CN107998017A - A kind of anti-wrinkle containing Flos Osmanthi Fragrantis extract, cosmetic composition and preparation method thereof - Google Patents
A kind of anti-wrinkle containing Flos Osmanthi Fragrantis extract, cosmetic composition and preparation method thereof Download PDFInfo
- Publication number
- CN107998017A CN107998017A CN201711336354.3A CN201711336354A CN107998017A CN 107998017 A CN107998017 A CN 107998017A CN 201711336354 A CN201711336354 A CN 201711336354A CN 107998017 A CN107998017 A CN 107998017A
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- Prior art keywords
- wrinkle
- cosmetic composition
- extract
- parts
- skin
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The present invention provides a kind of anti-wrinkle containing Flos Osmanthi Fragrantis extract, cosmetic composition, include the component of following parts by weight：10 20 parts of Flos Osmanthi Fragrantis extract, 5 10 parts of duckbilled flower extract, 10 20 parts of white willow bark extract.Said composition can not only substantially reduce skin roughness, reach anti-wrinkle effect, also with preferable skin lightening result, and it is safe and non-stimulating.
Description
Technical field
The present invention relates to a kind of anti-wrinkle containing Flos Osmanthi Fragrantis extract, cosmetic composition and preparation method thereof.
Background technology
Wrinkle and pigmentation are avoiding greatly in the primary outer feature of skin aging, and numerous woman eye.The skin of people
Skin was put into ageing state from 25 years old or so：Lipid is also reduced between sebum secretion amount and horn cell, in percutaneous moisture loss
Rise；Epidermal cell differentiation capability reduces, and cuticula is thinning, and atrophy of epidermis produces fine wrinkle.Corium produces insoluble collagen, elasticity
Reduce, hyaluronic acid also increases and reduces with the age, causes corium moisture content to reduce, and produces deeper wrinkle.
Furthermore under ultraviolet irradiation, active oxygen and lipid peroxide are produced in skin, lipid peroxide is made in oxidizing ferment
The materials such as malonaldehyde are resolved under, with albumen qualitative response, form brown plain spot, chromogenesis is calm.
Anti-aging cosmetics are dazzling currently on the market, and the main active of common light spot anti-wrinkle wrinkle has：Antioxygen
Change class；Steroids；Microelement kind；Anti-aging biochemical preparation and anti-aging natural extract class.These active ingredients, it is most of
For chemical synthesis preparation, skin care item are applied to, short time interior energy plays the effect of light spot anti-wrinkle, but use for a long time can be to skin
Skin brings injury, accelerates the aging of skin.
Flos Osmanthi Fragrantis extract：It is sweet in flavor, warm-natured, there are warm stomach soothing the liver, the function of kidney-nourishing cold dispelling.Sweet osmanthus energy skin maintenance, larynx of releiving
Throat, improves more phlegm, cough symptom, and promoting the production of body fluid, it is smelly to keep away, and sputum cough is controlled in preventing phlegm from forming and stopping coughing, reason lung appetizing, relaxing tendons and activating collaterals, intestines wind bloody flux,
Also strengthening the bones and muscles, promoting blood circulation, warm waist and knee, the blood stasis and other effects that disappears can also treat lumbar sprain, gastroptosis, taste-blindness rate, reed
Measles, stomach cold have a stomach-ache, halitosis, vision are unknown, the disease such as seminal emission, measles, Amenorrhea abdominal pain, halitosis, fuzzy viewing.In the prior art will
Compound less of Flos Osmanthi Fragrantis extract and other compositions.
The content of the invention
It is an object of the present invention to provide a kind of anti-wrinkle containing Flos Osmanthi Fragrantis extract, cosmetic composition, said composition both had
There is preferable skin lightening function, and anti-wrinkle can be played the role of.
To achieve the above object, the technical solution used in the present invention：A kind of anti-wrinkle containing Flos Osmanthi Fragrantis extract, skin lightening group
Compound, includes the component of following parts by weight：10-20 parts of Flos Osmanthi Fragrantis extract, 5-10 parts of duckbilled flower extract, white willow bark extract
10-20 parts.
Single extract is usually used in the prior art and carries out skin lightening or anti-wrinkle, but its effect is not as far as possible preferable,
Present inventor has found by numerous studies, Flos Osmanthi Fragrantis extract, duckbilled flower extract is compounded, its skin lightening result is notable
Better than independent extract；Flos Osmanthi Fragrantis extract, white willow bark extract are compounded, its anti-wrinkle significant effect is better than individually extraction
Thing；
Preferably, the weight ratio of Flos Osmanthi Fragrantis extract and the duckbilled flower extract is 2:1.By Flos Osmanthi Fragrantis extract, malabar nut
Extract is compounded according to said ratio, its skin lightening result is best.
Preferably, the weight ratio of the Flos Osmanthi Fragrantis extract and white willow bark extract is 1:1.By Flos Osmanthi Fragrantis extract, white willow
Bark extract is compounded according to said ratio, its anti-wrinkle effect is best.
Preferably, the composition further includes preservative, emulsifying agent, emollient, skin skin lightening agent, essence and water.It is preferred that
Ground, the emulsifying agent are selected from ceteareth -6, ceteareth -25, glycerin monostearate.The moisturizing
Agent is selected from White Mineral Oil, stearic acid, cetostearyl alcohol, olive oil, octanoic acid/certain herbaceous plants with big flowers acid triglyceride, shea butter, jojoba oil, silicon
Oil.The skin skin lightening agent is selected from glycerine, propane diols, 1,3 butanediols.
The present invention provides a kind of preparation method of composition described above, the preparation method is by each component raw material
Precise by weight ratio, is sufficiently mixed and stirs evenly, that is, obtains the composition.
Preferably, the formulation of the composition is solution, spray, powdery, paste or emulsion.
The present invention provides a kind of anti-wrinkle, skin lightening skin care item, including oil phase, water phase, the water mutually includes described above
Composition.
Preferably, the anti-wrinkle, skin lightening skin care item further include essence and preservative.
The beneficial effects of the present invention are：The present invention provides a kind of anti-wrinkle containing Flos Osmanthi Fragrantis extract, cosmetic composition,
Said composition can not only substantially reduce skin roughness, reach anti-wrinkle effect, also with preferable skin lightening result, and safely
It is non-stimulated.
Embodiment
Each raw material involved by following embodiments is the commercially available universal product unless otherwise instructed.
Embodiment 1
Anti-wrinkle of the present invention, a kind of embodiment of cosmetic composition, the composition include the component of following parts by weight：
15 parts of Flos Osmanthi Fragrantis extract, 7.5 parts of duckbilled flower extract, 15 parts of white willow bark extract.
Embodiment 2
Anti-wrinkle of the present invention, a kind of embodiment of cosmetic composition, the composition include the component of following parts by weight：
10 parts of Flos Osmanthi Fragrantis extract, 10 parts of duckbilled flower extract, 15 parts of white willow bark extract.
Embodiment 3
Anti-wrinkle of the present invention, a kind of embodiment of cosmetic composition, the composition include the component of following parts by weight：
20 parts of Flos Osmanthi Fragrantis extract, 5 parts of duckbilled flower extract, 15 parts of white willow bark extract.
Comparative example 1
The formula of comparative example 1 is：22.5 parts of Flos Osmanthi Fragrantis extract, 15 parts of white willow bark extract.
Comparative example 2
The formula of comparative example 2 is：22.5 parts of duckbilled flower extract, 15 parts of white willow bark extract.
The preparation method of embodiment 1-3 and documents 1-2：Each component raw material is accurately claimed by above-mentioned weight proportion
Amount, is sufficiently mixed and stirs evenly, you can.
First, 1-3 of embodiment of the present invention skin lightenings efficacy assessments are tested
By the present embodiment skin lightening whitening Chinese medicament composition be applied to prepare facial mask, the facial mask by following parts by weight raw material
It is prepared：30 parts of the present embodiment composition, 25 parts of glycerine, 5 parts of PLURONICS F87,4.5 parts of propane diols, dipotassium glycyrrhizinate 5
Part, 2 parts of Sodium Hyaluronate, 1.2 parts of imidazolidinyl urea, 0.7 part of methyl hydroxybenzoate, 0.5 part of coceth -7, PPG-1-PEG-9
0.3 part of bay glycol ethers, 0.2 part of Cremophor RH40,0.1 part of the bromo- 2- nitropropanes -1,3- glycol of 2-, Rosa centifolia
Oily 0.1 part, 330 parts of water.
The present embodiment facial mask is prepared by the method including following operating procedure：
(1) PLURONICS F87, dipotassium glycyrrhizinate, imidazolidinyl urea, 2- bromine 2- nitropropane -1,3- glycol are added to
In water, it is uniformly mixed, obtains mixed material 1, it is spare；Glycerine is added in Sodium Hyaluronate, is uniformly mixed, obtains mixed material 2；Will
Propane diols is added in methyl hydroxybenzoate, is uniformly mixed, is obtained mixed material 3, spare；Take Rosa centifolia caul-fat add coceth -7,
PPG-1-PEG-9 bays glycol ethers, Cremophor RH40, are uniformly mixed, obtain mixed material 4；
(2) mixed material 2 is added in mixed material 1, is uniformly mixed, obtains mixed material 5；Mixed material 3 is added mixed
In compound material 5, mixed material 6 is obtained；
(3) the present embodiment composition is added in mixed material 6, is uniformly mixed, obtains mixed material 7；
(4) mixed material 4 is added in mixed material 7, is uniformly mixed, up to the facial mask.
Clinical effectiveness is tested：
Patient data：Age, average age was 150 female patients of 30 years old at 25~35 years old, and patient shows as face
Portion's skin is obscure, jaundice, matt, and face has color spot, and patient is divided into 5 groups, be respectively 1 group of embodiment, 2 groups of embodiment,
2 groups of 3 groups of embodiment, 1 group of comparative example and comparative example, every group of 30 female patients.
Treatment method：Facial mask prepared by the application embodiment of the present invention, each 15~20 minutes of application, are rinsed dry with water
Only, application 3~4 times weekly, use 28 days as a treatment course, the therapeutic effect of two courses for the treatment of of statistics.Meanwhile suffer from during treatment
Person should be noted that the mood that keeps pleasant, gentle phychology.On diet, excessive pungent stimulation food is avoided, such as pungent, curried,
The foods such as garlic, avoid abuse cosmetics, few with or without dark cosmetics.
Criterion of therapeutical effect：
It is basic to cure：Facial fade>90%, i.e. color disappears substantially；
It is effective：Facial fade>76%, color substantially shoals；
Improve：Color spot area disappears>3%, color is thin out；
It is invalid：Color area regression≤3%, color change unobvious.
Efficient=(basic healing+effective)/total case.
Treatment results such as table 1, all cases do not occur obvious adverse reaction.From the results shown in Table 1, by sweet osmanthus
Extract, duckbilled flower extract are compounded, synergistic, its skin lightening result is significantly better than independent extract；The present invention is implemented
The composition of example 1-3 can be obviously improved obscure face skin, jaundice, tarnish, and face has the problems such as color spot, wherein implementing
The skin lightening result of example 1 is best.
The skin lightening result of 1 1-3 products of the embodiment of the present invention of table
| Test group | It is basic to cure | It is effective | Improve | It is invalid | It is efficient |
| 1 group of embodiment | 26 | 2 | 2 | 0 | 93.3% |
| 2 groups of embodiment | 24 | 2 | 4 | 0 | 86.7% |
| 3 groups of embodiment | 23 | 3 | 4 | 0 | 86.7% |
| 1 group of comparative example | 18 | 4 | 8 | 0 | 73.3% |
| 2 groups of comparative example | 16 | 5 | 9 | 0 | 70.0% |
Embodiment 4
Anti-wrinkle of the present invention, skin lightening composition a kind of embodiment, the composition includes the group of following parts by weight
Point：15 parts of Flos Osmanthi Fragrantis extract, 7.5 parts of duckbilled flower extract, 15 parts of white willow bark extract.
Embodiment 5
Anti-wrinkle of the present invention, skin lightening composition a kind of embodiment, the composition includes the group of following parts by weight
Point：20 parts of Flos Osmanthi Fragrantis extract, 7.5 parts of duckbilled flower extract, 10 parts of white willow bark extract.
Embodiment 6
Anti-wrinkle of the present invention, skin lightening composition a kind of embodiment, the composition includes the group of following parts by weight
Point：10 parts of Flos Osmanthi Fragrantis extract, 7.5 parts of duckbilled flower extract, 20 parts of white willow bark extract.
Comparative example 3
The formula of comparative example 3 is：30 parts by weight of Flos Osmanthi Fragrantis extract, 7.5 parts by weight of duckbilled flower extract.
Comparative example 4
The formula of comparative example 4 is：7.5 parts by weight of duckbilled flower extract, 30 parts by weight of white willow bark extract.
The preparation method of embodiment 4-6 and comparative example 3-4：Each component raw material is pressed into above-mentioned weight proportion precise,
It is sufficiently mixed and stirs evenly, you can.
2nd, 4-6 of embodiment of the present invention anti-wrinkle efficacy assessments are tested
Method：
Subject amounts to 40 people.Specific sex composition determines at random.If period there are 2 people adverse reaction occur, terminate and survey
Examination；As a result adverse reaction is not found.After subject has smeared composition made from 4-6 of the embodiment of the present invention, the roughness of skin
Have clear improvement.
1. the left and right eye of subject is selected as tested region.Every subject's left eye smears given the test agent, and (present invention is real
Apply composition made from a 4-6) sample sets are used as, right eye smears documents 4,5 and does not smear any sample as control
Group.
2. before smearing cosmetics using skin lens image analysis system and moisture content of skin tester determination experiment position
Dermatoglyph degree.
3. smear in the tested area (the same area) cleaned by clear water sooner or later daily and detect product, during the experiment, by
Examination person cannot apply the other any cosmetics erased outside tested sample in Test sites.
4. subject is after continuous use given the test agent one week, two weeks, three weeks and four weeks, weekly same time subject general
Smear position to clean, number positional is smeared using skin lens image analysis system and moisture content of skin tester measure by tester
Value.
5. the numerical value that statistics subject position measures every time, the change rule of analyzing skin texture and moisture
Rule.
As a result：
(1) dermatoglyph situation of change：
Change rate=(number of sets of sample is according to Tn-initial value T0)/initial value T0× 100%
Relative change rate=(number of sets of sample is according to Tn-blank control group data Tn)/blank control group data Tn × 100%
T0It is subjects skin's measured value before testing, Tn is skin measured value when each subject tests at each time point every time.
1st, skin roughness (Skin Roughness SR)
Skin roughness is in all sections of skin, with the difference on straight line between maximum gray scale peak value and minimal gray peak value
Value.The parameter is the maximum height of skin surface unevenness.
The difference of 2 recipient site skin roughness of table and initial value
Within 4 weeks test periods, after recipient site uses present composition sample, its skin roughness is always in reduction
Trend, and be negative value, relative change rate is negative value always, and is in reduction trend；It can be seen that from the data of table 2 by sweet osmanthus
Extract, white willow bark extract are compounded according to said ratio, can synergistic anti-wrinkle, use the present composition 4
Zhou Hou, skin roughness substantially reduce, and the anti-wrinkle effect of wherein embodiment 4 is best.
3rd, safety testing
Test material and method
Animal：Regular grade large ear rabbit 4,2.3-2.7 kilograms of weight, body looks into animal no abnormality seen.
Environmental condition：Room temperature：22 DEG C -26 DEG C, relative humidity：65% -69%；
Test method：
Foundation《Cosmetics health specification》(version in 2007) acute skin irritation test, before experiment 24 it is small when, will test
Back part of animal backbone diamond wool is cut, 3 centimetres of 3 cm x of unhairing scope.Tested 0.5 gram of no originality is taken directly to be applied to right side skin
On skin, with clean gauze cover, with nonirritant immobilization with adhesive tape 2 it is small when.Other side is negative control.After removing tested material
1 it is small when, 24 it is small when, 48 it is small when 72 it is small when observe and animal subject contact site dermoreaction and keep a record.
Under this experimental condition, 1-6 of embodiment of the present invention compositions press White Rabbit acute skin irritation test skin thorn
It is nonirritant to swash strength grading.
The Security test of 1-6 compositions of the embodiment of the present invention：
1-6 of embodiment of the present invention compositions safety, the examination of human body patch are demonstrated by zoopery and human body patch test
Test and carried out by our company professional.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than the present invention is protected
The limitation of scope is protected, although being explained in detail with reference to preferred embodiment to the present invention, those of ordinary skill in the art should
Understand, can be to technical scheme technical scheme is modified or replaced equivalently, without departing from the essence of technical solution of the present invention
And scope.
Claims (9)
1. a kind of anti-wrinkle containing Flos Osmanthi Fragrantis extract, cosmetic composition, it is characterised in that include the component of following parts by weight：Osmanthus
10-20 parts of flower extract, 5-10 parts of duckbilled flower extract, 10-20 parts of white willow bark extract.
2. anti-wrinkle according to claim 1, cosmetic composition, it is characterised in that the Flos Osmanthi Fragrantis extract and malabar nut carry
The weight ratio for taking thing is 2:1.
3. anti-wrinkle according to claim 1, cosmetic composition, it is characterised in that the Flos Osmanthi Fragrantis extract and white willow bark
The weight ratio of extract is 1:1.
4. anti-wrinkle according to claim 1, cosmetic composition, it is characterised in that the anti-aging, cosmetic composition also wrap
Include preservative, pH adjusting agent, thickener, emulsifying agent, essence, pigment and water.
5. anti-wrinkle according to claim 1, cosmetic composition, it is characterised in that the emulsifying agent is selected from cetostearyl alcohol
Polyethers -6, ceteareth -25, glycerin monostearate, the emollient are selected from White Mineral Oil, stearic acid, cetearyl alcohol
Alcohol, olive oil, octanoic acid/certain herbaceous plants with big flowers acid triglyceride, shea butter, jojoba oil, silicone oil, the skin skin lightening agent are selected from glycerine, third
Glycol, 1,3 butanediols.
A kind of 6. anti-wrinkle, preparation method of cosmetic composition as described in claim 1-5 is any, it is characterised in that the system
Preparation Method is by each component raw material precise by weight ratio, is sufficiently mixed and stirs evenly, that is, obtains the composition.
7. anti-wrinkle according to claim 1, cosmetic composition, it is characterised in that the anti-wrinkle, the formulation of cosmetic composition
For aqua, creme, finish, washing lotion or emulsion.
8. a kind of anti-wrinkle, skin lightening skin care item, it is characterised in that including oil phase, water phase, the water mutually includes such as claim 1-5
Any anti-wrinkle, cosmetic composition.
9. anti-wrinkle according to claim 8, skin lightening skin care item, it is characterised in that the anti-wrinkle, skin lightening skin care item further include
Essence and preservative.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711336354.3A CN107998017A (en) | 2017-12-11 | 2017-12-11 | A kind of anti-wrinkle containing Flos Osmanthi Fragrantis extract, cosmetic composition and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711336354.3A CN107998017A (en) | 2017-12-11 | 2017-12-11 | A kind of anti-wrinkle containing Flos Osmanthi Fragrantis extract, cosmetic composition and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107998017A true CN107998017A (en) | 2018-05-08 |
Family
ID=62058759
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711336354.3A Withdrawn CN107998017A (en) | 2017-12-11 | 2017-12-11 | A kind of anti-wrinkle containing Flos Osmanthi Fragrantis extract, cosmetic composition and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115137678A (en) * | 2022-05-24 | 2022-10-04 | 桂林拓普香料有限公司 | Pure natural sweet osmanthus moistening paste and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106333886A (en) * | 2016-08-29 | 2017-01-18 | 欧标（广州）化妆品有限公司 | Composition having moisture preserving and skin whitening and brightening effects and application thereof |
| CN106551870A (en) * | 2017-01-05 | 2017-04-05 | 云南祥琬生物科技有限公司 | A kind of compositionss with crease-resistant skin lightening effect, facial film and preparation method thereof |
-
2017
- 2017-12-11 CN CN201711336354.3A patent/CN107998017A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106333886A (en) * | 2016-08-29 | 2017-01-18 | 欧标（广州）化妆品有限公司 | Composition having moisture preserving and skin whitening and brightening effects and application thereof |
| CN106551870A (en) * | 2017-01-05 | 2017-04-05 | 云南祥琬生物科技有限公司 | A kind of compositionss with crease-resistant skin lightening effect, facial film and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 王建新 等: "《化妆品植物原料大全》", 30 June 2012 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115137678A (en) * | 2022-05-24 | 2022-10-04 | 桂林拓普香料有限公司 | Pure natural sweet osmanthus moistening paste and preparation method thereof |
| CN115137678B (en) * | 2022-05-24 | 2023-10-24 | 桂林拓普香料有限公司 | Pure natural osmanthus flower moisturizing cream and preparation method thereof |
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Application publication date: 20180508 |