CN1726308A - 制造氟代烯烃的方法 - Google Patents

制造氟代烯烃的方法 Download PDF

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Publication number
CN1726308A
CN1726308A CNA2003801059394A CN200380105939A CN1726308A CN 1726308 A CN1726308 A CN 1726308A CN A2003801059394 A CNA2003801059394 A CN A2003801059394A CN 200380105939 A CN200380105939 A CN 200380105939A CN 1726308 A CN1726308 A CN 1726308A
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CN
China
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ecf
raw material
pyrolysis
tfe
compounds
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Pending
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CNA2003801059394A
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English (en)
Chinese (zh)
Inventor
G·L·鲍尔
J·D·魏格尔特
K·亨特泽
G·劳尔
W·施韦尔特费格
A·A·波嫩利斯
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3M Innovative Properties Co
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3M Innovative Properties Co
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Publication of CN1726308A publication Critical patent/CN1726308A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/23—Preparation of halogenated hydrocarbons by dehalogenation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/263—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions
    • C07C17/269—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by condensation reactions of only halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/361—Preparation of halogenated hydrocarbons by reactions involving a decrease in the number of carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
    • C07C21/185—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine tetrafluorethene
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00—Electrolytic production of organic compounds
    • C25B3/01—Products
    • C25B3/11—Halogen containing compounds
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00—Electrolytic production of organic compounds
    • C25B3/20—Processes
    • C25B3/27—Halogenation
    • C25B3/28—Fluorination

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
CNA2003801059394A 2002-12-16 2003-11-14 制造氟代烯烃的方法 Pending CN1726308A (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US10/320,796 US6919015B2 (en) 2002-12-16 2002-12-16 Process for manufacturing fluoroolefins
US10/320,796 2002-12-16

Publications (1)

Publication Number Publication Date
CN1726308A true CN1726308A (zh) 2006-01-25

Family

ID=32506942

Family Applications (1)

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CNA2003801059394A Pending CN1726308A (zh) 2002-12-16 2003-11-14 制造氟代烯烃的方法

Country Status (8)

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US (2) US6919015B2 (enExample)
EP (1) EP1573088B1 (enExample)
JP (1) JP2006509831A (enExample)
CN (1) CN1726308A (enExample)
AU (1) AU2003290961A1 (enExample)
RU (1) RU2005114348A (enExample)
WO (1) WO2004061160A1 (enExample)
ZA (1) ZA200505678B (enExample)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102216246A (zh) * 2008-10-01 2011-10-12 3M创新有限公司 通过氟化材料热分解制备氟化烯烃的方法
CN102985396A (zh) * 2010-06-30 2013-03-20 3M创新有限公司 通过在存在氢气的情况下热解全氟化碳以制造全氟烯烃的方法
CN111155141A (zh) * 2020-01-20 2020-05-15 中国科学技术大学 一种电化学合成偕二氟烯烃的方法
CN112899707A (zh) * 2020-09-30 2021-06-04 中船重工（邯郸）派瑞特种气体有限公司 一种六氟乙烷的制备方法

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6919015B2 (en) * 2002-12-16 2005-07-19 3M Innovative Properties Company Process for manufacturing fluoroolefins
US7513985B2 (en) * 2005-10-17 2009-04-07 3M Innovative Properties Company Electrochemical fluorination of acrylic polymer and product therefrom
MD3967C2 (ro) * 2009-04-02 2010-05-31 Институт Химии Академии Наук Молдовы Procedeu electrochimic de obţinere a 7β,11-diacetoxi-drim-8-enei
JP5581676B2 (ja) * 2009-12-02 2014-09-03 セントラル硝子株式会社 フッ素ガス生成装置
JP2016013994A (ja) * 2014-07-03 2016-01-28 日華化学株式会社 テトラフルオロエチレン及び／又はヘキサフルオロプロピレンの製造方法
EP3002273A1 (en) 2014-10-01 2016-04-06 3M Innovative Properties Company Process and apparatus for producing fluorinated alkenes
US11014999B2 (en) * 2018-04-24 2021-05-25 Inhance Technologies, LLC Systems and methods for processing fluoropolymer materials and related workpieces
JP7017982B2 (ja) * 2018-05-18 2022-02-09 ダイキン工業株式会社 テトラフルオロエチレンおよびヘキサフルオロプロピレンの少なくとも１つの製造方法
CN112808174B (zh) * 2021-02-06 2024-08-30 福建德尔科技股份有限公司 一种四氟化碳热解装置及其控制方法
KR102704739B1 (ko) * 2022-06-21 2024-09-06 에스케이스페셜티 주식회사 전기화학적 불소화법을 이용한 pftpa의 제조 장치 및 방법
CN119980267B (zh) * 2025-03-20 2025-12-02 国滢进出口(上海)有限公司 一种六氟丙烯三聚体电解氟化制备3-五氟乙基-4-三氟甲基-十二氟己烷的方法

Family Cites Families (59)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2551573A (en) 1945-11-30 1951-05-08 Du Pont Pyrolysis of chloro-fluoro alkanes
US2519983A (en) 1948-11-29 1950-08-22 Minnesota Mining & Mfg Electrochemical process of making fluorine-containing carbon compounds
US2567011A (en) 1949-01-10 1951-09-04 Minnesota Mining & Mfg Fluorocarbon acids and derivatives
FR1131556A (fr) 1955-05-19 1957-02-25 Du Pont Procédé de préparation du tétrafluoréthylène
US3081245A (en) 1960-03-17 1963-03-12 Du Pont Method for the preparation of tetrafluoroethylene
US3662009A (en) 1969-11-24 1972-05-09 Phillips Petroleum Co Preparation of unsaturated fluorocompounds
US4076760A (en) 1970-06-24 1978-02-28 Hoechst Aktiengesellschaft Process for the preparation of fluorocarbon waxes
CA943973A (en) 1970-06-24 1974-03-19 Farbwerke Hoechst Aktiengesellschaft Vormals Meister Lucius And Bruning Process for the preparation of perfluorated compounds
US3832411A (en) 1971-02-02 1974-08-27 Liquid Nitrogen Processing Method for the depolymerization of polytetrafluoroethylene
US3753976A (en) 1972-07-17 1973-08-21 Smith Kline French Lab Process for preparing polyhalohemiacetal derivatives of polysaccharides
US3904501A (en) 1973-10-04 1975-09-09 Massachusetts Inst Technology Fluorine plasma synthesis for carbon monofluorides
US3957596A (en) 1974-05-21 1976-05-18 Ontario Research Foundation Production of fluorinated hydrocarbons
FR2343821A2 (fr) 1975-03-21 1977-10-07 Ugine Kuhlmann Electrolyseur perfectionne pour la preparation industrielle du fluor
GB1516648A (en) 1975-06-26 1978-07-05 Inst Khim Fiz An Sssr Process for regenerating used polytetrafluoroethylene
DE2739324C3 (de) 1977-09-01 1981-09-10 Hoechst Ag, 6000 Frankfurt Verfahren und Vorrichtung zur Durchführung elektrochemischer Reaktionen sowie dazu geeignete bipolare Elektroden
US4406768A (en) 1981-12-24 1983-09-27 Monsanto Company Electrochemical cell assembly
US4933060A (en) 1987-03-02 1990-06-12 The Standard Oil Company Surface modification of fluoropolymers by reactive gas plasmas
DE3730065A1 (de) 1987-03-14 1988-09-22 Bayer Ag Verfahren zur plasmapolymerisation
DE3729106A1 (de) * 1987-09-01 1989-03-09 Hoechst Ag Verfahren zur gewinnung von reinem tetrafluorethylen
GB8724561D0 (en) 1987-10-20 1987-11-25 Ici Plc Production process
JPH0230785A (ja) 1988-04-20 1990-02-01 Tokuyama Soda Co Ltd 電解フッ素化方法
SU1666581A1 (ru) 1988-07-08 1991-07-30 Предприятие П/Я В-8469 Установка дл электрохимического фторировани
US4950370A (en) 1988-07-19 1990-08-21 Liquid Air Corporation Electrolytic gas generator
US5026464A (en) 1988-08-31 1991-06-25 Agency Of Industrial Science And Technology Method and apparatus for decomposing halogenated organic compound
US5322904A (en) 1988-09-28 1994-06-21 Exfluor Research Corporation Liquid-phase fluorination
US4973773A (en) 1988-11-29 1990-11-27 E. I. Du Pont De Nemours And Company Production of tetrafluoroethylene
EP0455399A3 (en) 1990-04-24 1992-02-12 Minnesota Mining And Manufacturing Company Process for making organic fluorine compounds
US5387232A (en) 1990-05-31 1995-02-07 Synchrotech Medical Corporation Method and apparatus for esophageal pacing
CA2043504C (en) 1991-05-29 1995-01-17 Peter G. Tsantrizos High enthalpy plasma torch
US5399832A (en) 1991-08-05 1995-03-21 Kimoto Co., Ltd. Process and apparatus for using atmospheric-pressure plasma reactions
US5207999A (en) 1991-08-13 1993-05-04 Cameco Corporation Generation of fluorine via thermal plasma decomposition of metal fluoride
US5360635A (en) * 1992-01-02 1994-11-01 Air Products And Chemicals, Inc. Method for manufacturing inorganic membranes by organometallic chemical vapor deposition
US5322597A (en) 1992-07-30 1994-06-21 Minnesota Mining And Manufacturing Company Bipolar flow cell and process for electrochemical fluorination
JP3021218B2 (ja) * 1993-01-20 2000-03-15 株式会社トクヤマ ペルフルオロ炭化水素の製造方法
US5387323A (en) * 1993-08-31 1995-02-07 Minnesota Mining And Manufacturing Company Process for preparing fluorochemicals
US5488142A (en) 1993-10-04 1996-01-30 Minnesota Mining And Manufacturing Company Fluorination in tubular reactor system
DE4334015A1 (de) 1993-10-06 1995-04-13 Hoechst Ag Verfahren zur Herstellung von fluorierten Monomeren
CA2118081C (en) 1993-10-14 2006-10-03 Jacobus Swanepoel Production of fluorocarbon compounds
WO1995021126A1 (en) 1994-02-01 1995-08-10 E.I. Du Pont De Nemours And Company Preparation of hydrogen cyanide
US5744657A (en) 1994-12-22 1998-04-28 E. I. Du Pont De Nemours And Company Process for the preparation of perfluorocarbons
JP3946764B2 (ja) 1995-02-17 2007-07-18 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー テトラフルオロエチレンの合成法
WO1996030322A1 (en) 1995-03-31 1996-10-03 E.I. Du Pont De Nemours And Company Preparation of tetrafluoroethylene
WO1996030323A1 (en) 1995-03-31 1996-10-03 E.I. Du Pont De Nemours And Company Preparation of tetrafluoroethylene
US5684218A (en) 1995-03-31 1997-11-04 E. I. Du Pont De Nemours And Company Preparation of tetrafluoroethylene
US5633414A (en) 1995-03-31 1997-05-27 E. I. Du Pont De Nemours And Company Preparation of tetrafluoroethylene
US5858065A (en) 1995-07-17 1999-01-12 American Air Liquide Process and system for separation and recovery of perfluorocompound gases
IE80909B1 (en) 1996-06-14 1999-06-16 Air Liquide An improved process and system for separation and recovery of perfluorocompound gases
US5759237A (en) 1996-06-14 1998-06-02 L'air Liquide Societe Anonyme Pour L'etude Et, L'exploitation Des Procedes Georges Claude Process and system for selective abatement of reactive gases and recovery of perfluorocompound gases
JPH10110284A (ja) * 1996-10-07 1998-04-28 Tokuyama Corp 電解フッ素化方法
US5814127A (en) 1996-12-23 1998-09-29 American Air Liquide Inc. Process for recovering CF4 and C2 F6 from a gas
DE69738168T2 (de) 1997-05-02 2008-06-26 Minnesota Mining & Manufacturing Company, St. Paul Elektrochemische fluorierung mit unterbrochenem strom
US6267865B1 (en) 1997-05-02 2001-07-31 3M Innovative Properties Company Electrochemical fluorination using interrupted current
JP4782290B2 (ja) 1999-05-20 2011-09-28 ザ サウス アフリカン ニュークリア エナジー コーポレイション リミテッド フルオロ化
US6624337B1 (en) * 1999-06-04 2003-09-23 E. I. Du Pont De Nemours And Company Process for the manufacture of fluoroolefins
AU5901600A (en) 1999-06-30 2001-01-31 Kimberly-Clark Worldwide, Inc. Delivery of a skin health benefit agent to a treated substrate for transfer to skin
EP1253973B1 (en) 2000-02-10 2005-05-11 South African Nuclear Energy Corporation Limited Treatment of fluorocarbon feedstocks
DE60139673D1 (de) 2000-02-10 2009-10-08 South African Nuclear Energy Behandlung von fluorkohlenstoffeinsatzmaterialien
AU2001236913B2 (en) 2000-02-10 2005-08-25 3M Innovative Properties Company Treatment of fluorocarbon feedstocks
US6919015B2 (en) 2002-12-16 2005-07-19 3M Innovative Properties Company Process for manufacturing fluoroolefins

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102216246A (zh) * 2008-10-01 2011-10-12 3M创新有限公司 通过氟化材料热分解制备氟化烯烃的方法
CN102216246B (zh) * 2008-10-01 2014-06-18 3M创新有限公司 通过氟化材料热分解制备氟化烯烃的方法
CN102985396A (zh) * 2010-06-30 2013-03-20 3M创新有限公司 通过在存在氢气的情况下热解全氟化碳以制造全氟烯烃的方法
CN102985396B (zh) * 2010-06-30 2015-08-19 3M创新有限公司 通过在存在氢气的情况下热解全氟化碳以制造全氟烯烃的方法
CN111155141A (zh) * 2020-01-20 2020-05-15 中国科学技术大学 一种电化学合成偕二氟烯烃的方法
CN112899707A (zh) * 2020-09-30 2021-06-04 中船重工（邯郸）派瑞特种气体有限公司 一种六氟乙烷的制备方法
CN112899707B (zh) * 2020-09-30 2022-04-12 中船(邯郸)派瑞特种气体股份有限公司 一种六氟乙烷的制备方法

Also Published As

Publication number Publication date
WO2004061160A1 (en) 2004-07-22
EP1573088B1 (en) 2015-03-11
RU2005114348A (ru) 2006-01-20
ZA200505678B (en) 2007-02-28
US20040112758A1 (en) 2004-06-17
US20050240067A1 (en) 2005-10-27
AU2003290961A1 (en) 2004-07-29
JP2006509831A (ja) 2006-03-23
US7250540B2 (en) 2007-07-31
US6919015B2 (en) 2005-07-19
EP1573088A1 (en) 2005-09-14

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