CN1785245A - Method for preparing composite traditional Chinese medicine soft capsule - Google Patents
Method for preparing composite traditional Chinese medicine soft capsule Download PDFInfo
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- CN1785245A CN1785245A CN 200510124020 CN200510124020A CN1785245A CN 1785245 A CN1785245 A CN 1785245A CN 200510124020 CN200510124020 CN 200510124020 CN 200510124020 A CN200510124020 A CN 200510124020A CN 1785245 A CN1785245 A CN 1785245A
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Abstract
A Chinse medicine in the form of softgel is prepared from the powdered extract of Chinese-medicinal material (10-70 Wt%) and auxiliary (30-90) through mixing, preparing the core material, preparing shell material and die pressing.
Description
Technical field
The present invention relates to a kind of Chinese medicine composition preparation of soft capsule method.
Background technology
The traditional Chinese medical science belongs to the nasal sinusitis category with rhinitis, sinusitis.How because of affection of exogenous wind-cold or wind heat, for a long time and heat-transformation, the heat stagnation lung meridian, impairment of purifying function of the lung, pathogenic heat are followed through last criminal, and the nose key of burning causes a disease.It is basic principle that this disease treatment is gone up with dispelling wind to relieve the exterior syndrome, awakening consciousness, heat-clearing and toxic substances removing, promoting diuresis to eliminate damp pathogen.Formulated by Fructus Platycaryae strobilaceac preface (removing seed), Spica Prunellae, Flos Chrysanthemi Indici, the Radix Astragali, Flos Magnoliae, Radix Saposhnikoviae, the Radix Angelicae Dahuricae, Radix Glycyrrhizae, nine kinds of Chinese crude drug science of Rhizoma Chuanxiong, have hot loose dispel the wind, effect that heat clearing away is sensible, be mainly used in diseases such as the acute and chronic sinusitis of treatment.Sings and symptoms to sinusitis improves obviously, especially to symptoms such as headache and dizziness, the congested swelling of nasal mucosa, the congested hypertrophy of concha nasalis, nasal secretion, nasal sinuses tenderness.
Goal of the invention
The objective of the invention is to overcome the defective of existing hard capsule, provide a kind of instant effect, the patient is acceptant, preservation is convenient, a kind of Chinese medicine composition preparation of soft capsule method of production process environmental protection.
Summary of the invention
The object of the invention adopts following technical scheme to realize.
Extract powder that a kind of Chinese medicine composition composition soft capsule is extracted through the decocting in water precipitate with ethanol by Fructus Platycaryae strobilaceac preface (removing seed) 630g, Spica Prunellae 630g, Flos Chrysanthemi Indici 251g, Radix Astragali 420g, Flos Magnoliae 420g, Radix Saposhnikoviae 251g, Radix Angelicae Dahuricae 251g, Radix Glycyrrhizae 251g, Rhizoma Chuanxiong 251g and the adjuvant that can be made into soft capsule content are mixed and made into soft capsule content, adopt die pressing to make soft capsule soft capsule content with capsule casing material.
Contained effective ingredient of each medical material and pharmacological action division thereof are as follows in the prescription:
Fructus Platycaryae strobilaceac preface is the infructescence of juglandaceae plant Platycarya strobilacea Platycarya Strobilacea.Sieb.et.Zucc., this infructescence energy regulating qi and dispelling wind, reducing swelling and alleviating pain, removing dampness and killing parasites.Control the internal injury breast and expand, stomachache, muscles and bones convulsion pain, carbuncle, eczema, scabies.The chemical constitution study of this medicine finds to contain flavonoid, protein, aminoacid, organic acid, phenols, bran matter, sugar and polysaccharide glycoside etc.
Spica Prunellae is the dry fruit ear of labiate Spica Prunellae Prunella vulgaris L..The chemical constitution study of this medicine finds to contain sugar, phytosterin compound, organic acid, flavone compound, volatilization wet goods.Have and relieve inflammation or internal heat, make eye bright, eliminating stagnation, the repercussive effect is used for conjunctival congestion and swelling pain, order pearl nyctalgia, it is dizzy to have a headache, the scrofula goiter, acute mastitis swells and ache; Thyromegaly, tuberculous lymphadenitis, cyclomastopathy, hypertension.
Flos Chrysanthemi Indici is the dry capitulum of feverfew Herba Dendranthematis indici Chrysanthcmum indicum L..It has antipyretic and antidote functions, is used for the furuncle carbuncle, conjunctival congestion and swelling pain, and it is dizzy to have a headache.Flower contains volatile oil, contains chrysol, chrysanthone in the oil, still contains dl-Camphora, β-3-carene, sabinene and cephrol, in addition, separate in spending yejuhua lactone, the Flos Buddlejae glycoside.Other contains luteolin glycoside, the red glycoside chrysanthemaxanthin of chrysanthemum etc.
The Radix Astragali is the dry root of leguminous plant Radix Astagali Astragalus membranaceus (Fisch.) Bge.var.mongholicus (Bge.) Hsiao or Radix Astragali A.membranaceus (Fisch.) Bge..Its chemical constitution study is found main contain flavone, Saponin, astragalus polysaccharides constituents.Have invigorating QI to consolidate the body surface resistance, the diuresis poison holding, evacuation of pus, the function of expelling pus and promoting granulation, it is weak to be used for the deficiency of vital energy, anorexia and loose stool, sinking of QI of middle-JIAO, the chronic diarrhea proctoptosis, the metrorrhagia of having blood in stool, the exterior deficiency spontaneous perspiration, deficiency of vital energy edema, carbuncle is difficult bursts, and burst for a long time and do not hold back, blood deficiency and yellow complexion, interior-heat is quenched one's thirst; Chronic nephritis proteinuria, diabetes.
Flos Magnoliae is the alabastrum of Magnoliacea plant Y biondii(Pamp)D.L.Fu. Magnolia biondii Pamp., YULAN M.denudata Desr. or Flos Magnoliae M.sprengeri Pamp..Its main component is volatile oil such as α-2-pinene, eucalyptol, methyl chavicol, citral acetic acid bornyl ester, anti--Flos Caryophylli alkene, epoxy Flos Caryophylli alkene, lignan component.Have dispersing wind and cold, the effect of clearing the nasal passage is used for headche due to wind-cold, nasal obstruction, nasal sinusitis, turbid nasal discharge.
Radix Saposhnikoviae is the dry root of umbelliferae Saposhnikovia divaricata Saposhnikovia divaricata (Turcz.) Schischk..Its main component is a long-chain fatty acid, still contains volatile oil, peucedanin and chromone glycoside, also contains cimifugin and cimifugin glycoside etc.Have inducing diaphoresis to dispel wind, win and wet, the relieving convulsion function is used for headache due to common cold, rheumatic arthralgia, rubella pruritus, tetanus.
The Radix Angelicae Dahuricae is the dry root of samphire Radix Angelicae Dahuricae Angelica dahurica (Fisch.ex Hoffm.) Benth.etHook.f. or Radix angelicae dahuricae A.dahurica (Fisch.ex Hoffm.) Benth.et Hook.f.var.formosana (Boiss.) Shan et Yuan.The main volatile oil component that contains.Has diffusing wind dehumidifying, understand things pain-stopping, the effect of detumescence and apocenosis.Be used for headache due to common cold, supraorbital bone pain, nasal obstruction, nasal sinusitis, toothache, leucorrhea, skin infection swells and ache.
Radix Glycyrrhizae is the dry root and rhizome of glycyrrhizic legume Glycyrrhiza uralensis Fisch., Glycyrrhiza inflata Bat. G.inflata Bat. or the sweet fruit G.glabra L. of light fruit.Main component is triterpenoid saponin compounds and flavone compounds such as glycyrrhizin, enoxolone, glycyrrhizic acid.Has invigorating the spleen and replenishing QI, heat-clearing and toxic substances removing, expelling phlegm for arresting cough, relieving spasm to stop pain, coordinating the actions of various ingredients in a prescription.Be used for weakness of the spleen and stomach, fatigue and weakness, shortness of breath and palpitation, cough with copious phlegm, gastral cavity abdomen, the anxious pain of extremity contraction, carbuncle sore tumefacting virus, emergency drug toxicity, strong.
Rhizoma Chuanxiong is the dry rhizome of samphire Rhizoma Chuanxiong Ligusticum chuanxiong Hort..Main component is nitrogen-containing compounds such as volatile oil, ligustrazine, acidity or phenoloids such as ferulic acid.Have blood-activating and qi-promoting, the effect of wind-expelling pain-stopping is used for menoxenia, amenorrhea dysmenorrhea ， Disorder crust stomachache, the twinge of the breast side of body, tumbling and swelling, headache, rheumatic arthralgia.
The specific embodiment
According to the prescription medical material ingredient character of respectively distinguishing the flavor of, we take a kind of Chinese medicine composition composition soft capsule of following prepared:
A kind of Chinese medicine composition composition soft capsule is made soft capsule content by the Chinese medicine extract powder of 10-70% weight and the adjuvant mix homogeneously of 30-90% weight, adopts die pressing to make soft capsule soft capsule content with capsule casing material.
The Chinese medicine extract powder preparation:
Water with Fructus Platycaryae strobilaceac preface (removing seed) 630g, Spica Prunellae 630g, Flos Chrysanthemi Indici 251g, Radix Astragali 420g, Flos Magnoliae 420g, Radix Saposhnikoviae 251g, Radix Angelicae Dahuricae 251g, 8-12 times of raw material weight of Radix Glycyrrhizae 251g, Rhizoma Chuanxiong 251g adding extracts each 1-2 hour 2 times; Collecting decoction, filtration, filtrate decompression is concentrated into to relative density 1.12 (60 ℃), adds ethanol and reaches 60% to containing the alcohol amount, leaves standstill 24 hours, filter, filtrate recycling ethanol, drying is pulverized, and gets extract powder.
Soft capsule preparation:
A kind of Chinese medicine composition composition soft capsule of the present invention can prepare by the various appropriate method of soft capsule preparation, preferably make: with extract powder and the diluent (Polyethylene Glycol that comprises PEG400 or PEG600 liquid state by being prepared as follows method, fish oil, olive oil, Semen Maydis oil, soybean oil, refining Oleum Arachidis hypogaeae semen, Radix Oenotherae erythrosepalae oil, Herba Silybi mariani oil, Oleum Vitis viniferae, Oleum Ricini, castor oil hydrogenated, Oleum Helianthi, safflower oil, in the Oleum Hippophae any one or several, preferred PEG400 or olive oil), suspending agent (comprises PEG4000, the Polyethylene Glycol that PEG6000 is solid-state, aerosil, liquid paraffin, sucrose ester, lanoline, lecithin, Cera Flava, glyceryl monostearate, high fatty alcohol (C
18-C
32) in a kind of or several, preferred aerosil or Cera Flava) mix, cross the colloid mill mix homogeneously and make content, adopt die pressing to prepare soft capsule, soft capsule is washed ball, is done eventually, promptly with appropriate solvent through solidifying by cooling in wind, drying.
Beneficial effect of the present invention is embodied in following aspect:
1, medicine absorbs in human body steadily, has improved bioavailability, stable curative effect;
2, product hermeticity is good, has stoped distributing of bitterness and bad smell, and the patient is acceptant, and can long-term storage;
3, effective ingredient is even, and every capsules content uniformity is more easy to control;
4, in the soft capsule production process, can reduce dust, protection staff's health and environment.
Enumerate several embodiment that are used to that the invention process process is described rather than are used for limiting protection domain, as follows:
Embodiment 1
With Fructus Platycaryae strobilaceac preface (removing seed) 630g, Spica Prunellae 630g, Flos Chrysanthemi Indici 251g, Radix Astragali 420g, Flos Magnoliae 420g, Radix Saposhnikoviae 251g, Radix Angelicae Dahuricae 251g, Radix Glycyrrhizae 251g, Rhizoma Chuanxiong 251g, extract 2 times, add 12 times in water for the first time, decocted 1.5 hours, for the second time add 10 times in water, decocted 1.5 hours; Collecting decoction, filtration, filtrate decompression is concentrated into to relative density 1.12 (60 ℃), adds ethanol and reaches 60% to containing the alcohol amount, leaves standstill 24 hours, filter, filtrate recycling ethanol, drying is pulverized, and gets extract powder.
By the above extraction process powder 405g that gets dry extract, Astragaloside content 56mg.
Embodiment 2
With Fructus Platycaryae strobilaceac preface (removing seed) 630g, Spica Prunellae 630g, Flos Chrysanthemi Indici 251g, Radix Astragali 420g, Flos Magnoliae 420g, Radix Saposhnikoviae 251g, Radix Angelicae Dahuricae 251g, Radix Glycyrrhizae 251g, Rhizoma Chuanxiong 251g, extract 2 times, add 10 times in water for the first time, decocted 2 hours, for the second time add 8 times in water, decocted 2 hours; Collecting decoction, filtration, filtrate decompression is concentrated into to relative density 1.12 (60 ℃), adds ethanol and reaches 60% to containing the alcohol amount, leaves standstill 24 hours, filter, filtrate recycling ethanol, drying is pulverized, and gets extract powder.
Get extract powder 370g by above extraction process, Astragaloside content 45mg.
Embodiment 3
With Fructus Platycaryae strobilaceac preface (removing seed) 630g, Spica Prunellae 630g, Flos Chrysanthemi Indici 251g, Radix Astragali 420g, Flos Magnoliae 420g, Radix Saposhnikoviae 251g, Radix Angelicae Dahuricae 251g, Radix Glycyrrhizae 251g, Rhizoma Chuanxiong 251g, extract 2 times, add 10 times in water for the first time, decocted 2 hours, for the second time add 8 times in water, decocted 2 hours; Collecting decoction, filtration, filtrate decompression is concentrated into to relative density 1.12 (60 ℃), adds ethanol and reaches 60% to containing the alcohol amount, leaves standstill 24 hours, filter, filtrate recycling ethanol, drying is pulverized, and gets extract powder.
Extract powder art 280g
Soybean oil 260g
Lecithin 18g
Cera Flava 42g
Make 1000
By above mixed, cross the colloid mill mix homogeneously and make content, adopt pressing to prepare soft capsule, soft capsule is washed ball, is done eventually, promptly with appropriate solvent through solidifying by cooling in wind, drying.
Embodiment 4
With Fructus Platycaryae strobilaceac preface (removing seed) 630g, Spica Prunellae 630g, Flos Chrysanthemi Indici 251g, Radix Astragali 420g, Flos Magnoliae 420g, Radix Saposhnikoviae 251g, Radix Angelicae Dahuricae 251g, Radix Glycyrrhizae 251g, Rhizoma Chuanxiong 251g, extract 2 times, add 12 times in water for the first time, decocted 1.5 hours, for the second time add 10 times in water, decocted 1.5 hours; Collecting decoction, filtration, filtrate decompression is concentrated into to relative density 1.12 (60 ℃), adds ethanol and reaches 60% to containing the alcohol amount, leaves standstill 24 hours, filter, filtrate recycling ethanol, drying is pulverized, and gets extract powder.
Extract powder 320g
Olive oil 280g
Aerosil 50g
Make 1000
By above mixed, cross the colloid mill mix homogeneously and make content, adopt pressing to prepare soft capsule, soft capsule is washed ball, is done eventually, promptly with appropriate solvent through solidifying by cooling in wind, drying.
Embodiment 5
With Fructus Platycaryae strobilaceac preface (removing seed) 630g, Spica Prunellae 630g, Flos Chrysanthemi Indici 251g, Radix Astragali 420g, Flos Magnoliae 420g, Radix Saposhnikoviae 251g, Radix Angelicae Dahuricae 251g, Radix Glycyrrhizae 251g, Rhizoma Chuanxiong 251g, extract 2 times, add 12 times in water for the first time, decocted 1.5 hours, for the second time add 10 times in water, decocted 1.5 hours; Collecting decoction, filtration, filtrate decompression is concentrated into to relative density 1.12 (60 ℃), adds ethanol and reaches 60% to containing the alcohol amount, leaves standstill 24 hours, filter, filtrate recycling ethanol, drying is pulverized, and gets extract powder.
Extract powder 280
Oleum Vitis viniferae 250
Glyceryl monostearate 15g
Cera Flava 35g
Make 1000
By above mixed, cross the colloid mill mix homogeneously and make content, adopt pressing to prepare soft capsule, soft capsule is washed ball, is done eventually, promptly with appropriate solvent through solidifying by cooling in wind, drying.
Embodiment 6
With Fructus Platycaryae strobilaceac preface (removing seed) 630g, Spica Prunellae 630g, Flos Chrysanthemi Indici 251g, Radix Astragali 420g, Flos Magnoliae 420g, Radix Saposhnikoviae 251g, Radix Angelicae Dahuricae 251g, Radix Glycyrrhizae 251g, Rhizoma Chuanxiong 251g, extract 2 times, add 10 times in water for the first time, decocted 2 hours, for the second time add 8 times in water, decocted 2 hours; Collecting decoction, filtration, filtrate decompression is concentrated into to relative density 1.12 (60 ℃), adds ethanol and reaches 60% to containing the alcohol amount, leaves standstill 24 hours, filter, filtrate recycling ethanol, drying is pulverized, and gets extract powder.
Extract powder 260g
PEG400 260g
Aerosil 16g
PEG4000 44g
By above mixed, cross the colloid mill mix homogeneously and make content, adopt pressing to prepare soft capsule, soft capsule is washed ball, is done eventually, promptly with appropriate solvent through solidifying by cooling in wind, drying.
Embodiment 7
With Fructus Platycaryae strobilaceac preface (removing seed) 630g, Spica Prunellae 630g, Flos Chrysanthemi Indici 251g, Radix Astragali 420g, Flos Magnoliae 420g, Radix Saposhnikoviae 251g, Radix Angelicae Dahuricae 251g, Radix Glycyrrhizae 251g, Rhizoma Chuanxiong 251g, extract 2 times, add 12 times in water for the first time, decocted 1.5 hours, for the second time add 10 times in water, decocted 1.5 hours; Collecting decoction, filtration, filtrate decompression is concentrated into to relative density 1.12 (60 ℃), adds ethanol and reaches 60% to containing the alcohol amount, leaves standstill 24 hours, filter, filtrate recycling ethanol, drying is pulverized, and gets extract powder art.
Extract powder 280g
PEG600 290g
Gas phase titanium dioxide 10g
PEG6000 60g
Make 1000
By above mixed, cross the colloid mill mix homogeneously and make content, adopt pressing to prepare soft capsule, soft capsule is washed ball, is done eventually, promptly with appropriate solvent through solidifying by cooling in wind, drying.
Claims (4)
1, a kind of Chinese medicine composition preparation of soft capsule method, it is characterized in that it is by the Chinese medicine extract powder of 10-70% weight and the adjuvant mix homogeneously of 30-90% weight, make soft capsule content, adopt die pressing to make soft capsule soft capsule content with capsule casing material, wherein, described adjuvant comprises diluent liquid polyethylene glycol or animal and vegetable oil at least.
2, according to the described a kind of Chinese medicine composition preparation of soft capsule method of claim 1, it is characterized in that described Chinese medicine extract powder adopts following prepared: Fructus Platycaryae strobilaceac preface (removing seed) 630g, Spica Prunellae 630g, Flos Chrysanthemi Indici 251g, Radix Astragali 420g, Flos Magnoliae 420g, Radix Saposhnikoviae 251g, Radix Angelicae Dahuricae 251g, Radix Glycyrrhizae 251g, Rhizoma Chuanxiong 251g, decoct with water and extract 1-2 time, each 8-12 times of water, each 1-2 hour; Collecting decoction, filtration, filtrate decompression is concentrated into relative density 1.12 (60 ℃), adds ethanol and reaches 60% to containing the alcohol amount, leaves standstill 24 hours, filter, filtrate recycling ethanol, drying is pulverized, and gets extract powder.
3,, it is characterized in that described diluent comprises in the Polyethylene Glycol of PEG400 or PEG600 liquid state, fish oil, olive oil, Semen Maydis oil, soybean oil, refining Oleum Arachidis hypogaeae semen, Radix Oenotherae erythrosepalae oil, Herba Silybi mariani oil, Oleum Vitis viniferae, Oleum Ricini, castor oil hydrogenated, Oleum Helianthi, safflower oil, the Oleum Hippophae any one or several according to the described a kind of Chinese medicine composition preparation of soft capsule method of claim 1.
4, according to the described a kind of Chinese medicine composition preparation of soft capsule method of claim 1, it is characterized in that described adjuvant also comprises the solid-state Polyethylene Glycol of suspending agent PEG4000, PEG6000, aerosil, liquid paraffin, sucrose ester, lanoline, lecithin, Cera Flava, glyceryl monostearate, high fatty alcohol (C
18～C
32) in a kind of or several.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200510124020 CN1785245A (en) | 2005-11-28 | 2005-11-28 | Method for preparing composite traditional Chinese medicine soft capsule |
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| CN 200510124020 CN1785245A (en) | 2005-11-28 | 2005-11-28 | Method for preparing composite traditional Chinese medicine soft capsule |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102058560A (en) * | 2010-12-30 | 2011-05-18 | 张家界茅岩莓有限公司 | Dihydromyricetin soft capsules and preparation method thereof |
| CN102919846A (en) * | 2012-11-21 | 2013-02-13 | 塔城市星河生物工程有限责任公司 | Method for preparing edible plant amino acid soft capsule |
| CN103169784A (en) * | 2013-03-02 | 2013-06-26 | 赵明叶 | Traditional Chinese medicine for treating rhinitis |
-
2005
- 2005-11-28 CN CN 200510124020 patent/CN1785245A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102058560A (en) * | 2010-12-30 | 2011-05-18 | 张家界茅岩莓有限公司 | Dihydromyricetin soft capsules and preparation method thereof |
| CN102058560B (en) * | 2010-12-30 | 2013-07-24 | 张家界茅岩莓有限公司 | Dihydromyricetin soft capsules and preparation method thereof |
| CN102919846A (en) * | 2012-11-21 | 2013-02-13 | 塔城市星河生物工程有限责任公司 | Method for preparing edible plant amino acid soft capsule |
| CN103169784A (en) * | 2013-03-02 | 2013-06-26 | 赵明叶 | Traditional Chinese medicine for treating rhinitis |
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