CN112748073A - 一种材料原位表征样品池及其使用方法 - Google Patents
一种材料原位表征样品池及其使用方法 Download PDFInfo
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- CN112748073A CN112748073A CN201911048882.8A CN201911048882A CN112748073A CN 112748073 A CN112748073 A CN 112748073A CN 201911048882 A CN201911048882 A CN 201911048882A CN 112748073 A CN112748073 A CN 112748073A
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- 238000011065 in-situ storage Methods 0.000 title claims abstract description 77
- 239000000463 material Substances 0.000 title claims abstract description 28
- 238000012512 characterization method Methods 0.000 title claims abstract description 27
- 238000000034 method Methods 0.000 title abstract description 9
- 238000011282 treatment Methods 0.000 claims abstract description 32
- 238000010438 heat treatment Methods 0.000 claims abstract description 26
- 238000001816 cooling Methods 0.000 claims abstract description 16
- 239000000523 sample Substances 0.000 claims description 196
- 239000007789 gas Substances 0.000 claims description 21
- 239000002826 coolant Substances 0.000 claims description 19
- 238000007789 sealing Methods 0.000 claims description 15
- 230000003287 optical effect Effects 0.000 claims description 14
- 238000006243 chemical reaction Methods 0.000 claims description 9
- 239000002184 metal Substances 0.000 claims description 8
- 238000001228 spectrum Methods 0.000 claims description 6
- 210000004907 gland Anatomy 0.000 claims description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 4
- 239000010453 quartz Substances 0.000 claims description 3
- 230000008569 process Effects 0.000 abstract description 6
- 239000003054 catalyst Substances 0.000 description 11
- 238000002329 infrared spectrum Methods 0.000 description 11
- 230000003197 catalytic effect Effects 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 238000004566 IR spectroscopy Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000005033 Fourier transform infrared spectroscopy Methods 0.000 description 1
- 238000001069 Raman spectroscopy Methods 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001941 electron spectroscopy Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 238000004073 vulcanization Methods 0.000 description 1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/01—Arrangements or apparatus for facilitating the optical investigation
- G01N21/03—Cuvette constructions
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/01—Arrangements or apparatus for facilitating the optical investigation
- G01N21/03—Cuvette constructions
- G01N21/0332—Cuvette constructions with temperature control
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/01—Arrangements or apparatus for facilitating the optical investigation
- G01N21/03—Cuvette constructions
- G01N21/09—Cuvette constructions adapted to resist hostile environments or corrosive or abrasive materials
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- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
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- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
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- Analysing Materials By The Use Of Radiation (AREA)
Abstract
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CN201911048882.8A CN112748073B (zh) | 2019-10-31 | 2019-10-31 | 一种材料原位表征样品池及其使用方法 |
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CN201911048882.8A CN112748073B (zh) | 2019-10-31 | 2019-10-31 | 一种材料原位表征样品池及其使用方法 |
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CN112748073A true CN112748073A (zh) | 2021-05-04 |
CN112748073B CN112748073B (zh) | 2024-05-31 |
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Citations (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1069806A (zh) * | 1992-06-25 | 1993-03-10 | 厦门大学 | 原位红外光谱样品池 |
CN2226757Y (zh) * | 1995-04-08 | 1996-05-08 | 上海石油化工股份有限公司 | 一种气-固反应原位红外光谱样品池 |
CN2278217Y (zh) * | 1996-05-16 | 1998-04-08 | 厦门大学 | 高温原位显微拉曼样品池 |
CA2618209A1 (en) * | 2000-03-10 | 2001-09-20 | Textron Systems Corporation | Optical probes and methods for spectral analysis |
CN102221539A (zh) * | 2011-03-29 | 2011-10-19 | 钢铁研究总院 | 激光诱导击穿光谱原位分析仪 |
CN202281745U (zh) * | 2011-10-17 | 2012-06-20 | 中国石油化工股份有限公司 | 原位活化-红外光谱样品池 |
CN102564955A (zh) * | 2011-12-30 | 2012-07-11 | 浙江师范大学 | 一种原位双红外光谱池 |
CN202974859U (zh) * | 2012-11-26 | 2013-06-05 | 浙江泛泰仪器有限公司 | 真空原位仪 |
CN203037568U (zh) * | 2012-09-18 | 2013-07-03 | 中国石油天然气股份有限公司 | 一种双试样红外透射池 |
WO2013169872A1 (en) * | 2012-05-08 | 2013-11-14 | E.A. Fischione Instruments, Inc. | In situ holder assembly |
CN203502338U (zh) * | 2013-10-21 | 2014-03-26 | 东北石油大学 | 一种原位红外光谱反应池 |
US20160223803A1 (en) * | 2015-02-04 | 2016-08-04 | Georg-August-Universitaet Goettingen | Mounting device for a sample and method for removing a sample |
CN106198441A (zh) * | 2016-07-26 | 2016-12-07 | 中国科学院福建物质结构研究所 | 一种可模拟样品吸脱附过程的原位光谱测试装置 |
CN106680239A (zh) * | 2017-02-24 | 2017-05-17 | 中国科学院广州能源研究所 | 原位红外表征气体水合物生成和分解过程的装置及其使用方法 |
CN106706672A (zh) * | 2016-12-27 | 2017-05-24 | 中国科学院山西煤炭化学研究所 | 一种方形管催化剂动态结构原位表征装置及应用 |
CN107091817A (zh) * | 2017-06-23 | 2017-08-25 | 山东大学 | 火星模拟环境下的全光谱原位表征及联用实验装置及方法 |
CN107576717A (zh) * | 2017-10-24 | 2018-01-12 | 中国科学技术大学 | 一种用于不同扩散距离催化反应气相中间产物的原位探测装置 |
WO2018143832A1 (en) * | 2017-02-03 | 2018-08-09 | Uniwersytet Jagielloński | Reactor for spectroscopic studies |
CN208818635U (zh) * | 2018-09-29 | 2019-05-03 | 中国科学院大连化学物理研究所 | 具备激光加热的原位和频振动光谱检测装置 |
-
2019
- 2019-10-31 CN CN201911048882.8A patent/CN112748073B/zh active Active
Patent Citations (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1069806A (zh) * | 1992-06-25 | 1993-03-10 | 厦门大学 | 原位红外光谱样品池 |
CN2226757Y (zh) * | 1995-04-08 | 1996-05-08 | 上海石油化工股份有限公司 | 一种气-固反应原位红外光谱样品池 |
CN2278217Y (zh) * | 1996-05-16 | 1998-04-08 | 厦门大学 | 高温原位显微拉曼样品池 |
CA2618209A1 (en) * | 2000-03-10 | 2001-09-20 | Textron Systems Corporation | Optical probes and methods for spectral analysis |
CN102221539A (zh) * | 2011-03-29 | 2011-10-19 | 钢铁研究总院 | 激光诱导击穿光谱原位分析仪 |
CN202281745U (zh) * | 2011-10-17 | 2012-06-20 | 中国石油化工股份有限公司 | 原位活化-红外光谱样品池 |
CN102564955A (zh) * | 2011-12-30 | 2012-07-11 | 浙江师范大学 | 一种原位双红外光谱池 |
WO2013169872A1 (en) * | 2012-05-08 | 2013-11-14 | E.A. Fischione Instruments, Inc. | In situ holder assembly |
CN203037568U (zh) * | 2012-09-18 | 2013-07-03 | 中国石油天然气股份有限公司 | 一种双试样红外透射池 |
CN202974859U (zh) * | 2012-11-26 | 2013-06-05 | 浙江泛泰仪器有限公司 | 真空原位仪 |
CN203502338U (zh) * | 2013-10-21 | 2014-03-26 | 东北石油大学 | 一种原位红外光谱反应池 |
US20160223803A1 (en) * | 2015-02-04 | 2016-08-04 | Georg-August-Universitaet Goettingen | Mounting device for a sample and method for removing a sample |
CN106198441A (zh) * | 2016-07-26 | 2016-12-07 | 中国科学院福建物质结构研究所 | 一种可模拟样品吸脱附过程的原位光谱测试装置 |
CN106706672A (zh) * | 2016-12-27 | 2017-05-24 | 中国科学院山西煤炭化学研究所 | 一种方形管催化剂动态结构原位表征装置及应用 |
WO2018143832A1 (en) * | 2017-02-03 | 2018-08-09 | Uniwersytet Jagielloński | Reactor for spectroscopic studies |
CN106680239A (zh) * | 2017-02-24 | 2017-05-17 | 中国科学院广州能源研究所 | 原位红外表征气体水合物生成和分解过程的装置及其使用方法 |
CN107091817A (zh) * | 2017-06-23 | 2017-08-25 | 山东大学 | 火星模拟环境下的全光谱原位表征及联用实验装置及方法 |
CN107576717A (zh) * | 2017-10-24 | 2018-01-12 | 中国科学技术大学 | 一种用于不同扩散距离催化反应气相中间产物的原位探测装置 |
CN208818635U (zh) * | 2018-09-29 | 2019-05-03 | 中国科学院大连化学物理研究所 | 具备激光加热的原位和频振动光谱检测装置 |
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CN112748073B (zh) | 2024-05-31 |
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Effective date of registration: 20231226 Address after: 100728 No. 22 North Main Street, Chaoyang District, Beijing, Chaoyangmen Applicant after: CHINA PETROLEUM & CHEMICAL Corp. Applicant after: Sinopec (Dalian) Petrochemical Research Institute Co.,Ltd. Address before: 100728 No. 22 North Main Street, Chaoyang District, Beijing, Chaoyangmen Applicant before: CHINA PETROLEUM & CHEMICAL Corp. Applicant before: DALIAN RESEARCH INSTITUTE OF PETROLEUM AND PETROCHEMICALS, SINOPEC Corp. |
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