CN1261484C - 制备聚氧化烯聚醚产品的方法 - Google Patents

制备聚氧化烯聚醚产品的方法 Download PDF

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Publication number
CN1261484C
CN1261484C CNB028183851A CN02818385A CN1261484C CN 1261484 C CN1261484 C CN 1261484C CN B028183851 A CNB028183851 A CN B028183851A CN 02818385 A CN02818385 A CN 02818385A CN 1261484 C CN1261484 C CN 1261484C
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CN
China
Prior art keywords
product
alkylene oxide
polyoxyalkylene polyether
reactor
tubular reactor
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Expired - Lifetime
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CNB028183851A
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English (en)
Chinese (zh)
Other versions
CN1556829A (zh
Inventor
J·F·J·布朗斯
M·B·埃利维尔德
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Shell Internationale Research Maatschappij BV
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Shell Internationale Research Maatschappij BV
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/22—Organic complexes
    • B01J31/2204—Organic complexes the ligands containing oxygen or sulfur as complexing atoms
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2696—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the process or apparatus used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/20—Compounding polymers with additives, e.g. colouring
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/24—Nitrogen compounds
    • B01J27/26—Cyanides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2650/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G2650/22—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule characterised by the initiator used in polymerisation
    • C08G2650/24—Polymeric initiators

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Toxicology (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyethers (AREA)
CNB028183851A 2001-09-20 2002-09-19 制备聚氧化烯聚醚产品的方法 Expired - Lifetime CN1261484C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP01308020.5 2001-09-20
EP01308020A EP1295902A1 (en) 2001-09-20 2001-09-20 Process for preparing polyoxyalkylene polyether products.

Publications (2)

Publication Number Publication Date
CN1556829A CN1556829A (zh) 2004-12-22
CN1261484C true CN1261484C (zh) 2006-06-28

Family

ID=8182279

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB028183851A Expired - Lifetime CN1261484C (zh) 2001-09-20 2002-09-19 制备聚氧化烯聚醚产品的方法

Country Status (9)

Country Link
US (1) US20030073873A1 (enExample)
EP (2) EP1295902A1 (enExample)
JP (1) JP2005503463A (enExample)
KR (1) KR101021818B1 (enExample)
CN (1) CN1261484C (enExample)
AU (1) AU2002338739A1 (enExample)
DE (1) DE60236754D1 (enExample)
ES (1) ES2343312T3 (enExample)
WO (1) WO2003025045A1 (enExample)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060183882A1 (en) * 2001-12-21 2006-08-17 Dexheimer Edward M Continuous process for preparation of polyether polyols
DE10324998A1 (de) * 2003-06-03 2004-12-23 Basf Ag Herstellung von Polyetheralkoholen unter Verwendung der DMC-Katalyse
US20080033214A1 (en) * 2004-06-09 2008-02-07 Duijghuisen Henricus Petrus B Process of Preparing Odour-Lean Polyether Polyol
EP1640401A3 (de) * 2004-09-24 2006-04-12 Clariant Produkte (Deutschland) GmbH Polyethylenglykol und Alkoholethoxylate und deren Herstellung
DE102004059489C5 (de) 2004-12-10 2011-12-08 Clariant Produkte (Deutschland) Gmbh Verfahren zur Herstellung von reinen alpha-Alkoxy-omega-hydroxy-Polyalkylenglykolen
US7671228B2 (en) * 2005-03-29 2010-03-02 Basf Corporation Method of forming a polyethercarbonate polyol using a CO2-philic compound or substituent
DE102005034001A1 (de) * 2005-07-18 2007-01-25 Basf Ag Verfahren zur Herstellung von Polyetheralkoholen
US20080255378A1 (en) 2007-04-16 2008-10-16 Bayer Materialscience Llc High productivity process for non-phenolic ethoxylates
US7473677B2 (en) 2007-04-16 2009-01-06 Bayer Materialscience Llc High productivity process for alkylphenol ethoxylates
CN102753603B (zh) 2009-12-14 2015-01-14 陶氏环球技术有限责任公司 使用双金属氰化物催化剂连续制备低当量多元醇的方法
US10358404B2 (en) 2012-06-21 2019-07-23 Covestro Llc Process for the production of low molecular weight impact polyethers
US9890100B2 (en) 2013-03-14 2018-02-13 Covestro Llc Continuous process for the production of low molecular weight polyethers with a DMC catalyst
US10669368B2 (en) 2013-03-15 2020-06-02 Covestro Llc Method to increase the resistance of double metal cyanide catalysts to deactivation
US10258953B2 (en) 2016-08-05 2019-04-16 Covestro Llc Systems and processes for producing polyether polyols

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DD203735A1 (de) * 1981-12-24 1983-11-02 Adw Ddr Verfahren zur kontinuierlichen herstellung von polyetheralkoholen
ES2125496T3 (es) * 1993-10-22 1999-03-01 Dow Chemical Co Alquilenglicoles que tienen un contenido aumentado de hidroxilo primario.
US5689012A (en) * 1996-07-18 1997-11-18 Arco Chemical Technology, L.P. Continuous preparation of low unsaturation polyoxyalkylene polyether polyols with continuous additon of starter
US6423662B1 (en) * 1999-07-09 2002-07-23 Dow Global Technologies Inc. Incipient wetness method for making metal-containing cyanide catalysts
DE10008635A1 (de) * 2000-02-24 2001-09-06 Basf Ag Verfahren zur Herstellung von Polyetherpolyolen
US6596842B2 (en) 2001-07-16 2003-07-22 Shell Oil Company Polymerizing alkylene oxide with sound or radiation treated DMC

Also Published As

Publication number Publication date
US20030073873A1 (en) 2003-04-17
KR20040045449A (ko) 2004-06-01
EP1448662B1 (en) 2010-06-16
ES2343312T3 (es) 2010-07-28
WO2003025045A1 (en) 2003-03-27
CN1556829A (zh) 2004-12-22
EP1448662A1 (en) 2004-08-25
KR101021818B1 (ko) 2011-03-17
DE60236754D1 (de) 2010-07-29
EP1295902A1 (en) 2003-03-26
JP2005503463A (ja) 2005-02-03
AU2002338739A1 (en) 2003-04-01

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Granted publication date: 20060628