CL2011000514A1 - Modificacion de cristal b de la (9-isopropil-1,2,3,4-tetrahidro-1,4-metano-naftalen-5-il)-amida del acido sin-3-difluormetil-1-metil-1h-pirazol-4-carboxilico; composicion para el control de enfermedades fitopatogenas que comprende a dicha modificacion cristalina; y metodo para controlar enfermedades fitopatogenas que utiliza dicha composicion (div. sol. n°2466-06). - Google Patents

Modificacion de cristal b de la (9-isopropil-1,2,3,4-tetrahidro-1,4-metano-naftalen-5-il)-amida del acido sin-3-difluormetil-1-metil-1h-pirazol-4-carboxilico; composicion para el control de enfermedades fitopatogenas que comprende a dicha modificacion cristalina; y metodo para controlar enfermedades fitopatogenas que utiliza dicha composicion (div. sol. n°2466-06).

Info

Publication number
CL2011000514A1
CL2011000514A1 CL2011000514A CL2011000514A CL2011000514A1 CL 2011000514 A1 CL2011000514 A1 CL 2011000514A1 CL 2011000514 A CL2011000514 A CL 2011000514A CL 2011000514 A CL2011000514 A CL 2011000514A CL 2011000514 A1 CL2011000514 A1 CL 2011000514A1
Authority
CL
Chile
Prior art keywords
composition
modification
methane
methyl
phytopathogenic diseases
Prior art date
Application number
CL2011000514A
Other languages
English (en)
Inventor
Harald Walter
Hans Tobler
Josef Ehrenfreund
Martin Zeller
Fanny Giordano
Gottfried Seifert
Camilla Corsi
Original Assignee
Syngenta Participations Ag
Syngenta Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Syngenta Participations Ag, Syngenta Ltd filed Critical Syngenta Participations Ag
Publication of CL2011000514A1 publication Critical patent/CL2011000514A1/es

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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00Compounds containing amino groups bound to a carbon skeleton
    • C07C211/43Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C07C211/57Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings being part of condensed ring systems of the carbon skeleton
    • C07C211/61Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings being part of condensed ring systems of the carbon skeleton with at least one of the condensed ring systems formed by three or more rings
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/561,2-Diazoles; Hydrogenated 1,2-diazoles
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/06Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of six-membered aromatic rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/30Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
    • C07C209/32Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
    • C07C209/325Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups reduction by other means than indicated in C07C209/34 or C07C209/36
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/68Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
    • C07C209/70Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton by reduction of unsaturated amines
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2603/00Systems containing at least three condensed rings
    • C07C2603/56Ring systems containing bridged rings
    • C07C2603/58Ring systems containing bridged rings containing three rings
    • C07C2603/60Ring systems containing bridged rings containing three rings containing at least one ring with less than six members
    • C07C2603/66Ring systems containing bridged rings containing three rings containing at least one ring with less than six members containing five-membered rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Hydrogenated Pyridines (AREA)

Abstract

LA MODIFICACIÓN CRISTALINA B DE LA (9-ISOPROPIL-1 ,2,3,4-TETRAHIDRO-1 ,4-METANO-NAFTALEN-5-IL)-AMIDA DEL ÁCIDO SIN-3- DIFLUORMETII-1-METIL-1 H-PIRAZOL-4-CARBOXÍLICO, QUE TIENE UN PATRÓN DE DIFRACCIÓN DE POLVO DE RAYOS-X, EXPRESADOS EN TÉRMINOS DE ESPACIOS-D Y DE INTENSIDADES RELATIVAS, DONDE DICHO PATRÓN DE DIFRACCIÓN DE POLVO DE RAYOS-X COMPRENDE LAS SIGUIENTES LINEAS CARACTERISTICAS; 13,42 A(FUERTE), 9,76 A(MEDIO), 6,93 A(MEDIO), 6,74 A(MEDIO), 4,79 A(MEDIO), 4,73 A(MEDIO), Y 3,66 A(MEDIO), Y ADEMÁS TIENE EN EL TERMOGRAMA DE CALORIMETRÍA DE BARRIDO DIFERENCIAL UNA SEÑAL ENDOTÉRMICA CON UN PICO EN EL RANGO DE 120°C A 128°C. UNA COMPOSICIÓN PARA EL CONTROL DE ENFERMEDADES CAUSADAS POR FITOPATOGENOS EN PLANTAS ÚTILES O EN EL MATERIAL DE PROPAGACIÓN DE LAS MISMAS, QUE ADEMÁS DE LOS USUALES ADYUVANTES INERTES DE FORMULACIÓN, COMPRENDE COMO PRINCIPIO ACTIVO AL MENOS LA MODIFICACIÓN CRISTALINA B DE LA (9-ISOPROPIL-1 ,2,3,4-TETRAHIDRO- 1,4-METANO-NAFTALEN-5-IL)-AMIDA DEL ÁCIDO SIN-3-DIFLUORMETIL-1-METIL-1 H-PIRAZOL-4-CARBOXILICO. UN MÉTODO PARA CONTROLAR ENFERMEDADES CAUSADAS POR FITOPATÓGENOS EN PLANTAS ÚTILES O EN MATERIAL DE PROPAGACIÓN DE LAS MISMAS, QUE COMPRENDE APLICAR A LAS PLANTAS ÚTILES, AL LUGAR DE LAS MISMAS O AL MATERIAL DE PROPAGACIÓN DE LAS MISMAS UNA COMPOSICIÓN PARA EL CONTROL DE ENFERMEDADES CAUSADAS POR FITOPATÓGENOS.
CL2011000514A 2005-09-16 2011-03-10 Modificacion de cristal b de la (9-isopropil-1,2,3,4-tetrahidro-1,4-metano-naftalen-5-il)-amida del acido sin-3-difluormetil-1-metil-1h-pirazol-4-carboxilico; composicion para el control de enfermedades fitopatogenas que comprende a dicha modificacion cristalina; y metodo para controlar enfermedades fitopatogenas que utiliza dicha composicion (div. sol. n°2466-06). CL2011000514A1 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH15202005 2005-09-16
CH2962006 2006-02-24

Publications (1)

Publication Number Publication Date
CL2011000514A1 true CL2011000514A1 (es) 2011-05-06

Family

ID=37467494

Family Applications (1)

Application Number Title Priority Date Filing Date
CL2011000514A CL2011000514A1 (es) 2005-09-16 2011-03-10 Modificacion de cristal b de la (9-isopropil-1,2,3,4-tetrahidro-1,4-metano-naftalen-5-il)-amida del acido sin-3-difluormetil-1-metil-1h-pirazol-4-carboxilico; composicion para el control de enfermedades fitopatogenas que comprende a dicha modificacion cristalina; y metodo para controlar enfermedades fitopatogenas que utiliza dicha composicion (div. sol. n°2466-06).

Country Status (18)

Country Link
US (3) US7994341B2 (es)
EP (3) EP1928838B1 (es)
JP (1) JP5118043B2 (es)
CN (5) CN101979374A (es)
AR (1) AR058050A1 (es)
AU (1) AU2006291419B2 (es)
BR (1) BRPI0616238B1 (es)
CA (1) CA2622097C (es)
CL (1) CL2011000514A1 (es)
CO (1) CO6382182A2 (es)
CR (1) CR9805A (es)
EA (2) EA013638B1 (es)
EC (1) ECSP088264A (es)
ES (1) ES2397932T3 (es)
IL (2) IL189757A (es)
SG (1) SG165380A1 (es)
TW (2) TWI436984B (es)
WO (1) WO2007031323A1 (es)

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JP5558467B2 (ja) 2008-07-21 2014-07-23 ビーエーエスエフ ソシエタス・ヨーロピア 1,3−二置換ピラゾールカルボン酸エステルの調製方法
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BRPI0923527A2 (pt) * 2008-12-24 2016-08-09 Syngenta Ltd métodos de preparo de fungicidas
WO2011098386A1 (en) 2010-02-09 2011-08-18 Syngenta Participations Ag Process for the preparation of an anthranilic acid derivative
ES2478875T3 (es) * 2010-04-20 2014-07-23 Syngenta Participations Ag Proceso para preparar amidas de ácidos carboxílicos pirazólicos
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AR083876A1 (es) * 2010-11-15 2013-03-27 Bayer Cropscience Ag 5-halogenopirazolcarboxamidas
BR112013032988A2 (pt) * 2011-06-21 2016-08-16 Bayer Ip Gmbh método para a produção de pirazolilcarboxanilidas
US9145369B2 (en) * 2012-05-14 2015-09-29 Bayer Cropscience Ag Process for preparing 1-alkyl-3-fluoroalkyl-1H-pyrazole-4-carboxylic acid chlorides
EP2861064A4 (en) * 2012-06-11 2015-12-02 Syngenta Participations Ag METHODS OF MANUFACTURING SOLID MATERIALS AND ASSOCIATED MOTHERLAMERS
CN104649973B (zh) 2013-11-25 2017-02-15 沈阳中化农药化工研发有限公司 一种吡唑酰胺类化合物及其用途
GB201403438D0 (en) * 2014-02-27 2014-04-16 Syngenta Participations Ag Polymorphs
EP2980078A1 (en) 2014-07-29 2016-02-03 Solvay SA Process for the preparation of pyrazole-4-carboxamides
WO2016177318A1 (zh) 2015-05-06 2016-11-10 沈阳中化农药化工研发有限公司 一种酰胺类化合物及其制备方法和用途
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EP3455211A1 (en) 2016-05-10 2019-03-20 Solvay SA Composition comprising 3-(haloalkyl or formyl)-1h-pyrazole-4-carboxylic acids or esters, its manufacture and its use for the preparation of carboxamides
EP3494107A1 (en) 2016-08-02 2019-06-12 Solvay Sa Manufacture of hydrazinyl compounds useful in the manufacture of pyrazole carboxylic acid and derivatives, hydrazinyl compounds and their use
CN106045910B (zh) * 2016-08-15 2017-10-10 浙江永太科技股份有限公司 一种3‑(二氟甲基)‑1‑甲基‑1h‑吡唑‑4‑羧酸的合成方法
CN106279025B (zh) * 2016-08-15 2017-10-10 浙江永太科技股份有限公司 一种含吡唑环的二酯化合物及其制备方法
EP3535245A1 (en) 2016-11-07 2019-09-11 Solvay SA Process for the manufacture of carboxylic acids or carboxylic acid derivatives
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US20210171468A1 (en) 2017-12-22 2021-06-10 Solvay Sa Process for the manufacture of pyrazole carboxylic derivatives and precursors thereof
CN111454157B (zh) * 2020-05-14 2022-07-22 利民化学有限责任公司 一种3-硝基苯炔的制备方法
CN112174891B (zh) * 2020-11-02 2022-02-01 浙江省农业科学院 一种氟唑菌苯胺代谢物的制备方法
CN113235632B (zh) * 2021-04-14 2022-07-08 中铁二十四局集团有限公司 可自动实时纠偏的沉井下沉装置及施工方法

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US8680337B2 (en) 2014-03-25
CN101277938B (zh) 2012-01-11
CN101979375A (zh) 2011-02-23
CN101962363A (zh) 2011-02-02
CN101962364B (zh) 2013-01-09
CA2622097C (en) 2014-04-15
ES2397932T3 (es) 2013-03-12
SG165380A1 (en) 2010-10-28
TW201247628A (en) 2012-12-01
WO2007031323A1 (en) 2007-03-22
BRPI0616238A2 (pt) 2011-06-14
CR9805A (es) 2008-07-31
CN101962364A (zh) 2011-02-02
AU2006291419B2 (en) 2012-06-14
IL189757A (en) 2013-08-29
AU2006291419A1 (en) 2007-03-22
JP5118043B2 (ja) 2013-01-16
EP2253622A1 (en) 2010-11-24
EP2253623B1 (en) 2013-10-23
EA013638B1 (ru) 2010-06-30
TWI436984B (zh) 2014-05-11
IL217212A0 (en) 2012-01-31
EA201000345A1 (ru) 2010-06-30
TW200804292A (en) 2008-01-16
EP1928838A1 (en) 2008-06-11
AR058050A1 (es) 2008-01-23
ECSP088264A (es) 2008-04-28
CO6382182A2 (es) 2012-02-15
JP2009509935A (ja) 2009-03-12
EP1928838B1 (en) 2012-10-24
US8436037B2 (en) 2013-05-07
US20120065239A1 (en) 2012-03-15
US7994341B2 (en) 2011-08-09
CN101979374A (zh) 2011-02-23
IL189757A0 (en) 2008-08-07
US20090163569A1 (en) 2009-06-25
CN101277938A (zh) 2008-10-01
EA200800840A1 (ru) 2008-08-29
US20130253225A1 (en) 2013-09-26
BRPI0616238B1 (pt) 2016-01-19
EP2253623A1 (en) 2010-11-24
CA2622097A1 (en) 2007-03-22

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