CR9805A - Proceso para la produccion de amidas - Google Patents

Proceso para la produccion de amidas

Info

Publication number
CR9805A
CR9805A CR9805A CR9805A CR9805A CR 9805 A CR9805 A CR 9805A CR 9805 A CR9805 A CR 9805A CR 9805 A CR9805 A CR 9805A CR 9805 A CR9805 A CR 9805A
Authority
CR
Costa Rica
Prior art keywords
formula
compound
reaction
amidas
production
Prior art date
Application number
CR9805A
Other languages
English (en)
Inventor
Hans Tobler
Harald Walter
Josef Ehrenfreund
Camilla Corsi
Fanny Giordano
Martin Zeller
Gottfried Seifert
Shailesh Shah
Neil George
Original Assignee
Syngenta Participations Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Syngenta Participations Ag filed Critical Syngenta Participations Ag
Publication of CR9805A publication Critical patent/CR9805A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/43—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C07C211/57—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings being part of condensed ring systems of the carbon skeleton
    • C07C211/61—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings being part of condensed ring systems of the carbon skeleton with at least one of the condensed ring systems formed by three or more rings
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/06—Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/30—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
    • C07C209/32—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
    • C07C209/325—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups reduction by other means than indicated in C07C209/34 or C07C209/36
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
    • C07C209/70—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton by reduction of unsaturated amines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00—Systems containing at least three condensed rings
    • C07C2603/56—Ring systems containing bridged rings
    • C07C2603/58—Ring systems containing bridged rings containing three rings
    • C07C2603/60—Ring systems containing bridged rings containing three rings containing at least one ring with less than six members
    • C07C2603/66—Ring systems containing bridged rings containing three rings containing at least one ring with less than six members containing five-membered rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Agronomy & Crop Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Hydrogenated Pyridines (AREA)

Abstract

Se refiere al proceso para la preparacion de compuestos de la formula en la cual R1 y R2 son cada uno independientes de los otros hidrogeno o C1-C5 alkilo y R3 es CF3 o CF2H por a) reaccion de un compuesto de la formula (II) en la cual R1 y R2 son como estan definidas para la formula (I) con al menos un agente reductor para formar un compuesto de formula (III) en el cual R1 y R2 son como estan definidas para la formula (I), y b) reaccion de ese compuesto con al menos un agente reductor para formar un compuesto de la formula (IV) en el cual R1 y R2, son como estan definidos en la formula (I) y (c) reaccion de ese compuesto con un compuesto de formula (V) en el cual Q es cloro, fluor, bromo, yodo, hidroxido o C1-C6 alkoxi y R3 es como se define en la formula (I) para formar el compuesto de la formula (I); y para intermediarios novedosos para utilizarse en ese proceso.
CR9805A 2005-09-16 2008-03-07 Proceso para la produccion de amidas CR9805A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH15202005 2005-09-16
CH2962006 2006-02-24

Publications (1)

Publication Number Publication Date
CR9805A true CR9805A (es) 2008-07-31

Family

ID=37467494

Family Applications (1)

Application Number Title Priority Date Filing Date
CR9805A CR9805A (es) 2005-09-16 2008-03-07 Proceso para la produccion de amidas

Country Status (18)

Country Link
US (3) US7994341B2 (es)
EP (3) EP1928838B1 (es)
JP (1) JP5118043B2 (es)
CN (5) CN101979375A (es)
AR (1) AR058050A1 (es)
AU (1) AU2006291419B2 (es)
BR (1) BRPI0616238B1 (es)
CA (1) CA2622097C (es)
CL (1) CL2011000514A1 (es)
CO (1) CO6382182A2 (es)
CR (1) CR9805A (es)
EA (2) EA013638B1 (es)
EC (1) ECSP088264A (es)
ES (1) ES2397932T3 (es)
IL (2) IL189757A (es)
SG (1) SG165380A1 (es)
TW (2) TWI436984B (es)
WO (1) WO2007031323A1 (es)

Families Citing this family (43)

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JP4643441B2 (ja) * 2002-08-22 2011-03-02 シンジェンタ パーティシペーションズ アクチェンゲゼルシャフト 化合物
CN102524266B (zh) * 2006-04-06 2014-06-18 先正达参股股份有限公司 杀真菌组合物
EP2086944B1 (de) 2006-11-03 2010-01-13 Basf Se Verfahren zur herstellung von difluormethylpyrazolylcarboxylaten
US7994207B2 (en) * 2006-12-21 2011-08-09 Basf Se Process for preparing fluoromethyl-substituted heterocyclic compounds
CN101626684B (zh) * 2007-03-16 2013-10-30 辛根塔有限公司 杀微生物剂的固体形式
CN101679282B (zh) 2007-06-01 2012-11-28 巴斯夫欧洲公司 生产n-取代的(3-二卤甲基-1-甲基吡唑-4-基)羧酰胺的方法
JP5559678B2 (ja) 2007-06-15 2014-07-23 ビーエーエスエフ ソシエタス・ヨーロピア ジフルオロメチル置換ピラゾール化合物の製造方法
EP2008996A1 (en) * 2007-06-27 2008-12-31 Syngeta Participations AG Process for the production of pyrazoles
WO2009106619A1 (en) 2008-02-29 2009-09-03 Basf Se Process for preparing alkyl 2-alkoxymethylene-4,4-difluoro-3-oxobutyrates
KR20110010621A (ko) 2008-05-02 2011-02-01 바스프 에스이 할로겐-치환된 2-(아미노메틸리덴)-3-옥소부티르산 에스테르의 제조 방법
BRPI0911898A2 (pt) 2008-05-02 2015-10-13 Basf Se processo para preparar compostos, e, composto.
MX2010011433A (es) 2008-05-05 2010-11-12 Basf Se Procedimiento para la preparacion de compuestos pirazolicos sustituidos en posiciones 1,3,4.
BRPI0912383A2 (pt) 2008-05-08 2015-07-28 Basf Se Processo para preparar aril carboxamidas
JP2011520828A (ja) * 2008-05-14 2011-07-21 シンジェンタ リミテッド アミド類の製造方法
KR20110031501A (ko) 2008-07-21 2011-03-28 바스프 에스이 1,3-이치환된 피라졸카르복실산 에스테르의 제조 방법
JP5406302B2 (ja) * 2008-10-27 2014-02-05 シンジェンタ パーティシペーションズ アクチェンゲゼルシャフト ベンゾノルボルネンの製造方法
WO2010072631A1 (en) * 2008-12-24 2010-07-01 Syngenta Limited Methods for the preparation of fungicides
WO2011098386A1 (en) 2010-02-09 2011-08-18 Syngenta Participations Ag Process for the preparation of an anthranilic acid derivative
ES2478875T3 (es) 2010-04-20 2014-07-23 Syngenta Participations Ag Proceso para preparar amidas de ácidos carboxílicos pirazólicos
CN103097362B (zh) * 2010-06-07 2015-06-10 陶氏益农公司 作为杀真菌剂的吡嗪基甲酰胺
US8309747B2 (en) * 2010-07-06 2012-11-13 Chevron Phillips Chemical Company Lp Process for synthesizing bridged cyclopentadienyl-indenyl metallocenes
EP2632901B1 (en) 2010-10-27 2018-09-12 Solvay Sa Process for the preparation of pyrazole-4-carboxamides
US9375004B2 (en) * 2010-11-15 2016-06-28 Bayer Intellectual Property Gmbh 5-halogenopyrazolecarboxamides
CN103619822A (zh) * 2011-06-21 2014-03-05 拜耳知识产权有限责任公司 制备吡唑基甲酰苯胺类化合物的方法
EP2850066B1 (de) * 2012-05-14 2016-03-16 Bayer CropScience AG Verfahren zum herstellen von 1-alkyl-3-fluoralkyl-1h-pyrazol-4-carbonsäurechloriden
US20150175974A1 (en) * 2012-06-11 2015-06-25 Syngenta Participations Ag Producing solids and related mother liquors
CN104649973B (zh) 2013-11-25 2017-02-15 沈阳中化农药化工研发有限公司 一种吡唑酰胺类化合物及其用途
GB201403438D0 (en) * 2014-02-27 2014-04-16 Syngenta Participations Ag Polymorphs
EP2980078A1 (en) 2014-07-29 2016-02-03 Solvay SA Process for the preparation of pyrazole-4-carboxamides
EP3293179A4 (en) 2015-05-06 2018-09-19 Shenyang Sinochem Agrochemicals R & D Co., Ltd. Amide compound and the preparation method and use thereof
EP3408259A1 (en) 2016-01-28 2018-12-05 Solvay SA Halogen substituted diketones, pyrazole compounds and processes for the manufacture of pyrazole compounds
WO2017194517A1 (en) 2016-05-10 2017-11-16 Solvay Sa Composition comprising 3-(haloalkyl or formyl)-1h-pyrazole-4-carboxylic acids or esters, its manufacture and its use for the preparation of carboxamides
WO2018024644A1 (en) 2016-08-02 2018-02-08 Solvay Sa Manufacture of hydrazinyl compounds useful in the manufacture of pyrazole carboxylic acid and derivatives, hydrazinyl compounds and their use
CN106045910B (zh) * 2016-08-15 2017-10-10 浙江永太科技股份有限公司 一种3‑(二氟甲基)‑1‑甲基‑1h‑吡唑‑4‑羧酸的合成方法
CN106279025B (zh) * 2016-08-15 2017-10-10 浙江永太科技股份有限公司 一种含吡唑环的二酯化合物及其制备方法
WO2018083281A1 (en) 2016-11-07 2018-05-11 Solvay Sa Process for the manufacture of carboxylic acids or carboxylic acid derivatives
WO2018201272A1 (en) 2017-05-02 2018-11-08 Solvay Fluor Gmbh Process for the manufacture of carboxylic acids or carboxylic acid derivatives
WO2019044266A1 (ja) 2017-08-28 2019-03-07 株式会社日本ファインケム ピラゾール－４－カルボキサミド誘導体の製造方法
EP3495351A1 (en) 2017-12-08 2019-06-12 Solvay Sa Oxidation of a pyrazolyl ketone compound to the corresponding carboxylic acid
US20210171468A1 (en) 2017-12-22 2021-06-10 Solvay Sa Process for the manufacture of pyrazole carboxylic derivatives and precursors thereof
CN111454157B (zh) * 2020-05-14 2022-07-22 利民化学有限责任公司 一种3-硝基苯炔的制备方法
CN112174891B (zh) * 2020-11-02 2022-02-01 浙江省农业科学院 一种氟唑菌苯胺代谢物的制备方法
CN113235632B (zh) * 2021-04-14 2022-07-08 中铁二十四局集团有限公司 可自动实时纠偏的沉井下沉装置及施工方法

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DE10228103A1 (de) 2002-06-24 2004-01-15 Bayer Cropscience Ag Fungizide Wirkstoffkombinationen
JP4643441B2 (ja) * 2002-08-22 2011-03-02 シンジェンタ パーティシペーションズ アクチェンゲゼルシャフト 化合物
GB0224316D0 (en) * 2002-10-18 2002-11-27 Syngenta Participations Ag Chemical compounds
GB0422401D0 (en) * 2004-10-08 2004-11-10 Syngenta Participations Ag Fungicidal compositions
ES2354374T3 (es) * 2005-10-25 2011-03-14 Syngenta Participations Ag Derivados de amidas heterocíclicas útiles como microbiocidas.

Also Published As

Publication number Publication date
IL189757A (en) 2013-08-29
TW200804292A (en) 2008-01-16
EA201000345A1 (ru) 2010-06-30
AU2006291419A1 (en) 2007-03-22
CN101277938B (zh) 2012-01-11
IL217212A0 (en) 2012-01-31
US8436037B2 (en) 2013-05-07
US8680337B2 (en) 2014-03-25
US20120065239A1 (en) 2012-03-15
AU2006291419B2 (en) 2012-06-14
TWI436984B (zh) 2014-05-11
CN101979374A (zh) 2011-02-23
BRPI0616238B1 (pt) 2016-01-19
CN101979375A (zh) 2011-02-23
EP1928838A1 (en) 2008-06-11
EP2253622A1 (en) 2010-11-24
US20090163569A1 (en) 2009-06-25
ES2397932T3 (es) 2013-03-12
EA013638B1 (ru) 2010-06-30
CA2622097A1 (en) 2007-03-22
CN101962363A (zh) 2011-02-02
CN101277938A (zh) 2008-10-01
AR058050A1 (es) 2008-01-23
EA200800840A1 (ru) 2008-08-29
CO6382182A2 (es) 2012-02-15
BRPI0616238A2 (pt) 2011-06-14
CN101962364B (zh) 2013-01-09
CN101962364A (zh) 2011-02-02
EP2253623A1 (en) 2010-11-24
ECSP088264A (es) 2008-04-28
JP5118043B2 (ja) 2013-01-16
JP2009509935A (ja) 2009-03-12
CL2011000514A1 (es) 2011-05-06
US20130253225A1 (en) 2013-09-26
SG165380A1 (en) 2010-10-28
TW201247628A (en) 2012-12-01
US7994341B2 (en) 2011-08-09
IL189757A0 (en) 2008-08-07
EP1928838B1 (en) 2012-10-24
EP2253623B1 (en) 2013-10-23
CA2622097C (en) 2014-04-15
WO2007031323A1 (en) 2007-03-22

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