CN115137678B - Pure natural osmanthus flower moisturizing cream and preparation method thereof - Google Patents
Pure natural osmanthus flower moisturizing cream and preparation method thereof Download PDFInfo
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- CN115137678B CN115137678B CN202210575126.6A CN202210575126A CN115137678B CN 115137678 B CN115137678 B CN 115137678B CN 202210575126 A CN202210575126 A CN 202210575126A CN 115137678 B CN115137678 B CN 115137678B
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- 230000003020 moisturizing effect Effects 0.000 title claims abstract description 105
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- 235000019082 Osmanthus Nutrition 0.000 title claims abstract description 19
- 241000333181 Osmanthus Species 0.000 title claims abstract description 19
- 239000006071 cream Substances 0.000 title claims description 44
- 239000000284 extract Substances 0.000 claims abstract description 154
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims abstract description 50
- 235000013871 bee wax Nutrition 0.000 claims abstract description 28
- 239000012166 beeswax Substances 0.000 claims abstract description 28
- 229930003427 Vitamin E Natural products 0.000 claims abstract description 25
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 25
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 25
- 235000006708 antioxidants Nutrition 0.000 claims abstract description 25
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims abstract description 25
- 235000019165 vitamin E Nutrition 0.000 claims abstract description 25
- 229940046009 vitamin E Drugs 0.000 claims abstract description 25
- 239000011709 vitamin E Substances 0.000 claims abstract description 25
- 239000002826 coolant Substances 0.000 claims abstract description 24
- 239000002994 raw material Substances 0.000 claims abstract description 21
- 229940092258 rosemary extract Drugs 0.000 claims abstract description 19
- 235000020748 rosemary extract Nutrition 0.000 claims abstract description 19
- 239000001233 rosmarinus officinalis l. extract Substances 0.000 claims abstract description 19
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 17
- 235000008390 olive oil Nutrition 0.000 claims abstract description 14
- 239000004006 olive oil Substances 0.000 claims abstract description 14
- 238000002156 mixing Methods 0.000 claims description 168
- 239000000706 filtrate Substances 0.000 claims description 122
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 120
- 235000007688 Lycopersicon esculentum Nutrition 0.000 claims description 61
- 240000003768 Solanum lycopersicum Species 0.000 claims description 61
- 241000220225 Malus Species 0.000 claims description 49
- 238000004140 cleaning Methods 0.000 claims description 32
- 238000001694 spray drying Methods 0.000 claims description 32
- 239000000463 material Substances 0.000 claims description 29
- 238000010438 heat treatment Methods 0.000 claims description 28
- 244000242564 Osmanthus fragrans Species 0.000 claims description 26
- 235000019083 Osmanthus fragrans Nutrition 0.000 claims description 26
- 238000002791 soaking Methods 0.000 claims description 26
- 244000178231 Rosmarinus officinalis Species 0.000 claims description 25
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- 238000003756 stirring Methods 0.000 claims description 22
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- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims description 18
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 claims description 18
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 claims description 18
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims description 18
- 229940116229 borneol Drugs 0.000 claims description 18
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 claims description 18
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 claims description 18
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- UAJTZZNRJCKXJN-UHFFFAOYSA-M sodium;2-dodecoxy-2-oxoethanesulfonate Chemical compound [Na+].CCCCCCCCCCCCOC(=O)CS([O-])(=O)=O UAJTZZNRJCKXJN-UHFFFAOYSA-M 0.000 claims description 16
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- 238000002844 melting Methods 0.000 claims description 9
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- 239000007766 cera flava Substances 0.000 claims description 8
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 6
- 235000021016 apples Nutrition 0.000 claims description 6
- 238000004821 distillation Methods 0.000 claims description 6
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- 235000006886 Zingiber officinale Nutrition 0.000 claims description 5
- 239000002671 adjuvant Substances 0.000 claims description 5
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- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 3
- 230000002349 favourable effect Effects 0.000 description 3
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 2
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- 230000000052 comparative effect Effects 0.000 description 2
- MGJZITXUQXWAKY-UHFFFAOYSA-N diphenyl-(2,4,6-trinitrophenyl)iminoazanium Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1N=[N+](C=1C=CC=CC=1)C1=CC=CC=C1 MGJZITXUQXWAKY-UHFFFAOYSA-N 0.000 description 2
- 230000001815 facial effect Effects 0.000 description 2
- 229940002713 osmanthus fragrans flower extract Drugs 0.000 description 2
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- SBQLYHNEIUGQKH-UHFFFAOYSA-N omeprazole Chemical compound N1=C2[CH]C(OC)=CC=C2N=C1S(=O)CC1=NC=C(C)C(OC)=C1C SBQLYHNEIUGQKH-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9771—Ginkgophyta, e.g. Ginkgoaceae [Ginkgo family]
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/522—Antioxidants; Radical scavengers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention discloses a purely natural osmanthus flower moisturizing paste and a preparation method thereof, and particularly relates to the technical field of moisturizing paste, wherein raw materials (in parts by weight) used by the moisturizing paste A comprise 40-60 parts of olive oil, 10-18 parts of beeswax, 10-30 parts of osmanthus flower extract, 2-5 parts of vitamin E, 2-10 parts of auxiliary agent and 2-10 parts of antioxidant, and raw materials (in parts by weight) used by the moisturizing paste B comprise 40-60 parts of olive oil, 10-18 parts of beeswax, 6-10 parts of osmanthus flower extract, 2-10 parts of rosemary extract, 1-8 parts of cooling agent and 2-5 parts of vitamin E. The invention has the effects of moistening skin, maintaining beauty and keeping young, is beneficial to skin absorption and pore shrinkage, and is suitable for various skin types.
Description
Technical Field
The invention relates to the technical field of moisturizing cream, in particular to a pure natural osmanthus moisturizing cream and a preparation method thereof.
Background
With the increasing pursuit of health and the rapid development of dermatology, attention is paid to skin care. The skin of a person is degraded from 14 years old, the metabolism of the skin is gradually slowed down after 24 years old, the stratum corneum is gradually accumulated and thickened, except that the skin condition is influenced by age, the skin health is influenced by environmental pollution, ultraviolet radiation, eating habits, sleeping time and improper maintenance modes, and the skin is problematic, so that the skin is an indispensable link in daily life, and various skin care products are layered endlessly.
Nourishing skin care products are used in daily skin care, wherein the main function and efficacy of the moisturizing cream are to provide enough nutrition for skin, moisturize skin and moisturize skin, and the efficacy of the current moisturizing cream on skin needs to be further improved.
Disclosure of Invention
The invention aims to provide a purely natural osmanthus flower moisturizing paste and a preparation method thereof, which have the effects of moisturizing skin and maintaining beauty and keeping young, are beneficial to skin absorption and pore shrinkage, and are suitable for various skin types.
In order to achieve the above object, the present invention provides the following technical solutions: the all-natural osmanthus fragrans moisturizing cream comprises, by weight, 40-60 parts of olive oil, 10-18 parts of beeswax, 10-30 parts of osmanthus fragrans extract, 2-5 parts of vitamin E, 2-10 parts of auxiliary agent and 2-10 parts of antioxidant, and B, wherein the raw materials (by weight) of the moisturizing cream comprise, by weight, 40-60 parts of olive oil, 10-18 parts of beeswax, 6-10 parts of osmanthus fragrans extract, 2-10 parts of rosemary extract, 1-8 parts of cooling agent and 2-5 parts of vitamin E.
Preferably, the auxiliary agent comprises herba Houttuyniae extract, folium Ginkgo extract, and rhizoma Zingiberis recens extract, and the ratio of herba Houttuyniae extract, folium Ginkgo extract, and rhizoma Zingiberis recens extract is 1:1:1.
preferably, the antioxidant comprises tomato extract and apple extract, and the ratio of tomato extract to apple extract is 1:1.
preferably, the cooling agent comprises menthol and borneol, and the ratio of menthol to borneol is 1:1.
the invention also comprises a method for preparing the pure natural osmanthus flower moisturizing paste, which comprises the following specific steps:
step one: preparing moisturizing cream A:
s1: the houttuynia cordata extract, the ginkgo leaf extract and the ginger extract are mixed according to the weight ratio of 1:1:1, uniformly mixing to obtain an auxiliary agent;
s2: tomato extract and apple extract were mixed according to 1: mixing uniformly in proportion to obtain an antioxidant;
s3: heating and melting Cera flava in the moistening cream A raw material in water bath at 80-90deg.C, mixing melted Cera flava, oleum Olivarum, flos Osmanthi Fragrantis extract, vitamins, adjuvants, and antioxidant, heating to 70-80deg.C in water bath, and stirring to obtain mixed solution;
s4: cooling the mixed solution obtained in the step S3 to 40-50 ℃, then adding vitamin E, uniformly stirring, pouring into a moisturizing paste box, and solidifying to obtain moisturizing paste A;
step two: preparing moisturizing cream B:
s5: menthol and borneol are mixed according to the weight ratio of 1: mixing at a ratio of 1 to obtain a cooling agent;
s6: heating and melting Cera flava in the moistening cream B material in water bath at 80-90deg.C, mixing the melted Cera flava, flos Osmanthi Fragrantis extract, herba Rosmarini officinalis extract and cooling agent, heating in water bath to 70-80deg.C, and stirring to obtain mixed solution;
s7: and (3) cooling the mixed solution obtained in the step (S6) to 40-50 ℃, then adding vitamin E, uniformly stirring, and pouring into another moisturizing paste box for solidification to obtain the moisturizing paste B.
Preferably, the preparation method of the osmanthus fragrans flower extract comprises the following steps: according to the mass ratio of 1:10 mixing flos Osmanthi Fragrantis with distilled water, heating to 30-40deg.C, soaking for 3-6 hr, transferring into a distillation tank, distilling with steam for 4-6 hr, standing the distillate at room temperature for layering, collecting oil layer, adding anhydrous sodium sulfate 5-10% of the oil layer into the oil layer, standing for drying for 8-10 hr, filtering, and collecting filtrate to obtain flos Osmanthi Fragrantis extract.
Preferably, the preparation method of the houttuynia cordata extract comprises the following steps: cleaning and cutting herba houttuyniae, soaking for 1-2h, and mixing the materials according to a mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2-4h, taking filtrate, and then mixing the materials according to the mass ratio of 1:7, mixing filter residues with water, decocting and extracting for 1-3h, taking filtrate, and then, according to the mass ratio of 1:5 mixing the filter residue with water, decocting for 0.5-2h, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain herba Houttuyniae extract.
Preferably, the preparation method of the ginkgo leaf extract comprises the following steps: cleaning and cutting ginkgo leaves, soaking for 1-2h, and mixing according to the mass ratio of 1:8 mixing rosemary with water, decocting and extracting for 2-4h, taking filtrate, and then mixing the materials according to the mass ratio of 1: mixing filter residues with water, decocting and extracting for 1-3h, taking filtrate, and then mixing the filtrate with water according to a mass ratio of 1: mixing the residue with water, decocting for 0.5-2 hr, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain folium Ginkgo extract.
Preferably, the ginger extract is prepared by the following steps: cleaning and cutting ginger, soaking for 1-2h, and mixing according to a mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2-4h, taking filtrate, and then mixing the materials according to the mass ratio of 1: 8. mixing filter residues with water, decocting and extracting for 1-3h, taking filtrate, and then mixing the filtrate with water according to a mass ratio of 1: mixing the filter residue with water, decocting for 0.5-2h, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain herba Houttuyniae extract.
Preferably, the tomato extract is prepared by the following steps: cleaning and crushing tomatoes to obtain tomato serum, wherein the mass ratio of the tomato serum to the tomato serum is 1: mixing tomato serum with water, extracting with ultrasonic wave with power of 60-80w for 5-10min, extracting with 40-50deg.C water bath for 30-50min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain tomato extract.
Preferably, the apple extract is prepared by the following steps: cleaning and crushing apples to obtain apple liquid according to the mass ratio of 1:8 mixing apple liquid with water, extracting with ultrasonic wave with power of 60-80w for 5-10min, extracting with 40-50deg.C water bath for 30-50min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain apple extract.
Preferably, the rosemary extract is prepared by the following steps: grinding rosemary into powder, soaking for 0.5-2h, and mixing according to the mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2-5h, taking filtrate, and then mixing the materials according to the mass ratio of 1:8 mixing the filter residue with water, decocting for 1-3h, collecting filtrate, mixing the two filtrates, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain herba Rosmarini officinalis extract.
In the technical scheme, the invention has the technical effects and advantages that:
1. when in use, the moisturizing cream A is firstly smeared, and the osmanthus fragrans flower extract in the moisturizing cream A has the effects of moisturizing skin and maintaining beauty and keeping young, and is suitable for various skin types such as oily skin, dry skin, mixed skin, sensitive skin and the like.
2. The osmanthus fragrans extract has a good antibacterial effect, is beneficial to prolonging the shelf life of the moisturizing cream, and is aromatic and fragrant and suitable for consumers to select.
3. The tomato extract and apple extract in the moisturizing paste A have antioxidant effect, are beneficial to reducing irritation and injury of free radicals to skin, reduce melanin generation and precipitation, prevent generation of color spots and freckles, and prevent growth of fine wrinkles.
4. The houttuynia cordata extract in the moisturizing paste A is beneficial to telangiectasis, the ginkgo leaf extract has the effects of activating blood circulation, dilating blood vessels and accelerating blood circulation, and the ginger extract has the effect of warming skin, is beneficial to opening skin pores, and is further beneficial to absorbing active ingredients of the moisturizing paste by the skin.
5. After the moisturizing paste A is smeared for 15-20 minutes, the moisturizing paste B is smeared, the rosemary extract in the moisturizing paste B is favorable for shrinking pores, menthol and borneol in the cooling agent are favorable for cooling skin, further favorable for shrinking pores and preventing the pores of the skin from being large.
Detailed Description
The present invention will be described in further detail below in order to enable those skilled in the art to better understand the technical solutions of the present invention.
Example 1
The invention provides a purely natural osmanthus fragrans moisturizing paste which comprises a moisturizing paste A and a moisturizing paste B, wherein raw materials (in parts by weight) used by the moisturizing paste A comprise 40 parts of olive oil, 10 parts of beeswax, 10 parts of osmanthus fragrans extract, 2 parts of vitamin E, 2 parts of auxiliary agent and 2 parts of antioxidant, and raw materials (in parts by weight) used by the moisturizing paste B comprise 40 parts of olive oil, 10 parts of beeswax, 6 parts of osmanthus fragrans extract, 2 parts of rosemary extract, 1 part of cooling agent and 2 parts of vitamin E.
The auxiliary agent comprises houttuynia cordata extract, ginkgo leaf extract and ginger extract, wherein the ratio of the houttuynia cordata extract to the ginkgo leaf extract to the ginger extract is 1:1:1.
the antioxidant comprises tomato extract and apple extract, wherein the ratio of the tomato extract to the apple extract is 1:1.
the cooling agent comprises menthol and borneol, wherein the proportion of the menthol to the borneol is 1:1.
the invention also provides a method for preparing the pure natural osmanthus flower moisturizing paste, which comprises the following specific steps:
step one: preparing moisturizing cream A:
s1: preparing herba Houttuyniae extract: cleaning and cutting cordate houttuynia, soaking for 1h, and mixing the materials according to the mass ratio of 1: 10. mixing rosemary with water, decocting and extracting for 2 hours, taking filtrate, and then mixing the filtrate with water according to a mass ratio of 1:7, mixing filter residues with water, decocting and extracting for 1h, taking filtrate, and then mixing the filtrate with water according to a mass ratio of 1:5 mixing the filter residues with water, decocting and extracting for 0.5h, collecting filtrate, combining the three filtrates, concentrating under reduced pressure to obtain thick paste, and spray drying to obtain herba Houttuyniae extract;
preparing ginkgo leaf extract: cleaning and cutting ginkgo leaves, soaking for 1h, and mixing according to the mass ratio of 1:8 mixing rosemary with water, decocting and extracting for 2 hours, taking filtrate, and then mixing the filtrate with water according to the mass ratio of 1: mixing filter residues with water, decocting and extracting for 1h, taking filtrate, and then mixing the filtrate with water according to the mass ratio of 1: mixing the filter residue with water, decocting for 0.5h, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain folium Ginkgo extract;
preparing ginger extract: cleaning and cutting ginger, soaking for 1h, and mixing the raw materials according to the mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2 hours, taking filtrate, and then mixing the materials according to the mass ratio of 1:8, mixing filter residues with water, decocting and extracting for 1h, taking filtrate, and then mixing the filtrate with water according to a mass ratio of 1: mixing the filter residue with water, decocting for 0.5h, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain herba Houttuyniae extract;
the houttuynia cordata extract, the ginkgo leaf extract and the ginger extract are mixed according to the weight ratio of 1:1:1, uniformly mixing to obtain an auxiliary agent;
s2: preparation of tomato extract: cleaning and crushing tomatoes to obtain tomato serum, wherein the mass ratio of the tomato serum to the tomato serum is 1: mixing tomato serum with water, extracting with ultrasonic wave with power of 60w for 5min, extracting with 40deg.C water bath for 30min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain tomato extract;
preparing apple extract: cleaning and crushing apples to obtain apple liquid according to the mass ratio of 1:8, mixing apple liquid with water, extracting with ultrasonic wave assistance with power of 60w for 5min, extracting with water bath at 40deg.C for 30min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain apple extract;
tomato extract and apple extract were mixed according to 1: mixing uniformly in proportion to obtain an antioxidant;
s3: heating and melting beeswax in the moistening cream A raw material in water bath at 80deg.C, mixing melted beeswax, oleum Olivarum, flos Osmanthi Fragrantis extract, vitamins, adjuvants, and antioxidant, heating in water bath to 70deg.C, and stirring to obtain mixed solution;
the preparation method of the osmanthus fragrans extract comprises the following steps: according to the mass ratio of 1:10 mixing flos Osmanthi Fragrantis with distilled water, heating to 30deg.C, soaking for 3 hr, transferring into a distillation tank, distilling with steam for 4 hr, standing the distillate at room temperature for layering, collecting oil layer, adding anhydrous sodium sulfate 5% of the oil layer into the oil layer, standing for drying for 8 hr, filtering, and collecting filtrate to obtain flos Osmanthi Fragrantis extract;
s4: cooling the mixed solution obtained in the step S3 to 40 ℃, then adding vitamin E, uniformly stirring, pouring into a moisturizing paste box, and solidifying to obtain moisturizing paste A;
step two: preparing moisturizing cream B:
s5: menthol and borneol are mixed according to the weight ratio of 1: mixing at a ratio of 1 to obtain a cooling agent;
s6: heating and melting beeswax in the raw material of the moistening cream B in water bath at 80 ℃, mixing the melted beeswax, the sweet osmanthus extract, the rosemary extract and the cooling agent, heating in water bath to 70 ℃, and uniformly stirring to obtain a mixed solution;
the preparation method of the rosemary extract comprises the following steps: grinding rosemary into powder, soaking for 0.5h, and mixing the materials according to the mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2 hours, taking filtrate, and then mixing the materials according to the mass ratio of 1:8, mixing filter residues with water, decocting and extracting for 1h, mixing the two filtrates, concentrating the filtrate under reduced pressure to obtain thick paste, and spray-drying to obtain rosemary extract;
s7: and (3) cooling the mixed solution in the step (S6) to 40 ℃, then adding vitamin E, uniformly stirring, and pouring into another moisturizing paste box for solidification to obtain moisturizing paste B.
Example 2
The invention provides a purely natural osmanthus fragrans moisturizing paste which comprises a moisturizing paste A and a moisturizing paste B, wherein raw materials (in parts by weight) used by the moisturizing paste A comprise 50 parts of olive oil, 16 parts of beeswax, 20 parts of osmanthus fragrans extract, 3 parts of vitamin E, 6 parts of auxiliary agent and 6 parts of antioxidant, and raw materials (in parts by weight) used by the moisturizing paste B comprise 50 parts of olive oil, 16 parts of beeswax, 8 parts of osmanthus fragrans extract, 6 parts of rosemary extract, 5 parts of cooling agent and 3 parts of vitamin E.
The auxiliary agent comprises houttuynia cordata extract, ginkgo leaf extract and ginger extract, wherein the ratio of the houttuynia cordata extract to the ginkgo leaf extract to the ginger extract is 1:1:1.
the antioxidant comprises tomato extract and apple extract, wherein the ratio of the tomato extract to the apple extract is 1:1.
the cooling agent comprises menthol and borneol, wherein the proportion of the menthol to the borneol is 1:1.
the invention also provides a method for preparing the pure natural osmanthus flower moisturizing paste, which comprises the following specific steps:
step one: preparing moisturizing cream A:
s1: preparing herba Houttuyniae extract: cleaning and cutting cordate houttuynia, soaking for 1.5 hours, and mixing the materials according to the mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 3 hours, taking filtrate, and then mixing the materials according to the mass ratio of 1:7, mixing filter residues with water, decocting and extracting for 2 hours, taking filtrate, and then, according to the mass ratio of 1: mixing the filter residue with water, decocting for 1h, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain herba Houttuyniae extract;
preparing ginkgo leaf extract: cleaning and cutting ginkgo leaves, soaking for 1.5 hours, and mixing according to the mass ratio of 1:8 mixing rosemary with water, decocting and extracting for 3 hours, taking filtrate, and then mixing the materials according to the mass ratio of 1: mixing filter residues with water, decocting and extracting for 2 hours, taking filtrate, and then mixing the filtrate with water according to a mass ratio of 1: mixing the filter residue with water, decocting for 1h, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain folium Ginkgo extract;
preparing ginger extract: cleaning and cutting ginger, soaking for 1.5h, and mixing according to the mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 3 hours, taking filtrate, and then mixing the materials according to the mass ratio of 1:8, mixing filter residues with water, decocting and extracting for 2 hours, taking filtrate, and then mixing the filtrate with water according to a mass ratio of 1: mixing the filter residue with water, decocting for 1h, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain herba Houttuyniae extract;
the houttuynia cordata extract, the ginkgo leaf extract and the ginger extract are mixed according to the weight ratio of 1:1:1, uniformly mixing to obtain an auxiliary agent;
s2: preparation of tomato extract: cleaning and crushing tomatoes to obtain tomato serum, wherein the mass ratio of the tomato serum to the tomato serum is 1: mixing tomato serum with water, extracting with ultrasonic wave with power of 70w for 8min, extracting with 45deg.C water bath for 40min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain tomato extract;
preparing apple extract: cleaning and crushing apples to obtain apple liquid according to the mass ratio of 1:8, mixing apple liquid with water, extracting with ultrasonic wave assistance with the power of 70w for 8min, extracting with water bath at 45deg.C for 40min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain apple extract;
tomato extract and apple extract were mixed according to 1: mixing uniformly in proportion to obtain an antioxidant;
s3: heating beeswax in the moistening cream A material in water bath at 85deg.C to melt, mixing melted beeswax, oleum Olivarum, flos Osmanthi Fragrantis extract, vitamins, adjuvants, and antioxidant, heating to 75deg.C in water bath, and stirring to obtain mixed solution;
the preparation method of the osmanthus fragrans extract comprises the following steps: according to the mass ratio of 1:10 mixing flos Osmanthi Fragrantis with distilled water, heating to 35deg.C, soaking for 5 hr, transferring into a distillation tank, distilling with steam for 5 hr, standing the distillate at room temperature for layering, collecting oil layer, adding anhydrous sodium sulfate 8% of the oil layer into the oil layer, standing for drying for 9 hr, filtering, and collecting filtrate to obtain flos Osmanthi Fragrantis extract;
s4: cooling the mixed solution obtained in the step S3 to 45 ℃, then adding vitamin E, uniformly stirring, and pouring into a moisturizing paste box to be coagulated to obtain moisturizing paste A;
step two: preparing moisturizing cream B:
s5: menthol and borneol are mixed according to the weight ratio of 1: mixing at a ratio of 1 to obtain a cooling agent;
s6: heating and melting beeswax in the raw material of the moistening cream B in water bath at 85 ℃, mixing the melted beeswax, the sweet osmanthus extract, the rosemary extract and the cooling agent, heating in water bath to 75 ℃, and uniformly stirring to obtain a mixed solution;
the preparation method of the rosemary extract comprises the following steps: grinding rosemary into powder, soaking for 1h, and mixing the materials according to the mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2.5h, taking filtrate, and then mixing the materials according to the mass ratio of 1:8, mixing filter residues with water, decocting and extracting for 2 hours, taking filtrate, combining the two filtrates, concentrating the filtrate under reduced pressure to obtain thick paste, and spray-drying to obtain rosemary extract;
s7: and (3) cooling the mixed solution in the step (S6) to 45 ℃, then adding vitamin E, uniformly stirring, and pouring into another moisturizing paste box for solidification to obtain moisturizing paste B.
Example 3
The invention provides a purely natural osmanthus fragrans moisturizing paste which comprises a moisturizing paste A and a moisturizing paste B, wherein raw materials (in parts by weight) used by the moisturizing paste A comprise 60 parts of olive oil, 18 parts of beeswax, 30 parts of osmanthus fragrans extract, 5 parts of vitamin E, 10 parts of auxiliary agent and 10 parts of antioxidant, and raw materials (in parts by weight) used by the moisturizing paste B comprise 60 parts of olive oil, 18 parts of beeswax, 10 parts of osmanthus fragrans extract, 10 parts of rosemary extract, 8 parts of cooling agent and 5 parts of vitamin E.
The auxiliary agent comprises houttuynia cordata extract, ginkgo leaf extract and ginger extract, wherein the ratio of the houttuynia cordata extract to the ginkgo leaf extract to the ginger extract is 1:1:1.
the antioxidant comprises tomato extract and apple extract, wherein the ratio of the tomato extract to the apple extract is 1:1.
the cooling agent comprises menthol and borneol, wherein the proportion of the menthol to the borneol is 1:1.
the invention also provides a method for preparing the pure natural osmanthus flower moisturizing paste, which comprises the following specific steps:
step one: preparing moisturizing cream A:
s1: preparing herba Houttuyniae extract: cleaning and cutting cordate houttuynia, soaking for 2 hours, and mixing the materials according to the mass ratio of 1: 10. mixing rosemary with water, decocting and extracting for 4 hours, taking filtrate, and then mixing the filtrate with water according to a mass ratio of 1:7, mixing filter residues with water, decocting and extracting for 3 hours, taking filtrate, and then, according to the mass ratio of 1: mixing the filter residue with water, decocting for 2h, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain herba Houttuyniae extract;
preparing ginkgo leaf extract: cleaning and cutting ginkgo leaves, soaking for 2 hours, and mixing the materials according to the mass ratio of 1:8 mixing rosemary with water, decocting and extracting for 4 hours, taking filtrate, and then mixing the materials according to the mass ratio of 1: mixing filter residues with water, decocting and extracting for 3 hours, taking filtrate, and then mixing the filtrate with water according to a mass ratio of 1: mixing the filter residue with water, decocting for 2h, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain folium Ginkgo extract;
preparing ginger extract: cleaning and cutting ginger, soaking for 2 hours, and mixing the raw materials according to the mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 4 hours, taking filtrate, and then mixing the materials according to the mass ratio of 1:8, mixing filter residues with water, decocting and extracting for 3 hours, taking filtrate, and then, according to the mass ratio of 1: mixing the filter residue with water, decocting for 2h, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain herba Houttuyniae extract;
the houttuynia cordata extract, the ginkgo leaf extract and the ginger extract are mixed according to the weight ratio of 1:1:1, uniformly mixing to obtain an auxiliary agent;
s2: preparation of tomato extract: cleaning and crushing tomatoes to obtain tomato serum, wherein the mass ratio of the tomato serum to the tomato serum is 1: mixing tomato serum with water, extracting with ultrasonic wave assistance with power of 80w for 10min, extracting with 50deg.C water bath for 50min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain tomato extract;
preparing apple extract: cleaning and crushing apples to obtain apple liquid according to the mass ratio of 1:8, mixing apple liquid with water, extracting with ultrasonic wave assistance with power of 80w for 10min, extracting with 50deg.C water bath for 50min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain apple extract;
tomato extract and apple extract were mixed according to 1: mixing uniformly in proportion to obtain an antioxidant;
s3: heating and melting beeswax in the moistening cream A raw material in water bath at 90deg.C, mixing melted beeswax, oleum Olivarum, flos Osmanthi Fragrantis extract, vitamins, adjuvants, and antioxidant, heating in water bath to 80deg.C, and stirring to obtain mixed solution;
the preparation method of the osmanthus fragrans extract comprises the following steps: according to the mass ratio of 1:10 mixing flos Osmanthi Fragrantis with distilled water, heating to 40deg.C, soaking for 6 hr, transferring into a distillation tank, distilling with steam for 6 hr, standing the distillate at room temperature for layering, collecting oil layer, adding anhydrous sodium sulfate 10% of the oil layer into the oil layer, standing for drying for 10 hr, filtering, and collecting filtrate to obtain flos Osmanthi Fragrantis extract;
s4: cooling the mixed solution obtained in the step S3 to 50 ℃, then adding vitamin E, uniformly stirring, pouring into a moisturizing paste box, and solidifying to obtain moisturizing paste A;
step two: preparing moisturizing cream B:
s5: menthol and borneol are mixed according to the weight ratio of 1: mixing at a ratio of 1 to obtain a cooling agent;
s6: heating and melting beeswax in the raw material of the moistening cream B in water bath at 90 ℃, mixing the melted beeswax, the sweet osmanthus extract, the rosemary extract and the cooling agent, heating in water bath to 80 ℃, and uniformly stirring to obtain a mixed solution;
the preparation method of the rosemary extract comprises the following steps: grinding rosemary into powder, soaking for 2 hours, and mixing the materials according to the mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 5 hours, taking filtrate, and then mixing the materials according to the mass ratio of 1:8, mixing filter residues with water, decocting and extracting for 3 hours, taking filtrate, combining the two filtrates, concentrating the filtrate under reduced pressure to obtain thick paste, and spray-drying to obtain rosemary extract;
s7: and (3) cooling the mixed solution in the step (S6) to 50 ℃, then adding vitamin E, uniformly stirring, and pouring into another moisturizing paste box for solidification to obtain moisturizing paste B.
Comparative example
The invention provides a purely natural osmanthus fragrans moisturizing paste which comprises a moisturizing paste A and a moisturizing paste B, wherein raw materials (in parts by weight) used by the moisturizing paste A comprise 60 parts of olive oil, 18 parts of beeswax, 30 parts of osmanthus fragrans extract, 5 parts of vitamin E and 10 parts of antioxidant, and raw materials (in parts by weight) used by the moisturizing paste B comprise 60 parts of olive oil, 18 parts of beeswax, 10 parts of rosemary extract, 8 parts of cooling agent and 5 parts of vitamin E.
The antioxidant comprises tomato extract and apple extract, wherein the ratio of the tomato extract to the apple extract is 1:1.
the cooling agent comprises menthol and borneol, wherein the proportion of the menthol to the borneol is 1:1.
the method for preparing the purely natural osmanthus flower moisturizing paste is the same as that of the example 3.
Step one: preparing moisturizing cream A:
s1: preparation of tomato extract: cleaning and crushing tomatoes to obtain tomato serum, wherein the mass ratio of the tomato serum to the tomato serum is 1: mixing tomato serum with water, extracting with ultrasonic wave assistance with power of 80w for 10min, extracting with 50deg.C water bath for 50min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain tomato extract;
preparing apple extract: cleaning and crushing apples to obtain apple liquid according to the mass ratio of 1:8, mixing apple liquid with water, extracting with ultrasonic wave assistance with power of 80w for 10min, extracting with 50deg.C water bath for 50min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain apple extract;
tomato extract and apple extract were mixed according to 1: mixing uniformly in proportion to obtain an antioxidant;
s2: heating beeswax in the raw material of the moistening cream A in water bath at 90 ℃ to melt, then mixing the melted beeswax, olive oil, osmanthus fragrans extract, vitamins and antioxidants, heating in water bath to 80 ℃, and uniformly stirring to obtain a mixed solution;
the preparation method of the osmanthus fragrans extract comprises the following steps: according to the mass ratio of 1:10 mixing flos Osmanthi Fragrantis with distilled water, heating to 40deg.C, soaking for 6 hr, transferring into a distillation tank, distilling with steam for 6 hr, standing the distillate at room temperature for layering, collecting oil layer, adding anhydrous sodium sulfate 10% of the oil layer into the oil layer, standing for drying for 10 hr, filtering, and collecting filtrate to obtain flos Osmanthi Fragrantis extract;
s3: cooling the mixed solution obtained in the step S1 to 50 ℃, then adding vitamin E, uniformly stirring, pouring into a moisturizing paste box, and solidifying to obtain moisturizing paste A;
1. skin care experiment:
experiment group 1: selecting 4 women between 25-35 years old, wherein women 1-4 are oily skin, dry skin, mixed skin and sensitive skin respectively, and the 4 women face skin has fine lines and large pores, smearing the moisturizing paste A of the example 1 after cleaning the face in the morning and evening for 20 minutes, smearing the moisturizing paste B, and continuously using for one month;
experiment group 2: selecting 4 women between 25-35 years old, wherein the women 1-4 are oily skin, dry skin, mixed skin and sensitive skin respectively, and the 4 women face skin has the problems of fine lines and large pores, smearing the moisturizing paste A of the example 2 after cleaning the face in the morning and evening for 20 minutes, smearing the moisturizing paste B, and continuously using for one month;
experiment group 3: selecting 4 women between 25-35 years old, wherein the women 1-4 are oily skin, dry skin, mixed skin and sensitive skin respectively, and the 4 women face skin has the problems of fine lines and large pores, smearing the moisturizing paste A of the example 3 after cleaning the face in the morning and evening for 20 minutes, smearing the moisturizing paste B, and continuously using for one month;
control group 1: selecting 4 women between 25-35 years old, wherein the women 1-4 are oily skin, dry skin, mixed skin and sensitive skin respectively, and the 4 women face skin has the problems of fine lines and large pores, smearing the moisturizing paste A of the comparative example after cleaning the face in the morning and evening for 20 minutes, smearing the moisturizing paste B, and continuously using for one month;
control group 2: selecting 4 women between 25-35 years old, wherein the women 1-4 are oily skin, dry skin, mixed skin and sensitive skin respectively, and the 4 women face skin has the problems of fine lines and large pores, and smearing basic moisturizing cream purchased in the market after cleaning the face in the morning and evening, and continuously using for one month;
women in experimental group 1-3 and control group 1-2 were subjected to facial skin test before use, and were subjected to facial skin test again after one month of use:
the test instrument is selected from: VISA digital skin analyzer, omeprazole Y-B2006 skin moisture tester;
the evaluation grades are:
stage 1: the improvement degree of the test result is more than 50% compared with the test result before the test;
2 stages: the improvement degree of the test result is 20-50% compared with the improvement degree before the test;
3 stages: the improvement degree of the test result is 10-20% compared with the test result before the test;
4 stages: the improvement degree of the test result is 0-10% compared with the test result before the test;
5 stages: the test results were not improved at all compared to before the test;
the rating results are shown in Table 1:
TABLE 1
As can be seen from comparison of the experimental groups 1-3 and the control group 2, the moisturizing cream is beneficial to improving the problems of fine lines and large pores, improving the skin fineness, having the effect of beautifying, and being suitable for various skin types;
as can be seen from comparison of the experimental group 3 and the control group 1, the auxiliary agent added by the invention is beneficial to the skin to absorb the effective components of the moisturizing cream, and the use effect is improved.
2. And (3) measuring oxidation resistance:
a solution of DPPH at a concentration of 0.04mg/ml was prepared with 95% ethanol, and 1ml of the moisturizing cream A of examples 1 to 3 was taken as samples 1 to 3, respectively.
1ml of the sample and 3ml of DPPH solution were removed and placed in a test tube, and after thoroughly mixing, the mixture was allowed to stand at room temperature for 30 minutes in a dark place, and then the absorbance A1 was measured at 517 nm. The absorbance A0 was measured by using 1ml of ethanol instead of the sample solution as a blank, and the absorbance A2 was measured by using 3ml of ethanol instead of the DPPH solution. The calculation formula of the clearance rate of DPPH free radical is as follows:
DPPH radical clearance = (1- (A1-A2)/A0) ×100%;
the experimental results are shown in table 2:
TABLE 2
| DPPH radical scavenging Rate (%) | |
| Example 1 | 66.76 |
| Example 2 | 67.56 |
| Example 3 | 88.32 |
The data in the table show that the moisturizing cream has a certain scavenging ability to hydroxyl free radicals, and the effect is correspondingly enhanced along with the increase of the usage amount, so that the moisturizing cream has a stronger antioxidation ability.
3. And (3) antibacterial effect measurement:
the respective cases 1 to 3 were taken100 g of each of the cream A and the cream B, and then adding a bacterial liquid containing mould, wherein the mould content in each g of sample is 1 multiplied by 10 6 CFU/g, then placed at 25℃and sampled and analyzed after 30 days, the mold content in the samples was 0. The moisturizing cream disclosed by the invention is free from other preservatives, purely natural in components, safe and nontoxic.
While certain exemplary embodiments of the present invention have been described above by way of illustration only, it will be apparent to those of ordinary skill in the art that modifications may be made to the described embodiments in various different ways without departing from the spirit and scope of the invention. Accordingly, the foregoing description is illustrative in nature and is not to be construed as limiting the scope of the invention as claimed.
Claims (7)
1. A pure natural osmanthus flower moisturizing cream is characterized in that: the moisturizing cream comprises, by weight, 40-60 parts of olive oil, 10-18 parts of beeswax, 10-30 parts of sweet osmanthus extract, 2-5 parts of vitamin E, 2-10 parts of auxiliary agent and 2-10 parts of antioxidant, and 10-18 parts of beeswax, 6-10 parts of sweet osmanthus extract, 2-10 parts of rosemary extract, 1-8 parts of cooling agent and 2-5 parts of vitamin E;
the auxiliary agent comprises houttuynia cordata extract, ginkgo leaf extract and ginger extract, wherein the ratio of the houttuynia cordata extract to the ginkgo leaf extract to the ginger extract is 1:1:1, a step of;
the antioxidant comprises tomato extract and apple extract, wherein the ratio of the tomato extract to the apple extract is 1:1, a step of;
the cooling agent comprises menthol and borneol, wherein the proportion of the menthol to the borneol is 1:1.
2. a method for preparing the purely natural osmanthus flower moisturizing paste of claim 1, which is characterized in that: the method comprises the following specific steps:
step one: preparing moisturizing cream A:
s1: the houttuynia cordata extract, the ginkgo leaf extract and the ginger extract are mixed according to the weight ratio of 1:1:1, uniformly mixing to obtain an auxiliary agent;
s2: tomato extract and apple extract were mixed according to 1: mixing uniformly in proportion to obtain an antioxidant;
s3: heating and melting Cera flava in the moistening cream A raw material in water bath at 80-90deg.C, mixing melted Cera flava, oleum Olivarum, flos Osmanthi Fragrantis extract, adjuvants, and antioxidant, heating in water bath to 70-80deg.C, and stirring to obtain mixed solution;
s4: cooling the mixed solution obtained in the step S3 to 40-50 ℃, then adding vitamin E, uniformly stirring, pouring into a moisturizing paste box, and solidifying to obtain moisturizing paste A;
step two: preparing moisturizing cream B:
s5: menthol and borneol are mixed according to the weight ratio of 1: mixing at a ratio of 1 to obtain a cooling agent;
s6: heating and melting Cera flava in the moistening cream B material in water bath at 80-90deg.C, mixing melted Cera flava, oleum Olivarum, flos Osmanthi Fragrantis extract, herba Rosmarini officinalis extract and cooling agent, heating in water bath to 70-80deg.C, and stirring to obtain mixed solution;
s7: and (3) cooling the mixed solution obtained in the step (S6) to 40-50 ℃, then adding vitamin E, uniformly stirring, and pouring into another moisturizing paste box for solidification to obtain the moisturizing paste B.
3. The method for preparing the purely natural osmanthus flower moisturizing paste according to claim 2, wherein the method is characterized by comprising the following steps of: the preparation method of the osmanthus fragrans extract comprises the following steps: according to the mass ratio of 1:10 mixing flos Osmanthi Fragrantis with distilled water, heating to 30-40deg.C, soaking for 3-6 hr, transferring into a distillation tank, distilling with steam for 4-6 hr, standing the distillate at room temperature for layering, collecting oil layer, adding anhydrous sodium sulfate 5-10% of the oil layer into the oil layer, standing for drying for 8-10 hr, filtering, and collecting filtrate to obtain flos Osmanthi Fragrantis extract.
4. The method for preparing the purely natural osmanthus flower moisturizing paste according to claim 2, wherein the method is characterized by comprising the following steps of: the preparation method of the houttuynia cordata extract comprises the following steps: cleaning and cutting herba houttuyniae, soaking for 1-2h, and mixing the materials according to a mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2-4h, taking filtrate, and then mixing the materials according to the mass ratio of 1:7, mixing filter residues with water, decocting and extracting for 1-3h, taking filtrate, and then, according to the mass ratio of 1: mixing the filter residue with water, decocting for 0.5-2h, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain herba Houttuyniae extract;
the preparation method of the ginkgo leaf extract comprises the following steps: cleaning and cutting ginkgo leaves, soaking for 1-2h, and mixing according to the mass ratio of 1:8 mixing rosemary with water, decocting and extracting for 2-4h, taking filtrate, and then mixing the materials according to the mass ratio of 1: mixing filter residues with water, decocting and extracting for 1-3h, taking filtrate, and then mixing the filtrate with water according to a mass ratio of 1: mixing the filter residue with water, decocting for 0.5-2 hr, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain folium Ginkgo extract;
the preparation method of the ginger extract comprises the following steps: cleaning and cutting ginger, soaking for 1-2h, and mixing according to a mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2-4h, taking filtrate, and then mixing the materials according to the mass ratio of 1:8, mixing filter residues with water, decocting and extracting for 1-3h, taking filtrate, and then mixing the filtrate with water according to a mass ratio of 1: mixing the filter residue with water, decocting for 0.5-2 hr, collecting filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain rhizoma Zingiberis recens extract.
5. The method for preparing the purely natural osmanthus flower moisturizing paste according to claim 2, wherein the method is characterized by comprising the following steps of: the preparation method of the tomato extract comprises the following steps: cleaning and crushing tomatoes to obtain tomato serum, wherein the mass ratio of the tomato serum to the tomato serum is 1: mixing tomato serum with water, extracting with ultrasonic wave with power of 60-80w for 5-10min, extracting with 40-50deg.C water bath for 30-50min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain tomato extract.
6. The method for preparing the purely natural osmanthus flower moisturizing paste according to claim 2, wherein the method is characterized by comprising the following steps of: the preparation method of the apple extract comprises the following steps: cleaning and crushing apples to obtain apple liquid according to the mass ratio of 1:8 mixing apple liquid with water, extracting with ultrasonic wave with power of 60-80w for 5-10min, extracting with 40-50deg.C water bath for 30-50min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain apple extract.
7. The method for preparing the purely natural osmanthus flower moisturizing paste according to claim 2, wherein the method is characterized by comprising the following steps of: the preparation method of the rosemary extract comprises the following steps: grinding rosemary into powder, soaking for 0.5-2h, and mixing according to the mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2-5h, taking filtrate, and then mixing the materials according to the mass ratio of 1:8 mixing the filter residue with water, decocting for 1-3h, collecting filtrate, mixing the two filtrates, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain herba Rosmarini officinalis extract.
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| JP2014114235A (en) * | 2012-12-10 | 2014-06-26 | Maruzen Pharmaceut Co Ltd | Melanogenesis inhibitor and collagen production promoter |
| CN104146913A (en) * | 2014-08-20 | 2014-11-19 | 陕西知医堂药业有限公司 | Lithospermum paste and preparation method thereof |
| CN107982114A (en) * | 2016-10-25 | 2018-05-04 | 赖婷婷 | A kind of sweet osmanthus hand lotion and preparation method thereof |
| CN107998017A (en) * | 2017-12-11 | 2018-05-08 | 广州赛莱拉干细胞科技股份有限公司 | A kind of anti-wrinkle containing Flos Osmanthi Fragrantis extract, cosmetic composition and preparation method thereof |
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|---|---|---|---|---|
| JP2014114235A (en) * | 2012-12-10 | 2014-06-26 | Maruzen Pharmaceut Co Ltd | Melanogenesis inhibitor and collagen production promoter |
| CN104146913A (en) * | 2014-08-20 | 2014-11-19 | 陕西知医堂药业有限公司 | Lithospermum paste and preparation method thereof |
| CN107982114A (en) * | 2016-10-25 | 2018-05-04 | 赖婷婷 | A kind of sweet osmanthus hand lotion and preparation method thereof |
| CN107998017A (en) * | 2017-12-11 | 2018-05-08 | 广州赛莱拉干细胞科技股份有限公司 | A kind of anti-wrinkle containing Flos Osmanthi Fragrantis extract, cosmetic composition and preparation method thereof |
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Denomination of invention: A pure natural osmanthus moisturizing cream and its preparation method Granted publication date: 20231024 Pledgee: Bank of China Limited by Share Ltd. Guilin branch Pledgor: GUILIN FOUR SEASON SUNSHINE F&F Co.,Ltd. Registration number: Y2024450000002 |