CO5111029A1 - Proceso para preparar polvos basados en metales de nano- tamano - Google Patents

Proceso para preparar polvos basados en metales de nano- tamano

Info

Publication number
CO5111029A1
CO5111029A1 CO99052594A CO99052594A CO5111029A1 CO 5111029 A1 CO5111029 A1 CO 5111029A1 CO 99052594 A CO99052594 A CO 99052594A CO 99052594 A CO99052594 A CO 99052594A CO 5111029 A1 CO5111029 A1 CO 5111029A1
Authority
CO
Colombia
Prior art keywords
paste
tamano
nano
metals
copolymer
Prior art date
Application number
CO99052594A
Other languages
English (en)
Inventor
A F Broos Jacques
Ronald Van Voorst
Original Assignee
Dow Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Chemical Co filed Critical Dow Chemical Co
Publication of CO5111029A1 publication Critical patent/CO5111029A1/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/10—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of rare earths
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/20—Catalysts, in general, characterised by their form or physical properties characterised by their non-solid state
    • B01J35/23—Catalysts, in general, characterised by their form or physical properties characterised by their non-solid state in a colloidal state
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05—Metallic powder characterised by the size or surface area of the particles
    • B22F1/054—Nanosized particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/30—Making metallic powder or suspensions thereof using chemical processes with decomposition of metal compounds, e.g. by pyrolysis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/18—Methods for preparing oxides or hydroxides in general by thermal decomposition of compounds, e.g. of salts or hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F17/00—Compounds of rare earth metals
    • C01F17/20—Compounds containing only rare earth metals as the metal element
    • C01F17/206—Compounds containing only rare earth metals as the metal element oxide or hydroxide being the only anion
    • C01F17/212—Scandium oxides or hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F17/00—Compounds of rare earth metals
    • C01F17/20—Compounds containing only rare earth metals as the metal element
    • C01F17/206—Compounds containing only rare earth metals as the metal element oxide or hydroxide being the only anion
    • C01F17/218—Yttrium oxides or hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F17/00—Compounds of rare earth metals
    • C01F17/20—Compounds containing only rare earth metals as the metal element
    • C01F17/206—Compounds containing only rare earth metals as the metal element oxide or hydroxide being the only anion
    • C01F17/224—Oxides or hydroxides of lanthanides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F17/00—Compounds of rare earth metals
    • C01F17/20—Compounds containing only rare earth metals as the metal element
    • C01F17/206—Compounds containing only rare earth metals as the metal element oxide or hydroxide being the only anion
    • C01F17/224—Oxides or hydroxides of lanthanides
    • C01F17/229—Lanthanum oxides or hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F17/00—Compounds of rare earth metals
    • C01F17/20—Compounds containing only rare earth metals as the metal element
    • C01F17/206—Compounds containing only rare earth metals as the metal element oxide or hydroxide being the only anion
    • C01F17/224—Oxides or hydroxides of lanthanides
    • C01F17/235—Cerium oxides or hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F17/00—Compounds of rare earth metals
    • C01F17/20—Compounds containing only rare earth metals as the metal element
    • C01F17/206—Compounds containing only rare earth metals as the metal element oxide or hydroxide being the only anion
    • C01F17/241—Compounds containing only rare earth metals as the metal element oxide or hydroxide being the only anion containing two or more rare earth metals, e.g. NdPrO3 or LaNdPrO3
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
    • C01G23/0536—Producing by wet processes, e.g. hydrolysing titanium salts by hydrolysing chloride-containing salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C01G25/02—Oxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Nanotechnology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Chemical & Material Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Environmental & Geological Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • Catalysts (AREA)

Abstract

Un proceso para producir polvos de metal, que tiene un tamaño inferior a 200 nm, que comprende las etapas de mezclar por lo menos una sal de metal con un copolímero no hidrofílico que contiene un óxido de etileno para formar una pasta de sal de metal/copolímero, ycalcinar la pasta a una temperatura entre 300 y 3000°C para expulsar el agua y los orgánicos de dicha pasta, dejando como residuo un polvo con base en metal que tiene un tamaño de partícula menor a 200 nm;en donde dicho copolímero tiene un peso molecular promedio mayor que 400, un contenido de óxido de etileno de 1 a 90 por ciento y un equilibrio hidrofílico-lipofílico (EHL) entre-15 y 15.
CO99052594A 1998-08-19 1999-08-19 Proceso para preparar polvos basados en metales de nano- tamano CO5111029A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US9711998P 1998-08-19 1998-08-19

Publications (1)

Publication Number Publication Date
CO5111029A1 true CO5111029A1 (es) 2001-12-26

Family

ID=22261235

Family Applications (1)

Application Number Title Priority Date Filing Date
CO99052594A CO5111029A1 (es) 1998-08-19 1999-08-19 Proceso para preparar polvos basados en metales de nano- tamano

Country Status (16)

Country Link
US (1) US6527825B1 (es)
EP (1) EP1112223B1 (es)
JP (1) JP2002523618A (es)
KR (1) KR20010072724A (es)
CN (1) CN1313832A (es)
AR (1) AR021774A1 (es)
AT (1) ATE240261T1 (es)
AU (1) AU5570799A (es)
BR (1) BR9913381A (es)
CA (1) CA2340096A1 (es)
CO (1) CO5111029A1 (es)
DE (1) DE69907931D1 (es)
TR (1) TR200100553T2 (es)
TW (1) TW458827B (es)
WO (1) WO2000010913A1 (es)
ZA (1) ZA200101050B (es)

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US6844026B2 (en) * 2001-02-12 2005-01-18 Rhodia Chimie Preparation of particles by hydrolysis of a metal cation in the presence of a polymer
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KR100483482B1 (ko) * 2001-08-24 2005-04-15 일양화학 주식회사 오산화안티몬의 나노분말 제조 방법
EP1298092A1 (de) * 2001-09-28 2003-04-02 Spiess -Urania Chemicals GmbH Kontrollierte Morphogenese von Kupfersalzen
KR100476557B1 (ko) * 2002-04-24 2005-03-17 삼성전기주식회사 나노크기의 금속입자 형성방법 및 이를 이용한 전도층형성방법
CN1317285C (zh) * 2002-09-29 2007-05-23 辽宁师范大学 催化法合成镧系金属有机化合物及其热分解制备纳米尺寸的镧系金属粉末
CN1557817B (zh) * 2004-02-03 2011-09-14 辽宁师范大学 萘镧系金属有机化合物合成及其真空热解制备纳米尺寸镧系金属粉末
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US7482382B2 (en) * 2004-05-19 2009-01-27 The Texas A&M University System Process for preparing nano-sized metal oxide particles
US20070004840A1 (en) * 2004-05-19 2007-01-04 Texas A&M University Zinc oxide polymer nanocomposites and methods of producing zinc oxide polymer nanocomposites
CN1622283A (zh) * 2004-12-15 2005-06-01 贺平 复合氧化物半导体纳米材料的制备方法
JP4767562B2 (ja) * 2005-03-11 2011-09-07 住友大阪セメント株式会社 ナノ粒子の製造方法
EP1879833A4 (en) * 2005-05-02 2009-09-30 Symyx Technologies Inc HIGH SURFACE METAL, METAL OXIDE MATERIALS AND METHOD OF MANUFACTURING THEREOF
KR100713298B1 (ko) * 2005-09-08 2007-05-04 한화석유화학 주식회사 내열성이 우수한 금속산화물 및 이의 제조방법
JP4950569B2 (ja) * 2006-06-20 2012-06-13 大陽日酸株式会社 シール材
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EP2093192A1 (en) * 2008-02-25 2009-08-26 Koninklijke Philips Electronics N.V. Preparation of nanoparticles from metal salts
CN102076610A (zh) * 2008-07-08 2011-05-25 巴斯夫欧洲公司 纳米粒的表面修饰的铜化合物
CN102105245A (zh) * 2008-07-23 2011-06-22 建筑研究和技术有限公司 在多元醇中制备金属纳米颗粒的方法
JP2013512870A (ja) * 2009-12-02 2013-04-18 ビーエーエスエフ ソシエタス・ヨーロピア 表面改質粒子状銅塩による植物病原性微生物の防除方法
RU2442751C1 (ru) * 2010-11-08 2012-02-20 Учреждение Российской академии наук Институт проблем химико-энергетических технологий Сибирского отделения РАН (ИПХЭТ СО РАН) Способ получения наноразмерных частиц оксида меди
WO2012109126A1 (en) 2011-02-08 2012-08-16 Dow Global Technologies Llc System and method for reducing emissions from a combustion process
RU2461668C1 (ru) * 2011-03-16 2012-09-20 Федеральное государственное бюджетное учреждение науки Институт высокотемпературной электрохимии Уральского отделения Российской Академии наук Способ получения наноразмерных частиц сложных оксидов металлов
RU2505379C1 (ru) * 2012-10-30 2014-01-27 Федеральное государственное автономное образовательное учреждение высшего профессионального образования "Национальный исследовательский технологический университет "МИСиС" Способ получения нанопорошков оксида цинка с поверхностным модифицированием для использования в строительных герметиках
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Also Published As

Publication number Publication date
CN1313832A (zh) 2001-09-19
BR9913381A (pt) 2001-05-22
TW458827B (en) 2001-10-11
US6527825B1 (en) 2003-03-04
AR021774A1 (es) 2002-08-07
DE69907931D1 (de) 2003-06-18
ZA200101050B (en) 2001-10-18
EP1112223A1 (en) 2001-07-04
JP2002523618A (ja) 2002-07-30
ATE240261T1 (de) 2003-05-15
CA2340096A1 (en) 2000-03-02
WO2000010913A1 (en) 2000-03-02
KR20010072724A (ko) 2001-07-31
EP1112223B1 (en) 2003-05-14
AU5570799A (en) 2000-03-14
TR200100553T2 (tr) 2001-07-23

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