CN115054549B - Oil-control and antibacterial coptis chinensis shampoo - Google Patents
Oil-control and antibacterial coptis chinensis shampoo Download PDFInfo
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- CN115054549B CN115054549B CN202210760881.1A CN202210760881A CN115054549B CN 115054549 B CN115054549 B CN 115054549B CN 202210760881 A CN202210760881 A CN 202210760881A CN 115054549 B CN115054549 B CN 115054549B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses an oil-control and antibacterial coptis chinensis shampoo. Comprises the following components in parts by weight: 5-10 parts of coptis chinensis extract, 5-10 parts of inula flower extract, 10-20 parts of foaming agent, 1-3 parts of thickening agent, 1-3 parts of organic acid, 1-3 parts of humectant and 150-300 parts of water. The shampoo of the invention is added with the coptis extract and the inula flower extract, so that the antibacterial effect of the shampoo is endowed, and the coptis extract and the inula flower extract are combined to use synergistic effect. The shampoo has good oil control effect, no irritation to skin, and has effects of moistening skin, relieving itching and diminishing inflammation.
Description
Technical Field
The invention belongs to the technical field of cleaning product preparation, and particularly relates to an oil-control antibacterial coptis chinensis shampoo and a preparation method thereof.
Background
The shampoo is also called shampoo or shampoo, and is a basic care cosmetic for hair and scalp. The shampoo contains a plurality of components, the comprehensive effect of the components can play a role in cleaning scalp and hair, the most effective component in the shampoo is a surfactant, the surfactant plays a role in cleaning hair and scalp, foam can be generated when the shampoo is mixed with water, but the quantity of the foam cannot reflect the strength of the cleaning capability.
With the increasing functional demands of people on shampoos, natural plant extracts are added into the shampoos to achieve special effects, and the number of the natural plant extracts is increasing. The coptis is a perennial herb of Ranunculaceae, and has the effects of clearing heat and drying dampness, purging pathogenic fire and removing toxin, and is used for treating damp-heat distention and fullness, vomiting and acid regurgitation, diarrhea, jaundice, high-heat unconsciousness, heart fire hyperactivity, vexation and insomnia, blood heat hematemesis and epistaxis, conjunctival congestion, toothache, diabetes, carbuncle and furuncle; for external treatment of eczema, damp sore, ear canal purulent discharge, it is good at clearing heat from upper-jiao, and is used for conjunctival congestion, aphtha, turmeric even clear stomach and harmonize stomach to arrest vomiting, cold and heat accumulation, damp heat obstruction in middle energizer, distention and fullness and vomiting, yu Huang Lian soothing liver and harmonizing stomach to arrest vomiting, and vomiting and acid regurgitation. The bindweed is the whole grass or rhizome of the bindweed of Convolvulaceae, and the root-like stem: invigorating spleen, invigorating qi, promoting urination, regulating menstruation, and stopping leukorrhagia; can be used for treating dyspepsia due to spleen deficiency, menoxenia, leucorrhea, and milk deficiency; flower: pain relief; it is used for treating toothache by external application. At present, no report that the extracts of coptis chinensis and inula flowers are added into the shampoo to perform the functional component exists.
Disclosure of Invention
The invention aims to provide coptis oil-control antibacterial shampoo and a preparation method thereof.
The coptis oil-control antibacterial shampoo comprises the following components in parts by weight: 5-10 parts of coptis chinensis extract, 5-10 parts of inula flower extract, 10-20 parts of foaming agent, 1-3 parts of thickening agent, 1-3 parts of organic acid, 1-3 parts of humectant and 150-300 parts of water.
The extraction method of the coptis extract comprises the following steps: taking coptis chinensis, sun-drying, grinding into powder, adding 4-10 times of water in parts by weight, extracting for 3 times under reflux, combining filtrates, and concentrating to 1/5 of the volume of the filtrate.
The method for extracting the inula flowers extract comprises the following steps: taking inula flower, sun-drying, grinding into powder, adding 3-6 times of water by weight for reflux extraction for 3 times, combining filtrates, and concentrating to 1/5 of the volume of the filtrate.
The foaming agent is one or more of sodium laureth sulfate, sodium trideceth sulfate, sodium cocoyl glycinate and alkoxyl ethyl-beta-D-xylopyranoside.
The thickener is one or more of xanthan gum, cellulose, gellan gum and acrylic acid polymer.
The organic acid is one or more of citric acid, malic acid and tartaric acid.
The humectant is one or more of chitin, tremella polysaccharide, sodium hyaluronate and fibroin.
The preparation method of the coptis oil-control antibacterial shampoo comprises the following steps:
(1) According to the weight portions, 10 to 20 portions of foaming agent, 1 to 3 portions of thickening agent, 1 to 3 portions of organic acid, 1 to 3 portions of humectant and 150 to 300 portions of water are taken, heated to 50 to 80 ℃ and stirred for 20 to 40 minutes under the condition of 800 to 1500 rpm;
(2) Cooling to room temperature, adding Coptidis rhizoma extract 5-10 parts and flos Inulae extract 5-10 parts, and stirring at 500-800rpm for 10-30 min.
The invention has the beneficial effects that: the shampoo of the invention is added with the coptis extract and the inula flower extract, so that the antibacterial effect of the shampoo is endowed, and the coptis extract and the inula flower extract are combined to use synergistic effect. The shampoo has good oil control effect, no irritation to skin, and has effects of moistening skin, relieving itching and diminishing inflammation.
Detailed Description
The present invention will be described more fully hereinafter in order to facilitate an understanding of the present invention. This invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.
Example 1
The coptis oil-control antibacterial shampoo comprises the following components in parts by weight: 8 parts of coptis chinensis extract, 8 parts of inula flower extract, 15 parts of sodium laureth sulfate, 2 parts of xanthan gum, 2 parts of citric acid, 2 parts of chitin and 200 parts of water.
The extraction method of the coptis extract comprises the following steps: taking coptis chinensis, sun-drying, grinding into powder, adding 6 times of water in parts by weight, extracting for 3 times under reflux, combining filtrates, and concentrating to 1/5 of the volume of the filtrate.
The method for extracting the inula flowers extract comprises the following steps: taking inula flower, sun-drying, grinding into powder, adding 4 times of water by weight for reflux extraction for 3 times, combining filtrates, and concentrating to 1/5 of the volume of the filtrate.
The preparation method of the coptis oil-control antibacterial shampoo comprises the following steps:
(1) According to the weight parts, 15 parts of sodium laureth sulfate, 2 parts of xanthan gum, 2 parts of citric acid, 2 parts of chitin and 200 parts of water are taken, heated to 60 ℃, and stirred for 30min under the condition of 1000 rpm;
(2) Cooling to room temperature, adding Coptidis rhizoma extract 8 parts and flos Inulae extract 8 parts, and stirring at 600rpm for 20 min.
Example 2
The coptis oil-control antibacterial shampoo comprises the following components in parts by weight: 5 parts of coptis chinensis extract, 5 parts of inula flower extract, 12 parts of trideceth sodium sulfate, 1 part of cellulose, 1 part of malic acid, 1 part of sodium hyaluronate and 160 parts of water.
The extraction method of the coptis extract comprises the following steps: taking coptis chinensis, sun-drying, grinding into powder, adding 5 weight parts of water, extracting for 3 times under reflux, combining filtrates, and concentrating to 1/5 of the volume of the filtrate.
The method for extracting the inula flowers extract comprises the following steps: taking inula flower, sun-drying, grinding into powder, adding 3 times of water in parts by weight, reflux-extracting for 3 times, mixing filtrates, and concentrating to 1/5 of the volume of the filtrate.
The preparation method of the coptis oil-control antibacterial shampoo comprises the following steps:
(1) According to the weight portions, 12 portions of trideceth sodium sulfate, 1 portion of cellulose, 1 portion of malic acid, 1 portion of sodium hyaluronate and 160 portions of water are taken, heated to 50 ℃ and stirred for 20min under the condition of 1500 rpm;
(2) Cooling to room temperature, adding Coptidis rhizoma extract 5 parts and flos Inulae extract 5 parts, and stirring at 800rpm for 10 min.
Example 3
The coptis oil-control antibacterial shampoo comprises the following components in parts by weight: 10 parts of coptis chinensis extract, 10 parts of inula flower extract, 20 parts of alkoxyethyl-beta-D-xylopyranoside, 3 parts of gellan gum, 3 parts of tartaric acid, 3 parts of sodium hyaluronate and 300 parts of water.
The extraction method of the coptis extract comprises the following steps: taking coptis chinensis, sun-drying, grinding into powder, adding 8 times of water in parts by weight, extracting for 3 times under reflux, combining filtrates, and concentrating to 1/5 of the volume of the filtrate.
The method for extracting the inula flowers extract comprises the following steps: taking inula flower, sun-drying, grinding into powder, adding 5 times of water by weight for reflux extraction for 3 times, combining filtrates, and concentrating to 1/5 of the volume of the filtrate.
The preparation method of the coptis oil-control antibacterial shampoo comprises the following steps:
(1) According to the weight portions, 20 portions of alkoxyethyl-beta-D-xylopyranoside, 3 portions of gellan gum, 3 portions of tartaric acid, 3 portions of sodium hyaluronate and 300 portions of water are taken, and the mixture is heated to 80 ℃ and stirred for 40min under the condition of 800 rpm;
(2) Cooling to room temperature, adding Coptidis rhizoma extract 10 parts and flos Inulae extract 10 parts, and stirring at 500rpm for 30 min.
Example 4
The coptis oil-control antibacterial shampoo comprises the following components in parts by weight: 6 parts of coptis chinensis extract, 6 parts of inula flower extract, 11 parts of cocoyl sodium glycinate, 3 parts of acrylic acid polymer, 1 part of malic acid, 3 parts of tremella polysaccharide and 170 parts of water.
The extraction method of the coptis extract comprises the following steps: taking coptis chinensis, sun-drying, grinding into powder, adding 6 times of water in parts by weight, extracting for 3 times under reflux, combining filtrates, and concentrating to 1/5 of the volume of the filtrate.
The method for extracting the inula flowers extract comprises the following steps: taking inula flower, sun-drying, grinding into powder, adding 3 times of water in parts by weight, reflux-extracting for 3 times, mixing filtrates, and concentrating to 1/5 of the volume of the filtrate.
The preparation method of the coptis oil-control antibacterial shampoo comprises the following steps:
(1) According to the weight parts, 11 parts of sodium cocoyl glycinate, 3 parts of acrylic acid polymer, 1 part of malic acid, 3 parts of tremella polysaccharide and 170 parts of water are taken, the temperature is raised to 70 ℃, and stirring is carried out for 25min under the condition of 1100 rpm;
(2) Cooling to room temperature, adding Coptidis rhizoma extract 6 parts and flos Inulae extract 6 parts, and stirring at 600rpm for 12 min.
Comparative example 1
The coptis oil-control antibacterial shampoo comprises the following components in parts by weight: 16 parts of coptis extract, 15 parts of sodium laureth sulfate, 2 parts of xanthan gum, 2 parts of citric acid, 2 parts of chitin and 200 parts of water.
The extraction method of the coptis extract comprises the following steps: taking coptis chinensis, sun-drying, grinding into powder, adding 6 times of water in parts by weight, extracting for 3 times under reflux, combining filtrates, and concentrating to 1/5 of the volume of the filtrate.
The preparation method of the coptis oil-control antibacterial shampoo comprises the following steps:
(1) According to the weight parts, 15 parts of sodium laureth sulfate, 2 parts of xanthan gum, 2 parts of citric acid, 2 parts of chitin and 200 parts of water are taken, heated to 60 ℃, and stirred for 30min under the condition of 1000 rpm;
(2) Cooling to room temperature, adding 16 parts of Coptidis rhizoma extract, and stirring at 600rpm for 20 min.
Comparative example 2
The inula flower oil-control antibacterial shampoo comprises the following components in parts by weight: 16 parts of inula flower extract, 15 parts of sodium laureth sulfate, 2 parts of xanthan gum, 2 parts of citric acid, 2 parts of chitin and 200 parts of water.
The method for extracting the inula flowers extract comprises the following steps: taking inula flower, sun-drying, grinding into powder, adding 4 times of water by weight for reflux extraction for 3 times, combining filtrates, and concentrating to 1/5 of the volume of the filtrate.
The preparation method of the inula cappa oil-control antibacterial shampoo comprises the following steps:
(1) According to the weight parts, 15 parts of sodium laureth sulfate, 2 parts of xanthan gum, 2 parts of citric acid, 2 parts of chitin and 200 parts of water are taken, heated to 60 ℃, and stirred for 30min under the condition of 1000 rpm;
(2) Cooling to room temperature, adding 16 parts of the inula flower extract, and stirring at 600rpm for 20 min.
Experimental example:
the shampoo according to examples 1 to 4 and comparative examples 1 to 2 of the present invention was subjected to the antibacterial performance measurement of malassezia furfur by referring to GB15979-2002 "Disposable sanitary articles Standard", appendix C4", test method for antibacterial performance of dissolution antibacterial products", the measurement results are shown in Table 1:
TABLE 1
Note that: * Representing P <0.05 compared to example 1.
Product safety evaluation (human skin patch experiment):
the tested population is 60 women aged 20-40 years, the skin of the tested person is healthy, the skin allergy history does not exist, the tested person accords with the volunteer selection standard of the tested person, and the experimental products are the shampoo prepared in the examples 1-4 and the comparative examples 1-2.
The method comprises the steps of dividing the human body into 6 groups, selecting a spot tester for 10 persons in each group, dripping 0.05g of a test object into the spot tester in a closed spot test mode, attaching a special adhesive tape to the forehead of the head of a subject by external application, removing the test object after 24 hours, observing skin reactions after 2 hours, 6 hours, 12 hours, 24 hours and 48 hours respectively, and recording the results according to the skin reaction grading standard in cosmetic hygiene Specification.
The results of the human skin patch test showed that each group of subjects observed skin reactions at 0.5, 6, 12, 24, 48 hours by the shampoo of examples 1-4 and comparative examples 1-2, wherein no skin adverse reaction cases were found, indicating that the shampoo was safe to use.
Evaluation of using effect:
the tested group of people is 60 people who are 20-40 years old, the heads of the tested people have different degrees of hair oil and itch, the tested people are randomly divided into three groups, each group of 20 people, and the first group adopts the shampoo of the embodiment 1 of the invention, and the shampoo is used three times per week for one month; the shampoo of comparative examples 1 and 2 was used for the second and third groups, respectively, three times a week for one month.
Effect standard:
full effect: the hair grease and the greasy feeling are avoided, and the itching phenomenon completely disappears;
the method is effective: the hair grease is obviously improved, the greasy feeling is not obvious, and the scalp itching phenomenon is relieved;
invalidation: no obvious change is caused before and after the use.
TABLE 2
The above examples illustrate only a few embodiments of the invention, which are described in detail and are not to be construed as limiting the scope of the invention. It should be noted that it will be apparent to those skilled in the art that several variations and modifications can be made without departing from the spirit of the invention, which are all within the scope of the invention. Accordingly, the scope of protection of the present invention is to be determined by the appended claims.
Claims (6)
1. The coptis oil-control antibacterial shampoo is characterized by comprising the following components in parts by weight: 5-10 parts of coptis chinensis extract, 5-10 parts of inula flower extract, 10-20 parts of foaming agent, 1-3 parts of thickening agent, 1-3 parts of organic acid, 1-3 parts of humectant and 150-300 parts of water;
the extraction method of the coptis extract comprises the following steps: collecting Coptidis rhizoma, sun drying, grinding into powder, reflux extracting with 4-10 times of water for 3 times, mixing filtrates, and concentrating to 1/5 of the volume of the filtrate;
the method for extracting the inula flowers extract comprises the following steps: taking inula flower, sun-drying, grinding into powder, adding 3-6 times of water by weight for reflux extraction for 3 times, combining filtrates, and concentrating to 1/5 of the volume of the filtrate.
2. The coptis oil control antibacterial shampoo according to claim 1, wherein the foaming agent is one or more of sodium laureth sulfate, sodium trideceth sulfate, sodium cocoyl glycinate and alkoxyethyl-beta-D-xylopyranoside.
3. The coptis oil control antibacterial shampoo according to claim 1, wherein the thickening agent is one or more of xanthan gum, cellulose, gellan gum and acrylic acid polymer.
4. The oil control and bacteriostasis shampoo according to claim 1, wherein the organic acid is one or more of citric acid, malic acid and tartaric acid.
5. The coptis oil control antibacterial shampoo according to claim 1, wherein the humectant is one or more of chitin, tremella polysaccharide, sodium hyaluronate and fibroin.
6. The method for preparing the coptis oil-control antibacterial shampoo as claimed in claim 1, which is characterized by comprising the following steps:
(1) According to the weight portions, 10 to 20 portions of foaming agent, 1 to 3 portions of thickening agent, 1 to 3 portions of organic acid, 1 to 3 portions of humectant and 150 to 300 portions of water are taken, heated to 50 to 80 ℃ and stirred for 20 to 40 minutes under the condition of 800 to 1500 rpm;
(2) Cooling to room temperature, adding Coptidis rhizoma extract 5-10 parts and flos Inulae extract 5-10 parts, and stirring at 500-800rpm for 10-30 min.
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| CN202210760881.1A CN115054549B (en) | 2022-06-30 | 2022-06-30 | Oil-control and antibacterial coptis chinensis shampoo |
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| CN202210760881.1A CN115054549B (en) | 2022-06-30 | 2022-06-30 | Oil-control and antibacterial coptis chinensis shampoo |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001072569A (en) * | 1999-09-08 | 2001-03-21 | Noevir Co Ltd | Skin preparation for external use |
| CN105853890A (en) * | 2016-05-27 | 2016-08-17 | 济南思拓新源医药科技有限公司 | Medicine composition for stopping vomit and preparation method thereof |
| CN107789301A (en) * | 2017-12-06 | 2018-03-13 | 广州赛莱拉干细胞科技股份有限公司 | A kind of anti-acne skin care compositions and its application |
| CN111407707A (en) * | 2020-05-15 | 2020-07-14 | 广州路标科技有限公司 | Plant-derived skin health-care lotion and preparation method thereof |
| CN113893196A (en) * | 2021-10-29 | 2022-01-07 | 两面针（江苏）实业有限公司 | A bath product containing natural plant extract |
-
2022
- 2022-06-30 CN CN202210760881.1A patent/CN115054549B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001072569A (en) * | 1999-09-08 | 2001-03-21 | Noevir Co Ltd | Skin preparation for external use |
| CN105853890A (en) * | 2016-05-27 | 2016-08-17 | 济南思拓新源医药科技有限公司 | Medicine composition for stopping vomit and preparation method thereof |
| CN107789301A (en) * | 2017-12-06 | 2018-03-13 | 广州赛莱拉干细胞科技股份有限公司 | A kind of anti-acne skin care compositions and its application |
| CN111407707A (en) * | 2020-05-15 | 2020-07-14 | 广州路标科技有限公司 | Plant-derived skin health-care lotion and preparation method thereof |
| CN113893196A (en) * | 2021-10-29 | 2022-01-07 | 两面针（江苏）实业有限公司 | A bath product containing natural plant extract |
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