CZ287192B6 - Calcium salt dihydrate of 3-hydroxy-5-methylisoxazole, process of its preparation, fungicidal agent and protection method of plants - Google Patents
Calcium salt dihydrate of 3-hydroxy-5-methylisoxazole, process of its preparation, fungicidal agent and protection method of plants Download PDFInfo
- Publication number
- CZ287192B6 CZ287192B6 CZ1993840A CZ84093A CZ287192B6 CZ 287192 B6 CZ287192 B6 CZ 287192B6 CZ 1993840 A CZ1993840 A CZ 1993840A CZ 84093 A CZ84093 A CZ 84093A CZ 287192 B6 CZ287192 B6 CZ 287192B6
- Authority
- CZ
- Czechia
- Prior art keywords
- hydroxy
- methylisoxazole
- calcium salt
- dihydrate
- soil
- Prior art date
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- KGVPNLBXJKTABS-UHFFFAOYSA-N hymexazol Chemical compound CC1=CC(O)=NO1 KGVPNLBXJKTABS-UHFFFAOYSA-N 0.000 title claims abstract description 68
- 238000000034 method Methods 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 title claims description 16
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- 239000013078 crystal Substances 0.000 claims abstract description 10
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 5
- 239000000920 calcium hydroxide Substances 0.000 claims abstract description 5
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims abstract description 5
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- 239000000203 mixture Substances 0.000 claims description 64
- DLPFPZMDTCKEKF-UHFFFAOYSA-N O.O.[Ca].CC1=CC(O)=NO1 Chemical compound O.O.[Ca].CC1=CC(O)=NO1 DLPFPZMDTCKEKF-UHFFFAOYSA-N 0.000 claims description 28
- 159000000007 calcium salts Chemical class 0.000 claims description 23
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- 230000000855 fungicidal effect Effects 0.000 claims description 10
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- DMSMPAJRVJJAGA-UHFFFAOYSA-N benzo[d]isothiazol-3-one Chemical compound C1=CC=C2C(=O)NSC2=C1 DMSMPAJRVJJAGA-UHFFFAOYSA-N 0.000 claims description 6
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- GFISDBXSWQMOND-UHFFFAOYSA-N 2,5-dimethoxyoxolane Chemical compound COC1CCC(OC)O1 GFISDBXSWQMOND-UHFFFAOYSA-N 0.000 claims description 2
- OBNZPZAOTISUNM-UHFFFAOYSA-N 4-chloro-1,6-dimethylcyclohexa-2,4-dien-1-ol Chemical compound ClC1=CC(C(C=C1)(C)O)C OBNZPZAOTISUNM-UHFFFAOYSA-N 0.000 claims description 2
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- LVTJOONKWUXEFR-FZRMHRINSA-N protoneodioscin Natural products O(C[C@@H](CC[C@]1(O)[C@H](C)[C@@H]2[C@]3(C)[C@H]([C@H]4[C@@H]([C@]5(C)C(=CC4)C[C@@H](O[C@@H]4[C@H](O[C@H]6[C@@H](O)[C@@H](O)[C@@H](O)[C@H](C)O6)[C@@H](O)[C@H](O[C@H]6[C@@H](O)[C@@H](O)[C@@H](O)[C@H](C)O6)[C@H](CO)O4)CC5)CC3)C[C@@H]2O1)C)[C@H]1[C@H](O)[C@H](O)[C@H](O)[C@@H](CO)O1 LVTJOONKWUXEFR-FZRMHRINSA-N 0.000 description 1
- 239000008262 pumice Substances 0.000 description 1
- 229910052903 pyrophyllite Inorganic materials 0.000 description 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 1
- 238000012552 review Methods 0.000 description 1
- 230000002786 root growth Effects 0.000 description 1
- 125000002914 sec-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 235000010413 sodium alginate Nutrition 0.000 description 1
- 239000000661 sodium alginate Substances 0.000 description 1
- 229940005550 sodium alginate Drugs 0.000 description 1
- 229940077386 sodium benzenesulfonate Drugs 0.000 description 1
- 235000002639 sodium chloride Nutrition 0.000 description 1
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 description 1
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 1
- 235000019982 sodium hexametaphosphate Nutrition 0.000 description 1
- 235000019333 sodium laurylsulphate Nutrition 0.000 description 1
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 description 1
- 235000019830 sodium polyphosphate Nutrition 0.000 description 1
- 235000019832 sodium triphosphate Nutrition 0.000 description 1
- IXYACKYHUWCLAM-UHFFFAOYSA-M sodium;2-ethylhex-1-ene-1-sulfonate Chemical compound [Na+].CCCCC(CC)=CS([O-])(=O)=O IXYACKYHUWCLAM-UHFFFAOYSA-M 0.000 description 1
- FGDMJJQHQDFUCP-UHFFFAOYSA-M sodium;2-propan-2-ylnaphthalene-1-sulfonate Chemical compound [Na+].C1=CC=CC2=C(S([O-])(=O)=O)C(C(C)C)=CC=C21 FGDMJJQHQDFUCP-UHFFFAOYSA-M 0.000 description 1
- MZSDGDXXBZSFTG-UHFFFAOYSA-M sodium;benzenesulfonate Chemical compound [Na+].[O-]S(=O)(=O)C1=CC=CC=C1 MZSDGDXXBZSFTG-UHFFFAOYSA-M 0.000 description 1
- 244000000034 soilborne pathogen Species 0.000 description 1
- 239000004455 soybean meal Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 239000012086 standard solution Substances 0.000 description 1
- 229940037312 stearamide Drugs 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 150000003460 sulfonic acids Chemical class 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 229920001059 synthetic polymer Polymers 0.000 description 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
- QGHREAKMXXNCOA-UHFFFAOYSA-N thiophanate-methyl Chemical compound COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC QGHREAKMXXNCOA-UHFFFAOYSA-N 0.000 description 1
- 239000013008 thixotropic agent Substances 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- FHYUCVWDMABHHH-UHFFFAOYSA-N toluene;1,2-xylene Chemical group CC1=CC=CC=C1.CC1=CC=CC=C1C FHYUCVWDMABHHH-UHFFFAOYSA-N 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000010455 vermiculite Substances 0.000 description 1
- 229910052902 vermiculite Inorganic materials 0.000 description 1
- 235000019354 vermiculite Nutrition 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D261/00—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings
- C07D261/02—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings not condensed with other rings
- C07D261/06—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings not condensed with other rings having two or more double bonds between ring members or between ring members and non-ring members
- C07D261/10—Heterocyclic compounds containing 1,2-oxazole or hydrogenated 1,2-oxazole rings not condensed with other rings having two or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D261/12—Oxygen atoms
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/80—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11480892 | 1992-05-07 | ||
| JP4252393 | 1993-03-03 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CZ84093A3 CZ84093A3 (en) | 1994-02-16 |
| CZ287192B6 true CZ287192B6 (en) | 2000-10-11 |
Family
ID=26382231
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CZ1993840A CZ287192B6 (en) | 1992-05-07 | 1993-05-07 | Calcium salt dihydrate of 3-hydroxy-5-methylisoxazole, process of its preparation, fungicidal agent and protection method of plants |
Country Status (23)
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2174484A1 (en) * | 1995-04-20 | 1996-10-21 | Masaki Hashimoto | Cut flower preservative slurry composition |
| AU7728498A (en) * | 1997-06-09 | 1998-12-30 | Dustin Investments Cc | A composition for use as a pharmaceutical and in specific agricultural and industrial applications |
| EP1145621B8 (en) * | 1998-11-06 | 2008-10-15 | Mebiol Inc. | Water-holding carriers for plants and water-holding materials for growing plants |
| JP3182648B2 (ja) * | 1999-05-12 | 2001-07-03 | ティーディーケイ株式会社 | セラミック成形体の成形用のセラミック顆粒、その製造または処理方法、セラミック成形体およびその製造方法 |
| DE10001548A1 (de) * | 2000-01-14 | 2001-07-19 | Innovation Pro Terra Gmbh & Co | Pflanzsubstrate |
| DE10042894A1 (de) * | 2000-08-31 | 2002-03-14 | Thor Chemie Gmbh | Synergistische Biozidzusammensetzung mit 2-Methylisothiazolin-3-on |
| UA74713C2 (en) * | 2004-04-29 | 2006-01-16 | Inst Of System Innovations Sal | Using a calcium salt in easily soluble form as an adaptogen to hydrothermal meteostresses in the period of plant vegetation and a multipurpose fungicidal preparation on basis thereof |
| US7977119B2 (en) * | 2004-12-08 | 2011-07-12 | Agilent Technologies, Inc. | Chemical arrays and methods of using the same |
| US20070207927A1 (en) * | 2006-03-01 | 2007-09-06 | Rosa Fred C | Polymer based seed coating |
| EA014222B1 (ru) * | 2010-01-11 | 2010-10-29 | Виктор Валентинович МОХОВ | Биоорганический препарат для обработки растений (варианты) |
| CN105248450A (zh) * | 2011-01-28 | 2016-01-20 | 迪帕克·普兰吉万达斯·沙阿 | 包括硫、杀虫剂和农业化学赋形剂的杀虫剂组合物 |
| CN102516190B (zh) * | 2011-12-06 | 2014-04-09 | 西北农林科技大学 | 噁唑喹啉类有机铜化合物及其制备方法、制剂及在防治农业植物病害中的用途 |
| CN102516189B (zh) * | 2011-12-06 | 2014-04-09 | 西北农林科技大学 | 噁唑类有机铜化合物及其制备方法、制剂及在防治农业植物病害中的用途 |
| HK1215355A1 (zh) * | 2012-12-31 | 2016-08-26 | Dow Agrosciences Llc | 調節由雙二硫代氨基甲酸鹽殺真菌劑生產亞乙基雙異硫氰酸酯硫化物的生產率的組合物和方法 |
| WO2020203963A1 (ja) * | 2019-04-05 | 2020-10-08 | 三井化学アグロ株式会社 | 効力の増強された農薬組成物 |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
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| NL130992C (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1964-09-14 | |||
| GB1199737A (en) * | 1967-08-18 | 1970-07-22 | Sankyo Co | Process for the preparation of 3-Hydroxyisoxazole Compounds and Alkali Metal Salts thereof |
| GB1256835A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1969-07-03 | 1971-12-15 | ||
| JPS4838148B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1970-05-07 | 1973-11-15 | ||
| JPS4940933B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1970-08-19 | 1974-11-06 | ||
| JPS4838148A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1971-09-10 | 1973-06-05 | ||
| JPS5710083B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1972-04-25 | 1982-02-24 | ||
| JPS4922821A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1972-06-20 | 1974-02-28 | ||
| JPS5430097B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1972-06-29 | 1979-09-28 | ||
| JPS4940933A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1972-08-25 | 1974-04-17 | ||
| JPS5679605A (en) * | 1979-12-04 | 1981-06-30 | Sankyo Co Ltd | Preventing agent against damping-off of rice plant |
| JPS5687506A (en) * | 1979-12-19 | 1981-07-16 | Sankyo Co Ltd | Preventing agent against damping-off of rice plant |
| US4663364A (en) * | 1984-09-05 | 1987-05-05 | Kao Corporation | Biocidal fine powder, its manufacturing method and a suspension for agricultural use containing the above powder |
| JPS61151650A (ja) * | 1984-12-26 | 1986-07-10 | Konishiroku Photo Ind Co Ltd | ハロゲン化銀カラ−写真感光材料の処理方法 |
| DE3609939A1 (de) * | 1986-03-24 | 1987-10-01 | Cassella Ag | Fluessige zubereitung von 1,2-benzisothiazolin-3-on, ihre herstellung und verwendung |
| US5219875A (en) * | 1990-11-27 | 1993-06-15 | Rohm And Haas Company | Antimicrobial compositions comprising iodopropargyl butylcarbamate and 1,2-benzisothiazolin-3-one and methods of controlling microbes |
| JPH05108798A (ja) | 1991-10-17 | 1993-04-30 | Shinko Electric Ind Co Ltd | 画像処理方法と画像処理装置 |
| DE69830746T2 (de) | 1997-12-26 | 2006-04-27 | Zeon Corp. | Verfahren zur herstellung von verbindungen mit einem -ch2-chf- strukturelement |
| JP4529263B2 (ja) | 2000-09-18 | 2010-08-25 | 沖電気工業株式会社 | アイリス認識装置 |
| JP3973380B2 (ja) | 2001-07-25 | 2007-09-12 | シャープ株式会社 | 液晶表示装置 |
| JP4572625B2 (ja) | 2004-08-25 | 2010-11-04 | 三菱マテリアルシ−エムアイ株式会社 | モータ |
-
1993
- 1993-04-30 IL IL105577A patent/IL105577A/xx not_active IP Right Cessation
- 1993-05-03 LT LTIP508A patent/LT3180B/lt unknown
- 1993-05-04 DK DK93303446T patent/DK0569210T3/da active
- 1993-05-04 TW TW082103499A patent/TW272115B/zh active
- 1993-05-04 AT AT93303446T patent/ATE162046T1/de not_active IP Right Cessation
- 1993-05-04 ES ES93303446T patent/ES2114001T3/es not_active Expired - Lifetime
- 1993-05-04 DE DE69316262T patent/DE69316262T2/de not_active Expired - Fee Related
- 1993-05-04 EP EP93303446A patent/EP0569210B1/en not_active Expired - Lifetime
- 1993-05-06 PL PL93298838A patent/PL171674B1/pl not_active IP Right Cessation
- 1993-05-06 PL PL93315290A patent/PL172320B1/pl not_active IP Right Cessation
- 1993-05-06 HU HU9301315A patent/HU215381B/hu not_active IP Right Cessation
- 1993-05-06 RU RU93005331/04A patent/RU2091024C1/ru not_active IP Right Cessation
- 1993-05-06 UY UY23579A patent/UY23579A1/es not_active IP Right Cessation
- 1993-05-06 CA CA002095658A patent/CA2095658C/en not_active Expired - Fee Related
- 1993-05-07 SK SK447-93A patent/SK280972B6/sk unknown
- 1993-05-07 KR KR1019930007867A patent/KR100278876B1/ko not_active Expired - Fee Related
- 1993-05-07 CZ CZ1993840A patent/CZ287192B6/cs not_active IP Right Cessation
- 1993-05-07 LV LVP-93-300A patent/LV10447B/en unknown
- 1993-05-07 FI FI932070A patent/FI106525B/fi active
- 1993-05-07 CN CN93107075A patent/CN1070022C/zh not_active Expired - Fee Related
-
1994
- 1994-07-06 US US08/271,264 patent/US5472972A/en not_active Expired - Lifetime
- 1994-07-12 EE EE9400019A patent/EE03133B1/xx not_active IP Right Cessation
-
1995
- 1995-05-04 US US08/433,834 patent/US5554391A/en not_active Expired - Lifetime
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1998
- 1998-03-13 GR GR980400545T patent/GR3026360T3/el unknown
- 1998-04-08 HK HK98102958A patent/HK1003820A1/en not_active IP Right Cessation
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2000
- 2000-12-12 CN CNB001307959A patent/CN1149927C/zh not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PD00 | Pending as of 2000-06-30 in czech republic | ||
| MM4A | Patent lapsed due to non-payment of fee |
Effective date: 20080507 |