CN108836925B - Anti-allergy-dry traditional Chinese medicine extract composition, preparation method thereof and application thereof in cosmetics - Google Patents
Anti-allergy-dry traditional Chinese medicine extract composition, preparation method thereof and application thereof in cosmetics Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention belongs to the technical field of cosmetic compositions, and particularly relates to a composition of an anti-dry-allergy traditional Chinese medicine extract, a preparation method of the composition and application of the composition in cosmetics. The composition of the anti-dry-sensitive traditional Chinese medicine extract comprises the following components in parts by weight: 32-45 parts of polygonatum odoratum, 25-35 parts of radix ophiopogonis, 15-24 parts of liquorice, 9-13 parts of radix sophorae flavescentis and 3-8 parts of folium artemisiae argyi. The dry-sensitive extract composition is added into cosmetics, can resist skin dryness, resist slight itch, moisturize and nourish the skin, and can enhance the immunity of the skin, improve the moisturizing capability of the skin and relieve the skin by repairing the natural barrier of the skin. Has remarkable dry allergy resisting effect when added into cosmetics.
Description
Technical Field
The invention belongs to a composition in the technical field of cosmetic compositions, and particularly relates to a composition of an anti-dry-sensitive traditional Chinese medicine extract, a preparation method thereof and application thereof in cosmetics.
Background
The phenomenon of dry skin and easy sensitization caused by internal factors and external factors is the phenomenon of dry skin and easy sensitization. The skin of a human body is dry along with the change of the external environment, particularly the reduction of the water content of the skin in winter; in addition, with improper use of cosmetics, the barrier function of skin is reduced, the immunity of the skin is weakened, and the skin is more easily allergic and dry. In addition, with the increase of age, the skin function gradually declines, the skin metabolism is slowed down, the restoring force is reduced, and the water content of the skin is gradually reduced, so that the skin of people is easy to have symptoms of dryness, pruritus, dry skin and the like, is common in people of the next year, and seriously influences the daily life of people.
The commercially available anti-allergy raw materials are few in types, and most of the anti-allergy raw materials are synthetic raw materials, so that the skin discomfort is caused more easily, and the effect is not obvious. Therefore, the development of the anti-allergy traditional Chinese medicine extract composition has great market prospect.
Disclosure of Invention
The invention aims to provide an anti-allergy traditional Chinese medicine extract composition.
The invention aims to provide a mild non-irritating traditional Chinese medicine extract composition.
It is a further object of the present invention to provide an anti-dry sensitive cosmetic composition.
The invention further aims to provide a preparation method of the anti-dry-sensitive extraction composition.
It is a further object of the present invention to provide a method for preparing a cosmetic containing the anti-allergy extraction composition.
The invention further aims to provide an anti-dry-sensitive extraction composition and application thereof in cosmetics.
The traditional Chinese medicine extraction composition comprises five traditional Chinese medicines of Polygonatum odoratum (Mill.) Druce), Ophiopogon root (Ophiogon japonicus (L inn. f.) Ker-Gawl.), liquorice (Glycyrrhiza uralensis Fisch), Sophora flavescens (Sophora flavescens) and Folium Artemisiae argyi (Folium artemisiie argyi), and has the following effects:
(1) fragrant solomonseal rhizome: sweet and slightly cold; it enters lung and stomach meridians. The perennial herb and food homologous plant, polygonatum, has the effects of nourishing yin, moistening dryness, clearing heat, promoting fluid production, relieving cough and the like. The research shows that the polygonatum has the functions of increasing the immunity, delaying senility, resisting oxidation and the like. The polysaccharide contained in the polygonatum odoratum has good moisture retention, can effectively improve the moisture content of skin, slow down the loss rate of moisture, clear away free radicals in vivo, inhibit the formation of melanin, and play the roles of moistening skin and removing freckles.
(2) Radix ophiopogonis: sweet, slightly bitter and slightly cold; it enters heart, lung and stomach meridians. It is a commonly used yin-nourishing traditional Chinese medicine, and in Shen nong Ben Cao Jing, Mai Dong is listed as the superior product for nourishing yin and moistening lung, so it is said to be "taking for a long time to lighten body, not old and hunger-fast". Wherein the ophiopogonin D enhances cell activity and delays aging; the ophiopogonpolysaccharide can absorb moisture from the atmosphere to keep the skin moist, and can also absorb moisture from the deep layer of the skin to achieve the moisturizing effect.
(3) Licorice root: sweet and mild; it enters heart, lung, spleen and stomach meridians. The Glycyrrhrizae radix has antibacterial, antiinflammatory, antiallergic, skin melanin repairing, and skin melanin formation regulating effects.
(4) Flavescent sophora root: bitter and cold; it enters heart, liver, stomach, large intestine and bladder meridians. Has effects in clearing away heat, eliminating dampness, regulating immunity, and relieving inflammation.
(5) Folium artemisiae argyi: pungent, bitter and warm; it enters liver, spleen and kidney meridians. Dispelling cold, relieving pain, warming channels, stopping bleeding, resisting inflammation, bacteria and allergy.
The anti-dry-allergy traditional Chinese medicine extraction composition comprises the following components in parts by weight: 32-45 parts of polygonatum odoratum, 25-35 parts of radix ophiopogonis, 15-24 parts of liquorice, 9-13 parts of radix sophorae flavescentis and 3-8 parts of folium artemisiae argyi.
As a preferred embodiment, the anti-allergy traditional Chinese medicine extract composition comprises the following components in parts by weight: 34-43 parts of radix polygonati officinalis, 27-33 parts of radix ophiopogonis, 17-23 parts of liquorice, 10-13 parts of radix sophorae flavescentis and 3-7 parts of folium artemisiae argyi.
As another preferred embodiment, the traditional Chinese medicine extract composition comprises the following components in parts by weight: 36-41 parts of polygonatum odoratum, 28-32 parts of radix ophiopogonis, 19-23 parts of liquorice, 10-12 parts of radix sophorae flavescentis and 2-7 parts of folium artemisiae argyi.
As a further preferred embodiment, the traditional Chinese medicine extract composition comprises the following components in parts by weight: 33 parts of polygonatum odoratum, 31 parts of radix ophiopogonis, 18 parts of liquorice, 12 parts of radix sophorae flavescentis and 6 parts of folium artemisiae argyi; or preferably, 36 parts of polygonatum, 30 parts of radix ophiopogonis, 18 parts of liquorice, 11 parts of radix sophorae flavescentis and 5 parts of folium artemisiae argyi; or preferably, 39 parts of polygonatum, 28 parts of radix ophiopogonis, 19 parts of liquorice, 10 parts of radix sophorae flavescentis and 4 parts of folium artemisiae argyi.
The composition can be used for preventing skin dryness and allergy.
On the other hand, the invention also provides a preparation method for preparing the traditional Chinese medicine extract composition, which comprises the following steps:
(1) pretreating medicinal materials: weighing the traditional Chinese medicine raw materials, crushing, grinding, sieving and uniformly mixing;
(2) extraction: adding the mixture of the medicinal materials into 60-75% ethanol water solution, soaking at the temperature of 30-40 ℃, performing ultrasonic treatment, and performing hot reflux extraction to obtain an extracting solution;
(3) and (3) purification: and (3) centrifuging the extracting solution at a high speed, filtering, concentrating in vacuum, precipitating with 75-85% ethanol water solution, and freeze-drying the precipitate.
The traditional Chinese medicine extract composition is mainly applied to cosmetics, but specific cosmetics are not particularly limited. The cosmetic can be bath lotion, facial cleanser or essence; but is particularly preferably a body wash.
In a further aspect, the invention provides a cosmetic formulation comprising the above-described herbal extract composition, wherein the composition is present in an amount of 0.05-18% by weight.
As a preferred embodiment, the cosmetic product comprises said composition in an amount of 5-12% by weight.
In another aspect, the invention provides a body wash containing the traditional Chinese medicine composition, which comprises the following components in parts by weight: 7-14 parts of ammonium lauryl sulfate, 5-12 parts of sodium laureth sulfate, 2-8 parts of cocamidopropyl betaine, 0.5-1.5 parts of cocamide MEA, 1-5 parts of glycerol, 1-3 parts of ethylene glycol distearate, 0.3-0.8 part of hydroxypropyl methyl cellulose, 0.01-0.3 part of hyaluronic acid, 1-3 parts of sorbitol, 0.5-1.5 parts of sodium chloride, 0.3-1 part of phenoxyethanol, 0.2-0.3 part of sodium benzoate, 0.05-18 parts of a traditional Chinese medicine extraction composition and 62.5-81.2 parts of water.
The invention has the following beneficial effects:
the dry-sensitive extract composition is added into cosmetics, can resist skin dryness, resist micro itching, preserve moisture and nourish skin, enhances skin immunity by repairing natural skin barriers, improves skin moisturizing capability and relieves skin. When added into cosmetics, the anti-allergic effect is remarkable.
In the prior art, various traditional Chinese medicine extracts are found to have the effects of moistening, moisturizing, resisting bacteria and resisting allergy. However, when the traditional Chinese medicine extracts are applied independently, the effects of moistening and moisturizing, resisting bacteria and resisting allergy are not obvious, and the requirement of resisting dry allergy is difficult to meet. Although at present, a small part of the compound traditional Chinese medicine extract composition is also available, the anti-allergy effect is not obvious and even reduced; after a large number of compound formulas are screened, the invention discovers that the five traditional Chinese medicine extracts of polygonatum, ophiopogon root, liquorice, sophora flavescens and artemisia argyi can obtain obvious anti-allergic effect after being compounded, and the five components have synergistic effect. The traditional Chinese medicine extract is practically applied to cosmetics such as shower gel and the like, the anti-allergy effect is obvious, and experiments prove that the composition of the polygonatum, the radix ophiopogonis, the liquorice, the radix sophorae flavescentis and the folium artemisiae argyi has no irritation to a human body.
Drawings
FIG. 1 is a relational diagram of the anti-itch, anti-scaling and tightness tests of the shower gel prepared by a single traditional Chinese medicine extract and a traditional Chinese medicine extract composition.
FIG. 2 is a diagram showing the relationship between the extracts of various Chinese herbs and the bath lotion prepared from the composition of Chinese herbs for anti-itch, anti-scaling and tightening.
FIG. 3 is a diagram showing the relationship of a bath lotion prepared from a single Chinese medicinal extract, multiple Chinese medicinal extracts and an anti-allergy Chinese medicinal extract in a moisture retention test.
Detailed Description
The technical solutions of the present invention are further illustrated by the following specific examples, which do not represent limitations to the scope of the present invention. Insubstantial modifications and adaptations of the present invention by others of the concepts fall within the scope of the invention.
Example 1 anti-allergic traditional Chinese medicine extract composition (1) formula and preparation method
A Chinese medicinal extract composition with anti-allergic effect comprises Chinese medicinal materials in weight parts shown in Table (1)
TABLE 1 compositions (1)
The preparation method of the traditional Chinese medicine extract composition comprises the following steps:
(1) taking 100g of 5 traditional Chinese medicinal materials according to the weight part relation of the table 1, crushing, grinding, sieving by a 10-mesh sieve, and then uniformly mixing for later use.
(2) Adding 0.8L volume ratio ethanol water solution as extraction solvent, soaking for 1h, performing ultrasonic extraction at 35 deg.C for 30min, and extracting under reflux for 2h each time for 3 times to obtain extractive solution.
(3) Centrifuging the extractive solution at high speed, filtering, vacuum concentrating, precipitating with 80% ethanol water solution, and freeze drying the precipitate.
Example 2 anti-allergic traditional Chinese medicine extract composition (2) formula and preparation method
The formulation of composition (2) is shown in Table 2, and the preparation method is the same as that of example 1
TABLE 2 compositions (2)
| Components | Parts by weight |
| Radix polygonati officinalis | 36 |
| Radix Ophiopogonis | 30 |
| Licorice root, radix Glycyrrhizae | 18 |
| Sophora flavescens ait | 11 |
| |
5 |
Example 3 anti-allergic traditional Chinese medicine extract composition (3) formula and preparation method
The formulation of composition (3) is shown in Table 3, and the preparation method is the same as that of example 1
TABLE 3 compositions (3)
| Components | Parts by weight |
| Radix polygonati officinalis | 39 |
| Radix Ophiopogonis | 28 |
| Licorice root, radix Glycyrrhizae | 19 |
| Sophora flavescens ait | 10 |
| Folium Artemisiae Argyi | 4 |
Example 4 anti-allergy body wash
TABLE 4 anti-allergic bath lotion
The preparation method of the anti-allergy body wash comprises the following steps:
(1) adding sodium laureth sulfate into water, heating to 75-85 deg.C for dissolving, adding ammonium laureth sulfate, and stirring for dissolving.
(2) Pre-dispersing hydroxypropyl methyl cellulose by using glycerol, then adding the obtained product into the step (1), stirring, dispersing and dissolving, adding the cocamide MEA, the ethylene glycol distearate and the sodium benzoate after dissolving, adding the obtained mixture into the obtained product, dissolving, keeping the temperature for 15 minutes, and cooling.
(3) Cooling to 50 deg.C, adding cocamidopropyl betaine and sodium chloride, cooling to 40 deg.C, adding phenoxyethanol and anti-dry-sensitive Chinese medicinal extract composition (no composition is added in bath lotion 4), stirring for ten minutes, vacuumizing, inspecting, and discharging.
Comparative example 1 preparation of extract of single Chinese medicine
TABLE 5 extracts of the individual Chinese herbs
The preparation methods of comparative groups 1 to 5 were the same as in example 1 except that the herbal ingredients were Yuzhu, Maidong, gan Cao, ku shen and ai Ye, respectively. Thereby respectively preparing 100g of polygonatum extract, 100g of ophiopogon root extract, 100g of liquorice extract, 100g of sophora flavescens extract and 100g of artemisia leaf extract.
Shower gels 5-9 were prepared using the extracts of comparative groups 1-5. Wherein, except that the extracts are respectively single medicine extracts, the types, the contents and the preparation method of the other components are the same as the shower gel 1.
COMPARATIVE EXAMPLE 2 PREPARATION OF MULTI-TAPE TRADITIONAL CHINESE MEDICINE EXTRACTS
Comparative group 6: the difference from example 1 is that comparative group 6 does not contain the artemisia argyi extract.
Comparative group 7: the difference from example 1 is that comparative group 7 does not contain the sophora flavescens extract.
Comparative group 8: the difference from example 1 is that comparative group 8 does not contain an extract of ophiopogon root.
Comparative group 9: the difference from example 1 is that comparative group 9 did not contain licorice extract.
Comparative group 10: the difference from example 1 is that comparative group 10 did not contain Yuzhu extract.
Shower gels 10-14 were prepared using extracts of comparative groups 6-10. Wherein, except for different extracts, the other components, types, contents and preparation methods are the same as those of the shower gel 1.
Example 5 human Patch test
1. The test substance: 4 anti-allergy shower gels in embodiment 4 of the invention, namely shower gel 1, shower gel 2, shower gel 3 and shower gel 4;
2. subject: a total of 60 men, 35 women, age 20-55 years, meeting the volunteer enrollment criteria of the subject;
3. the test method comprises the following steps: placing the tested object in a proper spot sticking device by adopting a closed test method, sticking the tested object on the arm curve side of the tested object by using a hypoallergenic adhesive tape, lightly pressing the tested object by using a palm to uniformly stick the tested object on the skin, and continuing for 24 hours; blank control group means that subjects did not use body wash;
4. and (4) observing results: the test devices were removed after 24 hours, skin reactions were observed after 0.5h, 24h, 48h, respectively, and the results were recorded. The grade of adverse reaction of the skin is shown in Table 6, and the test results are shown in Table 7.
TABLE 6 skin reaction grading Standard for skin Enclosed Patch test
TABLE 7 test results of human skin patches
The results show that in 60 subjects, 0 of the shower gel 1, the shower gel 2 and the shower gel 3 has skin adverse reactions, and 5 of the shower gel 4 has grade-1 adverse reactions and grade-1 adverse reactions, which indicates that the anti-dry-allergy shower gel of embodiment 4 of the invention is safe and non-irritant, and the anti-dry-allergy Chinese medicinal extract composition can have a remarkable anti-dry-allergy effect on the skin.
Example 6 Instrument efficacy evaluation, human sensory evaluation
300 volunteers who are easy to be sensitive and easy to itch and have dry skin which is easy to be scaled up are selected, 20 volunteers are selected in each group after the group is formed, the group is continuously used for 4 weeks, and the results shown in table 8 are finally obtained.
Table 8: efficacy evaluation test results of examples and comparative examples
Fig. 1, 2, and 3 were obtained from the data in table 8.
FIG. 1 is a relational diagram of the anti-itch, anti-scaling and tightness tests of the shower gel prepared by a single traditional Chinese medicine extract and a traditional Chinese medicine extract composition.
FIG. 2 is a diagram showing the relationship between the extracts of various Chinese herbs and the bath lotion prepared from the composition of Chinese herbs for anti-itch, anti-scaling and tightening.
FIG. 3 is a diagram showing the relationship between a single herb extract and a plurality of herb extracts and a body wash prepared from anti-allergy herb extracts in a moisture retention test.
As can be seen from the above experimental data and fig. 1 to 3, the bath lotion 1 to 3 in example 4 has significantly improved moisturizing effect, and significantly improved degree of itching and scales, compared with the bath lotion 4, which indicates that the herbal extract has significant anti-allergy effect.
Compared with the shower gels 5-9 in the comparative example 1 and the shower gels 10-14 in the comparative example 2, the skin moisturizing effect is obviously improved, the itching degree is obviously reduced, the scales are obviously improved, the foam is rich, and the volunteers do not feel tight after the shower gels 1-3 in the example 4 are used. The anti-dry-allergy traditional Chinese medicine extract composition has more remarkable anti-dry-allergy effect, more excellent foam and better moisturizing effect than any four combinations of single traditional Chinese medicine extracts or traditional Chinese medicine extract compositions. In addition, compared with the commercial shower gel, the shower gel 1-3 provided by the invention has a remarkable use effect.
The above results show that the traditional Chinese medicine extract composition of the invention has the efficacy of anti-allergy and the synergistic effect among the components.
Having described preferred embodiments of the present invention in detail, it is believed that the inventors have expended considerable effort and time and, as a result of their several experiments, it will be appreciated that many modifications and variations are possible in light of the above teaching without undue experimentation.
Claims (15)
1. The composition is characterized by comprising the following components in parts by weight: 32-45 parts of radix polygonati officinalis, 25-35 parts of radix ophiopogonis, 15-24 parts of liquorice, 9-13 parts of radix sophorae flavescentis and 3-8 parts of folium artemisiae argyi; the composition is used for preventing skin dryness and allergy.
2. The composition according to claim 1, characterized by comprising the following components in parts by weight: 34-43 parts of radix polygonati officinalis, 27-33 parts of radix ophiopogonis, 17-23 parts of liquorice, 10-13 parts of radix sophorae flavescentis and 3-7 parts of folium artemisiae argyi.
3. The composition according to claim 1, characterized by comprising the following components in parts by weight: 36-41 parts of polygonatum odoratum, 28-32 parts of radix ophiopogonis, 19-23 parts of liquorice, 10-12 parts of radix sophorae flavescentis and 2-7 parts of folium artemisiae argyi.
4. The composition according to claim 1, characterized by comprising the following components in parts by weight: 33 parts of polygonatum odoratum, 31 parts of radix ophiopogonis, 18 parts of liquorice, 12 parts of radix sophorae flavescentis and 6 parts of folium artemisiae argyi.
5. The composition according to claim 1, characterized by comprising the following components in parts by weight: 36 parts of polygonatum, 30 parts of radix ophiopogonis, 18 parts of liquorice, 11 parts of radix sophorae flavescentis and 5 parts of folium artemisiae argyi.
6. The composition of claim 1, comprising the following components in parts by weight: 39 parts of polygonatum, 28 parts of radix ophiopogonis, 19 parts of liquorice, 10 parts of radix sophorae flavescentis and 4 parts of folium artemisiae argyi.
7. A process for preparing a composition according to any one of claims 1 to 6, comprising the steps of:
(1) pretreating medicinal materials: weighing the traditional Chinese medicine raw materials, crushing, grinding, sieving and uniformly mixing;
(2) extraction: adding the mixture of the medicinal materials into a 60-75% ethanol water solution, soaking at the temperature of 30-40 ℃, performing ultrasonic treatment, and performing hot reflux extraction to obtain an extracting solution;
(3) and (3) purification: and (3) centrifuging the extracting solution at a high speed, filtering, concentrating in vacuum, precipitating with 75-85% ethanol water solution, and freeze-drying the precipitate.
8. Use of a composition according to any one of claims 1 to 6 in cosmetics.
9. A cosmetic product comprising the composition of any one of claims 1 to 6, wherein the composition is present in the cosmetic product in an amount of from 0.05 to 18% by weight.
10. The cosmetic according to claim 9, wherein the composition is contained in the cosmetic in an amount of 5 to 12% by weight.
11. The use of claim 8, wherein the cosmetic is a body wash, facial cleanser, or essence.
12. The cosmetic according to claim 9, wherein the cosmetic is a body wash, a face wash or an essence.
13. Use according to claim 8, characterized in that the cosmetic product is a body wash.
14. The cosmetic according to claim 9, wherein the cosmetic is a body wash.
15. The shower gel containing the composition of any one of claims 1 to 6, which is characterized by comprising the following components in parts by weight: 7-14 parts of ammonium lauryl sulfate, 5-12 parts of sodium laureth sulfate, 2-8 parts of cocamidopropyl betaine, 0.5-1.5 parts of cocamide MEA, 1-5 parts of glycerol, 1-3 parts of ethylene glycol distearate, 0.3-0.8 part of hydroxypropyl methyl cellulose, 0.01-0.3 part of hyaluronic acid, 1-3 parts of sorbitol, 0.5-1.5 parts of sodium chloride, 0.3-1 part of phenoxyethanol, 0.2-0.3 part of sodium benzoate, 0.05-18 parts of a traditional Chinese medicine extraction composition and 62.5-81.2 parts of water.
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