CN1138769C - 合成5-(α-羟基烷基)苯并[1,3]二氧杂环戊烯的方法 - Google Patents

合成5-(α-羟基烷基)苯并[1,3]二氧杂环戊烯的方法 Download PDF

Info

Publication number
CN1138769C
CN1138769C CNB998151173A CN99815117A CN1138769C CN 1138769 C CN1138769 C CN 1138769C CN B998151173 A CNB998151173 A CN B998151173A CN 99815117 A CN99815117 A CN 99815117A CN 1138769 C CN1138769 C CN 1138769C
Authority
CN
China
Prior art keywords
benzo
formula
dioxole
compound
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CNB998151173A
Other languages
English (en)
Chinese (zh)
Other versions
CN1332736A (zh
Inventor
v
V·搏扎塔
D·布兰卡洛尼
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Endura SpA
Original Assignee
Endura SpA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Endura SpA filed Critical Endura SpA
Publication of CN1332736A publication Critical patent/CN1332736A/zh
Application granted granted Critical
Publication of CN1138769C publication Critical patent/CN1138769C/zh
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D317/00Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D317/08Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
    • C07D317/44Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D317/46Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems condensed with one six-membered ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D317/00Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D317/08Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
    • C07D317/44Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D317/46Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 ortho- or peri-condensed with carbocyclic rings or ring systems condensed with one six-membered ring
    • C07D317/48Methylenedioxybenzenes or hydrogenated methylenedioxybenzenes, unsubstituted on the hetero ring
    • C07D317/50Methylenedioxybenzenes or hydrogenated methylenedioxybenzenes, unsubstituted on the hetero ring with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to atoms of the carbocyclic ring
    • C07D317/54Radicals substituted by oxygen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Fats And Perfumes (AREA)
CNB998151173A 1998-12-30 1999-10-14 合成5-(α-羟基烷基)苯并[1,3]二氧杂环戊烯的方法 Expired - Lifetime CN1138769C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ITMI98A002857 1998-12-30
IT1998MI002857A IT1304513B1 (it) 1998-12-30 1998-12-30 Processo per la sintesi di 5-(alfa-idrossialchil)benzo(1,3)diossoli.

Publications (2)

Publication Number Publication Date
CN1332736A CN1332736A (zh) 2002-01-23
CN1138769C true CN1138769C (zh) 2004-02-18

Family

ID=11381378

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB998151173A Expired - Lifetime CN1138769C (zh) 1998-12-30 1999-10-14 合成5-(α-羟基烷基)苯并[1,3]二氧杂环戊烯的方法

Country Status (13)

Country Link
US (1) US6342613B1 (enExample)
EP (1) EP1140894B1 (enExample)
JP (1) JP4845266B2 (enExample)
KR (1) KR100682160B1 (enExample)
CN (1) CN1138769C (enExample)
AT (1) ATE256676T1 (enExample)
AU (1) AU756172B2 (enExample)
BR (1) BR9916471B1 (enExample)
CA (1) CA2352249C (enExample)
DE (1) DE69913735T2 (enExample)
IT (1) IT1304513B1 (enExample)
RU (1) RU2243224C2 (enExample)
WO (1) WO2000040575A1 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE602005023124D1 (de) * 2004-01-28 2010-10-07 Hoffmann La Roche Spirobenzodioxole und deren verwendung als cb1-antagonisten
WO2010079423A1 (en) * 2009-01-12 2010-07-15 Council Of Scientific & Industrial Research Inhibitors of phosphatidylinositol-3-kinase (pi3) and inducers of nitric oxide (no)
EP2289889A1 (en) 2009-08-18 2011-03-02 Endura S.p.a. Substituted alkynyl phenoxy compounds and their uses
CN102070596B (zh) * 2011-01-22 2013-02-27 浙江大学 二氢黄樟素的制备方法
GB201104156D0 (en) 2011-03-11 2011-04-27 Rothamstead Res Ltd Compositions and methods for controlling pesticide resistant pests
EP3141115A1 (en) 2015-09-09 2017-03-15 Endura S.p.a. Substituted methylenedioxybenzyl compounds and their uses as synergists
EP3141116B1 (en) 2015-09-09 2018-06-13 Endura S.p.a. 5,7-disubstituted 2,3-dihydrobenzofurans and their use as synergists
CN106632228B (zh) * 2016-08-05 2019-07-02 成都建中香料香精有限公司 一种二氢黄樟素的制备方法
WO2018150230A1 (en) 2017-02-14 2018-08-23 Anthea Aromatics Private Limited A process for preparation of alkenyl and alkyl derivatives of alkylenedioxybenzene
WO2022161628A1 (en) 2021-01-29 2022-08-04 Endura S.P.A. Process for the preparation of 3,4-methylenedioxypropiophenone

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1097270A (en) * 1965-10-13 1968-01-03 Shell Int Research Process for the preparation of methylene dioxybenzene, 1,3-benzoxathiole and derivatives thereof
US3908000A (en) * 1971-03-19 1975-09-23 Hoffmann La Roche Propynyl benzyl ethers as insecticidal agents
US3946040A (en) * 1971-03-19 1976-03-23 Hoffmann-La Roche Inc. Propynyl benzyl ethers
CH583677A5 (enExample) * 1972-02-03 1977-01-14 Basf Ag
JPS56164178A (en) * 1980-05-23 1981-12-17 Mitsubishi Chem Ind Ltd Preparation of 4-hydroxy-1,3-benzodioxole
EP0095454A3 (de) * 1982-05-13 1985-04-03 Gerot-Pharmazeutika Gesellschaft m.b.H. Neue kernsubstituierte Pyrogallol-Derivate
JP2521739B2 (ja) * 1987-01-27 1996-08-07 新日本薬品株式会社 肝臓疾患治療剤
ATE61588T1 (de) * 1987-08-03 1991-03-15 Delagrange Lab 1,4-dihydropyridine, verfahren zu ihrer herstellung und ihre verwendung als arzneimittel.
US5420301A (en) * 1988-03-18 1995-05-30 Ciba-Geigy Corporation Process for the preparation of substituted difluorobenzo-1,3-dioxoles
JP2760998B2 (ja) * 1988-08-16 1998-06-04 新日本薬品株式会社 肝臓疾患治療剤
SU1703648A1 (ru) * 1989-12-26 1992-01-07 Туркменский Государственный Университет Им.А.М.Горького 2-/2-Цианоэтил/-4,5-бензо-1,3-диоксолан, обладающий акарицидной активностью против иксодовых клещей рода Шаломма
DE4133155A1 (de) * 1991-10-07 1993-04-08 Bayer Ag Verfahren zur herstellung von 2,2-difluorbenzo (1,3)-dioxol-carbaldehyden und neuen zwischenprodukten
US5696301A (en) * 1996-01-23 1997-12-09 Ube Industries, Ltd. Process for preparing protocatechualdehyde

Also Published As

Publication number Publication date
AU756172B2 (en) 2003-01-09
ITMI982857A0 (it) 1998-12-30
IT1304513B1 (it) 2001-03-19
JP2002534423A (ja) 2002-10-15
JP4845266B2 (ja) 2011-12-28
CN1332736A (zh) 2002-01-23
EP1140894B1 (en) 2003-12-17
BR9916471B1 (pt) 2010-12-14
WO2000040575A1 (en) 2000-07-13
DE69913735T2 (de) 2004-07-29
ATE256676T1 (de) 2004-01-15
EP1140894A1 (en) 2001-10-10
CA2352249A1 (en) 2000-07-13
BR9916471A (pt) 2001-09-18
KR20010083955A (ko) 2001-09-03
DE69913735D1 (de) 2004-01-29
CA2352249C (en) 2007-09-11
KR100682160B1 (ko) 2007-02-12
AU1037700A (en) 2000-07-24
US6342613B1 (en) 2002-01-29
ITMI982857A1 (it) 2000-06-30
RU2243224C2 (ru) 2004-12-27

Similar Documents

Publication Publication Date Title
CN1093126C (zh) 合成被保护的(s)-3,4-二羟基丁酸酯的改进方法
CN1138769C (zh) 合成5-(α-羟基烷基)苯并[1,3]二氧杂环戊烯的方法
Mirk et al. Iodinated biaryls synthesized by the direct dehydrodimerization of iodoarenes using phenyliodine (III) bis (trifluoroacetate)(PIFA)
JPWO2008023836A1 (ja) ベンズアルデヒド化合物の製造方法
US4958033A (en) Process for preparing alcohols
CN101323567B (zh) 制备肉桂酸酯及其衍生物的方法
Gypser et al. D-Erythronolactone as a C 4 building unit. Part 2.1 A short and efficient synthesis of both enantiomers of epi-muricatacin, a diastereoisomer of the native acetogenin from Annona muricata
Yao et al. A practical approach to stereodefined cyclopropyl-substituted heteroarenes using a Suzuki-type reaction
CN116462619B (zh) 一种环戊烯酮衍生物的制备方法
EP1574509B1 (en) Process for the production of 1-acetoxy-3-(substituted phenyl)propenes
JPS62289549A (ja) N−(α−アルコキシエチル)−カルボン酸アミドの製造方法
US20060030719A1 (en) Cis-3,5-disubstituted-dihydro-furan-2-ones and the preparation and use thereof
Ley et al. Chemistry of insect antifeedants from azadirachta indica (Part 22): Functionalisation of the decalin fragment of azadirachtin via a claisen rearrangement reaction
JP4092391B2 (ja) ベンジルエーテル系デンドリマー化合物
CN119118922B (zh) 一种偶氮苯化合物制备2h-吲唑类化合物的非柱层析方法
Sartori et al. Solvent effect in the “fragment condensation” synthesis of calix [4] arenes and temperature dependent 1H-NMR studies of new dihomomonoxacalixarenes
CN120271545B (zh) 一种二苯并-α-吡喃酮类化合物的合成方法及其应用
KR100941736B1 (ko) 다이하이드로 퓨란 유도체와 금 촉매를 이용한 이의 합성
JP4707796B2 (ja) 5−アルキルベンゾジオキソールの合成法
KR100449310B1 (ko) 2-데옥시-l-리보스의 제조방법
CN115010693A (zh) 一种芳基乙醛缩醛的制备方法
CN109503531B (zh) 一种苯并呋喃类化合物的制备方法
JPH0696564B2 (ja) α−(ω−ヒドロキシアルキル)フルフリルアルコ−ル及びその製造法
JPH0681734B2 (ja) ビシクロヒユムレノンの製造方法
CN119504327A (zh) α,β未取代1,4-酮醛化合物及其无金属光催化水溶液乙醛α位选择性单一烷基化反应制备方法和应用

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CX01 Expiry of patent term
CX01 Expiry of patent term

Granted publication date: 20040218