CN113144126A - Compound Chinese medicinal preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff, and its preparation method and application - Google Patents
Compound Chinese medicinal preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff, and its preparation method and application Download PDFInfo
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Abstract
The invention discloses a compound traditional Chinese medicine preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff, and a preparation method and application thereof, wherein the compound traditional Chinese medicine preparation comprises a compound traditional Chinese medicine composition and a solvent, and the compound traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 10-15 parts of cacumen biotae, 20-25 parts of prepared fleece-flower root, 10-15 parts of glossy privet fruit, 10-15 parts of galangal, 8-10 parts of black mulberry fruit, 8-10 parts of astragalus membranaceus, 10-15 parts of black wolfberry, 8-12 parts of yam root, 6-9 parts of lotus stamen, 6-10 parts of dodder, 10-15 parts of eclipta prostrata, 8-10 parts of angelica sinensis, 8-10 parts of ligusticum wallichii, 8-10 parts of cortex dictamni and 8-10 parts of sophora flavescens. According to the compound traditional Chinese medicine preparation for hair growth, whitening prevention, oil control and dandruff removal and the preparation method and application thereof, the compound traditional Chinese medicine composition in the compound traditional Chinese medicine preparation conforms to the monarch, minister, assistant and guide principle in the traditional Chinese medicine theory, so that the compound traditional Chinese medicine preparation is safe, nontoxic, mild and non-irritant, has the effects of hair nourishing and hair care, whitening prevention, oil control and dandruff removal, inflammation diminishing, itching relieving and oil removal, and shampoo and scalp essence applied as products have the effect of conditioning scalp and hair follicle health.
Description
Technical Field
The invention relates to the technical field of hair care and nourishing products, in particular to a compound traditional Chinese medicine preparation for growing hair, preventing whitening, controlling oil and removing dandruff, and a preparation method and application thereof.
Background
Modern medicine considers that seborrheic alopecia is related to a plurality of influencing factors such as diseases, psychology, medicines, heredity, spirit, age, environmental seasons and the like, and the main reason is that excessive sebum secretion is accumulated around hair follicles, even follicle pores are pressed or blocked, and normal growth of hairs is hindered. Meanwhile, the patient's hair follicles are hypersensitive to androgens, and relatively high androgen levels cause shortening of the anagen phase of hairs, atrophy, degeneration and shedding of hair follicles, thereby gradually thinning the hairs. The hair whitening is related to nervous system dysfunction and immune response, and is caused by excessive anxiety, physical weakness due to chronic diseases or deficiency of heart blood and insufficiency of liver and spleen, so blood stasis and hair loss are caused to block blood paths, and the heart blood can not nourish hair, so the hair whitening is caused by hair loss. The products for preventing alopecia and blackening white hair on the market are not few, but because the medicine formula is not perfect and reasonable enough, or because the preparation process and the preparation form are not favorable for fully exerting the medicine efficacy, the ideal effect of the treatment can not be achieved generally, and the problem of diversified scalp of people is difficult to solve.
The scalp is used as soil for the hair to live, and the balance of the ecological environment is the basis of healthy growth of the hair. The scalp oil is a scalp greasy phenomenon caused by the damage of the ecological balance of the scalp and the imbalance of the secretion of scalp oil, and causes a plurality of scalp problems of scurf, itching or increased head oil and the like. At present, shampoo on the market mostly adopts chemical synthetic raw materials with bacteriostatic action to solve the effects of controlling oil and removing dandruff of scalp, for example: salicylic acid, piroctone olamine salt, zinc pyrithione and the like can solve the above problems to some extent, but the excessive removal of the cuticle causes deterioration of the scalp defense, and erythema, itching, stinging or allergy sometimes occurs, and is hardly applicable to sensitive scalp people.
The invention designs the preparation and application of the compound traditional Chinese medicine composition on the basis of the traditional Chinese medicine theory and by combining with the living habits of modern people, so as to solve the scalp problems of people who suffer from alopecia, white hair, oily hair, dandruff and the like. And the pure traditional Chinese medicine has no toxic or side effect and has good application prospect.
Disclosure of Invention
The invention aims to provide a compound traditional Chinese medicine preparation for hair growth, whitening prevention, oil control and dandruff removal and a preparation method and application thereof.
In order to achieve the aim, the invention provides a compound traditional Chinese medicine preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff, which comprises a compound traditional Chinese medicine composition and a solvent, wherein the mass ratio of the compound traditional Chinese medicine composition to the solvent is 1:10, and the compound traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 10-15 parts of cacumen biotae, 20-25 parts of prepared fleece-flower root, 10-15 parts of glossy privet fruit, 10-15 parts of galangal, 8-10 parts of black mulberry fruit, 8-10 parts of astragalus membranaceus, 10-15 parts of black wolfberry, 8-12 parts of yam root, 6-9 parts of lotus stamen, 6-10 parts of dodder, 10-15 parts of eclipta prostrata, 8-10 parts of angelica sinensis, 8-10 parts of ligusticum wallichii, 8-10 parts of cortex dictamni and 8-10 parts of sophora flavescens, wherein the solvent is water or an ethanol water solution, and the ethanol content in the ethanol water solution accounts for 1-75 wt%.
Preferably, the compound traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 10 parts of cacumen biotae, 25 parts of prepared fleece-flower root, 13 parts of glossy privet fruit, 13 parts of galangal, 8 parts of black mulberry fruit, 8 parts of astragalus membranaceus, 15 parts of black wolfberry, 12 parts of yam root, 6 parts of stamen nelumbinis, 6 parts of semen cuscutae, 13 parts of eclipta prostrata, 9 parts of angelica sinensis, 9 parts of ligusticum wallichii, 10 parts of cortex dictamni and 9 parts of sophora flavescens.
Preferably, the compound traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 15 parts of cacumen biotae, 20 parts of prepared fleece-flower root, 15 parts of glossy privet fruit, 10 parts of galangal, 10 parts of black mulberry fruit, 9 parts of astragalus membranaceus, 10 parts of black wolfberry, 10 parts of yam root, 9 parts of stamen nelumbinis, 9 parts of semen cuscutae, 15 parts of eclipta prostrata, 8 parts of angelica sinensis, 8 parts of ligusticum wallichii, 8 parts of cortex dictamni and 10 parts of sophora flavescens.
Preferably, the compound traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 13 parts of cacumen biotae, 23 parts of prepared fleece-flower root, 10 parts of glossy privet fruit, 15 parts of galangal, 9 parts of black mulberry fruit, 10 parts of astragalus membranaceus, 13 parts of black wolfberry, 8 parts of yam root, 8 parts of stamen nelumbinis, 10 parts of semen cuscutae, 10 parts of eclipta prostrata, 10 parts of angelica sinensis, 10 parts of ligusticum wallichii, 9 parts of cortex dictamni and 8 parts of sophora flavescens.
The preparation method of the compound traditional Chinese medicine preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff comprises the following steps:
(1) putting the compound traditional Chinese medicine composition with the formula amount into a pulverizer, pulverizing into powder, and sieving with a 50-mesh sieve to obtain crude medicinal powder for later use;
(2) placing the crude powder in an extraction soaking tank, adding 5-10 times of 75 wt% ethanol, soaking for 24-72 hr under sealed condition, and maintaining the temperature at 35-40 deg.C;
(3) intermittently stirring the substances in the extraction and soaking tank in the step (2), stirring once every 2-5 h, 20-30min each time, rotating speed of 150-;
(4) adding 5-10 times of 50 wt% ethanol into the dregs obtained after filtration in the step (3), soaking in a sealed environment for 24-72h, keeping the temperature between 35-40 ℃, stirring intermittently, stirring once every 2-5 h, 20-30min each time, rotating at the speed of 150-200r/min, centrifugally separating the mixture, and filtering with a microporous membrane to obtain a secondary extracting solution for later use;
(5) and (3) combining the primary extracting solution in the step (3) and the secondary extracting solution in the step (4), filtering by using a 0.1-1 mu m microporous filter membrane to obtain a refined extracting solution, aging for 24 hours, and sterilizing at high temperature to obtain the compound traditional Chinese medicine preparation.
The application of the compound Chinese medicinal preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff comprises the following steps: and adding the auxiliary material A into the compound traditional Chinese medicine preparation to prepare the anti-dandruff oil-control shampoo. The anti-dandruff oil-control shampoo comprises the following components in parts by weight: 1-40 parts of compound traditional Chinese medicine preparation, 8-12 parts of sodium laureth sulfate, 3-10 parts of cocamidopropyl betaine, 1-5 parts of sodium laureth sulfate, 0.3-2 parts of cocamide MEA, 100.2-0.5 part of polyquaternary ammonium salt, 0.1-0.5 part of hydroxypropyl guar hydroxypropyl trimethyl ammonium chloride, 0.1-0.2 part of camellia oil, 0.05-0.2 part of fructo-oligosaccharide, 0.05-0.2 part of sodium hyaluronate, 0.1-0.5 part of citric acid, 0.05-0.2 part of preservative, 0.3-0.8 part of essence and 100 parts of water.
The application of the compound Chinese medicinal preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff comprises the following steps: and adding the auxiliary material B into the compound traditional Chinese medicine preparation to prepare the softening shampoo. The softening shampoo comprises the following components in parts by weight: 1-30 parts of a compound traditional Chinese medicine preparation; 10-20 parts of cocoyl sarcosine sodium; 5-10 parts of cocoyl sodium glycinate; 1-5 parts of sodium lauroamphoacetate; 1-5 parts of decyl glucoside; 0.5-2 parts of guar hydroxypropyl trimethyl ammonium chloride; 0.1-0.5 part of acrylic acid (ester)/C10-30 alkanol acrylate crosslinked polymer; 1-5 parts of cocoyl hydroxy sulfobetaine; 100.5-2 parts of polyquaternium; 0.1-0.5 part of arginine; 0.1-1 part of panthenol; 0.1-0.5 parts of hydrolyzed wheat protein; 0.1-0.5 part of citric acid; 0.05-0.2 part of preservative; 0.3-0.8 part of essence and 100 parts of water.
The application of the compound Chinese medicinal preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff comprises the following steps: and adding the auxiliary material C into the compound traditional Chinese medicine preparation to prepare the scalp essence. The scalp essence comprises the following components in parts by weight: 40-70 parts of compound traditional Chinese medicine preparation, 0.2-2 parts of panthenol, 0.1-0.5 part of pyridoxine HCl, 0.5-1 part of dipotassium glycyrrhizinate, 0.05-0.2 part of preservative and 100 parts of water.
Therefore, the compound Chinese medicinal preparation for hair growth and whitening prevention, oil control and dandruff removal and the preparation method and application thereof adopt the structure, and the compound Chinese medicinal composition in the compound Chinese medicinal preparation conforms to the monarch, minister, assistant and guide principle in the Chinese medicinal theory, so the compound Chinese medicinal preparation is safe, nontoxic, mild and non-irritant, has the effects of hair nourishing and hair care, hair growth and whitening prevention, oil control and dandruff removal, inflammation diminishing and itching relieving and oil removal, and shampoo and scalp essence which are applied products have the effect of conditioning scalp and hair follicle health.
The technical solution of the present invention is further described in detail by the following examples.
Detailed Description
The embodiments of the present invention will be further explained below.
A compound traditional Chinese medicine preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff comprises a compound traditional Chinese medicine composition and a solvent, wherein the mass ratio of the compound traditional Chinese medicine composition to the solvent is 1:10, and the compound traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 10-15 parts of cacumen biotae, 20-25 parts of prepared fleece-flower root, 10-15 parts of glossy privet fruit, 10-15 parts of galangal, 8-10 parts of black mulberry fruit, 8-10 parts of astragalus membranaceus, 10-15 parts of black wolfberry, 8-12 parts of yam root, 6-9 parts of stamen nelumbinis, 6-10 parts of dodder, 10-15 parts of eclipta prostrata, 8-10 parts of angelica sinensis, 8-10 parts of ligusticum wallichii, 8-10 parts of cortex dictamni and 8-10 parts of radix sophorae flavescentis, wherein the solvent is water or an ethanol water solution, and the ethanol content in the ethanol water solution accounts for 1-75 wt%.
The preparation method of the compound traditional Chinese medicine preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff comprises the following steps:
(1) putting the compound traditional Chinese medicine composition with the formula amount into a pulverizer, pulverizing into powder, and sieving with a 50-mesh sieve to obtain crude medicinal powder for later use;
(2) placing the crude powder in an extraction soaking tank, adding 5-10 times of 75 wt% ethanol, soaking for 24-72 hr under sealed condition, and maintaining the temperature at 35-40 deg.C;
(3) intermittently stirring the substances in the extraction and soaking tank in the step (2), stirring once every 2-5 h, 20-30min each time, rotating speed of 150-;
(4) adding 5-10 times of 50 wt% ethanol into the dregs obtained after filtration in the step (3), soaking in a sealed environment for 24-72h, keeping the temperature between 35-40 ℃, stirring intermittently, stirring once every 2-5 h, 20-30min each time, rotating at the speed of 150-200r/min, centrifugally separating the mixture, and filtering with a microporous membrane to obtain a secondary extracting solution for later use;
(5) and (3) combining the primary extracting solution in the step (3) and the secondary extracting solution in the step (4), filtering by using a 0.1-1 mu m microporous filter membrane to obtain a refined extracting solution, aging for 24 hours, and sterilizing at high temperature to obtain the compound traditional Chinese medicine preparation.
The compound traditional Chinese medicine preparation has the following effects of components:
1. preparing fleece-flower root: tonifying essence and blood, checking malaria, detoxifying, moistening intestines and relaxing bowels; replenishing essence and blood, blackening hair and beard, strengthening bones and muscles, eliminating turbid pathogen and reducing blood fat. It contains lecithin and other nutritious components, and has the functions of nourishing blood, dispelling wind, regulating nerve and endocrine function, nourishing hair root, promoting the generation of hair melanin and blackening hair. Meanwhile, the fleece-flower root also contains chrysophanol and a large amount of starch, and after the starch is hydrolyzed, glucose can be generated, so that the fleece-flower root has a good hair-moistening effect and is the best traditional Chinese medicine raw material for preparing the hair conditioner.
2. Cacumen biotae: cooling blood, stopping bleeding, eliminating phlegm, relieving cough, promoting hair growth and blackening hair; can be used for treating hemorrhage, cough due to lung heat, scald, and alopecia due to blood heat.
3. Glossy privet fruit: tonifying liver and kidney, improving eyesight, and clearing away deficiency heat; can be used for treating dizziness, premature gray hair, blurred vision, and fever due to yin deficiency. Nourishing liver and kidney, improving eyesight, blackening hair, preventing alopecia and diminishing inflammation, contains abundant oleanolic acid, and has anti-alopecia and anti-inflammatory effects.
4. Galangal rhizome: warming stomach to arrest vomiting, dispelling cold to relieve pain; has antiinflammatory, antibacterial, antioxidant, antiinflammatory, blood circulation promoting, bacteria growth inhibiting, dandruff removing, antiinflammatory, and antipruritic effects. Promoting the absorption of nutrition by hair follicle tissues and promoting the growth of hair.
5. Black mulberry fruit: nourishing yin and blood, moistening intestines and promoting the production of body fluid; the mulberry contains glucose, sucrose, fructose, carotene, vitamins, malic acid, tartaric acid, mineral calcium, phosphorus, iron, copper, zinc and the like, can effectively supplement the trace elements, and has the effects of dispelling wind heat, healing wound pain, blackening beard and hair, resisting aging and the like.
6. Astragalus membranaceus (bge.) membranaceus: invigorating qi, invigorating yang, consolidating superficial resistance, arresting sweating, inducing diuresis, relieving swelling, promoting fluid production, nourishing blood, removing stagnation, relieving arthralgia, expelling toxin, expelling pus, healing sore, and promoting granulation.
7. Black wolfberry fruit: nourishing liver and kidney, improving eyesight, and moistening lung. Can be used for treating deficiency of liver-yin and kidney-yin, dizziness, blurred vision, visual deterioration, soreness of waist and knees, nocturnal emission, diabetes, and cough due to yin deficiency. Nourishing liver, improving eyesight, invigorating kidney, replenishing vital essence, resisting aging, and delaying aging.
8. Rhizoma dioscoreae root: before arthralgia due to wind-dampness; numbness of limbs; chest stuffiness and pain; chronic tracheitis; traumatic injury; abuse; abscess and swelling.
9. And (3) lotus stamen: has effects in clearing away heart-fire, invigorating kidney, stopping nocturnal emission, stopping bleeding, relieving summer-heat, relieving restlessness, promoting salivation, quenching thirst, regulating heart-qi, caring skin, and blackening hair. It is indicated for nocturnal emission, vomiting, epistaxis, metrorrhagia, leukorrhagia, dysentery, etc. It is suitable for patients with various symptoms such as restlessness, hemorrhage, premature gray hair, and male facial disability.
10. Dodder seed: has effects in invigorating kidney, nourishing liver, improving eyesight, consolidating fetus, and relieving diarrhea.
11. Snakehead intestine: tonify liver and kidney yin, cool blood and stop bleeding. The efficacy is as follows: is suitable for treating early white beard and hair, dizziness, insomnia, dreaminess, soreness of waist and knees, nocturnal emission, tinnitus, etc. caused by liver and kidney yin deficiency or yin deficiency and internal heat, and can blacken hair by invigorating liver and kidney.
12. Chinese angelica: enriching blood, promoting blood circulation, moistening dryness, smoothing intestine, dilating capillary vessels of scalp, strengthening hair, activating scalp, and preventing alopecia.
13. Ligusticum wallichii: has effects of promoting blood circulation, activating qi-flowing, dispelling pathogenic wind and relieving pain. The extract can expand head capillary, promote blood circulation, increase hair nutrition, make hair have good flexibility and function of not becoming brittle easily, improve hair tensile strength and extensibility, and delay growth of canities.
14, cortex dictamni: has the effects of clearing heat, eliminating dampness, dispelling wind, relieving itching and detoxifying.
15. Flavescent sophora root: has effects of clearing heat, eliminating dampness, inhibiting bacteria, relieving itching, promoting blood circulation, removing blood stasis, and promoting urination.
16. The ethanol has effects of relieving inflammation and promoting rapid absorption of scalp.
The compound traditional Chinese medicine composition disclosed by the invention selects natural traditional Chinese medicines based on the monarch, minister, assistant and assistant theory, and each medicinal material has the same effect and is coordinated with each other aiming at the pathogenesis of poliosis, alopecia, dandruff and the like. The Chinese arborvitae twig is used as a monarch drug for treating alopecia, has the main effects of preventing alopecia, growing hair and blackening hair, the tuber fleeceflower root and the glossy privet fruit are used as ministerial drugs, and the galangal, the black mulberry fruit, the astragalus membranaceus, the black medlar, the yam root, the stamen nelumbinis, the dodder, the snakehead intestine, the Chinese angelica, the ligusticum wallichii, the cortex dictamni and the radix sophorae flavescentis are used as adjuvant drugs to form a compound.
The application of the compound Chinese medicinal preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff comprises the following steps:
1. and adding the auxiliary material A into the compound traditional Chinese medicine preparation to prepare the anti-dandruff oil-control shampoo. The anti-dandruff oil-control shampoo comprises the following components in parts by weight: 1-40 parts of compound traditional Chinese medicine preparation, 8-12 parts of sodium laureth sulfate, 3-10 parts of cocamidopropyl betaine, 1-5 parts of sodium laureth sulfate, 0.3-2 parts of cocamide MEA, 100.2-0.5 part of polyquaternary ammonium salt, 0.1-0.5 part of hydroxypropyl guar hydroxypropyl trimethyl ammonium chloride, 0.1-0.2 part of camellia oil, 0.05-0.2 part of fructo-oligosaccharide, 0.05-0.2 part of sodium hyaluronate, 0.1-0.5 part of citric acid, 0.05-0.2 part of preservative, 0.3-0.8 part of essence and 100 parts of water.
The preparation method of the anti-dandruff oil-control shampoo comprises the following steps:
(1) stirring at room temperature, adding polyquaternium-10 and hydroxypropyl guar hydroxypropyl trimethyl ammonium chloride in a formula amount into water, dispersing until no agglomeration exists, heating to 75-85 ℃, and uniformly stirring until no particles exist;
(2) adding fructo-oligosaccharide, sodium hyaluronate, sodium laureth sulfate, cocamidopropyl betaine, sodium laureth sulfate and cocamide MEA, stirring to be uniform, and vacuumizing and homogenizing;
(3) cooling to 40-45 deg.C, adding compound Chinese medicinal preparation, antiseptic and essence, and adjusting pH to 5.5-6 with citric acid.
The compound traditional Chinese medicine preparation is prepared according to the general steps of shampoo after being added. The hair washed by the shampoo is dry and is also treated by hair conditioner. The added fructo-oligosaccharide can regulate the balance of scalp flora and inhibit the growth of harmful bacteria, thereby further improving the problems of scurf, oil production and itching of the head; hyaluronic acid can effectively repair damaged hair, so that the hair is soft, bright and smooth; the camellia oil nourishes hair from root to tip, and simultaneously, the scalp protection function is enhanced, and external pollution and stimulation are resisted. By using the anti-dandruff and oil-control shampoo, no additional hair conditioner is needed for nursing, and after the shampoo is used, hair is clean and smooth, and the effects of oil control, dandruff control and alopecia prevention can be effectively achieved.
2. And adding the auxiliary material B into the compound traditional Chinese medicine preparation to prepare the softening shampoo. The softening shampoo comprises the following components in parts by weight: 1-30 parts of a compound traditional Chinese medicine preparation; 10-20 parts of cocoyl sarcosine sodium; 5-10 parts of cocoyl sodium glycinate; 1-5 parts of sodium lauroamphoacetate; 1-5 parts of decyl glucoside; 0.5-2 parts of guar hydroxypropyl trimethyl ammonium chloride; 0.1-0.5 part of acrylic acid (ester)/C10-30 alkanol acrylate crosslinked polymer; 1-5 parts of cocoyl hydroxy sulfobetaine; 100.5-2 parts of polyquaternium; 0.1-0.5 part of arginine; 0.1-1 part of panthenol; 0.1-0.5 parts of hydrolyzed wheat protein; 0.1-0.5 part of citric acid; 0.05-0.2 part of preservative; 0.3-0.8 part of essence and 100 parts of water.
The preparation method of the softening shampoo comprises the following steps:
(1) stirring at room temperature, adding polyquaternium-10 and hydroxypropyl guar hydroxypropyl trimethyl ammonium chloride in formula amount into water, dispersing until no agglomeration, heating to 75-80 deg.C, and stirring uniformly until no granule exists;
(2) sequentially adding sodium cocoyl sarcosinate, sodium cocoyl glycinate, sodium lauroyl amphoacetate, decyl glucoside, cocoyl sulfobetaine and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, and stirring to be uniform;
(3) cooling to 60 deg.C, adding arginine, cooling to 40-45 deg.C, adding hydrolyzed wheat protein, compound Chinese medicinal preparation, antiseptic and essence, and adjusting pH to 5.5-6 with citric acid.
3. And adding the auxiliary material C into the compound traditional Chinese medicine preparation to prepare the scalp essence. The scalp essence comprises the following components in parts by weight: 40-70 parts of compound traditional Chinese medicine preparation, 0.2-2 parts of panthenol, 0.1-0.5 part of pyridoxine HCl, 0.5-1 part of dipotassium glycyrrhizinate, 0.05-0.2 part of preservative and 100 parts of water.
The preparation method of the scalp essence comprises the following steps:
heating water to 75-80 deg.C, sterilizing, cooling to 40-45 deg.C, adding the rest materials, and stirring.
Example 1 Compound Chinese medicinal preparation and preparation method thereof
The compound Chinese medicine preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff is implemented according to the following steps:
(1) putting 10 parts of cacumen biotae, 25 parts of prepared fleece-flower root, 13 parts of glossy privet fruit, 13 parts of galangal, 8 parts of black mulberry, 8 parts of astragalus membranaceus, 15 parts of black wolfberry, 12 parts of yam root, 6 parts of stamen nelumbinis, 6 parts of semen cuscutae, 13 parts of snakehead intestine, 9 parts of angelica, 9 parts of ligusticum wallichii, 10 parts of cortex dictamni and 9 parts of radix sophorae flavescentis into a pulverizer, pulverizing into powder, and sieving with a 50-mesh sieve to obtain crude medicinal powder for later use;
(2) placing the crude powder in an extraction soaking tank, adding 5 times of 75 wt% ethanol, soaking for 72h under sealed condition, and keeping the temperature at 37 deg.C;
(3) intermittently stirring the substances in the extraction and soaking tank in the step (2), stirring once every 2h, 30min each time, rotating speed 150r/min, centrifugally separating the mixture, and filtering with a microporous membrane to obtain a primary extracting solution for later use;
(4) adding 5 times of 50 wt% ethanol into the residue obtained after filtration in the step (3), soaking in a sealed environment for 72h, keeping the temperature at 37 ℃, stirring intermittently, stirring once every 2h for 30min each time at a rotation speed of 150r/min, centrifuging the mixture, and filtering with a microporous membrane to obtain a secondary extract for later use;
(5) and (3) combining the primary extracting solution in the step (3) and the secondary extracting solution in the step (4), filtering by using a 0.1-1 mu m microporous filter membrane to obtain a refined extracting solution, aging for 24 hours, and sterilizing at high temperature to obtain the compound traditional Chinese medicine preparation.
Example 2 Compound Chinese medicinal preparation and preparation method thereof
(1) Putting 15 parts of cacumen biotae, 20 parts of prepared fleece-flower root, 15 parts of glossy privet fruit, 10 parts of galangal, 10 parts of black mulberry, 9 parts of astragalus membranaceus, 10 parts of black wolfberry, 10 parts of yam root, 9 parts of stamen nelumbinis, 9 parts of semen cuscutae, 15 parts of snakehead intestine, 8 parts of angelica, 8 parts of ligusticum wallichii, 8 parts of cortex dictamni and 10 parts of radix sophorae flavescentis into a pulverizer, pulverizing into powder, and sieving with a 50-mesh sieve to obtain crude medicinal powder for later use;
(2) placing the crude powder in an extraction soaking tank, adding 5 times of 75 wt% ethanol, soaking for 48h under sealed condition, and keeping the temperature at 40 deg.C;
(3) intermittently stirring the substances in the extraction and soaking tank in the step (2), stirring once every 3h, 25min each time, rotating speed 200r/min, centrifugally separating the mixture, and filtering with a microporous filter membrane to obtain a primary extracting solution for later use;
(4) adding 5 times of 50 wt% ethanol into the dregs obtained after filtration in the step (3), soaking in a sealed condition for 48 hours at the temperature of 40 ℃, stirring intermittently, stirring once every 2 hours for 25 minutes every time at the rotating speed of 200r/min, centrifugally separating the mixture, and filtering with a microporous filter membrane to obtain a secondary extracting solution for later use;
(5) and (3) combining the primary extracting solution in the step (3) and the secondary extracting solution in the step (4), filtering by using a 0.1-1 mu m microporous filter membrane to obtain a refined extracting solution, aging for 24 hours, and sterilizing at high temperature to obtain the compound traditional Chinese medicine preparation.
Example 3 Compound Chinese medicinal preparation and preparation method thereof
(1) 13 parts of cacumen biotae, 23 parts of prepared fleece-flower root, 10 parts of glossy privet fruit, 15 parts of galangal, 9 parts of black mulberry, 10 parts of astragalus membranaceus, 13 parts of black wolfberry, 8 parts of yam root, 8 parts of stamen nelumbinis, 10 parts of semen cuscutae, 10 parts of eclipta prostrata, 10 parts of angelica sinensis, 10 parts of ligusticum wallichii, 9 parts of cortex dictamni and 8 parts of radix sophorae flavescentis are put into a pulverizer, pulverized into a powder state, and sieved by a 50-mesh sieve to obtain crude medicinal powder for later use;
(2) placing the crude powder in an extraction soaking tank, adding 5 times of 75 wt% ethanol, soaking for 24h under sealed condition, and keeping the temperature at 35 deg.C;
(3) intermittently stirring the substances in the extraction and soaking tank in the step (2), stirring once every 5h, 20min each time, rotating at the speed of 180r/min, centrifugally separating the mixture, and filtering with a microporous membrane to obtain a primary extracting solution for later use;
(4) adding 5 times of 50 wt% ethanol into the dregs obtained after filtration in the step (3), soaking in a sealed environment for 24 hours at the temperature of 35 ℃, stirring intermittently, stirring once every 2 hours for 20 minutes each time at the rotating speed of 180r/min, centrifugally separating the mixture, and filtering with a microporous filter membrane to obtain a secondary extracting solution for later use;
(5) and (3) combining the primary extracting solution in the step (3) and the secondary extracting solution in the step (4), filtering by using a 0.1-1 mu m microporous filter membrane to obtain a refined extracting solution, aging for 24 hours, and sterilizing at high temperature to obtain the compound traditional Chinese medicine preparation.
The compound traditional Chinese medicine preparation finally prepared in the above examples 1-3 has the same quality, about 1300-1500g, and the extracted compound traditional Chinese medicine preparation has high content of active substances, can promote division of hair root melanocyte, activate tyrosinase activity and melanin generation, prevent hair from whitening, and enable whitened hair to be moistened, maintained and turned black; meanwhile, the scalp hair-follicle bacterium fungal infection inflammation, folliculitis, lipid secretion imbalance, excessive dandruff, easy hair breakage and alopecia and the like are improved, scalp balance is reestablished, and the problem of multiple scalps is solved.
EXAMPLE 4 application of Compound Chinese medicinal preparation in dandruff removing and oil controlling shampoo
The formula is as follows: 25 parts of the compound traditional Chinese medicine preparation in the embodiment 1, 12 parts of sodium laureth sulfate, 8 parts of cocamidopropyl betaine, 3 parts of sodium laureth sulfate, 1 parts of cocamide MEA, and 100.3 parts of polyquaternium; 0.2 part of hydroxypropyl guar hydroxypropyl trimethyl ammonium chloride, 0.1 part of camellia oil, 0.05 part of fructo-oligosaccharide, 0.05 part of sodium hyaluronate, 0.11 part of preservative, 0.5 part of essence and 10% citric acid aqueous solution, and adding water to 100 parts.
EXAMPLE 5 scalp essence for use in Compound traditional Chinese medicine preparation
The formula is as follows: 60 parts of the compound traditional Chinese medicine preparation of the embodiment 2; 0.5 part of panthenol and 0.3 part of pyridoxine HCl; 0.5 part of dipotassium glycyrrhizinate, 0.05 part of preservative and 100 parts of water.
Hair growth whitening prevention, oil control and dandruff removal effect test
120 volunteers with white hair, alopecia, dandruff and oily hair were selected, aged 15-60 years, and the volunteers were randomly divided into 4 groups of 30 persons each. The scalp problems in 120 cases were not only single but also superimposed with a plurality of scalp problems.
Distribution of scalp test conditions for individuals table 1
| Distribution of scalp problems | White hair | Alopecia (baldness) | Itching (pruritus) | Dandruff | Oil discharge |
| Number of people | 40 | 85 | 20 | 35 | 35 |
Evaluation criteria Table 2
The first group of volunteers used the anti-dandruff oil-control shampoo prepared from the compound traditional Chinese medicine preparation in example 1 of the invention, sprayed with the scalp essence in example 5 of the invention after washing, and massaged properly with a horn comb until absorption, once in the morning and evening, and continuously used for 45 days.
The second group of volunteers used the anti-dandruff oil-control shampoo prepared from the compound traditional Chinese medicine preparation in example 2 of the invention, sprayed with the scalp essence in example 5 of the invention after washing, and massaged properly with a horn comb until absorption, once in the morning and evening, and continuously used for 45 days.
The third group of volunteers used the anti-dandruff oil-control shampoo prepared from the compound traditional Chinese medicine preparation in example 3 of the invention, sprayed with the scalp essence in example 5 of the invention after washing, and massaged properly with a horn comb until absorption, once in the morning and evening, and continuously used for 45 days.
The fourth group of volunteers used commercially available fleece-flower root hair loss prevention shampoo, and washed hair with the shampoo every day for 45 days continuously.
After 45 days, the using effect and the related number of people are counted, and the test results are shown in tables 3 to 6:
TABLE 3 first set of test results
| Traits | Improvement of white hair | Alopecia improvement | Amelioration of dandruff inflammation | Head oil improvement |
| Show effect | 10 | 19 | 21 | 23 |
| Is effective | 16 | 9 | 7 | 6 |
| Invalidation | 4 | 2 | 2 | 1 |
| Total effective rate | 86.6％ | 93.3％ | 93.3％ | 96.6％ |
TABLE 4 second set of test results
| Traits | Improvement of white hair | Alopecia improvement | Amelioration of dandruff inflammation | Head oil improvement |
| Show effect | 7 | 10 | 11 | 15 |
| Is effective | 17 | 15 | 15 | 12 |
| Invalidation | 6 | 5 | 4 | 4 |
| Total effective rate | 80.0％ | 83.3％ | 86.6％ | 90.0％ |
TABLE 5 third set of test results
| Traits | Improvement of white hair | Alopecia improvement | Amelioration of dandruff inflammation | Head oil improvement |
| Show effect | 6 | 9 | 10 | 10 |
| Is effective | 16 | 15 | 16 | 17 |
| Invalidation | 8 | 6 | 4 | 3 |
| Total effective rate | 73.3％ | 80.0％ | 86.6％ | 90.0％ |
TABLE 6 fourth set of test results
As can be seen from the data in table 3 and table 6, the dandruff and oil removing shampoo prepared by using the compound traditional Chinese medicine preparation of example 1 of the present invention has significantly better effects than scalp care products combined with other formulas, and is also better than commercially available fleece-flower root alopecia preventing shampoo. The shampoo and scalp essence prepared by the compound traditional Chinese medicine preparation can solve multiple scalp problems, has the effects of nourishing and protecting hair, growing hair and preventing whitening, controlling oil and removing dandruff, diminishing inflammation and relieving itching and removing oil, and finally achieves the effect of conditioning scalp hair follicle health. The commercial fleece-flower root hair loss prevention shampoo can only solve the problem of single hair oil, and has little effect on improving the white hair loss and diminishing inflammation.
Therefore, the compound Chinese medicinal preparation for hair growth and whitening prevention, oil control and dandruff removal and the preparation method and application thereof adopt the structure, and the compound Chinese medicinal composition in the compound Chinese medicinal preparation conforms to the monarch, minister, assistant and guide principle in the Chinese medicinal theory, so the compound Chinese medicinal preparation is safe, nontoxic, mild and non-irritant, has the effects of hair nourishing and hair care, hair growth and whitening prevention, oil control and dandruff removal, inflammation diminishing and itching relieving and oil removal, and shampoo and scalp essence which are applied products have the effect of conditioning scalp and hair follicle health.
Finally, it should be noted that: the above embodiments are only for illustrating the technical solutions of the present invention and not for limiting the same, and although the present invention is described in detail with reference to the preferred embodiments, those of ordinary skill in the art should understand that: modifications and equivalents may be made to the invention without departing from the spirit and scope of the invention.
Claims (8)
1. A compound traditional Chinese medicine preparation for hair growth, whitening prevention, oil control and dandruff removal is characterized in that: the compound traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 10-15 parts of cacumen biotae, 20-25 parts of prepared fleece-flower root, 10-15 parts of glossy privet fruit, 10-15 parts of galangal, 8-10 parts of black mulberry fruit, 8-10 parts of astragalus membranaceus, 10-15 parts of black wolfberry, 8-12 parts of yam root, 6-9 parts of lotus stamen, 6-10 parts of dodder, 10-15 parts of eclipta prostrata, 8-10 parts of angelica sinensis, 8-10 parts of ligusticum wallichii, 8-10 parts of cortex dictamni and 8-10 parts of sophora flavescens, wherein the solvent is water or an ethanol water solution, and the ethanol content in the ethanol water solution accounts for 1-75 wt%.
2. The compound traditional Chinese medicine preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff according to claim 1, which is characterized in that: the compound traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 10 parts of cacumen biotae, 25 parts of prepared fleece-flower root, 13 parts of glossy privet fruit, 13 parts of galangal, 8 parts of black mulberry fruit, 8 parts of astragalus membranaceus, 15 parts of black wolfberry, 12 parts of yam root, 6 parts of stamen nelumbinis, 6 parts of semen cuscutae, 13 parts of eclipta prostrata, 9 parts of angelica sinensis, 9 parts of ligusticum wallichii, 10 parts of cortex dictamni and 9 parts of sophora flavescens.
3. The compound traditional Chinese medicine preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff according to claim 1, which is characterized in that: the compound traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 15 parts of cacumen biotae, 20 parts of prepared fleece-flower root, 15 parts of glossy privet fruit, 10 parts of galangal, 10 parts of black mulberry fruit, 9 parts of astragalus membranaceus, 10 parts of black wolfberry, 10 parts of yam root, 9 parts of stamen nelumbinis, 9 parts of semen cuscutae, 15 parts of eclipta prostrata, 8 parts of angelica sinensis, 8 parts of ligusticum wallichii, 8 parts of cortex dictamni and 10 parts of sophora flavescens.
4. The compound traditional Chinese medicine preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff according to claim 1, which is characterized in that: the compound traditional Chinese medicine composition is prepared from the following raw materials in parts by weight: 13 parts of cacumen biotae, 23 parts of prepared fleece-flower root, 10 parts of glossy privet fruit, 15 parts of galangal, 9 parts of black mulberry fruit, 10 parts of astragalus membranaceus, 13 parts of black wolfberry, 8 parts of yam root, 8 parts of stamen nelumbinis, 10 parts of semen cuscutae, 10 parts of eclipta prostrata, 10 parts of angelica sinensis, 10 parts of ligusticum wallichii, 9 parts of cortex dictamni and 8 parts of sophora flavescens.
5. The preparation method of the compound traditional Chinese medicine preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff according to any of claims 1-4, which is characterized in that: the method comprises the following steps:
(1) putting the compound traditional Chinese medicine composition with the formula amount into a pulverizer, pulverizing into powder, and sieving with a 50-mesh sieve to obtain crude medicinal powder for later use;
(2) placing the crude powder in an extraction soaking tank, adding 5-10 times of 75 wt% ethanol, soaking for 24-72 hr under sealed condition, and maintaining the temperature at 35-40 deg.C;
(3) intermittently stirring the substances in the extraction and soaking tank in the step (2), stirring once every 2-5 h, 20-30min each time, rotating speed of 150-;
(4) adding 5-10 times of 50 wt% ethanol into the dregs obtained after filtration in the step (3), soaking in a sealed environment for 24-72h, keeping the temperature between 35-40 ℃, stirring intermittently, stirring once every 2-5 h, 20-30min each time, rotating at the speed of 150-200r/min, centrifugally separating the mixture, and filtering with a microporous membrane to obtain a secondary extracting solution for later use;
(5) and (3) combining the primary extracting solution in the step (3) and the secondary extracting solution in the step (4), filtering by using a 0.1-1 mu m microporous filter membrane to obtain a refined extracting solution, aging for 24 hours, and sterilizing at high temperature to obtain the compound traditional Chinese medicine preparation.
6. The application of the compound Chinese medicinal preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff as claimed in any of claims 1 to 4 is characterized in that: adding an auxiliary material A into the compound traditional Chinese medicine preparation to prepare the anti-dandruff oil-control shampoo, wherein the anti-dandruff oil-control shampoo comprises the following components in parts by weight: 1-40 parts of compound traditional Chinese medicine preparation, 8-12 parts of sodium laureth sulfate, 3-10 parts of cocamidopropyl betaine, 1-5 parts of sodium laureth sulfate, 0.3-2 parts of cocamide MEA, 100.2-0.5 part of polyquaternary ammonium salt, 0.1-0.5 part of hydroxypropyl guar hydroxypropyl trimethyl ammonium chloride, 0.1-0.2 part of camellia oil, 0.05-0.2 part of fructo-oligosaccharide, 0.05-0.2 part of sodium hyaluronate, 0.1-0.5 part of citric acid, 0.05-0.2 part of preservative, 0.3-0.8 part of essence and 100 parts of water.
7. The application of the compound Chinese medicinal preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff as claimed in any of claims 1 to 4 is characterized in that: and adding an auxiliary material B into the compound traditional Chinese medicine preparation to prepare the softening shampoo, wherein the softening shampoo comprises the following components in parts by weight: 1-30 parts of a compound traditional Chinese medicine preparation; 10-20 parts of cocoyl sarcosine sodium; 5-10 parts of cocoyl sodium glycinate; 1-5 parts of sodium lauroamphoacetate; 1-5 parts of decyl glucoside; 0.5-2 parts of guar hydroxypropyl trimethyl ammonium chloride; 0.1-0.5 part of acrylic acid (ester)/C10-30 alkanol acrylate crosslinked polymer; 1-5 parts of cocoyl hydroxy sulfobetaine; 100.5-2 parts of polyquaternium; 0.1-0.5 part of arginine; 0.1-1 part of panthenol; 0.1-0.5 parts of hydrolyzed wheat protein; 0.1-0.5 part of citric acid; 0.05-0.2 part of preservative; 0.3-0.8 part of essence and 100 parts of water.
8. The application of the compound Chinese medicinal preparation for promoting hair growth, preventing whitening, controlling oil and removing dandruff as claimed in any of claims 1 to 4 is characterized in that: adding an auxiliary material C into the compound traditional Chinese medicine preparation to prepare scalp essence, wherein the scalp essence comprises the following components in parts by weight: 40-70 parts of compound traditional Chinese medicine preparation, 0.2-2 parts of panthenol, 0.1-0.5 part of pyridoxine HCl, 0.5-1 part of dipotassium glycyrrhizinate, 0.05-0.2 part of preservative and 100 parts of water.
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