CN112587434B - Hair blackening agent, preparation method of hair blackening agent and washing and caring liquid - Google Patents
Hair blackening agent, preparation method of hair blackening agent and washing and caring liquid Download PDFInfo
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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Abstract
The invention provides a hair blackening agent, a preparation method of the hair blackening agent and a washing and caring liquid. The hair blackening agent comprises the following components in percentage by weight: fructus Ligustri Lucidi peptide composition 5-20%; 0.5-1% of ethanol; the first extract for promoting melanogenesis is 5-20%; 5-20% of wild walnut extract and the balance of deionized water. The fructus Ligustri Lucidi peptide composition comprises fructus Ligustri Lucidi high molecular peptide, fructus Ligustri Lucidi middle molecular peptide and fructus Ligustri Lucidi low molecular peptide, and the first extract for promoting melanogenesis comprises one or more of Polygoni Multiflori radix extract, black mulberry extract, Sargassum pallidum extract and Ganoderma atrum extract. The hair blackening agent can promote white hair to naturally blacken, thereby fundamentally solving the problem of white hair.
Description
Technical Field
The invention relates to the technical field of plant hair blacking, in particular to a hair blacking agent, a preparation method of the hair blacking agent and a washing and caring liquid.
Background
With the increase of life rhythm and environmental pollution and the excessive burden of mental labor, the phenomena of juvenile poliosis and middle-aged alopecia become more and more common.
In order to solve the problem of premature graying, people often use hair dyes to perform a blackening treatment on hair. The principle of using the hair dye to dye hair lies in that ammonia water is adopted to enable the hair to expand and soften, hair scales are opened, so that a dye intermediate and a coupling agent can be better diffused and permeate into a cortical layer, the dye intermediate and the coupling agent are subjected to oxidation reaction, coupling and condensation reaction to form larger dye molecules, and the dye molecules are sealed in hair fibers, so that the hair is dyed.
However, although the problem of white hair is solved for a while by dyeing hair with a hair dye, it is not fundamentally improved, so that newly growing hair is still white hair.
Disclosure of Invention
In order to solve the above problems, embodiments of the present disclosure provide a hair blackening agent, a preparation method of the hair blackening agent, and a washing and caring liquid. The first aspect of the embodiments of the present disclosure provides a hair blackening agent, which includes the following components by weight:
the balance of deionized water, wherein the glossy privet fruit peptide composition comprises glossy privet fruit high molecular peptide, glossy privet fruit medium molecular peptide and glossy privet fruit low molecular peptide, and the first extract for promoting melanogenesis comprises one or more of polygonum multiflorum extract, black mulberry extract, giant kelp extract and black ganoderma extract.
In one embodiment of the present disclosure, the hair blackening agent further comprises cacumen biotae extract, wherein the weight percentage of the cacumen biotae is 5-20%.
In another embodiment of the present disclosure, the weight percentage of the fructus ligustri lucidi peptide composition is 5-10%; the first extract for promoting melanogenesis accounts for 5-8 wt%; the weight percentage of the cacumen biotae extract is 5-10%; the weight percentage of the wild walnut extract is 10-15%.
In yet another embodiment of the present disclosure, the weight percentage of the fructus ligustri lucidi peptide composition is 7.5%; the weight percentage of the ethanol is 0.75 percent; the first extract for promoting melanogenesis is the polygonum multiflorum extract, wherein the weight percentage of the polygonum multiflorum extract is 6%; the weight percentage of the cacumen biotae extract is 7.5 percent; the weight percentage of the wild walnut extract is 12.5 percent.
In yet another embodiment of the present disclosure, the weight percentage of the fructus ligustri lucidi polymer peptide in the fructus ligustri lucidi peptide composition is 50%; the weight percentage of the molecular peptide in the glossy privet fruit is 20 percent; the weight percentage of the glossy privet fruit low-molecular peptide is 30%.
In a second aspect of the present disclosure, there is provided a method for preparing the hair blackening agent according to the first aspect of the present disclosure or any one of the embodiments of the first aspect of the present disclosure, wherein the method is implemented by the following steps:
mixing the glossy privet fruit high molecular peptide, the glossy privet fruit medium molecular peptide and the glossy privet fruit low molecular peptide at room temperature, and stirring until the glossy privet fruit high molecular peptide, the glossy privet fruit medium molecular peptide and the glossy privet fruit low molecular peptide are uniformly mixed to form the glossy privet fruit peptide composition.
In one embodiment of the present disclosure, the preparation method further comprises: and mixing the glossy privet fruit peptide composition, ethanol, the first extract for promoting melanogenesis, the wild walnut extract and deionized water at room temperature, and stirring until the mixture is uniformly mixed to obtain the hair blackening agent.
In another embodiment of the present disclosure, the fructus ligustri lucidi polymer peptide is prepared by the following steps:
putting the glossy privet fruit powder solution into a fermentation tank, and fermenting for 4-10 hours at the temperature of 40-50 ℃ to obtain fermentation liquor;
and mixing the fermentation liquor with the bacillus subtilis, stirring at a stirring speed of 150r/min, and carrying out ultrasonic treatment on the fermentation liquor for 3min to obtain the glossy privet fruit high-molecular peptide, wherein the ultrasonic power of the ultrasonic treatment is 1500-1800W.
In another embodiment of the present disclosure, the molecular peptide in fructus ligustri lucidi is prepared by the following steps:
putting the glossy privet fruit powder solution into a fermentation tank, and fermenting for 4-10 hours at the temperature of 40-50 ℃ to obtain fermentation liquor;
and mixing the fermentation liquor with bacillus subtilis, stirring at a stirring speed of 150r/min, and carrying out ultrasonic treatment on the fermentation liquor for 3min to obtain the ligustrum lucidum middle molecular peptide, wherein the ultrasonic power of the ultrasonic treatment is 2000W.
In another embodiment of the present disclosure, the fructus ligustri lucidi low molecular peptide is prepared by the following steps:
putting the glossy privet fruit powder solution into a fermentation tank, and fermenting for 4-10 hours at the temperature of 40-50 ℃ to obtain fermentation liquor;
and mixing the fermentation liquor with bacillus subtilis, stirring at a stirring speed of 150r/min, and carrying out ultrasonic treatment on the fermentation liquor for 3min to obtain the glossy privet fruit low-molecular-weight peptide, wherein the ultrasonic power of the ultrasonic treatment is 3000W.
In a third aspect of the present disclosure, there is provided a washing and caring solution, wherein the washing and caring solution comprises the following components by weight:
the balance of deionized water, wherein the hair blackening agent is the hair blackening agent of the first aspect of the present disclosure or any embodiment of the first aspect of the present disclosure.
In a fourth aspect of the present disclosure, there is provided a washing and caring solution, wherein the washing and caring solution comprises the following components by weight:
the balance of deionized water, wherein the hair blackening agent is the hair blackening agent of the first aspect of the present disclosure or any embodiment of the first aspect of the present disclosure.
The technical scheme provided by the embodiment of the disclosure can have the following beneficial effects: the hair blackening agent provided by the disclosure can fundamentally improve the white hair problem and promote the white hair to naturally turn black.
Detailed Description
The principles and spirit of the present invention will be described with reference to a number of exemplary embodiments. It is understood that these embodiments are given solely for the purpose of enabling those skilled in the art to better understand and to practice the invention, and are not intended to limit the scope of the invention in any way.
The Chinese hair is black, and the thick, black and moist hair can give people a vigorous and exciting feeling, so that people can glow and double the wind. However, thick and dark hair is not always seen by all people, and the incidence of canities is increasing in modern people.
According to the related art, experiments and mechanism researches aiming at different white hair people find that the color of the hair is mainly determined by the content of melanocytes and melanin in hair bulbs and hair papilla. Among them, melanocytes are mainly present in the epidermal basal layer and hair follicles. Tyrosinase is an important factor in determining melanin synthesis. The formation of white hair is often caused by a decrease in melanocytes and melanosomes, or a decrease in tyrosinase activity, which in turn causes melanin synthesis disorders.
Currently, melanin synthesis can be promoted to treat the white hair problem by activating the activity of tyrosinase and promoting the production of collagen.
The hair blackening agent provided by the embodiment of the disclosure can efficiently activate the tyrosinase, promote the spontaneous generation of the collagen to a normal level, further fundamentally improve the problem of white hair, and promote the white hair to naturally turn black.
In an exemplary embodiment of the present disclosure, the hair blackening agent may include the following components and weight percentages thereof:
the fructus Ligustri Lucidi peptide composition can include fructus Ligustri Lucidi high molecular peptide, fructus Ligustri Lucidi middle molecular peptide and fructus Ligustri Lucidi low molecular peptide. Promoting melanogenesis the first extract may be used to promote melanogenesis. In one embodiment, the first extract for promoting melanogenesis may include one or more of polygonum multiflorum extract, black mulberry extract, giant kelp extract and ganoderma atrum extract.
The fructus ligustri lucidi peptide composition comprises fructus ligustri lucidi high molecular peptide, fructus ligustri lucidi medium molecular peptide and fructus ligustri lucidi low molecular peptide, which can activate tyrosinase activity and promote collagen generation, thereby effectively promoting the natural blackening of white hair, and fundamentally solving the problem of white hair.
In the disclosed embodiment, the first extract for promoting melanogenesis and the extract of juglans sigillata can assist the glossy privet fruit peptide composition to activate the activity of tyrosinase and promote the generation of collagen on the one hand; on the other hand, the hair conditioner can nourish hair follicles and repair damaged hair scales so as to promote the hair to be smooth and moist.
In an exemplary embodiment of the present disclosure, the hair blackening agent may further include the following components and weight percentages thereof:
in the embodiment of the present disclosure, ethanol with an ethanol purity of 100% may be selected, and hydrous ethanol with a purity of less than 100% may also be selected, as long as the effective content of ethanol is finally ensured to be between 0.5% and 1%.
In one embodiment, 95% aqueous ethanol may be selected, and in this case, the 95% aqueous ethanol is present in an amount of 0.53% to 1.05% by weight of the hair blackening formulation.
In the embodiment of the disclosure, the addition of the cacumen biotae extract can further assist the glossy privet fruit peptide composition to activate the activity of tyrosinase and promote the generation of collagen, so that the natural blackening of white hair can be effectively promoted, and the problem of white hair can be fundamentally solved.
In another exemplary embodiment of the present disclosure, the hair blackening agent may further include the following components and weight percentages thereof:
in another exemplary embodiment of the present disclosure, the hair blackening agent may further include the following components and weight percentages thereof:
the hair blackening agent provided by the embodiment of the disclosure can effectively activate the activity of tyrosinase and promote the generation of collagen through reasonable proportioning and based on the glossy privet fruit high molecular peptide, the glossy privet fruit medium molecular peptide and the glossy privet fruit low molecular peptide contained in the glossy privet fruit peptide composition, thereby promoting the natural blackening of white hair and fundamentally solving the problem of white hair.
In yet another exemplary embodiment of the present disclosure, the fructus ligustri lucidi peptide composition may include the following components and weight percentages thereof:
50% of glossy privet fruit high-molecular peptide;
20% of molecular peptide in glossy privet fruit;
30% of glossy privet fruit low-molecular peptide.
Unlike conventional fructus Ligustri Lucidi extracts, the fructus Ligustri Lucidi peptide composition contains polypeptides related to fructus Ligustri Lucidi. Wherein the fructus Ligustri Lucidi peptide composition can be obtained by hydrolyzing fructus Ligustri Lucidi with enzyme or fermenting. The polypeptide (fructus Ligustri Lucidi peptide composition) of fructus Ligustri Lucidi can promote absorption via glycolipid, and effectively activate tyrosinase activity and promote collagen production, thereby promoting natural blackening of white hair.
A method for preparing the hair blackening agent according to the first aspect of the present disclosure will be described below. The preparation method is realized by the following steps:
mixing the glossy privet fruit high molecular peptide, the glossy privet fruit medium molecular peptide and the glossy privet fruit low molecular peptide at room temperature, and stirring until the glossy privet fruit high molecular peptide, the glossy privet fruit medium molecular peptide and the glossy privet fruit low molecular peptide are uniformly mixed to form the glossy privet fruit peptide composition.
Mixing fructus Ligustri Lucidi peptide composition and other raw materials except fructus Ligustri Lucidi peptide at room temperature, and stirring to mix well to obtain hair blackening agent.
In one embodiment, the fructus ligustri lucidi peptide composition, ethanol, the first extract for promoting melanogenesis, the pecan extract and water may be mixed at room temperature and stirred until mixed uniformly to obtain the hair blackening agent.
In another embodiment, fructus Ligustri Lucidi peptide composition, ethanol, melanogenesis promoting first extract, Juglandis Mandshuricae extract, folium Platycladi extract and water can be mixed at room temperature and stirred to mix well to obtain hair blackening agent.
It is understood that in the present disclosure, the stirring speed of stirring the mixture is not particularly limited, and in one embodiment, the stirring mixture can be stirred by a stirrer, wherein the stirring speed of the stirrer can be 500-.
In one embodiment of the present disclosure, the fructus ligustri lucidi polymer peptide can be prepared by the following steps:
putting the glossy privet fruit powder solution into a fermentation tank, and fermenting for 4-10 hours at the temperature of 40-50 ℃ to obtain fermentation liquor.
Mixing the fermentation liquor with the bacillus subtilis, stirring at a stirring speed of 150r/min, and carrying out ultrasonic treatment on the fermentation liquor for 3min to obtain the glossy privet fruit high-molecular peptide. Wherein, in the process of carrying out ultrasonic treatment on the fermentation liquor, the ultrasonic power of the ultrasonic treatment is 1500-1800W.
In this embodiment, the characteristics of bacillus subtilis capable of producing active protease, especially protease with endonuclease, are utilized, and the active protease is utilized to cleave the fructus ligustri lucidi to obtain fructus ligustri lucidi polymer peptide.
The active protease produced by the bacillus subtilis microorganism has strong protein enzymolysis capability, and can form glossy privet fruit high-molecular peptide by cutting peptide bond of protein. Further, the bacillus subtilis microorganism can also utilize the polypeptide in the hydrolysate as a nutrient substance to promote the growth and the metabolic products of the bacillus subtilis microorganism, thereby reducing the time for fermentation and producing active protease.
In one embodiment, the pH of the fermentation broth can be controlled to be 6.5-7.5, so as to provide a good reaction environment for the Bacillus subtilis to generate active protease and the fructus Ligustri Lucidi polymer peptide obtained by enzyme digestion of fructus Ligustri Lucidi with the active protease.
In one embodiment, the concentration of the fructus Ligustri Lucidi powder solution may be 0.04 g/ml. It can be understood that the concentration of the glossy privet fruit powder solution is set to be 0.04g/ml, so that the influence on the flowability of the fermentation liquor due to the excessive thickening of the fermentation liquor can be avoided, and the influence on the efficiency of obtaining the glossy privet fruit high-molecular peptide by enzyme digestion on glossy privet fruit can be further avoided. But also can ensure that the quantity of the glossy privet fruit high molecular peptides finally obtained is not influenced by too little glossy privet fruit effective substances caused by too low concentration of fermentation liquor.
In one embodiment of the present disclosure, the molecular peptide in fructus ligustri lucidi can be prepared by the following steps:
putting the glossy privet fruit powder solution into a fermentation tank, and fermenting for 4-10 hours at the temperature of 40-50 ℃ to obtain fermentation liquor.
Mixing the fermentation liquor with the bacillus subtilis, stirring at a stirring speed of 150r/min, and carrying out ultrasonic treatment on the fermentation liquor for 3min to obtain the molecular peptide in the glossy privet fruit. Wherein, in the process of carrying out ultrasonic treatment on the fermentation liquor, the ultrasonic power of the ultrasonic treatment is 2000W.
In one embodiment, the pH of the fermentation broth can be controlled to be 6.5-7.5, so as to provide a good reaction environment for the Bacillus subtilis to generate active protease, and the molecular peptide in the fructus Ligustri Lucidi can be obtained by using the active protease to perform enzyme digestion on the fructus Ligustri Lucidi.
In one embodiment, the concentration of the fructus Ligustri Lucidi powder solution may be 0.04 g/ml. It can be understood that the concentration of the glossy privet fruit powder solution is set to be 0.04g/ml, so that the influence on the flowability of the fermentation liquor due to the excessive thickening of the fermentation liquor can be avoided, and the influence on the efficiency of enzyme digestion on glossy privet fruit to obtain the molecular peptide in the glossy privet fruit can be further avoided. But also can ensure that the quantity of the glossy privet fruit high molecular peptides finally obtained is not influenced by too little glossy privet fruit effective substances caused by too low concentration of fermentation liquor.
In one embodiment of the present disclosure, the fructus ligustri lucidi low molecular peptide can be prepared by the following steps:
putting the glossy privet fruit powder solution into a fermentation tank, and fermenting for 4-10 hours at the temperature of 40-50 ℃ to obtain fermentation liquor.
Mixing the fermentation liquor with the bacillus subtilis, stirring at a stirring speed of 150r/min, and carrying out ultrasonic treatment on the fermentation liquor for 3min to obtain the glossy privet fruit low-molecular-weight peptide. Wherein, in the process of carrying out ultrasonic treatment on the fermentation liquor, the ultrasonic power of the ultrasonic treatment is 3000W.
In one embodiment, the pH of the fermentation broth can be controlled to be 6.5-7.5, so as to provide a good reaction environment for the Bacillus subtilis to generate active protease, and the fructus Ligustri Lucidi low molecular peptide is obtained by using the active protease to perform enzyme digestion on the fructus Ligustri Lucidi.
In one embodiment, the concentration of the fructus Ligustri Lucidi powder solution may be 0.04 g/ml. It can be understood that the concentration of the glossy privet fruit powder solution is set to be 0.04g/ml, so that the influence on the flowability of the fermentation liquor due to the excessive thickening of the fermentation liquor can be avoided, and the influence on the efficiency of enzyme digestion on glossy privet fruit to obtain the molecular peptide in the glossy privet fruit can be further avoided. But also can ensure that the quantity of the glossy privet fruit high molecular peptides finally obtained is not influenced by too little glossy privet fruit effective substances caused by too low concentration of fermentation liquor.
A shampoo to which the hair blackening agent according to the first aspect of the present disclosure is applied will be described below. Wherein, the washing and protecting liquid can comprise the following components in percentage by weight:
the washing and caring solution disclosed by the embodiment of the disclosure can be prepared in the following manner.
Glycolipid is added to deionized water and mixed and stirred until homogeneous to obtain a first mixture. Wherein, the stirring can be carried out for 10min at the stirring speed of 1000-2000 r/min. In one example, the stirring may be performed at a stirring speed of 1000r/min for 10 min.
Cocamidopropyl betaine is added to the first mixture and the mixture is stirred until homogeneous to give a second mixture. Wherein, the stirring can be carried out for 10min at a stirring speed of 1000 r/min.
The polyquaternium 22 is added to the second mixture, and the mixture is stirred until uniform to obtain a third mixture. Wherein, the stirring can be carried out for 20min at a stirring speed of 1000 r/min.
The polyquaternium 10 is added to the third mixture, and the mixture is stirred until uniform, so as to obtain a fourth mixture. Wherein, the stirring can be carried out for 20min at a stirring speed of 1000 r/min.
Adding hair blackening agent into the fourth mixture, and mixing and stirring uniformly to obtain a fifth mixture. Wherein, the stirring can be carried out for 20min at a stirring speed of 1000 r/min.
And adding sodium benzoate and essence into the fifth mixture, and mixing and stirring uniformly to obtain the washing and caring liquid disclosed by the embodiment of the disclosure. Wherein, the stirring can be carried out for 20min at a stirring speed of 1000 r/min.
It should be noted that, in the preparation of the rinse solution, the pH of the reaction solution may be controlled to be 6 to 7. In this example, the pH of the reaction solution was controlled to 6.5.
Next, another hair conditioner to which the hair blackening agent according to the first aspect of the present disclosure is applied will be described. Wherein, the washing and protecting liquid can comprise the following components in percentage by weight:
the washing and caring solution disclosed by the embodiment of the disclosure can be prepared in the following manner.
Stirring deionized water and sclerotium rolfsii gum for 20min at a stirring speed of 1000r/min, and homogenizing for 10min to obtain a first mixture.
Adding hair blackening agent, glycolipid and essence into the first mixture, mixing and stirring uniformly, and stirring at a stirring speed of 1000r/min for 20min to obtain the lotion of the embodiment of the disclosure.
It should be noted that, in the preparation of the rinse solution, the pH of the reaction solution may be controlled to be 6 to 7. In this example, the pH of the reaction solution was controlled to 6.5.
Hereinafter, examples of hair-blacking elements according to the present disclosure, application examples of a hair-washing liquid to which the hair-blacking elements according to the present disclosure are applied, and comparative examples will be described in detail.
In the following examples, experimental methods not specified for specific conditions were selected or determined according to conventional methods and conditions, or according to the commercial instructions.
In the following examples, unless otherwise specified, all experimental materials used are generally commercially available.
Example 1
According to one embodiment of the present disclosure, the hair blackening agent comprises the following components by weight:
the hair blackening agent of this example was prepared as follows:
mixing fructus Ligustri Lucidi peptide composition, ethanol, Polygoni Multiflori radix extract, wild Juglandis extract and water at room temperature, and stirring to mix well to obtain hair blackening agent. Wherein, the stirring speed can be 500-1000 r/min.
The ligustrum lucidum peptide composition can be prepared by adopting the following method:
mixing the glossy privet fruit high molecular peptide, the glossy privet fruit medium molecular peptide and the glossy privet fruit low molecular peptide according to the proportion of 5:2:3 at room temperature, and stirring until the mixture is uniformly mixed to form the glossy privet fruit peptide composition.
Further, the glossy privet fruit high molecular peptide can be prepared by adopting the following method:
putting 0.04g/ml glossy privet fruit powder solution into a fermentation tank, and fermenting for 4-10 hours at the temperature of 40-50 ℃ to obtain fermentation liquor. In this embodiment, 0.04g/ml ligustrum lucidum powder solution can be placed in a fermentation tank to be fermented for 8 hours at 42 ℃ to obtain fermentation liquor.
Mixing the fermentation liquor with the bacillus subtilis, stirring at a stirring speed of 150r/min, and carrying out ultrasonic treatment on the fermentation liquor for 3min to obtain the glossy privet fruit high-molecular peptide. Wherein, in the process of carrying out ultrasonic treatment on the fermentation liquor, the ultrasonic power of the ultrasonic treatment is 1500-1800W. The pH of the fermentation broth was controlled at 6.5.
The molecular peptide in glossy privet fruit can be prepared by the following steps:
putting 0.04g/ml glossy privet fruit powder solution into a fermentation tank, and fermenting for 4-10 hours at the temperature of 40-50 ℃ to obtain fermentation liquor. In this embodiment, 0.04g/ml ligustrum lucidum powder solution can be placed in a fermentation tank to be fermented for 8 hours at 42 ℃ to obtain fermentation liquor.
Mixing the fermentation liquor with the bacillus subtilis, stirring at a stirring speed of 150r/min, and carrying out ultrasonic treatment on the fermentation liquor for 3min to obtain the molecular peptide in the glossy privet fruit. Wherein, in the process of carrying out ultrasonic treatment on the fermentation liquor, the ultrasonic power of the ultrasonic treatment is 2000W. The pH of the fermentation broth was controlled at 6.5.
The glossy privet fruit low-molecular peptide can be prepared by the following steps:
putting 0.04g/ml glossy privet fruit powder solution into a fermentation tank, and fermenting for 4-10 hours at the temperature of 40-50 ℃ to obtain fermentation liquor. In this embodiment, 0.04g/ml ligustrum lucidum powder solution can be placed in a fermentation tank to be fermented for 8 hours at 42 ℃ to obtain fermentation liquor.
Mixing the fermentation liquor with the bacillus subtilis, stirring at a stirring speed of 150r/min, and carrying out ultrasonic treatment on the fermentation liquor for 3min to obtain the glossy privet fruit low-molecular-weight peptide. Wherein, in the process of carrying out ultrasonic treatment on the fermentation liquor, the ultrasonic power of the ultrasonic treatment is 3000W. The pH of the fermentation broth was controlled at 6.5.
Example 2
According to one embodiment of the present disclosure, the hair blackening agent comprises the following components by weight:
the preparation method of this example is the same as example 1.
Example 3
According to one embodiment of the present disclosure, the hair blackening agent comprises the following components by weight:
the hair blackening agent of this example was prepared as follows:
mixing fructus Ligustri Lucidi peptide composition, ethanol, Polygoni Multiflori radix extract, folium Platycladi extract, wild Juglandis extract and water at room temperature, and stirring to mix well to obtain hair blackening agent. Wherein, the stirring speed can be 500-1000 r/min. In this embodiment, the stirring speed may be 800 r/min.
It will be appreciated that ligustrum lucidum peptide compositions were prepared according to the method of example 1.
Example 4
According to one embodiment of the present disclosure, the hair blackening agent comprises the following components by weight:
the procedure of this example was the same as in example 3.
Example 5
According to one embodiment of the present disclosure, the hair blackening agent comprises the following components by weight:
the procedure of this example was the same as in example 3.
Application example 1 and application example 2 described below are each a hair conditioner to which the hair blackening agent described in the embodiments of the present disclosure is applied.
Application example 1
The washing and protecting liquid described in application example 1 can comprise the following components in percentage by weight:
since the preparation method of the rinse solution described in application example 1 is described above, it is not described herein again.
Application example 2
The washing and protecting liquid described in application example 2 can comprise the following components in percentage by weight:
since the preparation method of the rinse solution described in application example 2 has been described above, it is not described herein again.
Comparative example 1
The hair blackening agent of the comparative example 1 comprises the following components in percentage by weight:
comparative example 2
The hair blackening agent of the comparative example 2 comprises the following components in percentage by weight:
comparative example 3
The hair blackening agent of the comparative example 3 comprises the following components in percentage by weight:
comparative example 4
The hair blackening agent of comparative example 4 comprises the following components in percentage by weight:
comparative example 5
The hair blackening agent of the comparative example 5 comprises the following components in percentage by weight:
comparative example 6
The hair blackening agent of comparative example 6 comprises the following components in percentage by weight:
and (3) analyzing experimental data:
the test method comprises the following steps: volunteers 160 aged 18-65 years (with white hair problems) were randomized into 16 groups of 10 people each.
Hair care was carried out for 10 months using examples 1 to 5, application examples 1 to 2, comparative examples 1 to 6, two commercially available hair tonins and a blank control, respectively. Among them, the blank control group was a group for hair care using only deionized water.
The volunteers were subjected to hair care every 3 days, and the white hair rate of the volunteers was tested at months 6 and 10 after the hair care. Wherein the white hair rate is measured by a professional salon evaluator sensory evaluation mode in combination with a hair microscope.
Table 1 shows the results of the white hair test after hair care using examples 1 to 5, comparative examples 1 to 6, application example 1, application example 2, a commercial product, and a blank control, respectively.
TABLE 1 comparison of the white hair test results
As can be seen from table 1, in 6 months or 10 months after the volunteers had treated their hair with the hair tonics of examples and the lotions of examples (the lotions were those using the hair tonics), the white hair rate was significantly lower than that of the volunteers after treated their hair with the hair tonics of comparative examples, commercial products or blank control. The hair blackening agent can effectively promote white hair to naturally blacken.
Further, after the volunteers treated the hair with the hair blackening cream of the example and the lotion of the example, wherein the white hair rate of the 10 th month is obviously lower than that of the 6 th month, the continuous use of the hair blackening cream of the example of the present disclosure can effectively promote the white hair to naturally blacken, thereby fundamentally solving the problem of white hair.
The foregoing description of the implementation of the invention has been presented for purposes of illustration and description. It is not intended to be exhaustive or to limit the invention to the precise form disclosed, and modifications and variations are possible in light of the above teachings or may be acquired from practice of the invention. The embodiments were chosen and described in order to explain the principles of the invention and its practical application to enable one skilled in the art to utilize the invention in various embodiments and with various modifications as are suited to the particular use contemplated.
Claims (12)
1. The hair blackening cream is characterized by comprising the following components in percentage by weight:
the fructus ligustri lucidi peptide composition comprises fructus ligustri lucidi high molecular peptide, fructus ligustri lucidi medium molecular peptide and fructus ligustri lucidi low molecular peptide, and the first extract for promoting melanogenesis comprises polygonum multiflorum extract.
2. The hair relaxer as claimed in claim 1, further comprising an extract of cacumen biotae, wherein the weight percentage of cacumen biotae is 5-20%.
3. The hair blackening agent of claim 2, wherein the weight percentage of the fructus ligustri lucidi peptide composition is 5-10%; the first extract for promoting melanogenesis accounts for 5-8 wt%; the weight percentage of the cacumen biotae extract is 5-10%; the weight percentage of the wild walnut extract is 10-15%.
4. The hair blackening agent of claim 3, wherein the weight percentage of the fructus ligustri lucidi peptide composition is 7.5%; the weight percentage of the ethanol is 0.75 percent; the first extract for promoting melanogenesis is the polygonum multiflorum extract, wherein the weight percentage of the polygonum multiflorum extract is 6%; the weight percentage of the cacumen biotae extract is 7.5 percent; the weight percentage of the wild walnut extract is 12.5 percent.
5. The hair blackening agent of claim 1, wherein the weight percentage of the fructus ligustri lucidi polymer peptide in the fructus ligustri lucidi peptide composition is 50%; the weight percentage of the molecular peptide in the glossy privet fruit is 20 percent; the weight percentage of the glossy privet fruit low-molecular peptide is 30%.
6. A method for preparing the hair blackening agent of any one of claims 1 to 5, which is characterized by comprising the following steps:
mixing the glossy privet fruit high molecular peptide, the glossy privet fruit medium molecular peptide and the glossy privet fruit low molecular peptide at room temperature, and stirring until the glossy privet fruit high molecular peptide, the glossy privet fruit medium molecular peptide and the glossy privet fruit low molecular peptide are uniformly mixed to form the glossy privet fruit peptide composition.
7. The method of manufacturing according to claim 6, further comprising:
and mixing the glossy privet fruit peptide composition, ethanol, the first extract for promoting melanogenesis, the wild walnut extract and deionized water at room temperature, and stirring until the mixture is uniformly mixed to obtain the hair blackening agent.
8. The method according to claim 6, wherein the fructus Ligustri Lucidi polymer peptide is prepared by:
putting the glossy privet fruit powder solution into a fermentation tank, and fermenting for 4-10 hours at the temperature of 40-50 ℃ to obtain fermentation liquor;
and mixing the fermentation liquor with the bacillus subtilis, stirring at a stirring speed of 150r/min, and carrying out ultrasonic treatment on the fermentation liquor for 3min to obtain the glossy privet fruit high-molecular peptide, wherein the ultrasonic power of the ultrasonic treatment is 1500-1800W.
9. The preparation method of claim 6, wherein the molecular peptide in fructus Ligustri Lucidi is prepared by the following steps:
putting the glossy privet fruit powder solution into a fermentation tank, and fermenting for 4-10 hours at the temperature of 40-50 ℃ to obtain fermentation liquor;
and mixing the fermentation liquor with bacillus subtilis, stirring at a stirring speed of 150r/min, and carrying out ultrasonic treatment on the fermentation liquor for 3min to obtain the ligustrum lucidum middle molecular peptide, wherein the ultrasonic power of the ultrasonic treatment is 2000W.
10. The preparation method of claim 6, wherein the fructus Ligustri Lucidi low molecular peptide is prepared by the following steps:
putting the glossy privet fruit powder solution into a fermentation tank, and fermenting for 4-10 hours at the temperature of 40-50 ℃ to obtain fermentation liquor;
and mixing the fermentation liquor with bacillus subtilis, stirring at a stirring speed of 150r/min, and carrying out ultrasonic treatment on the fermentation liquor for 3min to obtain the glossy privet fruit low-molecular-weight peptide, wherein the ultrasonic power of the ultrasonic treatment is 3000W.
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