CN112237561B - Pure natural multifunctional compound essential oil and preparation method thereof - Google Patents
Pure natural multifunctional compound essential oil and preparation method thereof Download PDFInfo
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- CN112237561B CN112237561B CN202011181445.6A CN202011181445A CN112237561B CN 112237561 B CN112237561 B CN 112237561B CN 202011181445 A CN202011181445 A CN 202011181445A CN 112237561 B CN112237561 B CN 112237561B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9761—Cupressaceae [Cypress family], e.g. juniper or cypress
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention discloses a pure natural multifunctional compound essential oil and a preparation method thereof, wherein the pure natural multifunctional compound essential oil comprises the following raw materials: rosemary, clary sage, grapefruit, black pepper, tangerine, jasmine, juniper, Italian permanent flower, lemon, cypress. The essential oil has the effects of accelerating circulation and metabolism, compacting and firming skin, cleaning blood and removing dampness. By the method, the prepared essential oil has the advantages that the components are mutually synergistic, the penetrating power is strong, and the effect is better compared with the existing essential oil; the essential oil of the present invention has a pleasant aromatic odor; when in use, the essential oil has layering fragrance and long retention time.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to pure natural multifunctional compound essential oil and a preparation method thereof.
Background
Essential oils in a broad sense are generic terms referring to volatile material-containing products obtained by processing and extraction from spice plants or secretagogues. However, the essential oil used in daily life is a product containing an aromatic substance extracted from an aromatic plant by steam distillation, or squeezing, or cold milling, or dry distillation, and these products are mostly in a liquid state at normal temperature, and only a few varieties are in a solid state.
The essential oil is extracted from leaves, flowers, seeds, fruits, roots, barks, resins, hearts and other parts of plants by steam distillation, cold pressing, fat absorption and solvent extraction, and has high-concentration fragrance and volatility. In addition to essential oils extracted from a part of a plant, some plants extract essential oils from several parts, for example, bitter oranges extract essential oils from 3 parts of the buds, leaves and fruits.
At present, the single-component essential oil is an essence component extracted from the whole plant or a certain part of a plant, has high purity, and each plant essential oil has a chemical structure to determine the fragrance, color and fluidity of the plant essential oil and the mode of the system operation, so that each plant essential oil has a set of special functional characteristics. However, the single-component essential oil can be extracted by a large amount of plant materials, so that the cost is extremely high, the selling price is high, the single-component essential oil has single component, the single-component essential oil can be used on the skin after being fully diluted, the single-component essential oil with the concentration of 100 percent is very dangerous, and the single-component essential oil is volatile and corrosive, and the like, and needs to be sealed and stored by a lightproof glass bottle, so the problems of high selling price, single effect, inconvenience in use, unsafe use and the like exist; the compound essential oil is prepared according to different characteristics of various plant essential oils, the compound essential oil is prepared according to a certain proportion for use, the effect of the single-component essential oil can be exerted to the maximum, and in the compounding process of the essential oil, not only the absorption effect of the essential oil but also the fragrance harmony and the compatibility of the essential oil are considered. However, the existing compound essential oil is only prepared by simply mixing single-component essential oil, which is not beneficial to preparing the compound essential oil with better effect and unique fragrance.
Therefore, the compound essential oil with multiple functions, good efficacy and unique fragrance is a problem which needs to be solved urgently by the technical personnel in the field.
Disclosure of Invention
In view of the above, the invention provides a pure natural multifunctional compound essential oil and a preparation method thereof, and the essential oil has the effects of accelerating circulation and metabolism, compacting and firming skin, and cleaning blood and removing dampness. By the method, all components in the prepared essential oil are mutually synergistic, the penetrating power is strong, and the essential oil has a better effect compared with the existing essential oil; the essential oil of the invention has pleasant aromatic odor; when in use, the essential oil has layering fragrance and long retention time.
In order to achieve the purpose, the invention adopts the following technical scheme:
a pure natural multifunctional compound essential oil comprises the following raw materials: rosemary essential oil, clary sage, grapefruit, black pepper, tangerine, jasmine, juniper, Italian permanent flower, lemon, cypress.
The essential oil provided by the invention is extracted from plants containing natural active ingredients, the formula proportion is scientific, any artificially synthesized component is not added, the safety is realized, no toxic or side effect is caused, the raw materials are mutually cooperated, supplemented and enhanced, and the prepared compound essential oil is multifunctional; in addition, the essential oil provided by the invention has high safety, pleasant and aromatic smell, good stability, convenient use and wide application value.
Preferably, the feed comprises the following raw materials in parts by weight: 5-10 parts of rosemary, 5-10 parts of clary sage, 1-3 parts of grapefruit, 7-10 parts of black pepper, 3-6 parts of tangerine, 5-10 parts of jasmine, 2-5 parts of juniper, 1-5 parts of Italian permanent flower, 3-5 parts of lemon and 4-8 parts of cypress.
Preferably, the feed comprises the following raw materials in parts by weight: 8-10 parts of rosemary, 8-10 parts of clary sage, 1-3 parts of grapefruit, 8-10 parts of black pepper, 4-6 parts of tangerine, 5-8 parts of jasmine, 2-4 parts of juniper, 1-3 parts of Italian permanent flower, 3-5 parts of lemon and 4-6 parts of cypress.
Preferably, the feed comprises the following raw materials in parts by weight: 9 parts of rosemary, 9 parts of clary sage, 2 parts of grapefruit, 9 parts of black pepper, 5 parts of tangerine, 7 parts of jasmine, 3 parts of juniper, 2 parts of Italian permanent flower, 4 parts of lemon and 5 parts of cypress.
A large number of experiments show that the raw materials adopted by the invention can achieve a synergistic effect, and the obtained essential oil has strong penetrating power and better effect compared with the existing essential oil.
The preparation method of the pure natural multifunctional compound essential oil specifically comprises the following steps:
(1) weighing rosemary, clary sage, grapefruit, black pepper, tangerine, jasmine, juniper, Italian permanent flower, lemon and cypress in parts by weight;
(2) mixing and crushing the rosemary, the clary sage, the black pepper, the juniper and the cypress, extracting by adopting supercritical carbon dioxide, and refining by using a molecular distillation method to obtain first essential oil;
(3) crushing the grapefruit, the tangerine, the jasmine parviflora, the Italian permanent flower and the lemon, then placing the crushed grapefruit, the tangerine, the jasmine parviflora and the lemon in a squeezer for squeezing, filtering and collecting crude oil, and refining by using a molecular distillation method to obtain basic essential oil;
(4) and uniformly mixing the first essential oil and the base oil, and standing to obtain the multifunctional compound essential oil.
According to the difference between raw materials, the invention respectively adopts supercritical CO2The extraction technology and the squeezing process furthest extract effective substances in the raw materials, and the invention can directly mix the raw materials and then extract the effective substances by supercritical carbon dioxide by the proportion of partial raw materials, does not need to extract and mix the raw materials as much as possible, reduces the process steps and has remarkable progress.
Preferably, the supercritical carbon dioxide extraction in step (2) is carried out at 40-45 deg.C under 18-23MPa for 1-3h, and the flow rate of carbon dioxide is 15-20 kg/h.
Preferably, the feeding temperature of the molecular distillation method in the step (2) and the step (3) is 35-40 ℃, the sample injection speed is 500mL/h, the first-stage evaporation temperature is 105-110 ℃, and the second-stage evaporation temperature is 60-65 ℃.
Preferably, the standing time in the step (4) is 5-10 min.
According to the technical scheme, compared with the prior art, the invention has the following beneficial effects: the invention provides a pure natural multifunctional compound essential oil and a preparation method thereof. By the method, all components in the prepared essential oil are mutually synergistic, the penetrating power is strong, and the essential oil has a better effect compared with the existing essential oil; the essential oil of the present invention has a pleasant aromatic odor; when in use, the essential oil has layering fragrance and long retention time.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
A preparation method of pure natural multifunctional compound essential oil specifically comprises the following steps:
(1) weighing the following raw materials in parts by weight: 5 parts of rosemary, 5 parts of clary sage, 1 part of grapefruit, 7 parts of black pepper, 3 parts of tangerine, 5 parts of jasmine, 2 parts of juniper, 1 part of Italian permanent flower, 3 parts of lemon and 4 parts of cypress;
(2) mixing and crushing rosemary, clary sage, black pepper, juniper and cypress, extracting by supercritical carbon dioxide, and refining by a molecular distillation method to obtain first essential oil; extracting with supercritical carbon dioxide at 40-45 deg.C under 18-23MPa for 1-3 hr at flow rate of 15-20 kg/hr; the feeding temperature of the molecular distillation method is 35-40 ℃, the sample injection speed is 500mL/h, the first-stage evaporation temperature is 105-110 ℃, and the second-stage evaporation temperature is 60-65 DEG C
(3) Crushing grapefruit, tangerine, jasmine, Italian permanent flower and lemon, then placing the crushed grapefruit, tangerine, jasmine, Italian permanent flower and lemon into a squeezer for squeezing, filtering and collecting crude oil, and refining by using a molecular distillation method to obtain basic essential oil; the feeding temperature of the molecular distillation method is 35-40 ℃, the sample injection speed is 450-;
(4) mixing the first essential oil and the base oil uniformly, and standing for 5-10min to obtain the multifunctional compound essential oil.
Example 2
A preparation method of pure natural multifunctional compound essential oil specifically comprises the following steps:
(1) weighing the following raw materials in parts by weight: 10 parts of rosemary, 10 parts of clary sage, 3 parts of grapefruit, 10 parts of black pepper, 6 parts of tangerine, 10 parts of jasmine, 5 parts of juniper, 5 parts of Italian permanent flower, 5 parts of lemon and 8 parts of cypress;
(2) mixing and crushing rosemary, clary sage, black pepper, juniper and cypress, extracting by supercritical carbon dioxide, and refining by a molecular distillation method to obtain first essential oil; extracting with supercritical carbon dioxide at 40-45 deg.C under 18-23MPa for 1-3 hr at flow rate of 15-20 kg/hr; the feeding temperature of the molecular distillation method is 35-40 ℃, the sample injection speed is 500mL/h, the first-stage evaporation temperature is 105-110 ℃, and the second-stage evaporation temperature is 60-65 DEG C
(3) Crushing grapefruit, tangerine, jasmine, Italian permanent flower and lemon, then placing the crushed grapefruit, tangerine, jasmine, Italian permanent flower and lemon into a squeezer for squeezing, filtering and collecting crude oil, and refining by using a molecular distillation method to obtain basic essential oil; the feeding temperature of the molecular distillation method is 35-40 ℃, the sample injection speed is 450-;
(4) mixing the first essential oil and the base oil uniformly, and standing for 5-10min to obtain the multifunctional compound essential oil.
Example 3
A preparation method of pure natural multifunctional compound essential oil specifically comprises the following steps:
(1) weighing the following raw materials in parts by weight: 5 parts of rosemary, 10 parts of clary sage, 2 parts of grapefruit, 8 parts of black pepper, 5 parts of tangerine, 10 parts of jasmine, 2 parts of juniper, 1 part of Italian permanent flower, 3 parts of lemon and 4 parts of cypress;
(2) mixing and crushing rosemary, clary sage, black pepper, juniper and cypress, extracting by supercritical carbon dioxide, and refining by a molecular distillation method to obtain first essential oil; extracting with supercritical carbon dioxide at 40-45 deg.C under 18-23MPa for 1-3 hr at flow rate of 15-20 kg/hr; the feeding temperature of the molecular distillation method is 35-40 ℃, the sample injection speed is 500mL/h, the first-stage evaporation temperature is 105-110 ℃, and the second-stage evaporation temperature is 60-65 DEG C
(3) Crushing grapefruit, tangerine, jasmine, Italian permanent flower and lemon, then placing the crushed grapefruit, tangerine, jasmine, Italian permanent flower and lemon into a squeezer for squeezing, filtering and collecting crude oil, and refining by using a molecular distillation method to obtain basic essential oil; the feeding temperature of the molecular distillation method is 35-40 ℃, the sample injection speed is 500mL/h, the first-stage evaporation temperature is 105-110 ℃, and the second-stage evaporation temperature is 60-65 ℃;
(4) mixing the first essential oil and the base oil uniformly, and standing for 5-10min to obtain multifunctional compound essential oil.
Example 4
A preparation method of pure natural multifunctional compound essential oil specifically comprises the following steps:
(1) weighing the following raw materials in parts by weight: 8 parts of rosemary, 8 parts of clary sage, 1 part of grapefruit, 8 parts of black pepper, 4 parts of tangerine, 5 parts of jasmine, 2 parts of juniper, 1 part of Italian permanent flower, 3 parts of lemon and 4 parts of cypress;
(2) mixing and crushing rosemary, clary sage, black pepper, juniper and cypress, extracting by supercritical carbon dioxide, and refining by a molecular distillation method to obtain first essential oil; extracting with supercritical carbon dioxide at 40-45 deg.C under 18-23MPa for 1-3 hr at flow rate of 15-20 kg/hr; the feeding temperature of the molecular distillation method is 35-40 ℃, the sample injection speed is 500mL/h, the first-stage evaporation temperature is 105-110 ℃, and the second-stage evaporation temperature is 60-65 DEG C
(3) Crushing grapefruit, tangerine, jasmine, Italian permanent flower and lemon, then placing the crushed grapefruit, tangerine, jasmine, Italian permanent flower and lemon into a squeezer for squeezing, filtering and collecting crude oil, and refining by using a molecular distillation method to obtain basic essential oil; the feeding temperature of the molecular distillation method is 35-40 ℃, the sample injection speed is 450-;
(4) mixing the first essential oil and the base oil uniformly, and standing for 5-10min to obtain the multifunctional compound essential oil.
Example 5
A preparation method of pure natural multifunctional compound essential oil specifically comprises the following steps:
(1) weighing the following raw materials in parts by weight: 9 parts of rosemary, 9 parts of clary sage, 2 parts of grapefruit, 9 parts of black pepper, 5 parts of tangerine, 7 parts of jasmine, 3 parts of juniper, 2 parts of Italian permanent flower, 4 parts of lemon and 5 parts of cypress;
(2) mixing and crushing rosemary, clary sage, black pepper, juniper and cypress, extracting by supercritical carbon dioxide, and refining by a molecular distillation method to obtain first essential oil; extracting with supercritical carbon dioxide at 40-45 deg.C under 18-23MPa for 1-3 hr at flow rate of 15-20 kg/hr; the feeding temperature of the molecular distillation method is 35-40 ℃, the sample injection speed is 500mL/h, the first-stage evaporation temperature is 105-110 ℃, and the second-stage evaporation temperature is 60-65 DEG C
(3) Crushing grapefruit, tangerine, jasmine, Italian permanent flower and lemon, then placing the crushed grapefruit, tangerine, jasmine, Italian permanent flower and lemon into a squeezer to squeeze, filtering and collecting crude oil, and refining by using a molecular distillation method to obtain basic essential oil; the feeding temperature of the molecular distillation method is 35-40 ℃, the sample injection speed is 450-;
(4) mixing the first essential oil and the base oil uniformly, and standing for 5-10min to obtain multifunctional compound essential oil.
Application example
240 freckle volunteers were recruited, and each patient did not use facial melanin accumulation and pigmentation to the extent that they were accompanied by freckle sores. Each patient was divided into 4 groups of 60 patients each. The first group was applied with the compound essential oil of example 5 of the present invention, the second group was applied with the base oil prepared in step (3) of example 5 of the present invention (control group 1), the third group was applied with the first essential oil prepared in step (2) of example 5 of the present invention (control group 2), and the fourth group was applied with the commercial freckle-removing essential oil (control group 3). The application method comprises applying the composition to the affected part uniformly 2 times a day (once in the morning and once in the evening); the therapeutic effect was observed on trial days 5, 10 and 15, respectively. With the double-blind method, no skin irritation or allergy appeared, as shown in table 1. The curative effect is judged as follows: and (3) curing: the symptoms such as facial melanin pigmentation disappear, and the skin recovers to be healthy. Improvement: the facial melanin pigmentation symptom is improved, and the statistical significance P is less than 0.05. The effect is shown: facial melanin has some improvement, but no statistical significance, P > 0.05; and (4) invalidation: those with no change in symptoms.
Table 1 example 1 treatment
As can be seen from the table 1, compared with the spot removing products sold in the market, the essential oil has obvious curative effect on freckles and has higher efficiency; the control groups 2 and 3 have poor treatment effect compared with the compound essential oil, and the raw materials have a synergistic effect according to data, so that the compound essential oil has remarkable progress.
The compound essential oil has the effects of diminishing inflammation, resisting bacteria and oxidation, eliminating color spots, reducing wrinkles, enhancing immunity, repairing cells and the like. The multifunctional compound essential oil can be eaten (not more than 15 drops at a time, can be added into other foods), can be smeared, and can be used as oil for scraping therapy and skin care.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.
Claims (4)
1. The pure natural multifunctional compound essential oil is characterized by comprising the following raw materials in parts by weight: 5-10 parts of rosemary, 5-10 parts of clary sage, 1-3 parts of grapefruit, 7-10 parts of black pepper, 3-6 parts of tangerine, 5-10 parts of jasmine, 2-5 parts of juniper, 1-5 parts of Italian permanent flower, 3-5 parts of lemon and 4-8 parts of cypress;
the preparation method of the pure natural multifunctional compound essential oil specifically comprises the following steps:
(1) weighing rosemary, clary sage, grapefruit, black pepper, tangerine, jasmine, juniper, Italian permanent flower, lemon and cypress according to parts by weight;
(2) mixing and crushing the rosemary, the clary sage, the black pepper, the juniper and the cypress, extracting by adopting supercritical carbon dioxide, and refining by using a molecular distillation method to obtain first essential oil; the supercritical carbon dioxide extraction temperature is 40-45 ℃, the pressure is 18-23MPa, the time is 1-3h, and the flow rate of carbon dioxide is 15-20 kg/h;
(3) crushing the grapefruit, the tangerine, the jasmine flower, the Italian permanent flower and the lemon, then pressing in a squeezer, filtering and collecting crude oil, and refining by using a molecular distillation method to obtain basic essential oil;
(4) uniformly mixing the first essential oil and the base essential oil, and standing to obtain multifunctional compound essential oil;
the feeding temperature of the molecular distillation method in the step (2) and the step (3) is 35-40 ℃, the sample injection speed is 500mL/h, the first-stage evaporation temperature is 105-110 ℃, and the second-stage evaporation temperature is 60-65 ℃.
2. The pure natural multifunctional compound essential oil according to claim 1, which is characterized by comprising the following raw materials in parts by weight: 8-10 parts of rosemary, 8-10 parts of clary sage, 1-3 parts of grapefruit, 8-10 parts of black pepper, 4-6 parts of tangerine, 5-8 parts of jasmine, 2-4 parts of juniper, 1-3 parts of Italian permanent flower, 3-5 parts of lemon and 4-6 parts of cypress.
3. The pure natural multifunctional compound essential oil according to claim 1, which is characterized by comprising the following raw materials in parts by weight: 9 parts of rosemary, 9 parts of clary sage, 2 parts of grapefruit, 9 parts of black pepper, 5 parts of tangerine, 7 parts of jasmine, 3 parts of juniper, 2 parts of Italian permanent flower, 4 parts of lemon and 5 parts of cypress.
4. The pure natural multifunctional compound essential oil according to claim 1, wherein the standing time in the step (4) is 5-10 min.
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