CN115429726A

CN115429726A - Oxygen mask and preparation method thereof

Info

Publication number: CN115429726A
Application number: CN202210801657.2A
Authority: CN
Inventors: 谢秉辰; 李岳宾
Original assignee: Dongguan City Yan Cosmetics Co ltd
Current assignee: Dongguan City Yan Cosmetics Co ltd
Priority date: 2022-07-07
Filing date: 2022-07-07
Publication date: 2022-12-06

Abstract

The invention discloses an oxygen mask and a preparation method thereof, wherein the mask is prepared by mixing and reacting 95wt% of a component A and 5wt% of a component B; the component A comprises, based on 100 parts of the total mass of the component A, glyceryl stearate, squalane, centella asiatica extract, alcaligenes bacillus polysaccharides, tremella fruiting body extract, glycerin, sodium hyaluronate, collagen, polysorbate-20, caprylyl hydroximic acid-containing substance, hydrogen peroxide and the balance of water, which are prepared according to a certain mass; the component B comprises a substance containing octanoyl hydroximic acid, superoxide dismutase and the balance of water, wherein the substance is prepared according to a certain mass according to 100 parts of the total mass of the component B. The facial mask prepared by the invention has the effects of moisturizing, moistening, whitening, resisting oxidation and activating cell regeneration, can effectively eliminate various fine wrinkles and solves the problem of skin.

Description

Oxygen mask and preparation method thereof

Technical Field

The invention relates to the technical field of masks, in particular to an oxygen mask and a preparation method thereof.

Background

The skin is the largest respiratory organ of a human body, oxidation of the skin can be caused along with the increase of age or in the increasingly worsened air for a long time, further, the skin is dry and dull, fine wrinkles are generated, the oxidation of the skin is actually lack of oxygen, the oxygen in the air only accounts for about 25 percent, and the increasing harm of PM2.5 enhances the skin aging speed, so the most basic project for effectively preventing the skin aging is to supplement oxygen to the skin. The oxygen can activate aged cells, nourish withered cells, make the skin more fresh, bright and glossy, can provide the skin with the most thorough deep cleaning, improve skin problems such as wrinkles, color spots, melanin pigmentation, dark skin color and the like, and is more beneficial to the absorption of maintenance components and help to eliminate skin toxins. After the cells are activated, the skin is naturally younger, more elastic and firmer, and the skin aging can be postponed, the skin quality can be improved, and the function of skin cell regeneration can be provided.

Most of the existing facial masks on the market are facial mask products combining essence and facial mask paper, but the faces are different in size and width, so that the facial masks generally hardly meet the requirements of all facial shapes; the face fit degree is not enough, or the mask allowance is large, the essence is wasted, or the face cannot be effectively fitted to form wrinkles, so that the beauty effect is greatly reduced. Currently, oxygen bubble masks are sold on the market, and bubbles are generated mainly by foaming a surfactant (foaming agent) when a fluorine-containing compound in a mask formula naturally volatilizes in the air, and only by utilizing the gasification effect of the fluorine-containing compound to generate foams, but are not related to oxygen. In addition, the application of a large amount of fluorine-containing compounds pollutes the atmospheric environment and has a potential risk of damaging the ozone layer of the atmosphere. Therefore, the development of the mask which contains oxygen and has good beautifying effect has important practical significance.

Disclosure of Invention

The invention aims to overcome the defects of the prior art and provides an oxygen mask and a preparation method thereof, wherein the mask has the effects of moisturizing, moistening, whitening, resisting oxidation and activating cell regeneration, can effectively eliminate various fine wrinkles and solves the problem of skin.

In order to achieve the purpose, the invention adopts the following technical scheme:

an oxygen mask is prepared by mixing and reacting 95wt% of component A and 5wt% of component B; the component A comprises the following components in parts by weight based on 100 parts of the total mass of the component A: 0.1-0.15% of glycerol stearate, 0.1-0.15% of squalane, 5-10% of centella asiatica extract, 0.4-0.45% of alcaligenes polysaccharides, 0.1-0.2% of tremella fuciformis fruiting body extract, 2-3% of glycerol, 0.03-0.05% of sodium hyaluronate, 0.1-0.2% of collagen, 0.1-0.15% of polysorbate-20, 0.4-0.5% of caprylyl hydroximic acid-containing substance, 4-5% of hydrogen peroxide and the balance of water; the component B comprises the following components in parts by weight based on 100 parts of the total mass of the component B: 0.4-0.5 of caprylyl hydroximic acid-containing substance, 3-3.5wt% of superoxide dismutase and the balance of water.

The caprylyl hydroximic acid-containing substance is prepared from 1, 3-propylene glycol, 1, 2-hexanediol and caprylyl hydroximic acid according to a mass ratio of 65:30:5 mixing the mixture.

The component A comprises the following components in parts by weight based on 100 parts of the total mass of the component A: 0.1% of glyceryl stearate, 0.1% of squalane, 5% of centella asiatica extract, 0.4% of Alcaligenes polysaccharide, 0.1% of tremella fruiting body extract, 2% of glycerin, 0.03% of sodium hyaluronate, 0.1% of collagen, 0.1% of polysorbate-20, 0.4% of a caprylyl hydroximic acid-containing substance, 4% of hydrogen peroxide and the balance of water; the component B comprises the following components in parts by weight based on 100 parts of the total mass of the component B: 0.4% of substance containing octanoyl hydroximic acid, 3% of superoxide dismutase and the balance of water; the caprylyl hydroximic acid-containing substance is prepared from 1, 3-propylene glycol, 1, 2-hexanediol and caprylyl hydroximic acid according to a mass ratio of 65:30:5 mixing the mixture.

The component A comprises the following components in parts by weight based on 100 parts of the total mass of the component A: 0.15% of glyceryl stearate, 0.15% of squalane, 10% of centella asiatica extract, 0.45% of Alcaligenes polysaccharide, 0.2% of tremella fruiting body extract, 3% of glycerin, 0.05% of sodium hyaluronate, 0.2% of collagen, 0.15% of polysorbate-20, 0.5% of a caprylyl hydroximic acid-containing substance, 5% of hydrogen peroxide and the balance of water; the component B comprises the following components in parts by weight based on 100 parts of the total mass of the component B: 0.5 percent of substance containing caprylyl hydroximic acid, 3.5 percent of superoxide dismutase and the balance of water; the caprylyl hydroximic acid-containing substance is prepared from 1, 3-propylene glycol, 1, 2-hexanediol and caprylyl hydroximic acid according to a mass ratio of 65:30:5 mixing the mixture.

A preparation method of the oxygen mask comprises the following steps:

(a) Preparation of component A:

(1) Heating, stirring and uniformly mixing glyceryl stearate and squalane to obtain an oil phase mixture;

(2) Dissolving water, herba Centellae extract, alcaligenes polysaccharide, tremella sporophore extract, glycerol, sodium hyaluronate, collagen and vomit-20 in water under heating and stirring to obtain water phase mixture;

(3) Adding the oil phase mixture into the water phase mixture for homogenizing and emulsifying, wherein the emulsifying time is 5min, closing the homogenizing after the emulsifying is finished, cooling to 40 ℃ at the stirring speed of 70 r/min, adding hydrogen peroxide and the substance containing caprylyl hydroximic acid, and continuously stirring uniformly to obtain a component A;

(b) Preparation of component B: heating deionized water to 85 deg.C, stirring for 30min, cooling to 40 deg.C, adding superoxide dismutase and the substance containing octanoyl hydroximic acid, and stirring to obtain component B;

(c) 95% of the component A and the component B by mass: 5 percent of the components are mixed, and the oxygen mask is obtained after the component A and the component B fully react.

In the steps (1) and (2), the heating and stirring temperature is both 80 ℃; in the step (3), the emulsifying temperature is 80 ℃, and the emulsifying and stirring speed is 4000 revolutions per minute.

In step (b), the stirring rate was 20 rpm.

In the invention, the glyceryl stearate (also called glyceryl stearate) is used as an oil phase mixture emulsifier, so that oil and water can be better combined.

Squalane is hydrocarbon oil with excellent performance prepared by hydrogenating squalene extracted from deep-sea shark liver, and is also named deep-sea shark liver oil. Squalane is one of the components of skin sebum, namely a sebum membrane, namely one of the components of the outermost water-locking defense layer of the skin, and can help to construct the sebum membrane, enhance the self-moisturizing and water-locking capability of the skin, moisten the skin and strengthen the immunity of the skin.

The centella asiatica extract has the effect of relieving skin, has a good effect on oily skin and sensitive skin, and has the effects of astringing pores, replenishing water, moisturizing and calming the skin.

Alcaligenes polysaccharide is an extract obtained from fermentation of pure plants, and has thickening and moisturizing effects.

The tremella extract is rich in natural colloid, has the function of nourishing yin, can moisten skin after long-term use and has the efficacy of removing chloasma and freckles on the face.

Glycerin is a natural humectant.

Sodium hyaluronate Hyaluronic Acid (Hyaluronan, hyaluronic Acid), also known as uronic Acid, hyaluronic Acid, is a glycosaminoglycan composed of the basic structure of disaccharides (D-glucuronic Acid and N-acetylglucosamine), and is one of the main components of extracellular matrix. Hyaluronic acid is widely present in connective, epithelial and neural tissue. Unlike most glycosaminoglycans, hyaluronic acid is sulfur-free and forms in cell membranes rather than in high-k bodies, with relative molecular masses of up to 106 orders of magnitude. Its hyaluronic molecule can carry over 500 times of water, and is the best moisture-keeping component recognized at present.

Collagen can restore skin elasticity.

The hydrogen peroxide has bactericidal effect.

Caprylyl hydroximic acid is a skin conditioner, antibacterial agent. The peptide with antimicrobial activity is separated from the plant Leuconostoc albicans by using modern science and technology, and simultaneously the requirements of natural ingredients and peptide are met; has strong killing and inhibiting effects on staphylococcus aureus, escherichia coli, pseudomonas aeruginosa, candida albicans, aspergillus niger, klebsiella pneumoniae and bukholderia cepacia; is suitable for a wide pH value range, is a preservative substitute with skin conditioning effect, and is used in products for sensitive skin and removing acnes.

Polysorbate-20 is a water emulsifier, primarily to allow better oil to water binding.

The glyceryl stearates in the invention are purchased from Taiwan Xianglin chemical enterprises, inc.; alcaligenes polysaccharide was purchased from Taiwan platinum-rich chemical enterprises, inc.; collagen was purchased from Shanghai Hanxin science and technology Limited; superoxide dismutase was purchased from Kyowa Jitewei Biotech, inc.

The invention has the beneficial effects that: the component A and the component B are mixed to breed oxygen, the oxygen is injected into the mask liquid, when the mask liquid stays on the surface of the skin, fresh oxygen is provided for the skin, the cells are activated, water and oxygen are generated by the reaction of enzyme and hydrogen peroxide, and the enzyme is used as a catalyst, so that the cells have regeneration capacity, various fine wrinkles are eliminated, and various problems of the skin are solved.

Drawings

FIG. 1 is a graph showing a comparison between before and after mixing of component A and component B in example 1 of the present invention (I is before mixing, and II is after mixing);

FIG. 2 is a schematic diagram of a combustion-supporting wood stick with sparks after the component A and the component B are mixed according to example 1 of the invention (III is before the wood stick extends into the facial mask bag, and IV is after the wood stick extends into the facial mask bag).

Detailed Description

The invention is further described with reference to the accompanying drawings and the detailed description below:

example 1

An oxygen mask is prepared by mixing 95wt% of component A and 5wt% of component B and reacting.

The component A comprises the following components in parts by weight based on 100 parts of the total mass of the component A: 0.1% glyceryl stearate, 0.1% squalane, 5% centella asiatica extract, 0.4% alcaligenes polysaccharides, 0.1% tremella fuciformis fruiting body extract, 2% glycerin, 0.03% hyaluronic acid, 0.1% collagen, 0.1% polysorbate-20, 0.4% caprylyl hydroximic acid, 4% hydrogen peroxide, and the balance water.

The component B comprises the following components in parts by weight: 0.4% caprylyl hydroximic acid, 3% superoxide dismutase and the balance water.

Preparation method of oxygen mask

The raw materials are prepared according to the formula proportion, and the preparation method comprises the following steps:

(a) Preparation of component A:

(1) Uniformly stirring and mixing the glyceryl stearate and the squalane at 80 ℃ (the stirring speed is 50 revolutions per minute) to obtain an oil phase mixture;

(2) Dissolving water, herba Centellae extract, alcaligenes polysaccharide, tremella fruiting body extract, glycerol, sodium hyaluronate, collagen, and polysorbate-20 at 80 deg.C under heating and stirring (stirring rate is 50 rpm) to obtain water phase mixture;

(3) Slowly adding the oil phase mixture into the water phase mixture for homogenizing and emulsifying, wherein the emulsifying speed is controlled at 4000 revolutions per minute, the emulsifying time is 5min, after the emulsifying is finished, the homogenizing is closed, the stirring speed is controlled at 70 revolutions per minute, the temperature is reduced to 40 ℃, and hydrogen peroxide and the caprylyl hydroximic acid-containing substance are added and continuously stirred at the speed of 70 revolutions per minute for 5min to obtain a component A;

(b) Preparation of component B: heating deionized water to 85 deg.C, stirring at 20 rpm for 30min, cooling to 40 deg.C, adding superoxide dismutase and octanoyl hydroximic acid-containing substance, and continuing at 20 rpm for 5min to obtain component B;

(c) 95% of the component A and the component B by mass: mixing 5%, and reacting component A and component B to obtain the oxygen facial mask.

FIG. 1 is a graph comparing the composition A and composition B prepared in example 1 before and after mixing (I is before mixing and II is after mixing). The component B and the component A are separately packaged into a mask bag with two vertically separated containing cavities (the upper containing cavity is filled with the component B, and the lower containing cavity is filled with the component A), when the mask bag is used, the component A is extruded into the component B, and the component A and the component B react to generate a large amount of oxygen in the containing cavity of the lower mask bag to expand; the small wood stick with the spark is stretched into the mask bag, and the small wood stick is found to be re-combusted, which indicates that a large amount of pure oxygen is indeed generated in the mask bag.

Example 2

The component A comprises the following components in parts by weight based on 100 parts of the total mass of the component A: 0.15% of glyceryl stearate, 0.15% of squalane, 10% of centella asiatica extract, 0.45% of Alcaligenes polysaccharide, 0.2% of tremella fruiting body extract, 3% of glycerin, 0.05% of sodium hyaluronate, 0.2% of collagen, 0.15% of polysorbate-20, 0.5% of a caprylyl hydroximic acid-containing substance, 5% of hydrogen peroxide and the balance of water.

The component B comprises the following components in parts by weight based on 100 parts of the total mass of the component B: 0.5 percent of substance containing caprylyl hydroximic acid, 3.5 percent of superoxide dismutase and the balance of water.

Preparation method of oxygen mask

(a) Preparation of component A:

(1) Uniformly stirring and mixing the glycerol stearate and the squalane at the temperature of 80 ℃ (the stirring speed is 50 revolutions per minute) to obtain an oil phase mixture;

(b) Preparation of component B: heating deionized water to 85 deg.C, stirring at 20 r/min for 30min, cooling to 40 deg.C, adding superoxide dismutase and the substance containing octanoyl hydroximic acid, and continuing at 20 r/min for 5min to obtain component B;

After the component A and the component B of the mask product are mixed, a small wood stick with sparks is stretched into a mask bag, and the small wood stick is also found to be re-burnt, which indicates that the mixture reaction of the component A and the component B generates a large amount of pure oxygen.

The 150 volunteers were randomly screened into 3 groups, the first group tested the mask prepared in example 1, the second group tested the mask prepared in example 2, and the 3 rd group tested the commercially available oxygen bubble mask, with the following test results:

mask product	Example 1	Example 2	Is commercially available
				Brightness improvement more than 2 (number of people)	40	38	5
Brightness improvement more than 1 level (number of people)	10	12	29
				Brightness is not increased (number of people)	0	0	16
Average reduction rate of melanin%	28.5	24.7	10.1
				Average moisture retention%	93.7	92.1	92.6
Average improvement rate of skin elasticity%	9.55	9.11	2.14

The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.

Claims

1. An oxygen mask, comprising: the oxygen mask is formed by mixing and reacting 95wt% of component A and 5wt% of component B; the component A comprises the following components in parts by weight based on 100 parts of the total mass of the component A: 0.1-0.15% of glycerol stearate, 0.1-0.15% of squalane, 5-10% of centella asiatica extract, 0.4-0.45% of alcaligenes polysaccharides, 0.1-0.2% of tremella fuciformis fruiting body extract, 2-3% of glycerol, 0.03-0.05% of sodium hyaluronate, 0.1-0.2% of collagen, 0.1-0.15% of polysorbate-20, 0.4-0.5% of caprylyl hydroximic acid-containing substance, 4-5% of hydrogen peroxide and the balance of water; the component B comprises the following components in parts by weight based on 100 parts of the total mass of the component B: 0.4-0.5% of caprylyl hydroximic acid-containing substance, 3-3.5% of superoxide dismutase and the balance of water.

2. The oxygen mask of claim 1, wherein: the caprylyl hydroximic acid-containing substance is prepared from 1, 3-propylene glycol, 1, 2-hexanediol and caprylyl hydroximic acid according to a mass ratio of 65:30:5 mixing the mixture.

3. The oxygen mask of claim 1, wherein: the component A comprises the following components in parts by weight based on 100 parts of the total mass of the component A: 0.1% of glyceryl stearate, 0.1% of squalane, 5% of centella asiatica extract, 0.4% of Alcaligenes polysaccharide, 0.1% of tremella fruiting body extract, 2% of glycerin, 0.03% of sodium hyaluronate, 0.1% of collagen, 0.1-0.15% of polysorbate-20, 0.4% of caprylyl hydroximic acid-containing substance, 4% of hydrogen peroxide and the balance of water; the component B comprises the following components in parts by weight based on 100 parts of the total mass of the component B: 0.4% of substance containing octanoyl hydroximic acid, 3% of superoxide dismutase and the balance of water;

4. The oxygen mask of claim 1, wherein: the component A comprises the following components in parts by weight based on 100 parts of the total mass of the component A: 0.15% of glyceryl stearate, 0.15% of squalane, 10% of centella asiatica extract, 0.45% of alcaligenes polysaccharides, 0.2% of tremella fuciformis fruiting body extract, 3% of glycerin, 0.05% of sodium hyaluronate, 0.2% of collagen, 0.15% of polysorbate-20, 0.5% of a caprylyl hydroximic acid-containing substance, 5% of hydrogen peroxide and the balance of water; the component B comprises the following components in parts by weight based on 100 parts of the total mass of the component B: 0.5% of substance containing octanoyl hydroximic acid, 3.5% of superoxide dismutase and the balance of water;

5. A method for preparing the oxygen mask pack according to any one of claims 1 to 4, wherein: the method comprises the following steps:

(a) Preparation of component A:

(1) Heating, stirring and uniformly mixing the glycerol stearate and the squalane to obtain an oil phase mixture;

(2) Heating and stirring water, herba Centellae extract, alcaligenes polysaccharide, tremella fruiting body extract, glycerol, sodium hyaluronate, collagen, and polysorbate-20 to dissolve to obtain water phase mixture;

(3) Adding the oil phase mixture into the water phase mixture for homogenization and emulsification, wherein the emulsification time is 5min, closing homogenization after the emulsification is finished, cooling to 40 ℃ at the stirring speed of 70 r/min, adding hydrogen peroxide and the substance containing caprylyl hydroximic acid, and continuously stirring uniformly to obtain a component A;

(b) Preparation of component B: heating deionized water to 85 deg.C, stirring for 30min, cooling to 40 deg.C, adding superoxide dismutase and substance containing octanoyl hydroximic acid, and stirring to obtain component B;

6. The method of preparing an oxygen mask as claimed in claim 5, wherein: in the steps (1) and (2), the heating and stirring temperature is both 80 ℃; in the step (3), the emulsifying temperature is 80 ℃, and the emulsifying stirring speed is 4000 revolutions per minute.

7. The method of preparing an oxygen mask as claimed in claim 6, wherein: in step (b), the stirring rate was 20 rpm.