CN1821081A - 一种制备氧化锌纳米棒的方法 - Google Patents
一种制备氧化锌纳米棒的方法 Download PDFInfo
- Publication number
- CN1821081A CN1821081A CN 200610049679 CN200610049679A CN1821081A CN 1821081 A CN1821081 A CN 1821081A CN 200610049679 CN200610049679 CN 200610049679 CN 200610049679 A CN200610049679 A CN 200610049679A CN 1821081 A CN1821081 A CN 1821081A
- Authority
- CN
- China
- Prior art keywords
- zinc oxide
- zinc
- seed
- solution
- oxide nano
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 title claims abstract description 108
- 239000011787 zinc oxide Substances 0.000 title claims abstract description 54
- 238000004519 manufacturing process Methods 0.000 title 1
- ONDPHDOFVYQSGI-UHFFFAOYSA-N zinc nitrate Chemical compound [Zn+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ONDPHDOFVYQSGI-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000000034 method Methods 0.000 claims abstract description 17
- 239000008367 deionised water Substances 0.000 claims abstract description 6
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 6
- 238000001035 drying Methods 0.000 claims abstract description 6
- 238000002156 mixing Methods 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000002270 dispersing agent Substances 0.000 claims abstract description 4
- 239000002073 nanorod Substances 0.000 claims description 17
- VKYKSIONXSXAKP-UHFFFAOYSA-N hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 claims description 14
- 235000010299 hexamethylene tetramine Nutrition 0.000 claims description 7
- 239000004312 hexamethylene tetramine Substances 0.000 claims description 7
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 6
- 239000006185 dispersion Substances 0.000 claims description 6
- -1 polyoxyethylene Polymers 0.000 claims description 6
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 4
- 239000011701 zinc Substances 0.000 claims description 4
- 229910052725 zinc Inorganic materials 0.000 claims description 4
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 3
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 3
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 3
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 abstract description 12
- 238000006243 chemical reaction Methods 0.000 abstract description 6
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- AGGKEGLBGGJEBZ-UHFFFAOYSA-N tetramethylenedisulfotetramine Chemical compound C1N(S2(=O)=O)CN3S(=O)(=O)N1CN2C3 AGGKEGLBGGJEBZ-UHFFFAOYSA-N 0.000 abstract 1
- 229960001296 zinc oxide Drugs 0.000 description 41
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 18
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 9
- 238000003756 stirring Methods 0.000 description 6
- ZOIORXHNWRGPMV-UHFFFAOYSA-N acetic acid;zinc Chemical compound [Zn].CC(O)=O.CC(O)=O ZOIORXHNWRGPMV-UHFFFAOYSA-N 0.000 description 3
- 239000002086 nanomaterial Substances 0.000 description 3
- 239000004246 zinc acetate Substances 0.000 description 3
- 230000005540 biological transmission Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000005669 field effect Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
Description
Claims (2)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CNB2006100496799A CN100391848C (zh) | 2006-03-02 | 2006-03-02 | 一种制备氧化锌纳米棒的方法 |
Applications Claiming Priority (1)
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CNB2006100496799A CN100391848C (zh) | 2006-03-02 | 2006-03-02 | 一种制备氧化锌纳米棒的方法 |
Publications (2)
Publication Number | Publication Date |
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CN1821081A true CN1821081A (zh) | 2006-08-23 |
CN100391848C CN100391848C (zh) | 2008-06-04 |
Family
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Family Applications (1)
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CNB2006100496799A Expired - Fee Related CN100391848C (zh) | 2006-03-02 | 2006-03-02 | 一种制备氧化锌纳米棒的方法 |
Country Status (1)
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CN (1) | CN100391848C (zh) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101357320B (zh) * | 2008-09-18 | 2010-06-09 | 福州大学 | 一维纳米阵列氧化锌固相微萃取涂层及其制备方法 |
CN103043706A (zh) * | 2012-12-04 | 2013-04-17 | 华南师范大学 | 受激发强蓝紫光的氧化锌纳米棒的制备方法 |
CN103303965A (zh) * | 2013-05-14 | 2013-09-18 | 上海交通大学 | 顶端多尖型氧化锌纳米棒结构的制备方法 |
CN106119961A (zh) * | 2016-06-15 | 2016-11-16 | 河南师范大学 | 一种尺寸可控的单晶氧化锌纳米棒的制备方法 |
CN106475104A (zh) * | 2016-11-20 | 2017-03-08 | 吉林师范大学 | 一种可回收珊瑚型光催化剂及其制备方法 |
CN106564929A (zh) * | 2016-10-21 | 2017-04-19 | 上海纳米技术及应用国家工程研究中心有限公司 | 一种Ag掺杂ZnO纳米气敏材料的制备方法 |
CN107815851A (zh) * | 2017-11-11 | 2018-03-20 | 钱景 | 基于氧化锌纳米棒功能棉织物的生物传感器 |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1533985A (zh) * | 2003-03-31 | 2004-10-06 | 上海大学 | 一种纳米级氧化锌粉体的制备方法 |
KR100650528B1 (ko) * | 2003-11-06 | 2006-11-28 | (주)나노하이브리드 | 자외선 레이저용 ZnO 나노-어레이 및 ZnO 나노월어레이의 실리콘 기판상의 형성 방법 |
CN1562762A (zh) * | 2004-04-22 | 2005-01-12 | 上海交通大学 | 单分散无团聚及强紫外吸收的纳米氧化锌的制备方法 |
CN1308244C (zh) * | 2005-04-26 | 2007-04-04 | 华中师范大学 | 激发光强度和频率调谐荧光频率的纳米氧化锌及其制备方法 |
CN1313377C (zh) * | 2005-07-14 | 2007-05-02 | 天津大学 | 在水溶液中大面积快速制备一维氧化锌阵列薄膜的方法 |
-
2006
- 2006-03-02 CN CNB2006100496799A patent/CN100391848C/zh not_active Expired - Fee Related
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101357320B (zh) * | 2008-09-18 | 2010-06-09 | 福州大学 | 一维纳米阵列氧化锌固相微萃取涂层及其制备方法 |
CN103043706A (zh) * | 2012-12-04 | 2013-04-17 | 华南师范大学 | 受激发强蓝紫光的氧化锌纳米棒的制备方法 |
CN103043706B (zh) * | 2012-12-04 | 2014-09-10 | 华南师范大学 | 受激发强蓝紫光的氧化锌纳米棒的制备方法 |
CN103303965A (zh) * | 2013-05-14 | 2013-09-18 | 上海交通大学 | 顶端多尖型氧化锌纳米棒结构的制备方法 |
CN103303965B (zh) * | 2013-05-14 | 2015-04-01 | 上海交通大学 | 顶端多尖型氧化锌纳米棒结构的制备方法 |
CN106119961A (zh) * | 2016-06-15 | 2016-11-16 | 河南师范大学 | 一种尺寸可控的单晶氧化锌纳米棒的制备方法 |
CN106119961B (zh) * | 2016-06-15 | 2018-07-06 | 河南师范大学 | 一种尺寸可控的单晶氧化锌纳米棒的制备方法 |
CN106564929A (zh) * | 2016-10-21 | 2017-04-19 | 上海纳米技术及应用国家工程研究中心有限公司 | 一种Ag掺杂ZnO纳米气敏材料的制备方法 |
CN106475104A (zh) * | 2016-11-20 | 2017-03-08 | 吉林师范大学 | 一种可回收珊瑚型光催化剂及其制备方法 |
CN107815851A (zh) * | 2017-11-11 | 2018-03-20 | 钱景 | 基于氧化锌纳米棒功能棉织物的生物传感器 |
Also Published As
Publication number | Publication date |
---|---|
CN100391848C (zh) | 2008-06-04 |
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C14 | Grant of patent or utility model | ||
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EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Zhejiang Haina Polytron Technologies Inc Assignor: Zhejiang University Contract fulfillment period: 2008.10.20 to 2013.9.30 Contract record no.: 2008330001423 Denomination of invention: Process for preparing zinc oxide nano stick Granted publication date: 20080604 License type: Exclusive license Record date: 20081028 |
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Free format text: EXCLUSIVE LICENSE; TIME LIMIT OF IMPLEMENTING CONTACT: 2008.10.20 TO 2013.9.30; CHANGE OF CONTRACT Name of requester: ZHEJIANG PROVINCE HAINA TECHNOLOGY CO., LTD. Effective date: 20081028 |
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Change date: 20110818 Contract record no.: 2008330001423 Assignee after: Zhejiang Zhonghe Electromechanical Co., Ltd. Assignee before: Zhejiang Haina Polytron Technologies Inc |
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