CN115137678A - Pure natural sweet osmanthus moistening paste and preparation method thereof - Google Patents
Pure natural sweet osmanthus moistening paste and preparation method thereof Download PDFInfo
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- CN115137678A CN115137678A CN202210575126.6A CN202210575126A CN115137678A CN 115137678 A CN115137678 A CN 115137678A CN 202210575126 A CN202210575126 A CN 202210575126A CN 115137678 A CN115137678 A CN 115137678A
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- 235000019083 Osmanthus fragrans Nutrition 0.000 title claims abstract description 63
- 238000002360 preparation method Methods 0.000 title claims abstract description 34
- 239000000284 extract Substances 0.000 claims abstract description 128
- 239000006071 cream Substances 0.000 claims abstract description 86
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims abstract description 50
- 239000002994 raw material Substances 0.000 claims abstract description 32
- 235000013871 bee wax Nutrition 0.000 claims abstract description 28
- 239000012166 beeswax Substances 0.000 claims abstract description 28
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 27
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 26
- 235000006708 antioxidants Nutrition 0.000 claims abstract description 26
- 229930003427 Vitamin E Natural products 0.000 claims abstract description 25
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims abstract description 25
- 235000019165 vitamin E Nutrition 0.000 claims abstract description 25
- 229940046009 vitamin E Drugs 0.000 claims abstract description 25
- 239000011709 vitamin E Substances 0.000 claims abstract description 25
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- 239000001233 rosmarinus officinalis l. extract Substances 0.000 claims abstract description 21
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- 235000008390 olive oil Nutrition 0.000 claims abstract description 18
- 238000002156 mixing Methods 0.000 claims description 168
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 135
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- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 claims description 18
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims description 18
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- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims description 13
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 claims description 13
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- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 claims description 13
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- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 6
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- 238000001035 drying Methods 0.000 claims description 6
- UAJTZZNRJCKXJN-UHFFFAOYSA-M sodium;2-dodecoxy-2-oxoethanesulfonate Chemical compound [Na+].CCCCCCCCCCCCOC(=O)CS([O-])(=O)=O UAJTZZNRJCKXJN-UHFFFAOYSA-M 0.000 claims description 6
- 229940088594 vitamin Drugs 0.000 claims description 6
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- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 4
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- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- MGJZITXUQXWAKY-UHFFFAOYSA-N diphenyl-(2,4,6-trinitrophenyl)iminoazanium Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1N=[N+](C=1C=CC=CC=1)C1=CC=CC=C1 MGJZITXUQXWAKY-UHFFFAOYSA-N 0.000 description 2
- 230000036541 health Effects 0.000 description 2
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9771—Ginkgophyta, e.g. Ginkgoaceae [Ginkgo family]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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- A61K2800/522—Antioxidants; Radical scavengers
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention discloses a pure natural sweet osmanthus moistening cream and a preparation method thereof, and particularly relates to the technical field of moistening cream, wherein the moistening cream comprises moistening cream A and moistening cream B, raw materials (by weight) used by the moistening cream A comprise 40-60 parts of olive oil, 10-18 parts of beeswax, 10-30 parts of sweet osmanthus extract, 2-5 parts of vitamin E, 2-10 parts of auxiliary agent and 2-10 parts of antioxidant, and raw materials (by weight) used by the moistening cream B comprise 40-60 parts of olive oil, 10-18 parts of beeswax, 6-10 parts of sweet osmanthus extract, 2-10 parts of rosemary extract, 1-8 parts of freshener and 2-5 parts of vitamin E. The skin-care product has the effects of moistening skin, maintaining beauty and keeping young, is beneficial to skin absorption and shrinking pores, and is suitable for various skins.
Description
Technical Field
The invention relates to the technical field of moistening cream, and particularly relates to pure natural sweet osmanthus moistening cream and a preparation method thereof.
Background
With the increasing pursuit of health and the rapid development of dermatology, people pay more and more attention to skin care. The skin of a human deteriorates from 14 years old, the metabolism of the skin becomes slow gradually after 24 years old, the stratum corneum is gradually accumulated and thickened, except for the fact that the skin condition is influenced by age, the change of human hormones, the environmental pollution, ultraviolet radiation, dietary habits, sleeping time and improper maintenance modes can influence the health of the skin, and the skin is in problems, so that the skin care becomes an essential link in daily life, and various skin care products are in endless supply.
Nourishing skin care products are used in daily skin care, wherein the main function and effect of the moistening cream are to provide enough nutrition for skin, moisten and moisturize the skin, and the skin effect of the existing moistening cream needs to be further improved.
Disclosure of Invention
The invention aims to provide the pure natural sweet osmanthus moistening cream and the preparation method thereof, and the pure natural sweet osmanthus moistening cream has the effects of moistening skin, maintaining beauty and keeping young, is beneficial to skin absorption and pore contraction, and is suitable for various skins.
In order to achieve the above purpose, the invention provides the following technical scheme: a pure natural sweet osmanthus moistening paste comprises moistening paste A and moistening paste B, wherein the raw materials (in parts by weight) used for the moistening paste A comprise 40-60 parts of olive oil, 10-18 parts of beeswax, 10-30 parts of sweet osmanthus extract, 2-5 parts of vitamin E, 2-10 parts of an auxiliary agent and 2-10 parts of an antioxidant, and the raw materials (in parts by weight) used for the moistening paste B comprise 40-60 parts of olive oil, 10-18 parts of beeswax, 6-10 parts of sweet osmanthus extract, 2-10 parts of rosemary extract, 1-8 parts of a freshener and 2-5 parts of vitamin E.
Preferably, the adjuvant comprises houttuynia cordata extract, ginkgo leaf extract and ginger extract, and the ratio of the houttuynia cordata extract to the ginkgo leaf extract to the ginger extract is 1:1:1.
preferably, the antioxidant comprises tomato extract and apple extract, and the ratio of the tomato extract to the apple extract is 1:1.
preferably, the cooling agent comprises menthol and borneol, and the proportion of the menthol to the borneol is 1:1.
the invention also comprises a method for preparing the pure natural sweet osmanthus moistening cream, which comprises the following specific steps:
the method comprises the following steps: preparing moistening paste A:
s1: mixing herba Houttuyniae extract, folium Ginkgo extract, and rhizoma Zingiberis recens extract at a ratio of 1:1:1, uniformly mixing to obtain an auxiliary agent;
s2: mixing tomato extract and apple extract according to the weight ratio of 1:1, uniformly mixing the raw materials in a ratio to obtain an antioxidant;
s3: melting Cera flava in moistening paste A raw material in 80-90 deg.C water bath, mixing the melted Cera flava, oleum Olivarum, flos Osmanthi Fragrantis extract, vitamins, adjuvants, and antioxidant, heating to 70-80 deg.C water bath, and stirring to obtain mixed solution;
s4: cooling the mixed liquid obtained in the step S3 to 40-50 ℃, adding vitamin E, uniformly stirring, pouring into a moistening cream box, and solidifying to obtain moistening cream A;
step two: preparing moistening paste B:
s5: mixing Mentholum and Borneolum Syntheticum at a ratio of 1:1, mixing uniformly to obtain a freshener;
s6: melting Cera flava in the moistening paste B in 80-90 deg.C water bath, mixing the melted Cera flava, flos Osmanthi Fragrantis extract, herba Rosmarini officinalis extract and algefacient, heating to 70-80 deg.C in water bath, and stirring to obtain mixed solution;
s7: and (4) cooling the mixed liquid obtained in the step (S6) to 40-50 ℃, adding vitamin E, uniformly stirring, and pouring into another moistening cream box to solidify to obtain moistening cream B.
Preferably, the preparation method of the sweet osmanthus extract comprises the following steps: according to the mass ratio of 1:10 mixing sweet osmanthus with distilled water, heating to 30-40 ℃, soaking for 3-6h, transferring into a distillation retort after soaking, distilling with steam for 4-6h, standing and layering distillate at room temperature to collect an oil layer, adding anhydrous sodium sulfate accounting for 5-10% of the mass of the oil layer into the oil layer, standing and drying for 8-10h, filtering, and collecting filtrate to obtain the sweet osmanthus extract.
Preferably, the preparation method of the houttuynia cordata extract comprises the following steps: cleaning and chopping houttuynia cordata, soaking for 1-2h, and mixing the raw materials in a mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2-4h, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:7, mixing the filter residue with water, decocting and extracting for 1-3h, taking the filtrate, and mixing the filtrate according to a mass ratio of 1:5 mixing the filter residue with water, decocting and extracting for 0.5-2h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain thick paste, and spray drying to obtain the houttuynia cordata extract.
Preferably, the preparation method of the ginkgo biloba extract comprises the following steps: cleaning and chopping ginkgo leaves, soaking for 1-2h, and mixing the ginkgo leaves with the water according to a mass ratio of 1:8, mixing rosemary with water, decocting and extracting for 2-4h, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:6, mixing the filter residue with water, decocting and extracting for 1-3h, taking the filtrate, and mixing the filtrate according to the mass ratio of 1:5 mixing the filter residue with water, decocting and extracting for 0.5-2h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain a thick paste, and spray drying to obtain the ginkgo leaf extract.
Preferably, the preparation method of the ginger extract comprises the following steps: cleaning and chopping ginger, and soaking for 1-2h according to a mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2-4h, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1: 8. mixing the filter residue with water, decocting and extracting for 1-3h, taking the filtrate, and mixing the filtrate according to a mass ratio of 1:6 mixing the filter residue with water, decocting and extracting for 0.5-2h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain thick paste, and spray drying to obtain the houttuynia cordata extract.
Preferably, the preparation method of the tomato extract comprises the following steps: cleaning and crushing tomatoes to obtain tomato pulp, wherein the mass ratio of the tomato pulp to the tomato pulp is 1:5 mixing the tomato serum with water, extracting with ultrasonic wave auxiliary extraction power of 60-80w for 5-10min, extracting with 40-50 deg.C water bath for 30-50min, filtering, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain tomato extract.
Preferably, the preparation method of the apple extract comprises the following steps: washing and crushing apples to obtain apple liquid, wherein the mass ratio of the apple liquid to the apple liquid is 1:8, mixing the apple liquid with water, extracting with ultrasonic assistance, wherein the power of ultrasonic assistance extraction is 60-80w, the time is 5-10min, extracting with 40-50 ℃ water bath for 30-50min, filtering after extraction, taking filtrate, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain the apple extract.
Preferably, the preparation method of the rosemary extract comprises the following steps: grinding rosemary into powder, and soaking for 0.5-2h according to the mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2-5h, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:8 mixing the filter residue with water, decocting and extracting for 1-3h, taking the filtrate, combining the two filtrates, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain the rosemary extract.
In the technical scheme, the invention provides the following technical effects and advantages:
1. when in use, the moistening cream A is firstly smeared, and the sweet osmanthus extract in the moistening cream A firstly has the effects of moistening the skin and maintaining beauty and keeping young, and is suitable for various skin types such as oily skin, dry skin, mixed skin, sensitive skin and the like.
2. The sweet osmanthus extract has a good antibacterial effect, is beneficial to prolonging the quality guarantee period of the moistening paste, and finally, has strong fragrance and is suitable for consumers to select.
3. The tomato extract and the apple extract in the moistening paste A have antioxidant effect, and are helpful for reducing irritation and damage of free radicals to skin, reducing melanin generation and precipitation, preventing color spots and freckles, and preventing fine wrinkles.
4. The heartleaf houttuynia herb extract in the moistening cream A is beneficial to capillary vessel expansion, the ginkgo leaf extract has the effects of activating blood, expanding blood vessels and accelerating blood circulation, and the ginger extract has the effect of warming skin and is beneficial to opening skin pores, so that the effective components of the moistening cream can be absorbed by the skin.
5. After the moistening cream A is applied for 15-20 minutes, the moistening cream B is applied, the rosemary extract in the moistening cream B is helpful for shrinking pores, and the menthol and the borneol in the freshener are helpful for cooling the skin, further helpful for shrinking the pores and preventing the skin pores from being large.
Detailed Description
The present invention will be described in further detail below in order to enable those skilled in the art to better understand the technical solution of the present invention.
Example 1
The invention provides a pure natural sweet osmanthus moistening cream which comprises moistening cream A and moistening cream B, wherein the raw materials (in parts by weight) used by the moistening cream A comprise 40 parts of olive oil, 10 parts of beeswax, 10 parts of sweet osmanthus extract, 2 parts of vitamin E, 2 parts of an auxiliary agent and 2 parts of an antioxidant, and the raw materials (in parts by weight) used by the moistening cream B comprise 40 parts of olive oil, 10 parts of beeswax, 6 parts of sweet osmanthus extract, 2 parts of rosemary extract, 1 part of a freshener and 2 parts of vitamin E.
The auxiliary agent comprises houttuynia extract, ginkgo leaf extract and ginger extract, wherein the ratio of the houttuynia extract to the ginkgo leaf extract to the ginger extract is 1:1:1.
the antioxidant comprises a tomato extract and an apple extract, wherein the ratio of the tomato extract to the apple extract is 1:1.
the freshener comprises menthol and borneol, wherein the proportion of the menthol to the borneol is 1:1.
the invention also provides a method for preparing the pure natural sweet osmanthus moistening paste, which comprises the following specific steps:
the method comprises the following steps: preparing moistening paste A:
s1: preparing a houttuynia cordata extract: cleaning and chopping houttuynia cordata, soaking for 1h, and mixing the raw materials in a mass ratio of 1: 10. mixing rosemary with water, decocting and extracting for 2 hours, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:7, mixing the filter residue with water, decocting and extracting for 1 hour, taking the filtrate, and mixing the filtrate according to a mass ratio of 1:5 mixing the filter residue with water, decocting and extracting for 0.5h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain a thick paste, and spray drying to obtain the houttuynia cordata extract;
preparing a ginkgo leaf extract: cleaning and chopping ginkgo leaves, soaking for 1h, and mixing the ginkgo leaves with the water according to a mass ratio of 1:8, mixing rosemary with water, decocting and extracting for 2 hours, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:6, mixing the filter residue with water, decocting and extracting for 1h, taking the filtrate, and mixing the filtrate according to a mass ratio of 1:5 mixing the filter residue with water, decocting and extracting for 0.5h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain a thick paste, and spray drying to obtain the ginkgo leaf extract;
preparing a ginger extract: cleaning and chopping ginger, soaking for 1h, and mixing the ginger with the water according to a mass ratio of 1:10, mixing rosemary with water, decocting and extracting for 2 hours, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:8, mixing the filter residue with water, decocting and extracting for 1h, taking the filtrate, and mixing the filtrate with the water according to a mass ratio of 1:6 mixing the filter residue with water, decocting and extracting for 0.5h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain a thick paste, and spray drying to obtain the houttuynia cordata extract;
mixing herba Houttuyniae extract, folium Ginkgo extract, and rhizoma Zingiberis recens extract at a ratio of 1:1:1, uniformly mixing to obtain an auxiliary agent;
s2: preparing a tomato extract: cleaning and crushing tomatoes to obtain tomato pulp, wherein the mass ratio of the tomato pulp to the tomato pulp is 1:5 mixing the tomato pulp with water, extracting with ultrasonic assistance at a power of 60w for 5min, extracting with 40 deg.C water bath for 30min, filtering, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain tomato extract;
preparing an apple extract: washing and crushing apples to obtain apple liquid, wherein the mass ratio of the apple liquid to the apple liquid is 1:8, mixing apple liquid with water, extracting with ultrasonic assistance, wherein the power of ultrasonic assistance extraction is 60w, the time is 5min, extracting with 40 ℃ water bath for 30min, filtering after extraction, taking filtrate, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain the apple extract;
mixing tomato extract and apple extract according to the weight ratio of 1:1, uniformly mixing the raw materials in a ratio to obtain an antioxidant;
s3: heating beeswax in the moistening paste A raw material in a water bath at 80 ℃ to melt, then mixing the melted beeswax, olive oil, an osmanthus extract, vitamins, an auxiliary agent and an antioxidant, heating the mixture in the water bath to 70 ℃, and uniformly stirring the mixture to obtain a mixed solution;
the preparation method of the sweet osmanthus extract comprises the following steps: according to the mass ratio of 1:10 mixing sweet osmanthus with distilled water, heating to 30 ℃, soaking for 3h, transferring into a distillation retort after soaking, distilling with steam for 4h, standing and layering distillate at room temperature to collect an oil layer, adding anhydrous sodium sulfate with the mass of 5% of the oil layer into the oil layer, standing and drying for 8h, filtering, and collecting filtrate to obtain the sweet osmanthus extract;
s4: cooling the mixed liquid obtained in the step S3 to 40 ℃, adding vitamin E, uniformly stirring, pouring into a moistening cream box, and solidifying to obtain moistening cream A;
step two: preparing moistening paste B:
s5: mixing Mentholum and Borneolum Syntheticum at a ratio of 1:1, uniformly mixing the components in a ratio to obtain a freshener;
s6: heating beeswax in the moistening paste B raw material in a water bath at 80 ℃ to melt, then mixing the melted beeswax, the sweet osmanthus flower extract, the rosemary extract and the freshener, heating the mixture in the water bath to 70 ℃, and uniformly stirring the mixture to obtain a mixed solution;
the preparation method of the rosemary extract comprises the following steps: the rosemary is ground into powder and then soaked for 0.5h, and the weight ratio of the rosemary to the water is 1:10, mixing rosemary with water, decocting and extracting for 2 hours, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:8, mixing the filter residue with water, decocting and extracting for 1h, taking filtrate, combining the two filtrates, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain rosemary extract;
s7: and (4) cooling the mixed liquid obtained in the step (S6) to 40 ℃, adding vitamin E, uniformly stirring, pouring into another moistening cream box, and solidifying to obtain moistening cream B.
Example 2
The invention provides a pure natural sweet osmanthus moistening cream which comprises moistening cream A and moistening cream B, wherein raw materials (in parts by weight) used by the moistening cream A comprise 50 parts of olive oil, 16 parts of beeswax, 20 parts of sweet osmanthus extract, 3 parts of vitamin E, 6 parts of an auxiliary agent and 6 parts of an antioxidant, and raw materials (in parts by weight) used by the moistening cream B comprise 50 parts of olive oil, 16 parts of beeswax, 8 parts of sweet osmanthus extract, 6 parts of rosemary extract, 5 parts of a freshener and 3 parts of vitamin E.
The auxiliary agent comprises houttuynia extract, ginkgo leaf extract and ginger extract, wherein the ratio of the houttuynia extract to the ginkgo leaf extract to the ginger extract is 1:1:1.
the antioxidant comprises a tomato extract and an apple extract, wherein the ratio of the tomato extract to the apple extract is 1:1.
the freshener comprises menthol and borneol, wherein the proportion of the menthol to the borneol is 1:1.
the invention also provides a method for preparing the pure natural sweet osmanthus moistening cream, which comprises the following specific steps:
the method comprises the following steps: preparing moistening paste A:
s1: preparing a houttuynia cordata extract: cleaning and chopping houttuynia cordata, soaking for 1.5h, and mixing the raw materials in a mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 3 hours, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:7, mixing the filter residue with water, decocting and extracting for 2 hours, taking the filtrate, and mixing the filtrate according to a mass ratio of 1:5 mixing the filter residue with water, decocting and extracting for 1h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain a thick paste, and spray drying to obtain the houttuynia cordata extract;
preparing a ginkgo leaf extract: cleaning and chopping ginkgo leaves, soaking for 1.5h, and mixing the ginkgo leaves with the water according to a mass ratio of 1:8, mixing rosemary with water, decocting and extracting for 3 hours, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:6, mixing the filter residue with water, decocting and extracting for 2 hours, taking the filtrate, and mixing the filtrate according to a mass ratio of 1:5 mixing the filter residue with water, decocting and extracting for 1h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain a thick paste, and spray drying to obtain the ginkgo leaf extract;
preparing a ginger extract: cleaning and chopping ginger, and soaking for 1.5h according to a mass ratio of 1:10, mixing rosemary with water, decocting and extracting for 3 hours, taking filtrate, and then mixing the filtrate according to the mass ratio of 1:8, mixing the filter residue with water, decocting and extracting for 2 hours, taking the filtrate, and mixing the filtrate with the water according to a mass ratio of 1:6 mixing the filter residue with water, decocting and extracting for 1h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain thick paste, and spray drying to obtain the houttuynia cordata extract;
mixing herba Houttuyniae extract, folium Ginkgo extract, and rhizoma Zingiberis recens extract at a ratio of 1:1:1, uniformly mixing to obtain an auxiliary agent;
s2: preparing a tomato extract: cleaning and crushing tomatoes to obtain tomato pulp, wherein the mass ratio of the tomato pulp to the tomato pulp is 1: mixing tomato pulp with water, extracting with ultrasonic wave at power of 70w for 8min, extracting with 45 deg.C water bath for 40min, filtering, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain tomato extract;
preparing an apple extract: washing and crushing apples to obtain apple liquid, wherein the mass ratio of the apple liquid to the apple liquid is 1:8, mixing apple liquid with water, extracting with ultrasonic assistance, wherein the power of ultrasonic assistance extraction is 70w, the time is 8min, extracting with 45 ℃ water bath for 40min, filtering after extraction, taking filtrate, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain the apple extract;
mixing tomato extract and apple extract according to the weight ratio of 1:1, uniformly mixing the raw materials in a ratio to obtain an antioxidant;
s3: heating beeswax in the moistening paste A raw material in a water bath at 85 ℃ to melt, then mixing the melted beeswax, olive oil, an osmanthus fragrans extract, vitamins, an auxiliary agent and an antioxidant, heating the mixture in the water bath to 75 ℃, and uniformly stirring the mixture to obtain a mixed solution;
the preparation method of the sweet osmanthus extract comprises the following steps: according to the mass ratio of 1:10 mixing sweet osmanthus with distilled water, heating to 35 ℃, soaking for 5h, transferring into a distillation retort after soaking, distilling for 5h with steam, standing and layering distillate at room temperature to collect an oil layer, adding anhydrous sodium sulfate with the oil layer mass of 8%, standing and drying for 9h, filtering, and collecting filtrate to obtain the sweet osmanthus extract;
s4: cooling the mixed liquid obtained in the step S3 to 45 ℃, adding vitamin E, uniformly stirring, pouring into a moistening cream box, and solidifying to obtain moistening cream A;
step two: preparing moistening paste B:
s5: mixing Mentholum and Borneolum Syntheticum at a ratio of 1:1, mixing uniformly to obtain a freshener;
s6: heating beeswax in the moistening paste B raw material in a water bath at 85 ℃ to melt, then mixing the melted beeswax, the sweet osmanthus flower extract, the rosemary extract and the freshener, heating the mixture in the water bath to 75 ℃, and uniformly stirring the mixture to obtain a mixed solution;
the preparation method of the rosemary extract comprises the following steps: the rosemary is ground into powder and then soaked for 1h, and the mass ratio is 1:10 mixing rosemary with water, decocting and extracting for 2.5 hours, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:8 mixing the filter residue with water, decocting and extracting for 2h, taking filtrate, mixing the two filtrates, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain rosemary extract;
s7: and (4) cooling the mixed liquid obtained in the step (S6) to 45 ℃, adding vitamin E, uniformly stirring, pouring into another moistening cream box, and solidifying to obtain moistening cream B.
Example 3
The invention provides a pure natural sweet osmanthus moistening cream which comprises moistening cream A and moistening cream B, wherein raw materials (in parts by weight) used by the moistening cream A comprise 60 parts of olive oil, 18 parts of beeswax, 30 parts of sweet osmanthus extract, 5 parts of vitamin E, 10 parts of an auxiliary agent and 10 parts of an antioxidant, and raw materials (in parts by weight) used by the moistening cream B comprise 60 parts of olive oil, 18 parts of beeswax, 10 parts of sweet osmanthus extract, 10 parts of rosemary extract, 8 parts of a freshener and 5 parts of vitamin E.
The auxiliary agent comprises houttuynia cordata extract, ginkgo leaf extract and ginger extract, wherein the ratio of the houttuynia cordata extract to the ginkgo leaf extract to the ginger extract is 1:1:1.
the antioxidant comprises a tomato extract and an apple extract, wherein the ratio of the tomato extract to the apple extract is 1:1.
the freshener comprises menthol and borneol, wherein the proportion of the menthol to the borneol is 1:1.
the invention also provides a method for preparing the pure natural sweet osmanthus moistening cream, which comprises the following specific steps:
the method comprises the following steps: preparing moistening paste A:
s1: preparing a houttuynia cordata extract: cleaning and chopping houttuynia cordata, soaking for 2 hours, and mixing the raw materials in a mass ratio of 1: 10. mixing rosemary with water, decocting and extracting for 4 hours, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:7, mixing the filter residue with water, decocting and extracting for 3 hours, taking the filtrate, and mixing the filtrate according to a mass ratio of 1:5 mixing the filter residue with water, decocting and extracting for 2h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain a thick paste, and spray drying to obtain the houttuynia cordata extract;
preparing a ginkgo leaf extract: cleaning and chopping ginkgo leaves, soaking for 2 hours, and mixing the ginkgo leaves with the water according to a mass ratio of 1:8 mixing herba Rosmarini officinalis with water, decocting for 4 hr, taking the filtrate, and then mixing the filtrate according to the mass ratio of 1:6, mixing the filter residue with water, decocting and extracting for 3 hours, taking the filtrate, and mixing the filtrate according to a mass ratio of 1:5 mixing the filter residue with water, decocting and extracting for 2h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain a thick paste, and spray drying to obtain the ginkgo leaf extract;
preparing a ginger extract: cleaning and chopping ginger, soaking for 2 hours, and mixing the ginger powder with the water according to a mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 4 hours, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:8, mixing the filter residue with water, decocting and extracting for 3 hours, taking the filtrate, and mixing the filtrate according to a mass ratio of 1:6 mixing the filter residue with water, decocting and extracting for 2h, taking the filtrate, mixing the three filtrates, concentrating under reduced pressure to obtain thick paste, and spray drying to obtain the houttuynia cordata extract;
mixing herba Houttuyniae extract, folium Ginkgo extract, and rhizoma Zingiberis recens extract at a ratio of 1:1:1, uniformly mixing to obtain an auxiliary agent;
s2: preparing a tomato extract: cleaning and crushing tomatoes to obtain tomato pulp, wherein the mass ratio of the tomato pulp to the tomato pulp is 1: mixing tomato pulp with water, extracting with ultrasonic wave auxiliary extraction power of 80w for 10min, extracting with 50 deg.C water bath for 50min, filtering, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain tomato extract;
preparing an apple extract: washing and crushing apples to obtain apple liquid, wherein the mass ratio of the apple liquid to the apple liquid is 1:8, mixing the apple liquid with water, extracting with the aid of ultrasonic waves at the power of 80w for 10min, leaching with a water bath at 50 ℃ for 50min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain an apple extract;
mixing tomato extract and apple extract according to the weight ratio of 1:1, uniformly mixing the raw materials in a ratio to obtain an antioxidant;
s3: heating beeswax in the moistening paste A raw material in a water bath at 90 ℃ to melt, then mixing the melted beeswax, olive oil, an osmanthus fragrans extract, vitamins, an auxiliary agent and an antioxidant, heating the mixture in the water bath to 80 ℃, and uniformly stirring the mixture to obtain a mixed solution;
the preparation method of the sweet osmanthus extract comprises the following steps: according to the mass ratio of 1:10 mixing sweet osmanthus with distilled water, heating to 40 ℃, soaking for 6h, transferring into a distillation retort after soaking, distilling for 6h with steam, standing and layering distillate at room temperature to collect an oil layer, adding anhydrous sodium sulfate accounting for 10% of the oil layer by mass, standing and drying for 10h, filtering, and collecting filtrate to obtain the sweet osmanthus extract;
s4: cooling the mixed liquid obtained in the step S3 to 50 ℃, adding vitamin E, uniformly stirring, pouring into a moistening cream box, and solidifying to obtain moistening cream A;
step two: preparing moistening paste B:
s5: mixing Mentholum and Borneolum Syntheticum at a ratio of 1:1, mixing uniformly to obtain a freshener;
s6: heating beeswax in the moistening paste B raw material in a water bath at 90 ℃ to melt, then mixing the melted beeswax, the sweet osmanthus flower extract, the rosemary extract and the freshener, heating the mixture in the water bath to 80 ℃, and uniformly stirring the mixture to obtain a mixed solution;
the preparation method of the rosemary extract comprises the following steps: grinding rosemary into powder, soaking for 2 hours, and mixing the ground rosemary powder with the water according to a mass ratio of 1:10, mixing rosemary with water, decocting and extracting for 5 hours, taking filtrate, and then mixing the filtrate according to the mass ratio of 1:8 mixing the filter residue with water, decocting and extracting for 3h, taking filtrate, mixing the two filtrates, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain rosemary extract;
s7: and (5) cooling the mixed liquid obtained in the step (S6) to 50 ℃, adding vitamin E, uniformly stirring, pouring into another moistening paste box, and solidifying to obtain moistening paste B.
Comparative example
The invention provides a pure natural sweet osmanthus moistening cream which comprises moistening cream A and moistening cream B, wherein raw materials (in parts by weight) used by the moistening cream A comprise 60 parts of olive oil, 18 parts of beeswax, 30 parts of sweet osmanthus extract, 5 parts of vitamin E and 10 parts of antioxidant, and raw materials (in parts by weight) used by the moistening cream B comprise 60 parts of olive oil, 18 parts of beeswax, 10 parts of rosemary extract, 8 parts of freshener and 5 parts of vitamin E.
The antioxidant comprises a tomato extract and an apple extract, wherein the ratio of the tomato extract to the apple extract is 1:1.
the freshener comprises menthol and borneol, wherein the proportion of the menthol to the borneol is 1:1.
the method for preparing the pure natural sweet osmanthus moistening paste is the same as that in the embodiment 3.
The method comprises the following steps: preparing moistening paste A:
s1: preparing a tomato extract: cleaning and crushing tomatoes to obtain tomato pulp, wherein the mass ratio of the tomato pulp to the tomato pulp is 1: mixing tomato pulp with water, extracting with ultrasonic wave at power of 80w for 10min, extracting with 50 deg.C water bath for 50min, filtering, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain tomato extract;
preparing an apple extract: washing and crushing apples to obtain apple liquid, wherein the mass ratio of the apple liquid to the apple liquid is 1:8, mixing the apple liquid with water, extracting with the aid of ultrasonic waves at the power of 80w for 10min, leaching with a water bath at 50 ℃ for 50min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain an apple extract;
mixing tomato extract and apple extract according to the weight ratio of 1:1, uniformly mixing the raw materials in a ratio to obtain an antioxidant;
s2: heating beeswax in the moistening paste A raw material in a water bath at 90 ℃ to melt, then mixing the melted beeswax, olive oil, the sweet osmanthus flower extract, vitamins and an antioxidant, heating the mixture in the water bath to 80 ℃, and uniformly stirring the mixture to obtain a mixed solution;
the preparation method of the osmanthus extract comprises the following steps: according to the mass ratio of 1:10 mixing sweet osmanthus with distilled water, heating to 40 ℃, soaking for 6 hours, transferring into a distillation retort after soaking, distilling for 6 hours by using steam, standing and layering distillate at room temperature to collect an oil layer, adding anhydrous sodium sulfate accounting for 10 percent of the mass of the oil layer into the oil layer, standing and drying for 10 hours, filtering, and collecting filtrate to obtain a sweet osmanthus extract;
s3: cooling the mixed liquid obtained in the step S1 to 50 ℃, adding vitamin E, uniformly stirring, pouring into a moistening cream box, and solidifying to obtain moistening cream A;
1. skin care experiments:
experimental group 1: selecting 4 women between 25 and 35 years old, wherein the women 1 to 4 are oily skin, dry skin, mixed skin and sensitive skin respectively, and the facial skin of the 4 women has the problems of fine lines and large pores, cleaning the face in the morning and evening, applying the moistening cream A of the embodiment 1 for 20 minutes, applying the moistening cream B, and continuously using for one month;
experimental group 2: selecting 4 women between 25 and 35 years old, wherein the women 1 to 4 are oily skin, dry skin, mixed skin and sensitive skin respectively, and the facial skin of the 4 women has the problems of fine lines and large pores, cleaning the face in the morning and evening, applying the moistening cream A of the embodiment 2 for 20 minutes, applying the moistening cream B, and continuously using for one month;
experimental group 3: selecting 4 women between 25 and 35 years old, wherein the women 1 to 4 are oily skin, dry skin, mixed skin and sensitive skin respectively, and the facial skin of the 4 women has the problems of fine lines and large pores, cleaning the face in the morning and evening, applying the moistening cream A of the embodiment 3 for 20 minutes, applying the moistening cream B, and continuously using for one month;
control group 1: selecting 4 women between 25 and 35 years old, wherein the women 1 to 4 are respectively oily skin, dry skin, mixed skin and sensitive skin, and the facial skin of the 4 women has the problems of fine lines and large pores, smearing the moisturizing cream A of the comparative example 20 minutes after cleaning the face in the morning and evening, smearing the moisturizing cream B, and continuously using for one month;
control group 2: selecting 4 women between 25 and 35 years old, wherein the women 1 to 4 are oily skin, dry skin, mixed skin and sensitive skin respectively, and the facial skin of the 4 women has the problems of fine lines and large pores, and smearing the basic moistening cream purchased from the market after cleaning the face in the morning and evening for continuous use for one month;
women of experimental groups 1-3 and control groups 1-2 were tested for facial skin prior to use, and facial skin was again tested after one month of use:
selecting a test instrument: VISA digital skin analyzer, oumekang Y-B2006 skin moisture tester;
the evaluation grades are as follows:
level 1: the test result is improved by more than 50% compared with the test result before the test;
and 2, stage: the improvement degree of the test result is 20-50% compared with that before the test;
and 3, level: the improvement degree of the test result is 10-20% compared with that before the test;
4, level: the improvement degree of the test result is 0-10% compared with that before the test;
and 5, stage: the test results were not improved any more than before the test;
the rating results are shown in table 1:
TABLE 1
Compared with the experimental group 1-3 and the control group 2, the moisturizing cream disclosed by the invention is beneficial to improving the problems of fine lines and large pores, improving the skin fineness, and has the effect of beautifying, and is suitable for various skin types;
compared with the experimental group 3 and the control group 1, the auxiliary agent added in the invention is beneficial to the skin to absorb the effective components of the moistening cream, and the using effect is improved.
2. And (3) measuring the oxidation resistance:
95% ethanol is used for preparing a solution with the concentration of 0.04mg/ml DPPH, and 1ml of the moisturizing cream A of the embodiment 1-3 is taken as a sample 1-3 respectively.
1ml of sample and 3ml of DPPH solution are transferred into a test tube, mixed evenly, kept stand for 30min in the dark at room temperature, and then the absorbance value A1 is measured at 517 nm. The absorbance A0 was measured using 1ml of ethanol instead of the sample solution as a blank, and the absorbance A2 was measured using 3ml of ethanol instead of the DPPH solution. The clearance rate of DPPH free radicals is calculated by the formula:
DPPH radical clearance = (1- (A1-A2)/A0) × 100%;
the results are shown in Table 2:
TABLE 2
| DPPH radical scavenging Rate (%) | |
| Example 1 | 66.76 |
| Example 2 | 67.56 |
| Example 3 | 88.32 |
The data in the table show that the moisturizing cream has certain scavenging capacity for hydroxyl free radicals, the effect is correspondingly enhanced along with the increase of the using amount, and the moisturizing cream has stronger antioxidant capacity.
3. And (3) determining the bacteriostatic effect:
100 g of moisturizing cream A and moisturizing cream B in examples 1-3 are respectively taken, and then bacteria liquid containing mould is added, wherein the content of the mould in each gram of sample is 1 multiplied by 10 6 CFU/g, then placing at 25 ℃, sampling and analyzing after 30 days, wherein the mould content in the sample is 0. The moisturizing cream disclosed by the invention is free of other preservatives, is purely natural in components, and is safe and non-toxic.
While certain exemplary embodiments of the present invention have been described above by way of illustration only, it will be apparent to those of ordinary skill in the art that the described embodiments may be modified in various different ways without departing from the spirit and scope of the present invention. Accordingly, the foregoing description is illustrative in nature and is not to be construed as limiting the scope of the invention as claimed.
Claims (10)
1. A pure natural sweet osmanthus moistening paste is characterized in that: the nourishing cream comprises a nourishing cream A and a nourishing cream B, wherein raw materials (by weight part) used by the nourishing cream A comprise 40-60 parts of olive oil, 10-18 parts of beeswax, 10-30 parts of sweet osmanthus flower extract, 2-5 parts of vitamin E, 2-10 parts of an auxiliary agent and 2-10 parts of an antioxidant, and raw materials (by weight part) used by the nourishing cream B comprise 40-60 parts of olive oil, 10-18 parts of beeswax, 6-10 parts of sweet osmanthus flower extract, 2-10 parts of rosemary extract, 1-8 parts of a freshener and 2-5 parts of vitamin E.
2. The pure natural sweet osmanthus moistening paste according to claim 1, which is characterized in that: the auxiliary agent comprises houttuynia extract, ginkgo leaf extract and ginger extract, wherein the ratio of the houttuynia extract to the ginkgo leaf extract to the ginger extract is 1:1:1.
3. the pure natural osmanthus moisturizing cream as recited in claim 1, wherein: the antioxidant comprises a tomato extract and an apple extract, wherein the ratio of the tomato extract to the apple extract is 1:1.
4. the pure natural sweet osmanthus moistening paste according to claim 1, which is characterized in that: the freshener comprises menthol and borneol, wherein the proportion of the menthol to the borneol is 1:1.
5. a method for preparing the pure natural sweet osmanthus moistening paste as defined in any one of claims 1 to 4, which is characterized by comprising the following steps: the method comprises the following specific steps:
the method comprises the following steps: preparing moistening paste A:
s1: mixing herba Houttuyniae extract, folium Ginkgo extract, and rhizoma Zingiberis recens extract at a ratio of 1:1:1, uniformly mixing to obtain an auxiliary agent;
s2: mixing tomato extract and apple extract according to the weight ratio of 1:1, uniformly mixing to obtain an antioxidant;
s3: melting Cera flava in moistening paste A in water bath at 80-90 deg.C, mixing the melted Cera flava, oleum Olivarum, flos Osmanthi Fragrantis extract, vitamins, adjuvants, and antioxidant, heating in water bath to 70-80 deg.C, and stirring to obtain mixed solution;
s4: cooling the mixed liquid obtained in the step S3 to 40-50 ℃, adding vitamin E, uniformly stirring, pouring into a moistening cream box, and solidifying to obtain moistening cream A;
step two: preparing moistening paste B:
s5: mixing Mentholum and Borneolum Syntheticum at a ratio of 1:1, uniformly mixing the components in a ratio to obtain a freshener;
s6: melting Cera flava in the moistening paste B in 80-90 deg.C water bath, mixing the melted Cera flava, flos Osmanthi Fragrantis extract, herba Rosmarini officinalis extract and algefacient, heating to 70-80 deg.C in water bath, and stirring to obtain mixed solution;
s7: and (4) cooling the mixed liquid obtained in the step (S6) to 40-50 ℃, adding vitamin E, uniformly stirring, and pouring into another moistening cream box to solidify to obtain moistening cream B.
6. The preparation method of the pure natural sweet osmanthus moistening paste according to claim 5, characterized by comprising the following steps: the preparation method of the sweet osmanthus extract comprises the following steps: according to the mass ratio of 1:10 mixing sweet osmanthus with distilled water, heating to 30-40 ℃, soaking for 3-6h, transferring into a distillation retort after soaking, distilling with steam for 4-6h, standing and layering distillate at room temperature to collect an oil layer, adding anhydrous sodium sulfate accounting for 5-10% of the mass of the oil layer into the oil layer, standing and drying for 8-10h, filtering, and collecting filtrate to obtain the sweet osmanthus extract.
7. The preparation method of the pure natural sweet osmanthus moistening paste according to claim 5, wherein the preparation method comprises the following steps: the preparation method of the houttuynia cordata extract comprises the following steps: cleaning and chopping houttuynia cordata, soaking for 1-2h, and mixing the raw materials in a mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2-4h, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:7, mixing the filter residue with water, decocting and extracting for 1-3h, taking the filtrate, and mixing the filtrate according to a mass ratio of 1:5 mixing the filter residue with water, decocting and extracting for 0.5-2h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain soft extract, and spray drying to obtain herba Houttuyniae extract;
the preparation method of the ginkgo leaf extract comprises the following steps: cleaning and chopping ginkgo leaves, soaking for 1-2h, and mixing the ginkgo leaves with the water according to a mass ratio of 1:8, mixing rosemary with water, decocting and extracting for 2-4h, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:6, mixing the filter residue with water, decocting and extracting for 1-3h, taking the filtrate, and mixing the filtrate according to the mass ratio of 1:5 mixing the filter residue with water, decocting and extracting for 0.5-2h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain a thick paste, and spray drying to obtain the ginkgo leaf extract;
the preparation method of the ginger extract comprises the following steps: cleaning and chopping ginger, and soaking for 1-2h according to a mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2-4h, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:8, mixing the filter residue with water, decocting and extracting for 1-3h, taking the filtrate, and mixing the filtrate according to a mass ratio of 1:6 mixing the filter residue with water, decocting and extracting for 0.5-2h, taking the filtrate, combining the three filtrates, concentrating under reduced pressure to obtain thick paste, and spray drying to obtain the houttuynia cordata extract.
8. The preparation method of the pure natural sweet osmanthus moistening paste according to claim 5, wherein the preparation method comprises the following steps: the preparation method of the tomato extract comprises the following steps: cleaning and crushing tomatoes to obtain tomato pulp, wherein the mass ratio of the tomato pulp to the tomato pulp is 1:5 mixing the tomato serum with water, extracting with ultrasonic wave auxiliary extraction power of 60-80w for 5-10min, extracting with 40-50 deg.C water bath for 30-50min, filtering, concentrating the filtrate under reduced pressure to obtain soft extract, and spray drying to obtain tomato extract.
9. The preparation method of the pure natural sweet osmanthus moistening paste according to claim 5, wherein the preparation method comprises the following steps: the preparation method of the apple extract comprises the following steps: washing and crushing apples to obtain apple liquid, wherein the mass ratio of the apple liquid to the apple liquid is 1:8 mixing apple liquid with water, extracting with ultrasonic assistance, wherein the ultrasonic assistance extraction power is 60-80w, the time is 5-10min, extracting with 40-50 ℃ water bath for 30-50min, filtering to obtain filtrate, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain the apple extract.
10. The preparation method of the pure natural sweet osmanthus moistening paste according to claim 5, characterized by comprising the following steps: the preparation method of the rosemary extract comprises the following steps: grinding rosemary into powder, and soaking for 0.5-2h according to the mass ratio of 1:10 mixing rosemary with water, decocting and extracting for 2-5h, taking filtrate, and then mixing the filtrate with the water according to a mass ratio of 1:8 mixing the filter residue with water, decocting and extracting for 1-3h, taking the filtrate, mixing the two filtrates, concentrating the filtrate under reduced pressure to obtain thick paste, and spray drying to obtain the rosemary extract.
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| JP2014114235A (en) * | 2012-12-10 | 2014-06-26 | Maruzen Pharmaceut Co Ltd | Melanogenesis inhibitor and collagen production promoter |
| CN104146913A (en) * | 2014-08-20 | 2014-11-19 | 陕西知医堂药业有限公司 | Lithospermum paste and preparation method thereof |
| CN107982114A (en) * | 2016-10-25 | 2018-05-04 | 赖婷婷 | A kind of sweet osmanthus hand lotion and preparation method thereof |
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Denomination of invention: A pure natural osmanthus moisturizing cream and its preparation method Granted publication date: 20231024 Pledgee: Bank of China Limited by Share Ltd. Guilin branch Pledgor: GUILIN FOUR SEASON SUNSHINE F&F Co.,Ltd. Registration number: Y2024450000002 |
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