CN112741786A

CN112741786A - Various herbal skin-care essential oil

Info

Publication number: CN112741786A
Application number: CN202110184211.5A
Authority: CN
Inventors: 季汉钱
Original assignee: Shanghai Ting Hui Hui Biotechnology Co ltd
Current assignee: Shanghai Ting Hui Hui Biotechnology Co ltd
Priority date: 2021-02-08
Filing date: 2021-02-08
Publication date: 2021-05-04

Abstract

The invention discloses various herbal refreshing skin care essential oils which comprise the following raw materials in parts by weight: 20-30 parts of base oil, 5-9 parts of lavender, 5-9 parts of mint, 5-9 parts of eucalyptus, 5-9 parts of tea tree, 5-9 parts of rosemary, 5-9 parts of wintergreen, 5-9 parts of rose, 5-9 parts of ylang-ylang, 5-9 parts of lemon grass, 6-10 parts of sweet almond oil, 6-10 parts of jojoba oil, 6-8 parts of organic solvent, 8-12 parts of humectant, 10-14 parts of sodium hyaluronate, 4-8 parts of fixative, 6-12 parts of polydimethylsiloxane, 4-8 parts of antioxidant, 2-8 parts of dipotassium glycyrrhizinate, 8-14 parts of madecassoside and 8-16 parts of vitamin E10. The herbal refreshing skin care essential oil can play roles in sterilizing and diminishing inflammation, conditioning skin inflammation (such as skin infection, pox, dermatophytosis, skin itch and mosquito and insect bite), and refreshing and restoring consciousness by adding the herbal essential oil: the massage on temple has effects of refreshing brain, preventing and treating driving, meeting, and learning, and can be used for dredging channels and collaterals.

Description

Various herbal skin-care essential oil

Technical Field

The invention relates to the technical field of essential oil, in particular to various herbal refreshing skin care essential oil.

Background

In a broad sense, the essential oil is a generic term of volatile aromatic substances obtained by processing and extracting aromatic plants or odoriferous animals, and generally, the essential oil is a volatile aromatic substance extracted from flowers, leaves, roots, seeds, fruits, barks, resins, hearts and the like of the plants by a steam distillation method, a cold pressing method, a liposuction method or a solvent extraction method, the essential oil is diluted (compound essential oil) and undiluted (single essential oil) such as cactus seed oil, the volatility of the essential oil is strong, the essential oil is rapidly volatilized once contacting air, so the essential oil must be stored in a sealable dark bottle, the essential oil is a substance extracted from leaves, flowers, seeds, fruits, roots, barks, resins, hearts and the like of the plants by the steam distillation method, the cold pressing method, the liposuction method and the solvent extraction method, and has high-concentration aroma and volatility, except that some parts of the plants can extract essential oil, some plants can extract essential oil from a plurality of parts, the essential oil skin care is from France, Europe is aroused, the two years of the essential oil skin care are popular, but many people do not know about the essential oil skin care, the face cleaning with the essential oil can deeply remove dirt in pores, promote blood circulation of facial skin, discharge waste toxin in vivo, make the face glossy, and achieve the effects of cleaning, moisturizing and tendering care.

The existing more skin care essential oil is greasy in use feeling, easy to cause acne or allergy, single in efficacy, generally capable of achieving the effects of moisturizing and moistening, and free of other effects, and when the essential oil is processed, more chemical components are added, so that the burden of skin can be increased.

Disclosure of Invention

Aiming at the defects of the prior art, the invention provides various herbal refreshing skin-care essential oils, and solves the problems that the existing more skin-care essential oils are greasy in use feeling, easy to cause acne or allergy, single in efficacy, generally achieve the effects of moisturizing and moistening, have no other efficacy, and increase the burden of skin due to more chemical components added during processing of the essential oils.

In order to achieve the purpose, the invention is realized by the following technical scheme: the herbal skin care essential oil comprises the following raw materials in parts by weight: 20-30 parts of base oil, 5-9 parts of lavender, 5-9 parts of mint, 5-9 parts of eucalyptus, 5-9 parts of tea tree, 5-9 parts of rosemary, 5-9 parts of wintergreen, 5-9 parts of rose, 5-9 parts of ylang-ylang, 5-9 parts of lemon grass, 6-10 parts of sweet almond oil, 6-10 parts of jojoba oil, 6-8 parts of organic solvent, 8-12 parts of humectant, 10-14 parts of sodium hyaluronate, 4-8 parts of fixative, 6-12 parts of polydimethylsiloxane, 4-8 parts of antioxidant, 2-8 parts of dipotassium glycyrrhizinate, 8-14 parts of madecassoside and 10-16 parts of vitamin E.

Preferably, the raw materials comprise the following components: 25 parts of base oil, 7 parts of lavender, 7 parts of mint, 7 parts of eucalyptus, 7 parts of tea tree, 7 parts of rosemary, 7 parts of wintergreen, 7 parts of rose, 7 parts of ylang, 7 parts of lemon grass, 8 parts of sweet almond oil, 8 parts of jojoba oil, 7 parts of organic solvent, 10 parts of humectant, 12 parts of sodium hyaluronate, 6 parts of fixative, 9 parts of polydimethylsiloxane, 6 parts of antioxidant, 5 parts of dipotassium glycyrrhizinate, 11 parts of madecassoside and 13 parts of vitamin E.

Preferably, the raw materials comprise the following components: 30 parts of base oil, 9 parts of lavender, 9 parts of mint, 9 parts of eucalyptus, 9 parts of tea tree, 9 parts of rosemary, 9 parts of wintergreen, 9 parts of rose, 9 parts of ylang, 9 parts of lemon grass, 10 parts of sweet almond oil, 10 parts of jojoba oil, 8 parts of organic solvent, 12 parts of humectant, 14 parts of sodium hyaluronate, 8 parts of fixative, 12 parts of polydimethylsiloxane, 8 parts of antioxidant, 8 parts of dipotassium glycyrrhizinate, 14 parts of madecassoside and 16 parts of vitamin E.

Preferably, the raw materials comprise the following components: 20 parts of base oil, 5 parts of lavender, 5 parts of mint, 5 parts of eucalyptus, 5 parts of tea tree, 5 parts of rosemary, 5 parts of wintergreen, 5 parts of rose, 5 parts of ylang, 5 parts of lemon grass, 6 parts of sweet almond oil, 6 parts of jojoba oil, 6 parts of organic solvent, 8 parts of humectant, 10 parts of sodium hyaluronate, 4 parts of fixative, 6 parts of polydimethylsiloxane, 4 parts of antioxidant, 2 parts of dipotassium glycyrrhizinate, 8 parts of madecassoside and 10 parts of vitamin E.

Preferably, the base oil is one or a mixture of more of seabuckthorn fruit oil, grape seed oil, wheat germ oil, olive oil and jojoba oil, the organic solvent is one or a mixture of two or more of ethanol, ethyl acetate and cyclohexane, the fixative is musk, benzoin grease and coumarin, and the weight ratio of the musk, the benzoin grease and the coumarin is 2:1: 3.

Preferably, the preparation method of the multiple herbal refreshing skin care essential oils specifically comprises the following steps:

s1, extraction of herbaceous plants: (1) washing and drying lavender, crushing the lavender into coarse powder passing through a 10-20-mesh sieve, performing supercritical CO2 fluid extraction, wherein the weight-volume ratio of liquid to material is 1:10-20, the weight-volume ratio refers to that solid is counted by g, liquid is counted by mL, the following is the same, the extraction temperature is 42-50 ℃, the extraction pressure is 20-25MPa, the separation temperature is 50-60 ℃, the separation pressure is 4.5-5.5MPa, the extraction time is 1.5-2.5 hours, so that lavender essential oil is obtained, (2) washing and drying mint, crushing the mint into coarse powder passing through the 10-20-mesh sieve, performing supercritical CO2 fluid extraction, the weight-volume ratio of liquid to material is 1:10-20, the weight-volume ratio refers to that solid is counted by g, liquid is counted by mL, the following is the same, the extraction temperature is 42-50 ℃, the extraction pressure is 20-25MPa, the separation temperature is 50-60 ℃, and the separation, extracting for 1.5-2.5 hours to obtain mint essential oil, (3) cleaning and drying Eucalyptus globulus Labill, crushing into 10-20-mesh coarse powder, performing supercritical CO2 fluid extraction, wherein the weight-volume ratio of liquid materials is 1:10-20, the weight-volume ratio refers to that solid is measured in g, liquid is measured in mL, the extraction temperature is 42-50 ℃, the extraction pressure is 20-25MPa, the separation temperature is 50-60 ℃, the separation pressure is 4.5-5.5MPa, and the extraction time is 1.5-2.5 hours to obtain the eucalyptus globulus Labill essential oil, (4) selecting the initial tea tree essential oil just obtained by squeezing, putting the tea tree essential oil into a percolation cylinder, heating and stirring by taking an ethanol water solution as a solvent, filtering after extraction is finished to obtain an extracting solution, adding an ethanol solution with the volume fraction of 80-90% for microwave extraction, putting the extracting solution into a 5-DEG space environment for refrigerating for 2-3 hours, then oil-water separation is carried out, then micro-membrane filtration is carried out, and reduced pressure concentration is carried out to obtain finished tea tree essential oil, (5) rosemary is cleaned and dried, and is crushed into coarse powder which is sieved by a sieve with 10-20 meshes, supercritical CO2 fluid extraction is carried out, the weight-volume ratio of liquid materials is 1:10-20, the weight-volume ratio refers to that solid is counted by g, liquid is counted by mL, the same is carried out, the extraction temperature is 42-50 ℃, the extraction pressure is 20-25MPa, the separation temperature is 50-60 ℃, the separation pressure is 4.5-5.5MPa, the extraction time is 1.5-2.5 hours, rosemary essential oil is obtained, (6) ethanol solution with 1.5 times and 70-80 wt% of weight is added into picked wintergreen leaves, ultrasonic extraction is carried out for 30-50 minutes at the temperature of 60-70 ℃, filtration is carried out, the filtrate is concentrated to be dried and is crushed to obtain extract, (, pulverizing into 10-20 mesh coarse powder, performing supercritical CO2 fluid extraction, wherein the weight-volume ratio of liquid to material is 1:10-20, the weight-volume ratio is that solid is counted by g, liquid is counted by mL, the extraction temperature is 42-50 ℃, the extraction pressure is 20-25MPa, the separation temperature is 50-60 ℃, the separation pressure is 4.5-5.5MPa, and the extraction time is 1.5-2.5 hours, so as to obtain rose essential oil, (8) cleaning and drying cananga odorata, pulverizing into 10-20 mesh coarse powder, performing supercritical CO2 fluid extraction, the weight-volume ratio of liquid to material is 1:10-20, the weight-volume ratio is that solid is counted by g, liquid is counted by mL, the extraction temperature is 42-50 ℃, the extraction pressure is 20-25MPa, the separation temperature is 50-60 ℃, the separation pressure is 4.5-5.5MPa, and the extraction time is 1.5-2.5 hours, obtaining cananga odorata essential oil, (9) cleaning fresh lemons by using tap water, adding salt for bleaching for 2 hours, fishing out, draining, putting the fresh lemons into a freezing chamber with the temperature above minus twenty ℃ for freezing for 24 hours to prevent loss of substances such as iron, potassium and the like and emission of aromatic ketone, breaking the frozen lemons into lemon pulp by using an ice crusher for later use, putting the lemon pulp into an extraction device to apply microwave radiation to lemon peel fragments, collecting generated essential oil steam and cooling to obtain crude lemon essential oil, putting the obtained lemon essential oil into a non-toxic, sterile and non-radiative all-glass distiller to distill to obtain distillate, separating and purifying: putting the distillate into a solvent bottle to absorb primary essence, putting the primary essence into a tetrafluoro stopper three-layer tower device to be filtered to obtain lemon essential oil, (10) cleaning and drying lemon grass, crushing the lemon grass into coarse powder which is sieved by a sieve with 10-20 meshes, and extracting by supercritical CO2 fluid, wherein the weight-volume ratio of liquid to material is 1:10-20, the weight-volume ratio refers to that solid is measured by g, liquid is measured by mL, the extraction temperature is 42-50 ℃, the extraction pressure is 20-25MPa, the separation temperature is 50-60 ℃, the separation pressure is 4.5-5.5MPa, and the extraction time is 1.5-2.5 hours, so that the lemon grass essential oil is obtained;

s2, preparation of mixed crude oil: pouring the lavender essential oil, the mint essential oil, the eucalyptus essential oil, the tea tree essential oil, the rosemary essential oil, the wintergreen essential oil, the rose essential oil, the ylang essential oil, the lemon essential oil and the lemongrass essential oil which are prepared in the step S1 into a mixer, starting the mixer to mix the plant essential oil, setting the temperature in the mixer to be 30-50 ℃, setting the mixing time to be 1-2 hours, and controlling the mixing speed to be 120 plus 160 revolutions per minute so as to obtain mixed crude oil after the plant essential oil and the lemongrass essential oil are fully mixed uniformly;

s3, preparing essential oil: pouring the mixed crude oil prepared in the step S2 into base oil, adding a proper amount of sweet almond oil and jojoba oil, stirring and mixing the mixture at the temperature of 50-70 ℃, adding a proper amount of organic solvent, humectant and sodium hyaluronate, continuously mixing for 20-40 minutes, controlling the mixing temperature at 20-40 ℃, finally adding a proper amount of fixative, polydimethylsiloxane, antioxidant, dipotassium glycyrrhizinate, madecassoside and vitamin E, stirring for 1-2 hours, and controlling the stirring temperature at 10-30 ℃ to obtain essential oil;

s4, sterilization of essential oil: and (3) placing the essential oil prepared in the step (S3) into a sterile disinfection box for sterilization, wherein the sterilization temperature is 100-120 ℃, and the sterilization time is 1-2 hours, so that various herbal refreshing skin-care essential oils can be obtained.

Advantageous effects

The invention provides various herbal refreshing skin care essential oils. Compared with the prior art, the method has the following beneficial effects: the herbal refreshing skin care essential oil comprises the following raw materials in parts by weight: 20-30 parts of base oil, 5-9 parts of lavender, 5-9 parts of mint, 5-9 parts of eucalyptus, 5-9 parts of tea tree, 5-9 parts of rosemary, 5-9 parts of wintergreen, 5-9 parts of rose, 5-9 parts of ylang-ylang, 5-9 parts of lemon grass, 6-10 parts of sweet almond oil, 6-10 parts of jojoba oil, 6-8 parts of organic solvent, 8-12 parts of humectant, 10-14 parts of sodium hyaluronate, 4-8 parts of fixative, 6-12 parts of polydimethylsiloxane, 4-8 parts of antioxidant, 2-8 parts of dipotassium glycyrrhizinate, 8-14 parts of madecassoside and 8-16 parts of vitamin E10-16 parts, and the herbal essential oil can be added to achieve the effects of sterilizing, diminishing inflammation and conditioning skin inflammation (such as skin infection), Pox, beriberi, skin itch, mosquito bites and insect bites), and refreshment: the massage on temples and the like has the effects of refreshing, preventing driving, meeting and learning from getting tired, can dredge channels and collaterals, relieve the problems of shoulders, necks, lumbar vertebrae, joints and the like and relieve fatigue and the like by using the massage, is comfortable and not greasy when used, and can not increase the burden of skin.

Detailed Description

The following will clearly and completely describe the technical solutions in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The invention provides three technical schemes: the herbal skin care essential oil comprises the following raw materials in parts by weight: 20-30 parts of base oil, 5-9 parts of lavender, 5-9 parts of mint, 5-9 parts of eucalyptus, 5-9 parts of tea tree, 5-9 parts of rosemary, 5-9 parts of wintergreen, 5-9 parts of rose, 5-9 parts of ylang-ylang, 5-9 parts of lemon grass, 6-10 parts of sweet almond oil, 6-10 parts of jojoba oil, 6-8 parts of organic solvent, 8-12 parts of humectant, 10-14 parts of sodium hyaluronate, 4-8 parts of fixative, 6-12 parts of polydimethylsiloxane, 4-8 parts of antioxidant, 2-8 parts of dipotassium glycyrrhizinate, 8-14 parts of madecassoside and 10-16 parts of vitamin E.

In the invention, the preparation method of the various herbal refreshing skin care essential oils specifically comprises the following embodiments:

example 1

S1, extraction of herbaceous plants: (1) washing and drying 7 parts of lavender, crushing the lavender into coarse powder passing through a 15-mesh sieve, performing supercritical CO2 fluid extraction, wherein the weight-volume ratio of liquid to material is 1:15, the weight-volume ratio refers to that solid is counted by g, liquid is counted by mL, the following are the same, the extraction temperature is 46 ℃, the extraction pressure is 22MPa, the separation temperature is 55 ℃, the separation pressure is 5MPa, and the extraction time is 2 hours, so that lavender essential oil is obtained, (2) washing and drying 7 parts of mint, crushing the mint into coarse powder passing through the 15-mesh sieve, performing supercritical CO2 fluid extraction, wherein the weight-volume ratio of liquid to material is 1:15, the weight-volume ratio refers to that solid is counted by g, liquid is counted by mL, the following is the same, the extraction temperature is 46 ℃, the extraction pressure is 23MPa, the separation temperature is 55 ℃, the separation pressure is 5MPa, and the extraction time is 2 hours, so that mint essential oil is obtained, (3) washing and drying 7, the weight volume ratio of liquid materials is 1:15, the weight volume ratio refers to that solid is g, liquid is mL, the extraction temperature is 46 ℃, the extraction pressure is 22MPa, the separation temperature is 55 ℃, the separation pressure is 5MPa, and the extraction time is 2 hours, so that the you jiali essential oil is obtained, (4) the initial tea tree essential oil obtained just after being squeezed is selected, the tea tree essential oil is put into a percolation cylinder, ethanol water solution is used as a solvent, heating and stirring are carried out, after the extraction is finished, filtration is carried out, an extracting solution is obtained, the ethanol solution with the volume fraction of 85% is added for microwave extraction, the extracting solution is put into a 5-degree space environment for refrigeration for 2.5 hours, then oil-water separation is carried out, then microfilm filtration and reduced pressure concentration are carried out, so that the finished product tea tree essential oil is obtained, (5) 7 parts of rosemary are cleaned and dried, crushed into 15-mesh coarse powder, supercritical CO2 fluid extraction is carried out, the weight volume ratio is that the solid is counted by g, the liquid is counted by mL, the following is the same, the extraction temperature is 46 ℃, the extraction pressure is 22MPa, the separation temperature is 55 ℃, the separation pressure is 5MPa, and the extraction time is 2 hours, rosemary essential oil is obtained, (6) ethanol solution with the weight of 1.5 times and 75 wt% of the picked ilex chinensis leaves is added into the picked 7 parts of ilex chinensis, the mixture is filtered after ultrasonic extraction at 65 ℃ for 40 minutes, the filtrate is concentrated to be dry and then crushed, the wintergreen extract is obtained, (7) 7 parts of roses are cleaned and dried, then crushed into coarse powder which is sieved by a 15-mesh sieve, supercritical CO2 fluid extraction is carried out, the weight volume ratio of liquid materials is 1:15, the weight volume ratio is that the solid is counted by g, the following is the same, the extraction temperature is 46 ℃, the extraction pressure is 22MPa, the separation temperature is 55 ℃, the separation pressure is 5MPa, and the extraction time is 2 hours, the rose essential oil, supercritical CO2 fluid extraction, wherein the weight-volume ratio of liquid to material is 1:15, the weight-volume ratio of liquid is that solid is measured in g, liquid is measured in mL, the following is the same, the extraction temperature is 46 ℃, the extraction pressure is 22MPa, the separation temperature is 55 ℃, the separation pressure is 5MPa, and the extraction time is 2 hours, thus obtaining cananga odorata essential oil, (9) cleaning 7 fresh lemons with tap water, adding salt for bleaching for 2 hours, then fishing out and draining, putting the lemons into a freezing chamber with the temperature above-twenty ℃ below zero for freezing for 24 hours, preventing the loss of substances such as iron, potassium and the like and the diffusion of aromatic ketone, crushing the frozen lemons into lemon pulp by an ice crusher for later use, putting the lemon pulp into an extraction device for applying microwave radiation to lemon peel fragments, collecting the generated essential oil vapor and cooling, thus obtaining crude lemon essential oil, putting the obtained lemon essential oil into a nontoxic, aseptic and non-radiative all-glass distiller for distillation, obtaining distillate, separating and purifying: putting the distillate into a solvent bottle to absorb primary essence, putting the primary essence into a tetrafluoro stopper three-layer tower device to be filtered to obtain lemon essential oil, (10) cleaning and drying 7 parts of lemongrass, crushing the lemongrass into coarse powder which is sieved by a 15-mesh sieve, and performing supercritical CO2 fluid extraction, wherein the weight-volume ratio of liquid to material is 1:15, the weight-volume ratio refers to that solid is measured in g, liquid is measured in mL, the extraction temperature is 46 ℃, the extraction pressure is 22MPa, the separation temperature is 55 ℃, the separation pressure is 5MPa, and the extraction time is 2 hours to obtain the lemongrass essential oil;

s2, preparation of mixed crude oil: pouring the lavender essential oil, the mint essential oil, the eucalyptus essential oil, the tea tree essential oil, the rosemary essential oil, the wintergreen essential oil, the rose essential oil, the ylang essential oil, the lemon essential oil and the lemongrass essential oil which are prepared in the step S1 into a mixer, starting the mixer to mix the plant essential oil, setting the temperature in the mixer to be 40 ℃, setting the mixing time to be 1.5 hours, and controlling the mixing speed to be 140 revolutions per minute so as to fully and uniformly mix the plant essential oil and the mint essential oil to obtain mixed crude oil;

s3, preparing essential oil: pouring the mixed crude oil prepared in the step S2 into 25 parts of base oil, adding 8 parts of sweet almond oil and 8 parts of jojoba oil, stirring and mixing the mixture at 60 ℃, adding 7 parts of organic solvent, 10 parts of humectant and 12 parts of sodium hyaluronate, continuously mixing for 30 minutes, controlling the mixing temperature at 30 ℃, finally adding 6 parts of fixative, 9 parts of polydimethylsiloxane, 6 parts of antioxidant, 5 parts of dipotassium glycyrrhizinate, 11 parts of madecassoside and 13 parts of vitamin E, stirring for 1.5 hours, and controlling the stirring temperature at 20 ℃ to obtain essential oil;

s4, sterilization of essential oil: and (4) placing the essential oil prepared in the step (S3) into a sterile disinfection box for sterilization, wherein the sterilization temperature is 110 ℃, and the sterilization time is 1.5 hours, so that the various herbal refreshing skin-care essential oils can be obtained.

Example 2

S1, extraction of herbaceous plants: (1) cleaning and drying 9 parts of lavender, crushing into 20-mesh coarse powder, performing supercritical CO2 fluid extraction, wherein the weight-volume ratio of liquid to material is 1:20, the weight-volume ratio refers to that solid is counted by g, liquid is counted by mL, the same is shown below, the extraction temperature is 50 ℃, the extraction pressure is 25MPa, the separation temperature is 0 ℃, the separation pressure is 5.5MPa, and the extraction time is 2.5 hours, so that lavender essential oil is obtained, (2) cleaning and drying 9 parts of mint, crushing into 20-mesh coarse powder, performing supercritical CO2 fluid extraction, wherein the weight-volume ratio of liquid to material is 1:20, the weight-volume ratio refers to that solid is counted by g, liquid is counted by mL, the same is extracted at 50 ℃, the extraction pressure is 25MPa, the separation temperature is 0 ℃, the separation pressure is 5.5MPa, and the extraction time is 2.5 hours, so that mint essential oil is obtained, (3) cleaning and drying 9 parts of eucalyptus, crushing into 20-mesh coarse powder, performing supercritical CO2, the weight-volume ratio of liquid materials is 1:20, the weight-volume ratio refers to that solid is g, liquid is mL, the extraction temperature is 50 ℃, the extraction pressure is 25MPa, the separation temperature is 0 ℃, the separation pressure is 5.5MPa, and the extraction time is 2.5 hours, the eucalyptus essential oil is obtained, (4) the initial tea tree essential oil obtained just after squeezing is selected, the tea tree essential oil is put into a percolation cylinder, ethanol water solution is used as a solvent, heating and stirring are carried out, after the extraction is finished, filtration is carried out, an extracting solution is obtained, then the ethanol solution with the volume fraction of 90% is added for microwave extraction, the extracting solution is put into a 5-degree space environment for refrigeration for 3 hours, then oil-water separation is carried out, micro-membrane filtration and decompression concentration are carried out, the finished product tea tree essential oil is obtained, (5) 9 parts of rosemary are cleaned and dried, crushed into coarse powder which is sieved by a 20-mesh sieve, supercritical CO2 fluid is extracted, the weight volume ratio is that the solid is counted by g, the liquid is counted by mL, the following is the same, the extraction temperature is 50 ℃, the extraction pressure is 25MPa, the separation temperature is 0 ℃, the separation pressure is 5.5MPa, and the extraction time is 2.5 hours, thus obtaining the rosemary essential oil, (6) 9 parts of picked wintergreen leaves are added with ethanol solution with the weight of 1.5 times and 80 wt% of the picked wintergreen leaves, the mixture is subjected to ultrasonic extraction for 50 minutes at 70 ℃, then filtered, the filtrate is concentrated to dryness and then crushed, thus obtaining the wintergreen extract, (7) 9 parts of roses are cleaned and dried, then crushed into 20-mesh coarse powder, the supercritical CO2 fluid extraction is carried out, the weight volume ratio of liquid materials is 1:20, the weight volume ratio is that the solid is counted by g, the following is the same, the extraction temperature is 50 ℃, the extraction pressure is 25MPa, the separation temperature is 0 ℃, the separation pressure is 5.5MPa, the extraction time is 2.5 hours, thus obtaining the rose essential oil, (8) 7, supercritical CO2 fluid extraction, wherein the weight-volume ratio of liquid to material is 1:20, the weight-volume ratio refers to that solid is measured in g, liquid is measured in mL, the following is the same, the extraction temperature is 50 ℃, the extraction pressure is 25MPa, the separation temperature is 0 ℃, the separation pressure is 5.5MPa, and the extraction time is 2.5 hours, thus obtaining cananga odorata essential oil, (9) cleaning 9 fresh lemons with tap water, adding salt for bleaching for 2 hours, then fishing out and draining, putting the lemons into a freezing chamber with the temperature above-twenty ℃ below zero for freezing for 24 hours, preventing the loss of substances such as iron, potassium and the like and the emission of aromatic ketone, breaking the frozen lemons into lemon pulp by an ice crusher for standby, putting the lemon pulp into an extraction device for applying microwave radiation to the lemon peel fragments, collecting the generated essential oil vapor and cooling, thus obtaining crude lemon essential oil, putting the obtained lemon essential oil into a non-toxic, sterile and non-radiative all-glass distiller for distillation, obtaining distillate, separating and purifying: putting the distillate into a solvent bottle to absorb primary essence, putting the primary essence into a tetrafluoro stopper three-layer tower device to be filtered to obtain lemon essential oil, (10) cleaning and drying 9 parts of lemongrass, crushing into 20-mesh coarse powder, performing supercritical CO2 fluid extraction, wherein the liquid-material weight-volume ratio is 1:20, the weight-volume ratio refers to that solid is measured by g, liquid is measured by mL, the extraction temperature is 50 ℃, the extraction pressure is 25MPa, the separation temperature is 0 ℃, the separation pressure is 5.5MPa, and the extraction time is 2.5 hours to obtain the lemongrass essential oil;

s2, preparation of mixed crude oil: pouring the lavender essential oil, the mint essential oil, the eucalyptus essential oil, the tea tree essential oil, the rosemary essential oil, the wintergreen essential oil, the rose essential oil, the ylang essential oil, the lemon essential oil and the lemongrass essential oil which are prepared in the step S1 into a mixer, starting the mixer to mix the plant essential oil, setting the temperature in the mixer to be 50 ℃, setting the mixing time to be 2 hours, and controlling the mixing speed to be 160 revolutions per minute so as to fully and uniformly mix the plant essential oil and the mint essential oil to obtain mixed crude oil;

s3, preparing essential oil: pouring the mixed crude oil prepared in the step S2 into 30 parts of base oil, adding 10 parts of sweet almond oil and 10 parts of jojoba oil, stirring and mixing the mixture at 70 ℃, adding 8 parts of organic solvent, 12 parts of humectant and 14 parts of sodium hyaluronate, continuously mixing for 40 minutes, controlling the mixing temperature at 40 ℃, finally adding 8 parts of fixative, 12 parts of polydimethylsiloxane, 8 parts of antioxidant, 8 parts of dipotassium glycyrrhizinate, 4 parts of madecassoside and 16 parts of vitamin E, stirring for 2 hours, and controlling the stirring temperature at 30 ℃ to obtain essential oil;

s4, sterilization of essential oil: and (4) placing the essential oil prepared in the step (S3) into a sterile disinfection box for sterilization, wherein the sterilization temperature is 120 ℃, and the sterilization time is 2 hours, so that various herbal refreshing skin care essential oils can be obtained.

Example 3

S1, extraction of herbaceous plants: (1) cleaning and drying 5 parts of lavender, crushing the lavender into 10-mesh coarse powder, performing supercritical CO2 fluid extraction, wherein the weight-volume ratio of liquid to material is 1:10, the weight-volume ratio refers to that the solid is calculated by g, the liquid is calculated by mL, the extraction temperature is 42 ℃, the extraction pressure is 20MPa, the separation temperature is 50 ℃, the separation pressure is 4.5MPa, and the extraction time is 1.5 hours, so as to obtain lavender essential oil, (2) cleaning and drying 5 parts of mint, crushing the mint into 10-mesh coarse powder, performing supercritical CO2 fluid extraction, wherein the weight-volume ratio of the liquid to material is 1:10, the weight-volume ratio refers to that the solid is calculated by g, the liquid is calculated by mL, the extraction temperature is 42 ℃, the extraction pressure is 20MPa, the separation temperature is 50 ℃, the separation pressure is 4.5MPa, and the extraction time is 1.5 hours, obtaining mint essential oil, (3) cleaning and drying 5 parts of eucalyptus, crushing the mint oil into 10-mesh coarse powder, performing supercritical CO, the weight-volume ratio of liquid to material is 1:10, the weight-volume ratio refers to that solid is g, liquid is mL, the extraction temperature is 42 ℃, the extraction pressure is 20MPa, the separation temperature is 50 ℃, the separation pressure is 4.5MPa, and the extraction time is 1.5 hours, so that the eucalyptus essential oil is obtained, (4) the initial tea tree essential oil obtained just after squeezing is selected, the tea tree essential oil is put into a percolation cylinder, ethanol water solution is used as a solvent, heating and stirring are carried out, after the extraction is finished, filtration is carried out, so that an extracting solution is obtained, the ethanol solution with the volume fraction of 80% is added for microwave extraction, the extracting solution is put into a 5-degree space environment for refrigeration for 2 hours, then oil-water separation is carried out, micro-membrane filtration and reduced pressure concentration are carried out, so that the finished product tea tree essential oil is obtained, (5) 5 parts of rosemary are cleaned and dried, crushed into coarse powder which is sieved by a 10-mesh sieve, supercritical, the weight volume ratio is that the solid is counted by g, the liquid is counted by mL, the following is the same, the extraction temperature is 42 ℃, the extraction pressure is 20MPa, the separation temperature is 50 ℃, the separation pressure is 4.5MPa, and the extraction time is 1.5 hours, thus obtaining rosemary essential oil, (6) 5 parts of picked wintergreen leaves are added with 70 wt% ethanol solution with the weight of 1.5 times of the weight of the wintergreen leaves, the mixture is subjected to ultrasonic extraction for 30 minutes at 60 ℃, the filtration is carried out, the filtrate is concentrated to be dry and then is crushed, thus obtaining wintergreen extract, (7) 5 parts of roses are cleaned and dried, then are crushed into 10-mesh coarse powder, the supercritical CO2 fluid extraction is carried out, the weight volume ratio of liquid materials is 1:10, the weight volume ratio is that the solid is counted by g, the liquid is counted by mL, the following is the same, the extraction temperature is 42 ℃, the extraction pressure is 20MPa, the separation temperature is 50 ℃, the separation pressure is 4.5MPa, the extraction time is 1.5, supercritical CO2 fluid extraction, wherein the weight-volume ratio of liquid to material is 1:10, the weight-volume ratio refers to that solid is measured in g, liquid is measured in mL, the following is the same, the extraction temperature is 42 ℃, the extraction pressure is 20MPa, the separation temperature is 50 ℃, the separation pressure is 4.5MPa, and the extraction time is 1.5 hours, thus obtaining cananga odorata essential oil, (9) 5 parts of fresh lemon is cleaned by tap water, then is added with salt and rinsed for 2 hours, then is taken out and drained, then is put into a freezing chamber with the temperature above-twenty ℃ below zero for freezing for 24 hours, thereby preventing the loss of substances such as iron, potassium and the like and the emission of aromatic ketone, the frozen lemon is crushed into lemon pulp by an ice crusher for standby, the lemon pulp is put into an extraction device for applying microwave radiation to the lemon peel fragments, the generated essential oil vapor is collected and cooled, thus obtaining crude lemon essential oil, the obtained lemon essential oil is put into a non-toxic, sterile and, obtaining distillate, separating and purifying: putting the distillate into a solvent bottle to absorb primary essence, putting the primary essence into a tetrafluoro stopper three-layer tower device to be filtered to obtain lemon essential oil, (10) cleaning and drying 5 parts of lemongrass, crushing the lemongrass into 10-mesh-sieve coarse powder, extracting by using supercritical CO2 fluid, wherein the weight-volume ratio of liquid to material is 1:10, the weight-volume ratio refers to that solid is measured by g, liquid is measured by mL, the extraction temperature is 42 ℃, the extraction pressure is 20MPa, the separation temperature is 50 ℃, the separation pressure is 4.5MPa, and the extraction time is 1.5 hours to obtain the lemongrass essential oil;

s2, preparation of mixed crude oil: pouring the lavender essential oil, the mint essential oil, the eucalyptus essential oil, the tea tree essential oil, the rosemary essential oil, the wintergreen essential oil, the rose essential oil, the ylang essential oil, the lemon essential oil and the lemongrass essential oil which are prepared in the step S1 into a mixer, starting the mixer to mix the plant essential oil, setting the temperature in the mixer to be 30 ℃, setting the mixing time to be 1 hour, and controlling the mixing speed to be 120 revolutions per minute so as to fully and uniformly mix the plant essential oil and the mint essential oil to obtain mixed crude oil;

s3, preparing essential oil: pouring the mixed crude oil prepared in the step S2 into 20 parts of base oil, adding 6 parts of sweet almond oil and 6 parts of jojoba oil, stirring and mixing the mixture at 50 ℃, adding 6 parts of organic solvent, 8 parts of humectant and 10 parts of sodium hyaluronate, continuously mixing for 20 minutes, controlling the mixing temperature at 20 ℃, finally adding 4 parts of fixative, 6 parts of polydimethylsiloxane, 4 parts of antioxidant, 2 parts of dipotassium glycyrrhizinate, 8 parts of madecassoside and 1 part of vitamin E, stirring for 1 hour, and controlling the stirring temperature at 10 ℃ to obtain essential oil;

s4, sterilization of essential oil: and (4) placing the essential oil prepared in the step (S3) into a sterile disinfection box for sterilization, wherein the sterilization temperature is 100 ℃, and the sterilization time is 1 hour, so that the various herbal refreshing skin-care essential oils can be obtained.

Comparative experiment

Randomly selecting skin care essential oil on the market as a control group, respectively testing the moisture retention, the comfort and the anti-inflammation of the skin care essential oil, wherein the testing conditions are consistent with the above conditions, recording the results, operating at the same time and under the same conditions, and simultaneously counting data and making a statistical table chart in the testing process, wherein the statistical table chart is shown in the following table.

As shown in the table above, the herbal essential oil can be added to sterilize and diminish inflammation, condition skin inflammation (such as skin infection, pox, dermatophytosis, skin pruritus and mosquito and insect bite), and refresh and restore consciousness: the massage on temples and the like has the effects of refreshing, preventing driving, meeting and learning from getting tired, can dredge channels and collaterals, relieve the problems of shoulders, necks, lumbar vertebrae, joints and the like and relieve fatigue and the like by using the massage, is comfortable and not greasy when used, and can not increase the burden of skin.

It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. A plurality of herbal refreshing skin care essential oil is characterized in that: the raw materials comprise the following components in parts by weight: 20-30 parts of base oil, 5-9 parts of lavender, 5-9 parts of mint, 5-9 parts of eucalyptus, 5-9 parts of tea tree, 5-9 parts of rosemary, 5-9 parts of wintergreen, 5-9 parts of rose, 5-9 parts of ylang-ylang, 5-9 parts of lemon grass, 6-10 parts of sweet almond oil, 6-10 parts of jojoba oil, 6-8 parts of organic solvent, 8-12 parts of humectant, 10-14 parts of sodium hyaluronate, 4-8 parts of fixative, 6-12 parts of polydimethylsiloxane, 4-8 parts of antioxidant, 2-8 parts of dipotassium glycyrrhizinate, 8-14 parts of madecassoside and 10-16 parts of vitamin E.

2. The plurality of herbal cooling skin care essential oils of claim 1, wherein: the raw materials comprise the following components: 25 parts of base oil, 7 parts of lavender, 7 parts of mint, 7 parts of eucalyptus, 7 parts of tea tree, 7 parts of rosemary, 7 parts of wintergreen, 7 parts of rose, 7 parts of ylang, 7 parts of lemon grass, 8 parts of sweet almond oil, 8 parts of jojoba oil, 7 parts of organic solvent, 10 parts of humectant, 12 parts of sodium hyaluronate, 6 parts of fixative, 9 parts of polydimethylsiloxane, 6 parts of antioxidant, 5 parts of dipotassium glycyrrhizinate, 11 parts of madecassoside and 13 parts of vitamin E.

3. The plurality of herbal cooling skin care essential oils of claim 1, wherein: the raw materials comprise the following components: 30 parts of base oil, 9 parts of lavender, 9 parts of mint, 9 parts of eucalyptus, 9 parts of tea tree, 9 parts of rosemary, 9 parts of wintergreen, 9 parts of rose, 9 parts of ylang, 9 parts of lemon grass, 10 parts of sweet almond oil, 10 parts of jojoba oil, 8 parts of organic solvent, 12 parts of humectant, 14 parts of sodium hyaluronate, 8 parts of fixative, 12 parts of polydimethylsiloxane, 8 parts of antioxidant, 8 parts of dipotassium glycyrrhizinate, 14 parts of madecassoside and 16 parts of vitamin E.

4. The plurality of herbal cooling skin care essential oils of claim 1, wherein: the raw materials comprise the following components: 20 parts of base oil, 5 parts of lavender, 5 parts of mint, 5 parts of eucalyptus, 5 parts of tea tree, 5 parts of rosemary, 5 parts of wintergreen, 5 parts of rose, 5 parts of ylang, 5 parts of lemon grass, 6 parts of sweet almond oil, 6 parts of jojoba oil, 6 parts of organic solvent, 8 parts of humectant, 10 parts of sodium hyaluronate, 4 parts of fixative, 6 parts of polydimethylsiloxane, 4 parts of antioxidant, 2 parts of dipotassium glycyrrhizinate, 8 parts of madecassoside and 10 parts of vitamin E.

5. The plurality of herbal cooling skin care essential oils of claim 1, wherein: the base oil is one or a mixture of more of seabuckthorn fruit oil, grape seed oil, wheat germ oil, olive oil and jojoba oil, the organic solvent is one or a mixture of two or more of ethanol, ethyl acetate and cyclohexane, the fragrance fixative is musk, benzoin grease and coumarin, and the weight ratio of the musk, the benzoin grease and the coumarin is 2:1: 3.

6. The plurality of herbal cooling skin care essential oils of claims 1-5, wherein: the preparation method specifically comprises the following steps: