CN1159309C - 胡椒醛的制备方法 - Google Patents

胡椒醛的制备方法 Download PDF

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Publication number
CN1159309C
CN1159309C CNB018043488A CN01804348A CN1159309C CN 1159309 C CN1159309 C CN 1159309C CN B018043488 A CNB018043488 A CN B018043488A CN 01804348 A CN01804348 A CN 01804348A CN 1159309 C CN1159309 C CN 1159309C
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CN
China
Prior art keywords
piperonylaldehyde
preparation
acid
organic solvent
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CNB018043488A
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English (en)
Chinese (zh)
Other versions
CN1400972A (zh
Inventor
ʤ
原田胜正
־
白井昌志
斯波晃司
古谷敏男
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Ube Corp
Original Assignee
Ube Industries Ltd
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Publication date
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Publication of CN1400972A publication Critical patent/CN1400972A/zh
Application granted granted Critical
Publication of CN1159309C publication Critical patent/CN1159309C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
    • C07D317/44—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D317/46—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems condensed with one six-membered ring
    • C07D317/48—Methylenedioxybenzenes or hydrogenated methylenedioxybenzenes, unsubstituted on the hetero ring
    • C07D317/50—Methylenedioxybenzenes or hydrogenated methylenedioxybenzenes, unsubstituted on the hetero ring with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to atoms of the carbocyclic ring
    • C07D317/54—Radicals substituted by oxygen atoms

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Hydrogenated Pyridines (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CNB018043488A 2000-02-02 2001-02-02 胡椒醛的制备方法 Expired - Fee Related CN1159309C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2000024638 2000-02-02
JP24638/2000 2000-02-02

Publications (2)

Publication Number Publication Date
CN1400972A CN1400972A (zh) 2003-03-05
CN1159309C true CN1159309C (zh) 2004-07-28

Family

ID=18550592

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB018043488A Expired - Fee Related CN1159309C (zh) 2000-02-02 2001-02-02 胡椒醛的制备方法

Country Status (7)

Country Link
US (1) US6686482B2 (enExample)
EP (1) EP1253147B1 (enExample)
CN (1) CN1159309C (enExample)
AT (1) ATE273969T1 (enExample)
NO (1) NO327235B1 (enExample)
TW (1) TWI291954B (enExample)
WO (1) WO2001057016A1 (enExample)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100335476C (zh) * 2005-12-14 2007-09-05 四川大学 以对甲基苯酚为原料制备洋茉莉醛的方法
JP5494488B2 (ja) * 2008-10-07 2014-05-14 宇部興産株式会社 芳香族アルデヒド化合物の製造法
CN101659650B (zh) * 2009-09-24 2012-09-05 上海力智生化科技有限公司 一锅法制备洋茉莉醛的方法
CN101899033B (zh) * 2010-04-29 2012-05-23 东营益盟盛化工有限公司 洋茉莉醛的化学合成制备方法
CN103724316B (zh) * 2013-12-20 2016-02-10 暨南大学 芝麻酚中间产物胡椒醛的制备方法与应用
CN103923056B (zh) * 2014-04-30 2016-05-25 成都建中香料香精有限公司 3,4-亚甲基二氧基苯甲醛的合成方法
CN104151285A (zh) * 2014-08-14 2014-11-19 江苏亚泰化工有限公司 一种制备3,4-亚甲二氧基杏仁酸的方法
CN105693688B (zh) * 2016-04-01 2019-07-05 福建仁宏医药化工有限公司 一种洋茉莉醛中间体3,4-亚甲二氧基苯乙醇酸的反应处理方法
CN105777704A (zh) * 2016-04-01 2016-07-20 衢州信步化工科技有限公司 一种洋茉莉醛的双塔连续化精馏工艺
CN105777705B (zh) * 2016-04-01 2018-09-21 福建仁宏医药化工有限公司 一种洋茉莉醛中间体合成反应后期处理方法
CN106349208A (zh) * 2016-08-25 2017-01-25 宿迁市万和泰化工有限公司 一种洋茉莉醛的制备方法
CN106349209A (zh) * 2016-08-25 2017-01-25 宿迁市万和泰化工有限公司 一种洋茉莉醛的合成工艺
CN117143069A (zh) * 2023-09-07 2023-12-01 玉溪健坤生物药业有限公司 一种3,4-亚甲二氧基苯乙醇酸及胡椒醛的制备方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2754490A1 (de) * 1977-12-07 1979-06-13 Haarmann & Reimer Gmbh Verfahren zur herstellung von 3,4-methylendioxymandelsaeure
JP3282372B2 (ja) * 1994-06-07 2002-05-13 宇部興産株式会社 ピペロナールの製法
JPH0899971A (ja) * 1994-09-30 1996-04-16 Ube Ind Ltd ピペロナールの精製方法

Also Published As

Publication number Publication date
NO327235B1 (no) 2009-05-18
WO2001057016A1 (en) 2001-08-09
CN1400972A (zh) 2003-03-05
US6686482B2 (en) 2004-02-03
US20030013897A1 (en) 2003-01-16
ATE273969T1 (de) 2004-09-15
NO20023633L (no) 2002-08-28
EP1253147B1 (en) 2004-08-18
TWI291954B (enExample) 2008-01-01
EP1253147A4 (en) 2003-05-28
EP1253147A1 (en) 2002-10-30
NO20023633D0 (no) 2002-07-31

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Granted publication date: 20040728

Termination date: 20140202