CN115364010A - Rosemary amino acid shampoo and preparation method thereof - Google Patents
Rosemary amino acid shampoo and preparation method thereof Download PDFInfo
- Publication number
- CN115364010A CN115364010A CN202211019055.8A CN202211019055A CN115364010A CN 115364010 A CN115364010 A CN 115364010A CN 202211019055 A CN202211019055 A CN 202211019055A CN 115364010 A CN115364010 A CN 115364010A
- Authority
- CN
- China
- Prior art keywords
- percent
- rosemary
- amino acid
- shampoo
- laureth sulfate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002453 shampoo Substances 0.000 title claims abstract description 64
- 150000001413 amino acids Chemical class 0.000 title claims abstract description 44
- 244000178231 Rosmarinus officinalis Species 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title abstract description 10
- 235000001014 amino acid Nutrition 0.000 claims abstract description 56
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 claims abstract description 32
- 229940057950 sodium laureth sulfate Drugs 0.000 claims abstract description 27
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical compound [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 claims abstract description 27
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 24
- -1 polydimethylsiloxane Polymers 0.000 claims abstract description 20
- PXEDJBXQKAGXNJ-QTNFYWBSSA-L disodium L-glutamate Chemical compound [Na+].[Na+].[O-]C(=O)[C@@H](N)CCC([O-])=O PXEDJBXQKAGXNJ-QTNFYWBSSA-L 0.000 claims abstract description 19
- 229940079779 disodium cocoyl glutamate Drugs 0.000 claims abstract description 18
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000004471 Glycine Substances 0.000 claims abstract description 16
- 239000004220 glutamic acid Substances 0.000 claims abstract description 16
- 235000013922 glutamic acid Nutrition 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims abstract description 14
- 229940092258 rosemary extract Drugs 0.000 claims abstract description 14
- 235000020748 rosemary extract Nutrition 0.000 claims abstract description 14
- 239000001233 rosmarinus officinalis l. extract Substances 0.000 claims abstract description 14
- 102000011782 Keratins Human genes 0.000 claims abstract description 13
- 108010076876 Keratins Proteins 0.000 claims abstract description 13
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 12
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 12
- 239000011780 sodium chloride Substances 0.000 claims abstract description 12
- XMSXQFUHVRWGNA-UHFFFAOYSA-N Decamethylcyclopentasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 XMSXQFUHVRWGNA-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229940086555 cyclomethicone Drugs 0.000 claims abstract description 6
- 229920002907 Guar gum Polymers 0.000 claims abstract description 4
- 229920000289 Polyquaternium Polymers 0.000 claims abstract description 4
- 239000000665 guar gum Substances 0.000 claims abstract description 4
- 229960002154 guar gum Drugs 0.000 claims abstract description 4
- 235000010417 guar gum Nutrition 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 23
- 239000001331 rosmarinus officinalis leaf Substances 0.000 claims description 20
- 102000008186 Collagen Human genes 0.000 claims description 15
- 108010035532 Collagen Proteins 0.000 claims description 15
- 229920001436 collagen Polymers 0.000 claims description 15
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 14
- 125000000400 lauroyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 13
- 239000000284 extract Substances 0.000 claims description 12
- 239000003921 oil Substances 0.000 claims description 12
- GKQHIYSTBXDYNQ-UHFFFAOYSA-M 1-dodecylpyridin-1-ium;chloride Chemical compound [Cl-].CCCCCCCCCCCC[N+]1=CC=CC=C1 GKQHIYSTBXDYNQ-UHFFFAOYSA-M 0.000 claims description 11
- 239000002253 acid Substances 0.000 claims description 11
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 11
- 229940015975 1,2-hexanediol Drugs 0.000 claims description 10
- 238000004140 cleaning Methods 0.000 claims description 10
- FHKSXSQHXQEMOK-UHFFFAOYSA-N hexane-1,2-diol Chemical compound CCCCC(O)CO FHKSXSQHXQEMOK-UHFFFAOYSA-N 0.000 claims description 10
- TWMBOHVOMWFMJI-UHFFFAOYSA-N 2-hydroxyethyl phosphono hydrogen phosphate Chemical compound OCCOP(O)(=O)OP(O)(O)=O TWMBOHVOMWFMJI-UHFFFAOYSA-N 0.000 claims description 7
- OYINQIKIQCNQOX-UHFFFAOYSA-M 2-hydroxybutyl(trimethyl)azanium;chloride Chemical compound [Cl-].CCC(O)C[N+](C)(C)C OYINQIKIQCNQOX-UHFFFAOYSA-M 0.000 claims description 6
- 244000007835 Cyamopsis tetragonoloba Species 0.000 claims description 6
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 claims description 6
- VFKZECOCJCGZQK-UHFFFAOYSA-M 3-hydroxypropyl(trimethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCCO VFKZECOCJCGZQK-UHFFFAOYSA-M 0.000 claims description 5
- 229940008099 dimethicone Drugs 0.000 claims description 5
- 230000002829 reductive effect Effects 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 4
- 125000002801 octanoyl group Chemical group C(CCCCCCC)(=O)* 0.000 claims description 4
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 3
- 230000000249 desinfective effect Effects 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 229940058206 rosemary oil Drugs 0.000 claims description 3
- 239000010668 rosemary oil Substances 0.000 claims description 3
- 238000005070 sampling Methods 0.000 claims description 3
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 2
- AFQGAXFMOMNYDL-UHFFFAOYSA-N n-octyloctan-1-amine;hydrochloride Chemical compound Cl.CCCCCCCCNCCCCCCCC AFQGAXFMOMNYDL-UHFFFAOYSA-N 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 3
- 239000007788 liquid Substances 0.000 claims 2
- 238000004945 emulsification Methods 0.000 claims 1
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 abstract 2
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 abstract 2
- FFOWJDCTFSWUMJ-JXMROGBWSA-N geranyl phosphate Chemical compound CC(C)=CCC\C(C)=C\COP(O)(O)=O FFOWJDCTFSWUMJ-JXMROGBWSA-N 0.000 abstract 2
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 abstract 1
- 235000019270 ammonium chloride Nutrition 0.000 abstract 1
- 125000002350 geranyl group Chemical group [H]C([*])([H])/C([H])=C(C([H])([H])[H])/C([H])([H])C([H])([H])C([H])=C(C([H])([H])[H])C([H])([H])[H] 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- TVWXRUVDPUAFFG-UHFFFAOYSA-N zinc oxygen(2-) hydrochloride Chemical compound [O-2].[Zn+2].Cl TVWXRUVDPUAFFG-UHFFFAOYSA-N 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 18
- 238000012360 testing method Methods 0.000 description 15
- 230000000052 comparative effect Effects 0.000 description 14
- 210000004761 scalp Anatomy 0.000 description 11
- 235000019198 oils Nutrition 0.000 description 10
- 201000004384 Alopecia Diseases 0.000 description 9
- 208000001840 Dandruff Diseases 0.000 description 8
- 231100000360 alopecia Toxicity 0.000 description 7
- 239000000047 product Substances 0.000 description 6
- 239000000686 essence Substances 0.000 description 5
- 230000003405 preventing effect Effects 0.000 description 5
- 238000011156 evaluation Methods 0.000 description 4
- 230000014759 maintenance of location Effects 0.000 description 4
- 208000003251 Pruritus Diseases 0.000 description 3
- 239000003755 preservative agent Substances 0.000 description 3
- 230000002335 preservative effect Effects 0.000 description 3
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000001139 anti-pruritic effect Effects 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000002085 irritant Substances 0.000 description 2
- 231100000021 irritant Toxicity 0.000 description 2
- 230000007803 itching Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 239000000419 plant extract Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 239000004909 Moisturizer Substances 0.000 description 1
- KWQYZJLZQNYFAI-UHFFFAOYSA-N OCC1OP(O)(=O)O1 Chemical compound OCC1OP(O)(=O)O1 KWQYZJLZQNYFAI-UHFFFAOYSA-N 0.000 description 1
- VJKGWQAUECALGS-UHFFFAOYSA-N OCCP(O)(=O)OP(O)=O Chemical compound OCCP(O)(=O)OP(O)=O VJKGWQAUECALGS-UHFFFAOYSA-N 0.000 description 1
- 241001454295 Tetranychidae Species 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000003656 anti-hair-loss Effects 0.000 description 1
- 239000003908 antipruritic agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000003648 hair appearance Effects 0.000 description 1
- 230000003646 hair health Effects 0.000 description 1
- 230000003676 hair loss Effects 0.000 description 1
- 208000024963 hair loss Diseases 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 230000000670 limiting effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000001333 moisturizer Effects 0.000 description 1
- RGUVUPQQFXCJFC-UHFFFAOYSA-N n-hydroxyoctanamide Chemical compound CCCCCCCC(=O)NO RGUVUPQQFXCJFC-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4926—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having six membered rings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Chemical & Material Sciences (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Inorganic Chemistry (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses rosemary amino acid shampoo and a preparation method thereof, wherein the rosemary amino acid shampoo comprises the following components in percentage by mass: 72 to 78 percent of water, 5 to 7 percent of sodium laureth sulfate, 5 to 7 percent of cocamidopropyl betaine, 1.5 to 2.0 percent of disodium cocoyl glutamate, 1.5 to 1.8 percent of sodium laureth sulfate, 1.5 to 1.8 percent of polydimethylsiloxane, 1.2 to 1.6 percent of dimethiconol, 1.2 to 1.6 percent of cocamide DEA, 1.2 to 1.6 percent of cyclomethicone, 0.4 to 0.8 percent of hydrolysis keratin, 0.3 to 0.5 percent of sodium chloride, 0.15 to 0.25 percent of lauroyl amino acid TEA, 0.1 to 0.2 percent of glycine, 0.05 to 0.15 percent of glutamic acid, 0.3 to 0.6 percent of polyquaternium-6 percent of polyquaternium, 0.3 to 0.6 percent of rosemary extract, 0.05 to 0.05 percent of zinc oxide chloride, 0.05 to 0.05 percent of guar gum, 0.05 to 0.05 percent of 15 percent of geranyl ammonium chloride, 0.05 to 0.05 percent of geranyl phosphate, 0.15 percent of geranyl amino acid TEA, 0.05 to 0.05 percent of geranyl phosphate, 0.05 percent of geranyl alcohol and 15 percent of geranyl alcohol.
Description
Technical Field
The invention belongs to the technical field of shampoo products, and particularly relates to rosemary amino acid shampoo and a preparation method thereof.
Background
The shampoo is the most widely used shampoo at present, and along with the improvement of living standard of people, the requirements of people on the shampoo are not only used for washing off grease, dirt and dust attached to scalp and hair, but also the shampoo is not needed to stimulate the scalp, does not increase burden on the scalp, has great cleaning force, and can improve the problems of the scalp and the hair quality.
However, the shampoo in the current market is generally added with essence and preservative, which easily stimulates scalp and cannot effectively improve scalp problems, the function of the product is single, some products have strong cleaning force but are not mild enough, and do not have the effects of preventing alopecia, preserving moisture and the like, and some products have good dandruff removing effect but do not have the effects of preventing alopecia, enabling hair to be smooth and the like; therefore, the development of the shampoo which has good cleaning effect, is mild and non-irritant and can solve the problems of dandruff, alopecia, damaged hair and the like is the research and development direction of products.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide the rosemary amino acid shampoo and the preparation method thereof.
The purpose of the invention is realized as follows:
rosemary amino acid shampoo comprises the following components in percentage by mass: 72 to 78 percent of water, 5 to 7 percent of sodium laureth sulfate, 5 to 7 percent of cocamidopropyl betaine, 1.5 to 2.0 percent of disodium cocoyl glutamate, 1.5 to 1.8 percent of sodium laureth sulfate, 1.5 to 1.8 percent of polydimethylsiloxane, 1.2 to 1.6 percent of dimethiconol, 1.2 to 1.6 percent of cocamide DEA, 1.2 to 1.6 percent of cyclopolydimethylsiloxane, 0.4 to 0.8 percent of hydrolyzed keratin, 0.3 to 0.5 percent of sodium chloride, 0.15 to 0.25 percent of lauroyl collagen amino acid TEA, 0.1 to 0.2 percent of glycine, 0.05 to 0.15 percent of glutamic acid, 60.3 to 0.6 percent of polyquaternium, 0.3 to 0.6 percent of rosemary extract, 0.1 to 0.3 percent of lauryl pyridinium chloride, 0.05 to 0.20 percent of hydroxypropyl trimethyl ammonium chloride, 0.05 to 0.05 percent of rosemary oil, 0.05 to 0.15 percent of ethylene glycol, 0.05 to 0.15 percent of dioctyl ammonium chloride, 0.15 percent of dioctyl glycol and 0.15 percent of ethylene glycol.
Further, the rosemary amino acid shampoo comprises the following components in percentage by mass: water 75%, sodium laureth sulfate 6%, cocamidopropyl betaine 6%, disodium cocoyl glutamate 1.8%, sodium laureth sulfate 1.6%, dimethicone 1.6%, dimethiconol 1.5%, cocamide DEA 1.5%, cyclomethicone 1.4%, hydrolyzed keratin 0.6%, sodium chloride 0.4%, lauroyl collagen amino acid TEA salt 0.2%, glycine 0.15%, glutamic acid 0.1%, polyquaternium-60.5%, rosemary extract 0.5%, rosemary leaf extract 0.5%, lauryl pyridinium chloride 0.2%, guar hydroxypropyltrimonium chloride 0.1%, rosemary leaf oil 0.1%, hydroxyethyl diphosphate 0.1%, 1, 2-hexanediol 0.05%, caprylyl hydroxamic acid 0.1%.
Further, the mass concentration of the sodium laureth sulfate is 70%.
Further, the mass concentration of the cocamidopropyl betaine is 65%.
Further, the pH value of the rosemary amino acid shampoo is 5.5-6.5.
The invention also discloses a preparation method of the rosemary amino acid shampoo, which comprises the following steps:
(1) Weighing the components according to the formula ratio, cleaning and disinfecting production equipment;
(2) Sequentially putting water, sodium laureth sulfate, lauroyl collagen amino acid TEA salt, cocamidopropyl betaine and disodium cocoyl glutamate into a stirring pot, heating to 85 ℃, stirring for 2-3 min to completely dissolve the sodium laureth sulfate, the lauroyl collagen amino acid TEA salt and the disodium cocoyl glutamate, and continuously stirring to cool the sodium laureth sulfate, the sodium cocoyl collagen amino acid TEA salt and the disodium cocoyl glutamate;
(3) When the temperature is reduced to 55-65 ℃, sodium lauryl sulfate, polydimethylsiloxane, cocamide DEA, cyclopolydimethylsiloxane and guar gum hydroxypropyl trimethyl ammonium chloride are sequentially added, and the mixture is stirred for 25-35 min until the mixture is emulsified uniformly;
(4) When the temperature is reduced to below 45 ℃, sequentially adding dimethiconol, hydrolyzed keratin, sodium chloride, polyquaternium-6, rosemary extract, rosemary leaf extract, lauryl pyridinium chloride, rosemary leaf oil, glycine, glutamic acid, hydroxyethylidene phosphate, 1, 2-hexanediol and caprylyl hydroximic acid, uniformly stirring, and continuously stirring for 25-35 min to reduce the temperature;
(5) When the temperature is reduced to below 40 ℃, sampling and inspecting;
(6) Taking out the shampoo from the pot and standing after the shampoo is qualified, thus obtaining the rosemary amino acid shampoo.
Wherein in the step (2), the stirring speed is 750-850 r/min, and the stirring time is 30-50 min; in the step (3) and the step (4), the stirring speed is 400-600 r/min.
Compared with the prior art, the invention has the beneficial effects that:
1. according to the rosemary amino acid shampoo, rosemary plant extract essence and amino acid are added, so that the shampoo can nourish and beautify hair and provide nutrition power for hair health; the formula is mild in faintly acid, can reduce stimulation close to the acid scalp, care hair and keep scalp healthy, and is suitable for pregnant women and infants; alcohol, hormone, animal raw materials, petroleum surfactant, essence and preservative are not added, so that the shampoo is safe and non-irritant.
2. According to the rosemary amino acid shampoo, the coconut oil acyl disodium glutamate serving as the component has good decontamination and foam increasing capabilities, and also has certain antistatic and sterilization capabilities under an acidic condition, and the component is mild and low in irritation and has no harm to skin; the rosemary essence has good effects of regulating water and oil balance and inhibiting spider mites, and also can promote scalp blood circulation, improve alopecia, reduce dandruff and improve scalp problems; the component caprylyl hydroximic acid has stronger antibacterial capability, is a novel preservative substitute, and the component 1, 2-hexanediol also has antibacterial effect, is safer and can be used with confidence; the ingredient hydrolyzed keratin can quickly permeate into the hair core, and can supplement nutrition lost in the hair, so that the hair is more full and healthy; the ingredient glycine, known as "amino acid moisturizer", helps hair absorb and retain moisture, and nourish dry damaged hair; the glutamic acid can help hair and skin to resist free radicals, improve oxidation resistance, delay hair aging, effectively prolong hair vitality, increase hair elasticity, and prevent hair loss.
3. According to the rosemary amino acid shampoo, the rosemary plant extract essence and a plurality of amino acids are added, so that the shampoo can clean and beautify hair, refresh scalp and enable hair to be fluffy and natural; meanwhile, the hair conditioner can smooth and care the hair, improve the quality of frizzy hair and enable the beautiful hair to be smooth, bright, elegant and natural.
Detailed Description
The present invention is described in more detail below by way of specific embodiments.
Example 1
Rosemary amino acid shampoo comprises the following components in percentage by mass: water 72%, sodium laureth sulfate 7%, cocamidopropyl betaine 7%, disodium cocoyl glutamate 2%, sodium laureth sulfate 1.7%, dimethicone 1.8%, dimethiconol 1.6%, cocamide DEA 1.4%, cyclomethicone 1.6%, hydrolyzed keratin 0.8%, sodium chloride 0.3%, lauroyl collagen amino acid TEA salt 0.25%, glycine 0.2%, glutamic acid 0.15%, polyquaternium-60.3%, rosemary extract 0.5%, rosemary leaf extract 0.6%, lauryl pyridinium chloride 0.3%, guar hydroxypropyltrimonium chloride 0.2%, rosemary leaf oil 0.1%, hydroxyethyl diphosphate 0.05%, 1, 2-hexanediol 0.1%, caprylyl hydroxamic acid 0.05%.
Example 2
Rosemary amino acid shampoo comprises the following components in percentage by mass: water 74%, sodium laureth sulfate 7%, cocamidopropyl betaine 5%, disodium cocoyl glutamate 2%, sodium laureth sulfate 1.8%, dimethicone 1.5%, dimethiconol 1.5%, cocamide DEA 1.6%, cyclomethicone 1.5%, hydrolyzed keratin 0.8%, sodium chloride 0.5%, lauroyl collagen amino acid TEA salt 0.2%, glycine 0.1%, glutamic acid 0.05%, polyquaternium-60.6%, rosemary extract 0.6%, rosemary leaf extract 0.3%, lauryl pyridinium chloride 0.25%, guar hydroxypropyltrimonium chloride 0.15%, rosemary oil 0.15%, hydroxyethyl diphosphate 0.15%, 1, 2-hexanediol 0.1%, caprylyl hydroxamic acid 0.15%.
Example 3
Rosemary amino acid shampoo comprises the following components in percentage by mass: water 75%, sodium laureth sulfate 6%, cocamidopropyl betaine 6%, disodium cocoyl glutamate 1.8%, sodium laureth sulfate 1.6%, dimethicone 1.6%, dimethiconol 1.5%, cocamide DEA 1.5%, cyclomethicone 1.4%, hydrolyzed keratin 0.6%, sodium chloride 0.4%, lauroyl collagen amino acid TEA salt 0.2%, glycine 0.15%, glutamic acid 0.1%, polyquaternium-60.5%, rosemary extract 0.5%, rosemary leaf extract 0.5%, lauryl pyridinium chloride 0.2%, guar hydroxypropyltrimonium chloride 0.1%, rosemary leaf oil 0.1%, hydroxyethyl diphosphate 0.1%, 1, 2-hexanediol 0.05%, caprylyl hydroxamic acid 0.1%.
Example 4
Rosemary amino acid shampoo comprises the following components in percentage by mass: 78% of water, 5% of sodium laureth sulfate, 6% of cocamidopropyl betaine, 1.5% of disodium cocoyl glutamate, 1.5% of sodium laureth sulfate, 1.6% of polydimethylsiloxane, 1.2% of dimethiconol, 1.2% of cocamide DEA, 1.2% of cyclopolydimethylsiloxane, 0.4% of hydrolyzed keratin, 0.5% of sodium chloride, 0.15% of lauroyl collagen amino acid TEA, 0.15% of glycine, 0.05% of glutamic acid, 60.4% of polyquaternium, 0.3% of rosemary extract, 0.4% of rosemary leaf extract, 0.1% of laurylpyridinium chloride, 0.05% of guar hydroxypropyltrimonium chloride, 0.05% of rosemary leaf oil, 0.1% of hydroxyethyldiphosphonate, 0.05% of 1, 2-hexanediol, and 0.1% of caprylhydroxamic acid.
The preparation method of the rosemary amino acid shampoo in the embodiments 1 to 4 comprises the following steps:
(1) Weighing the components according to the formula ratio, cleaning and disinfecting production equipment;
(2) Sequentially adding water, sodium laureth sulfate, lauroyl collagen amino acid TEA salt, cocamidopropyl betaine, and disodium cocoyl glutamate into a stirring pot, heating to 85 deg.C, stirring for 3min for dissolving completely, and stirring at 800r/min for 40min to cool;
(3) Cooling to 60 deg.C, sequentially adding sodium lauryl sulfate, polydimethylsiloxane, cocamide DEA, cyclopolydimethylsiloxane, and guar gum hydroxypropyl trimethyl ammonium chloride, stirring at 500r/min for 30min to emulsify;
(4) Cooling to below 45 deg.C, sequentially adding dimethiconol, hydrolyzed keratin, sodium chloride, polyquaternium-6, herba Rosmarini officinalis extract, herba Rosmarini officinalis leaf extract, laurylpyridinium chloride, herba Rosmarini officinalis leaf oil, glycine, glutamic acid, hydroxyethyl diphosphate, 1, 2-hexanediol, and caprylyl hydroximic acid, stirring, and stirring at 500r/min for 30min to cool;
(5) When the temperature is reduced to below 40 ℃, sampling and inspecting;
(6) Taking out the shampoo from the pot and standing after the shampoo is qualified, thus obtaining the rosemary amino acid shampoo.
Comparative example 1
The shampoo of comparative example 1 contains components and a preparation method thereof referring to example 1, except that rosemary extract, rosemary leaf extract and rosemary leaf oil are not added, and the water content is 73.2% by mass.
Comparative example 2
The shampoo of comparative example 2 contains components and a preparation method thereof referring to example 2, except that glycine and glutamic acid are not added, and the water content by mass is 74.15%.
Comparative example 3
The shampoo of comparative example 3 contains the components and the preparation method thereof refer to example 3, except that disodium cocoyl glutamate is not added, and the water content is 76.8% by mass.
Determination of Using effects
In order to further test the actual effect of the rosemary amino acid shampoo provided by the invention, the inventor carries out further comparative tests.
Test samples: rosemary amino acid shampoos prepared in examples 1 to 4 of the present invention and shampoos prepared in comparative examples 1 to 3 of the present invention.
Test evaluation indexes are as follows: the shampoo has cleaning, dandruff removing, antipruritic, alopecia preventing, moisture keeping, and softening effects.
The test population is as follows: selecting 140 volunteers, wherein 126 female volunteers and 14 male volunteers; 14 pregnant women, 7 lactating women, 7 elderly people, and the rest are pregnant women, middle aged people or young people; divided into 7 groups of 20 persons each.
The test method comprises the following steps: the first group of test population used the rosemary amino acid shampoo prepared in example 1; the second group of test population used the rosemary amino acid shampoo prepared in example 2; the third group of test population used the rosemary amino acid shampoo prepared in example 3; the fourth group of test persons used the rosemary amino acid shampoo prepared in example 4; the shampoo prepared in comparative example 1 was used by a fifth group of test persons; the shampoo prepared in comparative example 1 was used by a sixth group of test persons; the shampoo prepared in comparative example 3 was used by a seventh group of test persons; and no other hair care products are used in the test period, and after the shampoo is continuously used for two times, the using effect of the shampoo is evaluated according to test evaluation indexes.
Counting the number of the tested volunteers in each group of the evaluation indexes, wherein the test evaluation results are shown in the following table:
as can be seen from the data in the above table, the use of the rosemary amino acid shampoos of examples 1 to 4 containing rosemary extract, rosemary leaf oil, glycine, glutamic acid, and disodium cocoyl glutamate all showed excellent cleansing effect, anti-dandruff antipruritic effect, anti-alopecia effect, and moisture retention and softness of hair.
After the shampoo of comparative example 1 which does not contain rosemary extract, rosemary leaf extract and rosemary leaf oil is used, the cleaning effect, the dandruff removing and itching relieving effect and the alopecia preventing effect are poor, and the moisture retention and the softness of hair are general; after the shampoo of the comparative example 2 which does not contain glycine and glutamic acid is used, the anti-hair loss effect, the moisture retention and the softness of hair are poor, and the cleaning effect and the anti-dandruff and itching-relieving effect are general; after the shampoo of comparative example 3, which does not contain the cocoyl disodium glutamate, is used, the cleaning effect is poor, the dandruff removing and itching relieving effects, the alopecia preventing effect and the moisture retention and the smoothness of hair are general.
The above-described embodiments are merely illustrative of the present invention and are not meant to be limiting, and any obvious modifications thereof which would occur to persons skilled in the art without departing from the spirit and scope of the invention are therefore considered to be within the appended claims.
Claims (8)
1. The rosemary amino acid shampoo is characterized by comprising the following components in percentage by mass: 72 to 78 percent of water, 5 to 7 percent of sodium laureth sulfate, 5 to 7 percent of cocamidopropyl betaine, 1.5 to 2.0 percent of disodium cocoyl glutamate, 1.5 to 1.8 percent of sodium laureth sulfate, 1.5 to 1.8 percent of polydimethylsiloxane, 1.2 to 1.6 percent of dimethiconol, 1.2 to 1.6 percent of cocamide DEA, 1.2 to 1.6 percent of cyclopolydimethylsiloxane, 0.4 to 0.8 percent of hydrolyzed keratin, 0.3 to 0.5 percent of sodium chloride, 0.15 to 0.25 percent of lauroyl collagen amino acid TEA, 0.1 to 0.2 percent of glycine, 0.05 to 0.15 percent of glutamic acid, 60.3 to 0.6 percent of polyquaternium, 0.3 to 0.6 percent of rosemary extract, 0.1 to 0.3 percent of lauryl pyridinium chloride, 0.05 to 0.20 percent of hydroxypropyl trimethyl ammonium chloride, 0.05 to 0.05 percent of rosemary oil, 0.05 to 0.15 percent of ethylene glycol, 0.05 to 0.15 percent of dioctyl ammonium chloride, 0.15 percent of dioctyl glycol and 0.15 percent of ethylene glycol.
2. The rosemary amino acid shampoo according to claim 1, comprising the following components in percentage by mass: water 75%, sodium laureth sulfate 6%, cocamidopropyl betaine 6%, disodium cocoyl glutamate 1.8%, sodium laureth sulfate 1.6%, dimethicone 1.6%, dimethiconol 1.5%, cocamide DEA 1.5%, cyclomethicone 1.4%, hydrolyzed keratin 0.6%, sodium chloride 0.4%, lauroyl collagen amino acid TEA salt 0.2%, glycine 0.15%, glutamic acid 0.1%, polyquaternium-60.5%, rosemary extract 0.5%, rosemary leaf extract 0.5%, lauryl pyridinium chloride 0.2%, guar hydroxypropyltrimonium chloride 0.1%, rosemary leaf oil 0.1%, hydroxyethyl diphosphate 0.1%, 1, 2-hexanediol 0.05%, caprylyl hydroxamic acid 0.1%.
3. Rosemary amino acid shampoo according to claim 1 or 2, wherein the sodium laureth sulfate is present at a concentration of 70% by weight.
4. Rosemary amino acid shampoo according to claim 1 or 2 wherein the mass concentration of cocamidopropyl betaine is 65%.
5. The rosemary amino acid shampoo of claim 1 or 2, wherein the rosemary amino acid shampoo has a pH of from 5.5 to 6.5.
6. A method for preparing rosemary amino acid shampoo as claimed in claim 1 or 2 comprising the steps of:
(1) Weighing the components according to the formula ratio, cleaning and disinfecting production equipment;
(2) Sequentially putting water, sodium laureth sulfate, lauroyl collagen amino acid TEA salt, cocamidopropyl betaine and disodium cocoyl glutamate into a stirring pot, heating to 85 ℃, stirring for 2-3 min to completely dissolve the sodium laureth sulfate, the lauroyl collagen amino acid TEA salt and the disodium cocoyl glutamate, and continuously stirring to cool the sodium laureth sulfate, the sodium cocoyl collagen amino acid TEA salt and the disodium cocoyl glutamate;
(3) Cooling to 55-65 ℃, sequentially adding sodium lauryl sulfate, polydimethylsiloxane, cocamide DEA, cyclopolydimethylsiloxane and guar gum hydroxypropyl trimethyl ammonium chloride, and stirring for 25-35 min until emulsification is uniform;
(4) Cooling to below 45 ℃, then sequentially adding dimethiconol, hydrolyzed keratin, sodium chloride, polyquaternium-6, rosemary extract, rosemary leaf extract, lauryl pyridinium chloride, rosemary leaf oil, glycine, glutamic acid, hydroxyethyl diphosphate, 1, 2-hexanediol and caprylyl hydroximic acid, uniformly stirring, and continuously stirring for 25-35 min to cool;
(5) When the temperature is reduced to below 40 ℃, sampling and inspecting;
(6) Taking the liquid out of the pot and standing after the liquid is qualified, thus obtaining the rosemary amino acid shampoo.
7. The method for preparing rosemary amino acid shampoo as claimed in claim 6, wherein in the step (2), the stirring speed is 750 to 850r/min, and the stirring time is 30 to 50min.
8. The method for preparing rosemary amino acid shampoo according to claim 6, wherein in the step (3) and the step (4), the stirring speed is 400-600 r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211019055.8A CN115364010B (en) | 2022-08-24 | 2022-08-24 | Rosemary amino acid shampoo and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211019055.8A CN115364010B (en) | 2022-08-24 | 2022-08-24 | Rosemary amino acid shampoo and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN115364010A true CN115364010A (en) | 2022-11-22 |
| CN115364010B CN115364010B (en) | 2024-01-26 |
Family
ID=84066826
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202211019055.8A Active CN115364010B (en) | 2022-08-24 | 2022-08-24 | Rosemary amino acid shampoo and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115364010B (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108670884A (en) * | 2018-08-18 | 2018-10-19 | 安徽国科生物科技有限公司 | A kind of hair follicle maintenance shampoo and preparation method thereof with the hair restoration factor |
| CN110025519A (en) * | 2019-04-18 | 2019-07-19 | 广州科恩生物技术有限公司 | A kind of amino acid shampoo that moisturizing is releived |
| KR20200139970A (en) * | 2019-06-05 | 2020-12-15 | 주식회사 피알앤 | Shampoo for preventing loss of hair andpromoting growth of hair and method for manufacturing the same |
| KR102192004B1 (en) * | 2019-06-24 | 2020-12-16 | 김영지 | Shampoo composition for preventing hair loss and improving state of hair |
| CN112206188A (en) * | 2020-09-23 | 2021-01-12 | 禹州森茂迷迭香生物科技有限公司 | Rosemary anti-hair loss shampoo and preparation method thereof |
| US20220105016A1 (en) * | 2019-02-04 | 2022-04-07 | Symrise Ag | Active agents for skin and hair care with physicochemical modifying properties |
-
2022
- 2022-08-24 CN CN202211019055.8A patent/CN115364010B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108670884A (en) * | 2018-08-18 | 2018-10-19 | 安徽国科生物科技有限公司 | A kind of hair follicle maintenance shampoo and preparation method thereof with the hair restoration factor |
| US20220105016A1 (en) * | 2019-02-04 | 2022-04-07 | Symrise Ag | Active agents for skin and hair care with physicochemical modifying properties |
| CN110025519A (en) * | 2019-04-18 | 2019-07-19 | 广州科恩生物技术有限公司 | A kind of amino acid shampoo that moisturizing is releived |
| KR20200139970A (en) * | 2019-06-05 | 2020-12-15 | 주식회사 피알앤 | Shampoo for preventing loss of hair andpromoting growth of hair and method for manufacturing the same |
| KR102192004B1 (en) * | 2019-06-24 | 2020-12-16 | 김영지 | Shampoo composition for preventing hair loss and improving state of hair |
| CN112206188A (en) * | 2020-09-23 | 2021-01-12 | 禹州森茂迷迭香生物科技有限公司 | Rosemary anti-hair loss shampoo and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN115364010B (en) | 2024-01-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109498494B (en) | Refreshing oil-control silicone-oil-free shampoo and preparation method thereof | |
| CN108078796B (en) | Silicone-oil-free moistening and smoothing hair mask and preparation method thereof | |
| KR20090120726A (en) | A shampoo composite and making method thereof | |
| CN113332191A (en) | Shampoo and preparation method thereof | |
| CN111329825A (en) | Ginger mild anti-dandruff shampoo and preparation method thereof | |
| CN107184406A (en) | One kind is planted extraction without anti-corrosion ginger without silicone oil shampoo and preparation method thereof | |
| CN115252495B (en) | Rosemary amino acid hair conditioner and preparation method thereof | |
| CN110638717A (en) | Softening composition and shampoo thereof | |
| CN112120980A (en) | Foundation-strengthening and vitality-reinforcing shampoo and preparation method thereof | |
| CN107233269A (en) | A kind of hair conditioner and preparation method thereof | |
| CN108703929A (en) | It is a kind of that there is the shampoo and preparation method thereof for nourishing scalp efficacy | |
| CN112807251A (en) | Silicone-oil-free shampoo with scalp care effect and preparation process thereof | |
| CN112999138A (en) | Plant dandruff-removing and itching-relieving composition, plant dandruff-removing and itching-relieving shampoo and preparation method thereof | |
| CN108721177A (en) | Camellia amino acid shampoo | |
| CN113876672A (en) | Amino acid mild tear-free natural plant shampoo and preparation method thereof | |
| JP4716476B2 (en) | Hair rinse | |
| CN106491456A (en) | A kind of scalp care compositions with anti-dandruff effect and its preparation method and application | |
| CN116135201A (en) | Washing and caring product for improving hair drying speed and fluffiness after washing and preparation method thereof | |
| CN115364010A (en) | Rosemary amino acid shampoo and preparation method thereof | |
| CN114366680A (en) | Shampoo composition for maintaining scalp health, preventing alopecia and strengthening hair and preparation method thereof | |
| CN108158921A (en) | A kind of plant composition comprising tea bran and rosemary and its preparation method and application | |
| CN114366693A (en) | Shampoo shower gel for infants and children | |
| CN114469760A (en) | Anti-hair loss composition, anti-hair loss washing and protecting product and preparation method thereof | |
| CN114306198A (en) | Bubble-formulation hair conditioner | |
| CN113559016A (en) | Amino acid shampoo capable of relieving and relieving itching for dry scalp |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |