims abstract 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 15
- 239000002904 solvent Substances 0.000 claims description 11
- 239000012071 phase Substances 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 7
- -1 ammonium chloride Chemical class 0.000 claims description 3
- 238000004821 distillation Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 2
- WHIVNJATOVLWBW-UHFFFAOYSA-N n-butan-2-ylidenehydroxylamine Chemical compound CCC(C)=NO WHIVNJATOVLWBW-UHFFFAOYSA-N 0.000 claims description 2
- 239000003960 organic solvent Substances 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims 6
- 238000000354 decomposition reaction Methods 0.000 claims 4
- 150000003839 salts Chemical class 0.000 claims 4
- 150000003377 silicon compounds Chemical class 0.000 claims 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
- 239000000370 acceptor Substances 0.000 claims 2
- BTHCBXJLLCHNMS-UHFFFAOYSA-N acetyloxysilicon Chemical compound CC(=O)O[Si] BTHCBXJLLCHNMS-UHFFFAOYSA-N 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 2
- 238000006243 chemical reaction Methods 0.000 claims 2
- 238000004132 cross linking Methods 0.000 claims 2
- 238000004880 explosion Methods 0.000 claims 2
- 239000007787 solid Substances 0.000 claims 2
- 230000002378 acidificating effect Effects 0.000 claims 1
- 235000019270 ammonium chloride Nutrition 0.000 claims 1
- 150000003863 ammonium salts Chemical class 0.000 claims 1
- 239000006227 byproduct Substances 0.000 claims 1
- 230000003197 catalytic effect Effects 0.000 claims 1
- 239000007795 chemical reaction product Substances 0.000 claims 1
- 239000013078 crystal Substances 0.000 claims 1
- 229920005645 diorganopolysiloxane polymer Polymers 0.000 claims 1
- 229920001971 elastomer Polymers 0.000 claims 1
- 239000000806 elastomer Substances 0.000 claims 1
- 238000005516 engineering process Methods 0.000 claims 1
- 239000002360 explosive Substances 0.000 claims 1
- 239000000706 filtrate Substances 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- 150000001367 organochlorosilanes Chemical class 0.000 claims 1
- 238000005191 phase separation Methods 0.000 claims 1
- 239000002002 slurry Substances 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- 230000001960 triggered effect Effects 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- 150000001412 amines Chemical class 0.000 abstract description 4
- 239000004971 Cross linker Substances 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 238000002955 isolation Methods 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 10
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 6
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 5
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 5
- 229910000077 silane Inorganic materials 0.000 description 5
- KDSNLYIMUZNERS-UHFFFAOYSA-N 2-methylpropanamine Chemical compound CC(C)CN KDSNLYIMUZNERS-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- BHRZNVHARXXAHW-UHFFFAOYSA-N sec-butylamine Chemical compound CCC(C)N BHRZNVHARXXAHW-UHFFFAOYSA-N 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 description 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 2
- 229920002554 vinyl polymer Polymers 0.000 description 2
- AJDIZQLSFPQPEY-UHFFFAOYSA-N 1,1,2-Trichlorotrifluoroethane Chemical compound FC(F)(Cl)C(F)(Cl)Cl AJDIZQLSFPQPEY-UHFFFAOYSA-N 0.000 description 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- TVJPBVNWVPUZBM-UHFFFAOYSA-N [diacetyloxy(methyl)silyl] acetate Chemical compound CC(=O)O[Si](C)(OC(C)=O)OC(C)=O TVJPBVNWVPUZBM-UHFFFAOYSA-N 0.000 description 1
- PXAJQJMDEXJWFB-UHFFFAOYSA-N acetone oxime Chemical compound CC(C)=NO PXAJQJMDEXJWFB-UHFFFAOYSA-N 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000005755 formation reaction Methods 0.000 description 1
- JJWLVOIRVHMVIS-UHFFFAOYSA-N isopropylamine Chemical compound CC(C)N JJWLVOIRVHMVIS-UHFFFAOYSA-N 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/0834—Compounds having one or more O-Si linkage
- C07F7/0892—Compounds with a Si-O-N linkage
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3838897A DE3838897C1 (nl) | 1988-11-17 | 1988-11-17 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DD298403A5 true DD298403A5 (de) | 1992-02-20 |
Family
ID=6367344
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DD89334522A DD298403A5 (de) | 1988-11-17 | 1989-11-13 | Verfahren zur herstellung von ketoximosilanen |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US4925964A (nl) |
| EP (1) | EP0369359A3 (nl) |
| JP (1) | JPH02180889A (nl) |
| BR (1) | BR8905815A (nl) |
| DD (1) | DD298403A5 (nl) |
| DE (1) | DE3838897C1 (nl) |
| YU (1) | YU217089A (nl) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0757757B2 (ja) * | 1990-10-22 | 1995-06-21 | 信越化学工業株式会社 | オキシムシランの着色防止方法 |
| US5145912A (en) * | 1990-12-17 | 1992-09-08 | Dow Corning Corporation | Method for preparing oximosilane-functional vinylic copolymers |
| US5717052A (en) * | 1992-09-17 | 1998-02-10 | Alliedsignal Inc. | Di-, tri- and tetrafunctional methyl isobutyl and methyl amyl ketoxime-based silanes |
| US5405930A (en) * | 1992-09-17 | 1995-04-11 | Alliedsignal Inc. | Di-, tri- and tetrafunctional methyl isobutyl and methyl amyl ketoxime-based silanes |
| US5359108A (en) * | 1992-09-17 | 1994-10-25 | Alliedsignal Inc. | Di-, tri- and tetrafunctional methyl isobutyl and methyl amyl ketoxime-based silanes |
| KR20020053466A (ko) * | 2000-12-27 | 2002-07-05 | 정종순 | 옥심형 실란의 제조방법 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3448136A (en) * | 1965-12-27 | 1969-06-03 | Stauffer Chemical Co | Aminoxysilanes |
| BE758713A (fr) * | 1969-11-12 | 1971-05-10 | Rhone Poulenc Sa | Iminoxyorganoxysilanes |
| DE2220101C3 (de) * | 1972-04-25 | 1975-03-13 | Bayer Ag, 5090 Leverkusen | Verfahren zur Umsetzung halogenhaltiger Substanzen mit Verbindungen, die reaktionsfähire Wasserstoffatome enthalten |
| JPS5176228A (en) * | 1974-12-26 | 1976-07-01 | Shinetsu Chemical Co | Oruganoshiranno seizohoho |
| US4380660A (en) * | 1982-07-01 | 1983-04-19 | Allied Corporation | Producing alkoxysilanes and alkoxy-oximinosilanes |
| DE3703484C1 (nl) * | 1987-02-05 | 1988-09-15 | Sintesa Chemie Gmbh, 8901 Kissing, De |
-
1988
- 1988-11-17 DE DE3838897A patent/DE3838897C1/de not_active Expired - Fee Related
-
1989
- 1989-11-07 US US07/432,509 patent/US4925964A/en not_active Expired - Fee Related
- 1989-11-11 EP EP19890120934 patent/EP0369359A3/de not_active Withdrawn
- 1989-11-13 DD DD89334522A patent/DD298403A5/de not_active IP Right Cessation
- 1989-11-15 YU YU02170/89A patent/YU217089A/xx unknown
- 1989-11-16 JP JP1296321A patent/JPH02180889A/ja active Pending
- 1989-11-17 BR BR898905815A patent/BR8905815A/pt unknown
Also Published As
| Publication number | Publication date |
|---|---|
| JPH02180889A (ja) | 1990-07-13 |
| US4925964A (en) | 1990-05-15 |
| EP0369359A3 (de) | 1991-03-27 |
| BR8905815A (pt) | 1990-06-12 |
| EP0369359A2 (de) | 1990-05-23 |
| DE3838897C1 (nl) | 1990-01-18 |
| YU217089A (en) | 1991-10-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ENJ | Ceased due to non-payment of renewal fee |