CN1213015C - 芳族羧酸的制备 - Google Patents

芳族羧酸的制备 Download PDF

Info

Publication number
CN1213015C
CN1213015C CNB018131026A CN01813102A CN1213015C CN 1213015 C CN1213015 C CN 1213015C CN B018131026 A CNB018131026 A CN B018131026A CN 01813102 A CN01813102 A CN 01813102A CN 1213015 C CN1213015 C CN 1213015C
Authority
CN
China
Prior art keywords
reaction
heat
reactor
reaction zone
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB018131026A
Other languages
English (en)
Chinese (zh)
Other versions
CN1443152A (zh
Inventor
D·A·格拉哈姆
P·A·哈姆利
T·伊肯汉斯
M·波利尔科夫
D·C·沃德库克
R.奥利弗
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Invista Technologies Sarl
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of CN1443152A publication Critical patent/CN1443152A/zh
Application granted granted Critical
Publication of CN1213015C publication Critical patent/CN1213015C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CNB018131026A 2000-07-19 2001-07-17 芳族羧酸的制备 Expired - Fee Related CN1213015C (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US21938800P 2000-07-19 2000-07-19
US60/219,388 2000-07-19
US09/905,094 US6765113B2 (en) 2000-07-19 2001-07-13 Production of aromatic carboxylic acids
US09/905,094 2001-07-13

Publications (2)

Publication Number Publication Date
CN1443152A CN1443152A (zh) 2003-09-17
CN1213015C true CN1213015C (zh) 2005-08-03

Family

ID=26913840

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB018131026A Expired - Fee Related CN1213015C (zh) 2000-07-19 2001-07-17 芳族羧酸的制备

Country Status (19)

Country Link
US (2) US6765113B2 (enExample)
EP (1) EP1301456B1 (enExample)
JP (1) JP2004504289A (enExample)
KR (1) KR20030019595A (enExample)
CN (1) CN1213015C (enExample)
AR (1) AR029852A1 (enExample)
AT (1) ATE400543T1 (enExample)
AU (1) AU2001275960A1 (enExample)
BR (1) BR0112990B1 (enExample)
CA (1) CA2413748C (enExample)
DE (1) DE60134744D1 (enExample)
DZ (1) DZ3117A1 (enExample)
EG (1) EG22982A (enExample)
ES (1) ES2309080T3 (enExample)
IN (1) IN2002MU01837A (enExample)
MX (1) MX236902B (enExample)
MY (1) MY127798A (enExample)
RU (1) RU2003104827A (enExample)
WO (1) WO2002006201A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102076408B (zh) * 2008-04-30 2014-08-27 英威达技术有限公司 用于制备芳族羧酸的在超临界或近超临界水中的催化氧化反应

Families Citing this family (74)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6765113B2 (en) * 2000-07-19 2004-07-20 E.I. Du Pont De Nemours And Company Production of aromatic carboxylic acids
EP1402942B8 (en) * 2001-05-15 2010-04-14 Mitsubishi Chemical Corporation Process for producing a compound
DE60316968T2 (de) * 2002-07-09 2008-07-31 Invista Technologies S.à.r.l., Wilmington Verfahren zur herstellung aromatischer dicarbonsäuren unter superkritischen bedingungen
JP3987929B2 (ja) * 2003-04-17 2007-10-10 独立行政法人産業技術総合研究所 第三級カルボン酸の製造法
US7049465B2 (en) * 2003-07-10 2006-05-23 Eastman Chemical Company Process for energy recovery in processes for the preparation of aromatic carboxylic acids
US7213540B2 (en) * 2004-02-05 2007-05-08 Eastman Chemical Company Steam recompression in carboxylic acid processes
JP2006016304A (ja) * 2004-06-30 2006-01-19 Mitsui Chemicals Inc 芳香族カルボン酸の製造方法
US7582793B2 (en) * 2004-09-02 2009-09-01 Eastman Chemical Company Optimized liquid-phase oxidation
US7683210B2 (en) * 2004-09-02 2010-03-23 Eastman Chemical Company Optimized liquid-phase oxidation
US7495125B2 (en) 2004-09-02 2009-02-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7482482B2 (en) 2004-09-02 2009-01-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7608732B2 (en) * 2005-03-08 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7361784B2 (en) 2004-09-02 2008-04-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7741515B2 (en) 2004-09-02 2010-06-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7608733B2 (en) 2004-09-02 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7586000B2 (en) * 2004-09-02 2009-09-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7371894B2 (en) * 2004-09-02 2008-05-13 Eastman Chemical Company Optimized liquid-phase oxidation
US7568361B2 (en) 2004-09-02 2009-08-04 Eastman Chemical Company Optimized liquid-phase oxidation
US7572932B2 (en) * 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
US7589231B2 (en) 2004-09-02 2009-09-15 Eastman Chemical Company Optimized liquid-phase oxidation
US7399882B2 (en) 2004-09-02 2008-07-15 Eastman Chemical Company Optimized liquid-phase oxidation
US7507857B2 (en) 2004-09-02 2009-03-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7381836B2 (en) 2004-09-02 2008-06-03 Eastman Chemical Company Optimized liquid-phase oxidation
US7563926B2 (en) 2004-09-02 2009-07-21 Eastman Chemical Company Optimized liquid-phase oxidation
US7504535B2 (en) 2004-09-02 2009-03-17 Eastman Chemical Company Optimized liquid-phase oxidation
US7692036B2 (en) 2004-11-29 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7692037B2 (en) * 2004-09-02 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7390921B2 (en) 2004-09-02 2008-06-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7572936B2 (en) 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
US7910769B2 (en) * 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation
MX2007003810A (es) * 2004-10-01 2007-04-25 Invista Tech Sarl Proceso para producir acidos carboxilicos heteroaromaticos.
US7560566B2 (en) * 2004-10-01 2009-07-14 Invista North America S.A.R.L. Process for producing heteroaromatic carboxylic acids
KR20070103000A (ko) * 2004-12-20 2007-10-22 프로세스 디자인 센터 비.브이 방향족 카르복실산의 제조방법
WO2006080404A1 (ja) * 2005-01-26 2006-08-03 Japan Science And Technology Agency マイクロリアクター及びそれを用いた接触反応方法
US7897809B2 (en) * 2005-05-19 2011-03-01 Eastman Chemical Company Process to produce an enrichment feed
US7557243B2 (en) 2005-05-19 2009-07-07 Eastman Chemical Company Enriched terephthalic acid composition
US7884231B2 (en) * 2005-05-19 2011-02-08 Eastman Chemical Company Process to produce an enriched composition
US7919652B2 (en) * 2005-05-19 2011-04-05 Eastman Chemical Company Process to produce an enriched composition through the use of a catalyst removal zone and an enrichment zone
US7880031B2 (en) * 2005-05-19 2011-02-01 Eastman Chemical Company Process to produce an enrichment feed
US7741516B2 (en) * 2005-05-19 2010-06-22 Eastman Chemical Company Process to enrich a carboxylic acid composition
US20060264656A1 (en) * 2005-05-19 2006-11-23 Fujitsu Limited Enrichment process using compounds useful in a polyester process
US20060264662A1 (en) * 2005-05-19 2006-11-23 Gibson Philip E Esterification of an enriched composition
US7834208B2 (en) * 2005-05-19 2010-11-16 Eastman Chemical Company Process to produce a post catalyst removal composition
US20060264664A1 (en) * 2005-05-19 2006-11-23 Parker Kenny R Esterification of an exchange solvent enriched composition
US7884232B2 (en) * 2005-06-16 2011-02-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7732363B2 (en) * 2005-12-20 2010-06-08 Chevron U.S.A. Inc. Regeneration of acidic catalysts
US7678727B2 (en) * 2005-12-20 2010-03-16 Chevron U.S.A. Inc. Regeneration of ionic catalyst by hydrogenation using a homogeneous catalyst
US7355068B2 (en) 2006-01-04 2008-04-08 Eastman Chemical Company Oxidation system with internal secondary reactor
US7358389B2 (en) * 2006-01-04 2008-04-15 Eastman Chemical Company Oxidation system employing internal structure for enhanced hydrodynamics
US20070208199A1 (en) * 2006-03-01 2007-09-06 Kenny Randolph Parker Methods and apparatus for isolating carboxylic acid
US7501537B2 (en) * 2006-03-01 2009-03-10 Eastman Chemical Company Polycarboxylic acid production system employing oxidative digestion with reduced or eliminated upstream liquor exchange
US7863483B2 (en) * 2006-03-01 2011-01-04 Eastman Chemical Company Carboxylic acid production process
US8697906B2 (en) * 2006-03-01 2014-04-15 Grupo Petrotemex, S.A. De C.V. Methods and apparatus for producing a low-moisture carboxylic acid wet cake
US7462736B2 (en) * 2006-03-01 2008-12-09 Eastman Chemical Company Methods and apparatus for isolating carboxylic acid
US7847121B2 (en) * 2006-03-01 2010-12-07 Eastman Chemical Company Carboxylic acid production process
US8173835B2 (en) * 2006-03-01 2012-05-08 Grupo Petrotemex, S.A. De C.V. Method and apparatus for drying carboxylic acid
US20070208194A1 (en) * 2006-03-01 2007-09-06 Woodruff Thomas E Oxidation system with sidedraw secondary reactor
US7420082B2 (en) * 2006-03-01 2008-09-02 Eastman Chemical Company Polycarboxylic acid production system employing hot liquor removal downstream of oxidative digestion
US7772424B2 (en) * 2006-03-01 2010-08-10 Eastman Chemical Company Polycarboxylic acid production system employing enhanced evaporative concentration downstream of oxidative digestion
US7816556B2 (en) * 2006-03-01 2010-10-19 Eastman Chemical Company Polycarboxylic acid production system employing enhanced multistage oxidative digestion
US7888529B2 (en) * 2006-03-01 2011-02-15 Eastman Chemical Company Process to produce a post catalyst removal composition
DE102006016302A1 (de) * 2006-04-06 2007-10-25 Süd-Chemie AG Verfahren zur Oxidation von Alkylbenzolen
US7674739B2 (en) * 2006-04-21 2010-03-09 Chevron U.S.A. Inc. Regeneration of ionic liquid catalyst using a metal in the absence of added hydrogen
JP5344510B2 (ja) * 2006-07-28 2013-11-20 国立大学法人東北大学 酸化方法
GB0621970D0 (en) * 2006-11-03 2006-12-13 Invista Technologies S O R L Oxidation reactions-1
GB0621968D0 (en) * 2006-11-03 2006-12-13 Invista Technologies S O R L Oxidation reactions-II
US7465824B2 (en) * 2007-02-08 2008-12-16 Bp Corporation North America Inc. Process for the production of high purity aromatic carboxylic acids using a benzoic acid and water solvent for oxidation and purification
KR101278303B1 (ko) * 2008-01-25 2013-06-25 삼성석유화학(주) 다단계의 산화방식을 적용한 친환경적인 테레프탈산 제조방법
GB0808200D0 (en) * 2008-05-06 2008-06-11 Invista Technologies Srl Power recovery
US20130255259A1 (en) * 2008-10-24 2013-10-03 Invista North America S.A R.L. Power recovery for use in start-up or re-start of a pure terephthalic acid production process
US20100113735A1 (en) * 2008-10-31 2010-05-06 Eastman Chemical Company Integrated Co-Production of Dicarboxylic Acids
JP6487543B2 (ja) * 2014-10-31 2019-03-20 エルジー・ケム・リミテッド 蒸留装置
CN104907008B (zh) * 2015-06-04 2017-10-27 河北科技大学 一种甲苯直接氧化制备苯甲酸和苯甲醛的反应装置和方法
WO2019028097A1 (en) * 2017-08-01 2019-02-07 Bp Corporation North America Inc. METHOD FOR PREHEATING WATER OF BOILER SUPPLY IN THE MANUFACTURE OF PURIFIED AROMATIC CARBOXYLIC ACIDS

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2245528A (en) * 1938-10-18 1941-06-10 Du Pont Catalytic oxidation of alkyl substituted aromatic compounds
US4550198A (en) * 1982-11-04 1985-10-29 Georgia Tech Research Institute Purification of terephthalic acid by supercritical fluid extraction
US5171880A (en) * 1987-09-01 1992-12-15 Allied-Signal Inc. Oxidation of organic compounds having benzylic carbon atoms in water
GB9102393D0 (en) 1991-02-05 1991-03-20 Ici Plc Production of terephthalic acid
GB9104776D0 (en) 1991-03-07 1991-04-17 Ici Plc Process for the production of terephthalic acid
US5250193A (en) * 1992-07-28 1993-10-05 Air Products And Chemicals, Inc. Wet oxidation of aqueous streams
US5674405A (en) * 1995-07-28 1997-10-07 Modar, Inc. Method for hydrothermal oxidation
WO1998038150A1 (en) 1997-02-27 1998-09-03 E.I. Du Pont De Nemours And Company Production of terephthalic acid
JP2001079571A (ja) * 1999-09-14 2001-03-27 Toshiba Corp 超臨界水酸化反応方法、超臨界水反応プラントおよびユーティリティプラント
US6765113B2 (en) * 2000-07-19 2004-07-20 E.I. Du Pont De Nemours And Company Production of aromatic carboxylic acids

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102076408B (zh) * 2008-04-30 2014-08-27 英威达技术有限公司 用于制备芳族羧酸的在超临界或近超临界水中的催化氧化反应

Also Published As

Publication number Publication date
BR0112990A (pt) 2003-06-24
US20040199006A1 (en) 2004-10-07
JP2004504289A (ja) 2004-02-12
US6765113B2 (en) 2004-07-20
EP1301456B1 (en) 2008-07-09
ES2309080T3 (es) 2008-12-16
CA2413748C (en) 2010-12-14
MY127798A (en) 2006-12-29
MX236902B (es) 2006-05-15
DZ3117A1 (fr) 2004-09-19
RU2003104827A (ru) 2004-07-10
ATE400543T1 (de) 2008-07-15
DE60134744D1 (de) 2008-08-21
US7238833B2 (en) 2007-07-03
CA2413748A1 (en) 2002-01-24
IN2002MU01837A (enExample) 2005-02-04
AR029852A1 (es) 2003-07-16
KR20030019595A (ko) 2003-03-06
BR0112990B1 (pt) 2012-12-11
EG22982A (en) 2003-12-31
US20020028968A1 (en) 2002-03-07
AU2001275960A1 (en) 2002-01-30
CN1443152A (zh) 2003-09-17
WO2002006201A1 (en) 2002-01-24
MXPA03000502A (es) 2003-10-15
EP1301456A1 (en) 2003-04-16

Similar Documents

Publication Publication Date Title
CN1213015C (zh) 芳族羧酸的制备
CN110026225B (zh) 一种具有可见光催活性的In-NH2/g-C3N4复合材料及其应用
JP5889389B2 (ja) 排水処理用触媒を用いた排水の処理方法
CN1230409C (zh) 改进的羧酸生产工艺
KR101432517B1 (ko) 순수 형태를 포함하는 방향족 카르복실산의 제조 방법 및제조 장치
CN1822900A (zh) 用于生产芳族羧酸的设备和方法
CN1248238A (zh) 对苯二酸的生产
SA03240429B1 (ar) عملية لإنتاج أحماض كربوكسيلية أروماتية aromatic carboxylic acids
RU2695221C2 (ru) Находящиеся под давлением сырьевые смеси, содержащие неочищенные ароматические карбоновые кислоты
RU2678993C2 (ru) Рецикл конденсата высокого давления при производстве очищенных ароматических карбоновых кислот
CN1255371C (zh) 起动反应器的方法和反应器系统
CN1569785A (zh) 制备甲醇的方法
CN101045683A (zh) 高纯度对苯二甲酸的制造方法
CN2791044Y (zh) 对苯二甲酸的生产装置
CN1281569C (zh) 一种催化氧化体系制备壬二酸的方法
CN1156430C (zh) 均三甲苯均相氧化生产3.5—二甲基苯甲酸的方法
CN1090170C (zh) 生产芳族羧酸的方法
CN1665771A (zh) 在超临界条件下制备芳香族二羧酸的方法
TW593259B (en) Production of aromatic carboxylic acids
RU2568113C1 (ru) Способ производства метанола и установка для его осуществления
JP4955881B2 (ja) 熱反応ガスを冷却するための、例えば無水フタル酸の製造における、方法および装置
CN101035763A (zh) 杂芳族羧酸的制造方法
CN106006578A (zh) 含有机物的氮气的净化处理工艺、净化处理反应器及净化处理系统
CN1406922A (zh) 纯多级冷凝物喷射

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
ASS Succession or assignment of patent right

Owner name: INVISTA TECH SARL

Free format text: FORMER OWNER: E. I. DU PONT DE NEMOURS AND CO.

Effective date: 20051223

C41 Transfer of patent application or patent right or utility model
TR01 Transfer of patent right

Effective date of registration: 20051223

Address after: Zurich Switzerland

Patentee after: INVISTA TECHNOLOGIES S.A.R.L.

Address before: Wilmington, Delaware, USA

Patentee before: E. I. du Pont de Nemours and Co.

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20050803

Termination date: 20160717