CN114557921A - Multiple-oil skin softening composition, preparation method thereof, scalp nourishing and moisturizing composition and scalp anti-dandruff oil-control deodorizing composition - Google Patents
Multiple-oil skin softening composition, preparation method thereof, scalp nourishing and moisturizing composition and scalp anti-dandruff oil-control deodorizing composition Download PDFInfo
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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Abstract
The invention relates to a multiple-oil skin softening composition, a preparation method thereof, a scalp nourishing and moisturizing composition and a scalp anti-dandruff oil-control deodorizing composition. The preparation method comprises the following steps: mixing and heating mesoporous silica and the multiple grease composition, stirring and grinding to obtain a mixture a; carrying out ultrasonic treatment on the mixture a to obtain a mixture b; heating the mixture b under the condition of a microwave field to obtain a mixture c; and (3) cooling the mixture c to a non-flowing state to obtain the multi-oil skin softening composition. The preparation method of the multiple grease smoothing composition comprises the steps of mixing, heating, stirring and grinding the mesoporous silica and the multiple grease composition, and then carrying out ultrasonic and microwave treatment, so that sticky grease is wrapped in the mesoporous silica, the mesoporous silica has the light and smooth feeling of feathers, meanwhile, the sticky property of the grease can be reduced, and the moisturizing effect can be well kept.
Description
Technical Field
The invention belongs to the field of daily chemicals, and particularly relates to a multiple-oil skin softening composition, a preparation method thereof, a scalp nourishing and moisturizing composition and a scalp anti-dandruff, oil-control and deodorizing composition.
Background
The existing skin care products mostly adopt the technical idea of 'nourishing the skin with oil', particularly have better effects on dry skin and damaged skin, the history of 'nourishing the skin with oil' can also be traced back to the ancient Egypt period at the earliest, the most commonly used grease of the ancient Egypt people at that time is castor oil and Egypt acid leaf wood oil, and the grease is coated on the skin to treat skin problems such as eczema and the like.
However, "nourishing the skin with oil" brings about a non-negligible problem that the skin feels sticky and the skin feeling experience is not pleasant.
Therefore, the technical scheme of the invention is provided.
Disclosure of Invention
In order to solve the problems in the prior art, the invention provides a multiple-oil skin softening composition, a preparation method thereof, a scalp nourishing and moisturizing composition, a scalp anti-dandruff oil-controlling and deodorizing composition. The preparation method of the multiple grease smoothing composition comprises the steps of mixing, heating, stirring and grinding the mesoporous silica and the multiple grease composition, and then carrying out ultrasonic and microwave treatment, so that sticky grease is wrapped in the mesoporous silica, the mesoporous silica has the light and smooth feeling of feathers, meanwhile, the sticky property of the grease can be reduced, and the moisturizing effect can be well kept. It is emphasized that most of the sticky grease can be improved by the technical scheme of the invention. Such as: ether-based oils (such as tarragon, fennel, nutmeg, pink lotus, tropical basil, and western yellow pine), aldehyde-based oils (such as lemon myrtle, thailand green lemon leaf, and balm), ester-based oils (such as ammi anise, michelia figo, clary sage, shea butter, and jojoba), phenol, and aromatic-based oils (such as cacao butter, cacao butter seed, thyme from wild thyme, tarragon, and liang river vine).
The scheme of the invention is to provide a preparation method of a multiple-oil skin softening composition, which comprises the following steps:
(1) mixing and heating mesoporous silica and the multiple grease composition, stirring and grinding to obtain a mixture a;
(2) carrying out ultrasonic treatment on the mixture a to obtain a mixture b;
(3) heating the mixture b under the condition of a microwave field to obtain a mixture c;
(4) and (3) cooling the mixture c to a non-flowing state to obtain the multi-oil skin softening composition.
Preferably, in the step (1), the multiple grease composition comprises the following raw materials: jojoba fat, shea butter, dahua cocoa butter, and shea butter.
Preferably, in the step (1), the multiple grease composition comprises the following raw materials: avocado oil, shea butter, dahua cocoa butter, and avocado oil unsaponifiables.
Preferably, in the step (1), the rotation speed of the stirring and grinding is 9000-11000 r/min; the stirring and grinding time is 15-25 min.
Preferably, in the step (2), the time of the ultrasonic treatment is 45-55 min.
Preferably, in the step (3), the heating time is 50-60 min.
Based on the same technical concept, the invention further provides a multiple-oil skin softening composition prepared by the method.
Based on the same technical concept, the invention further provides a scalp nourishing and moisturizing composition, which comprises the following raw materials in percentage by weight: 0.8-1.2% of sclerotium rolfsii gum, 4.5-5.5% of multiple oil and fat skin softening composition, 2-4% of 1, 3-butanediol, 8-12% of hair blackening agent, 0.4-0.6% of preservative and the balance of water.
Based on the same technical concept, the invention further provides a scalp anti-dandruff oil-control deodorization composition, which comprises the following raw materials in percentage by weight: 0.8-1.2% of sclerotium rolfsii gum, 4.5-5.5% of multiple grease smoothing composition, 2-4% of 1, 3-butanediol, 2-4% of deoiling factor, 0.8-1.2% of plant deodorization factor, 0.4-0.6% of preservative and the balance of water.
In order to facilitate understanding of the invention, the function of some of the materials of the invention will be explained.
Jojoba lipid: according to researches, the skin care product can rapidly improve the appearance of skin, remarkably reduce excessive greasy skin oil and pores within 14 days, reduce skin redness, increase skin comfort and improve skin glossiness.
Shea butter: has the effects of moisturizing and smoothing skin, and is often used as a skin conditioner.
Dahua cocoa resin: the plant sterol extract is prepared from seeds of the hydrangea macrophylla, belongs to a natural product, is rich in lauric acid, has good water absorption effect and moisturizing performance, contains phytosterol, is a non-saponifiable matter, acts on a cell layer, and is used for regulating secretion and balance of skin surface oil. Such phytosterols have been used in skin care methods and to promote healing of ulcers.
Butyrospermum parkii oil: the cosmetic and skin care product mainly has antioxidant and humectant effects. The extract of Butyrospermum parkii is an inhibitor of xanthine oxidase, has effects of scavenging superoxide radical generated by xanthine-xanthine oxidase system, activating skin, and can be used in anti-aging cosmetics and moisturizing.
Avocado oil: the hair conditioner contains abundant vitamins, sterols, lecithin and the like, has good nutrition and osmosis, can fully nourish the skin, make the skin white, fine and glossy, has a good recovery effect on dry and heat-damaged hair, makes the hair soft and glossy, and is also suitable for improving dry and aged skin and preventing striae gravidarum. It is often added into winter care oil, repair type face cream, etc.
Avocado oil unsaponifiable matter: the skin care product has the advantages of extremely high nutrition, high moisture, good ductility and good permeability, is easy to be absorbed by the skin, is helpful for locking moisture and promoting cell regeneration, and is suitable for dry and aged skin.
The invention has the beneficial effects that:
according to the preparation method of the multiple grease smoothing composition, the mesoporous silica and the multiple grease composition are mixed, heated, stirred and ground, and then ultrasonic treatment and microwave treatment are carried out, so that sticky grease is wrapped in the mesoporous silica, the mesoporous silica has the light and smooth feeling of feathers, meanwhile, the sticky property of the grease can be reduced, and the moisturizing effect can be well kept.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the drawings without creative efforts.
FIG. 1 is a graph of results of a use test using a conventional moisturizing grease system commercially available;
FIG. 2 is a graph showing the results of the use test using the scalp nourishing moisturizing composition obtained in example 4;
fig. 3 is a graph showing the results of the use test using the dandruff control oil and malodor composition obtained in example 5.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the technical solutions of the present invention will be described in detail below. It is to be understood that the described embodiments are merely exemplary of the invention, and not restrictive of the full scope of the invention. All other embodiments, which can be derived by a person skilled in the art from the examples given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
In this example, the weight percentages of the raw materials are shown in table 1. In the embodiment, the actual weight of the raw materials can be proportionally increased or decreased according to the requirement.
Table 1 raw material usage percentage
This example provides a method for preparing a multiple-lipid skin softening composition, comprising the steps of:
(1) mixing and heating 0.9g of mesoporous silica, 529g of jojoba fat, 216g of shea butter, 216g of cocoa butter of dahua, 1g of shea butter and 37.1g of glycerin, stirring and grinding for 25min under the condition of 9000r/min to obtain a mixture a;
(2) carrying out ultrasonic treatment on the mixture a for 45min in an ultrasonic environment, and utilizing ultrasonic waves to enable small molecular grease to effectively enter the mesoporous silicon to obtain a mixture b;
(3) heating the mixture b for 50min under the condition of a microwave field to obtain a mixture c;
(4) and (3) cooling the mixture c to a non-flowing state to obtain the multi-oil skin softening composition.
Example 2
In this example, the weight percentages of the raw materials are shown in table 2. In the embodiment, the actual weight of the raw materials can be proportionally increased or decreased according to the requirement.
TABLE 2 percentage of raw materials used
This example provides a method for preparing a multiple-lipid skin softening composition, comprising the steps of:
(1) mixing 6.8g of mesoporous silica, 51.67g of jojoba fat, 20.73g of shea butter, 20.73g of dahua cocoa resin and 0.07g of shea butter, heating, and stirring and grinding for 15min at the condition of 11000r/min to obtain a mixture a;
(2) carrying out ultrasonic treatment on the mixture a for 55min in an ultrasonic environment, and utilizing ultrasonic waves to enable the small molecular grease to effectively enter the mesoporous silicon to obtain a mixture b;
(3) heating the mixture b for 60min under the condition of a microwave field to obtain a mixture c;
(4) and (3) cooling the mixture c to a non-flowing state to obtain the multi-oil skin softening composition.
Example 3
In this example, the weight percentages of the raw materials are shown in table 3. In the embodiment, the actual weight of the raw materials can be proportionally increased or decreased according to the requirement.
TABLE 3 percentage of raw materials used
| Kind of raw material | Ratio of |
| Avocado oil | 51％ |
| Butyrospermum parkii fruit resin | 20％ |
| Cocoa resin of dahua | 10％ |
| Avocado oil unsaponifiable matter | 9％ |
| Mesoporous silica | 10％ |
This example provides a method for preparing a multiple-lipid skin softening composition, comprising the steps of:
(1) mixing 10g of mesoporous silica with 51g of avocado oil, 20g of shea butter, 10g of cocoa butter, and 9g of avocado oil unsaponifiable matter, heating, stirring and grinding for 20min under the condition of 10000r/min to obtain a mixture a;
(2) carrying out ultrasonic treatment on the mixture a for 50min in an ultrasonic environment, and utilizing ultrasonic waves to enable small molecular grease to effectively enter the mesoporous silicon to obtain a mixture b;
(3) heating the mixture b for 55min under the condition of a microwave field to obtain a mixture c;
(4) and (3) cooling the mixture c to a non-flowing state to obtain the multi-oil skin softening composition.
Example 4
In this example, the weight percentages of the raw materials are shown in table 4. In the embodiment, the actual weight of the raw materials can be proportionally increased or decreased according to the requirement.
TABLE 4 percentage of raw materials used
The embodiment provides a preparation method of a scalp nourishing and moisturizing composition, which comprises the following steps: mixing 10g of sclerotium rolfsii gum, 50g of multiple oil skin softening composition, 30g of 1, 3-butanediol, 100g of hair blackening agent, 5g of preservative and 805g of water, homogenizing, and stabilizing the system to obtain the scalp nourishing and moisturizing composition.
Example 5
In this example, the weight percentages of the raw materials are shown in table 5. In the embodiment, the actual weight of the raw materials can be proportionally increased or decreased according to the requirement.
TABLE 5 percent of raw materials used
This example provides a method for preparing an anti-dandruff, oil-controlling, and deodorant composition for scalp, comprising: mixing 10g of sclerotium rolfsii gum, 50g of multiple oil softening composition, 30g of 1, 3-butanediol, 30g of deoiling factor, 10g of plant deodorization factor, 5g of preservative and 865g of water, homogenizing, and stabilizing the system to obtain the scalp nourishing and moisturizing composition.
In order to demonstrate the skin feel effect of the multiple oil skin softening composition of the present invention, the multiple oil skin softening composition obtained in example 1 was tested with reference to tables 6 and 7. Wherein, table 6 is a skin feeling reference sample list, and table 7 is a skin feeling characteristic scale common to the skin of cream skin care products.
Table 6 skin feel reference sample list
After detection, the extensibility of the multiple oil skin softening composition is 14 minutes, so that the ointment which is not easy to spread is easier to spread; in addition, the skin moistening degree can reach 10-14 minutes, the skin feeling is better, and when the solvent is used less, the obtained multiple-oil skin softening composition can be drier and more comfortable, and the skin moistening degree is 5-7 minutes.
TABLE 7 common skin feel characteristics of cream skin care products
After testing, the fineness of the multi-oil skin softening composition can reach 10-15 minutes, so that the originally not-fine paste is more fine; the coating is easier and can reach 10-15 minutes; the skin hand-sticking degree reaches the hand-sticking-free touch feeling, and can reach 10-15 minutes; no uncomfortable residual feeling; the overall absorption speed is high.
Also, the scalp nourishing moisturizing composition and the scalp anti-dandruff oil-controlling deodorizing composition containing the multiple oil skin softening composition were subjected to the use effect test. FIG. 1 is a graph showing the results of a use test using a conventional moisturizing grease system on the market; FIG. 2 is a graph showing the results of the usage test of the scalp nourishing moisturizing composition obtained in example 4; fig. 3 is a graph showing the results of the use test using the dandruff control oil and malodor composition obtained in example 5.
It can be seen from the results that the scalp nourishing and moisturizing composition and the scalp anti-dandruff, oil-controlling and deodorizing composition obtained in examples 4 and 5 can improve the glossiness of the scalp, have good moisture retention, and can adjust the microecology of the scalp to achieve a state of oil balance, thereby achieving the effects of oil control and anti-dandruff.
The above description is only for the specific embodiments of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can easily think of the changes or substitutions within the technical scope of the present invention, and shall cover the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the appended claims.
Claims (9)
1. A preparation method of a multiple-oil skin softening composition is characterized by comprising the following steps:
(1) mixing and heating mesoporous silica and the multiple grease composition, stirring and grinding to obtain a mixture a;
(2) carrying out ultrasonic treatment on the mixture a to obtain a mixture b;
(3) heating the mixture b under the condition of a microwave field to obtain a mixture c;
(4) and (3) cooling the mixture c to a non-flowing state to obtain the multi-oil skin softening composition.
2. The method for preparing the multiple-oil skin softening composition according to claim 1, wherein in the step (1), the multiple-oil composition comprises the following raw materials: jojoba fat, shea butter, dahua cocoa butter, and shea butter.
3. The method for preparing the multiple-oil skin softening composition according to claim 1, wherein in the step (1), the multiple-oil composition comprises the following raw materials: avocado oil, shea butter, dahua cocoa butter, and avocado oil unsaponifiables.
4. The preparation method of the multiple-oil skin softening composition according to claim 1, wherein in the step (1), the rotation speed of stirring and grinding is 9000-11000 r/min; the stirring and grinding time is 15-25 min.
5. The method for preparing the multi-oil skin softening composition according to claim 1, wherein in the step (2), the ultrasonic treatment time is 45-55 min.
6. The method for preparing the multi-oil skin softening composition according to claim 1, wherein the heating time in the step (3) is 50-60 min.
7. A multi-oil skin softening composition prepared by the method of any one of claims 1 to 6.
8. The scalp nourishing and moisturizing composition is characterized by comprising the following raw materials in percentage by weight: 0.8-1.2% of sclerotium rolfsii gum, 4.5-5.5% of multiple oil and fat skin softening composition, 2-4% of 1, 3-butanediol, 8-12% of hair blackening agent, 0.4-0.6% of preservative and the balance of water.
9. The dandruff-removing, oil-controlling and deodorizing composition for the scalp is characterized by comprising the following raw materials in percentage by weight: 0.8-1.2% of sclerotium rolfsii gum, 4.5-5.5% of multiple grease smoothing composition, 2-4% of 1, 3-butanediol, 2-4% of deoiling factor, 0.8-1.2% of plant deodorization factor, 0.4-0.6% of preservative and the balance of water.
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| CN202210169611.3A CN114557921A (en) | 2022-02-23 | 2022-02-23 | Multiple-oil skin softening composition, preparation method thereof, scalp nourishing and moisturizing composition and scalp anti-dandruff oil-control deodorizing composition |
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| CN202210169611.3A CN114557921A (en) | 2022-02-23 | 2022-02-23 | Multiple-oil skin softening composition, preparation method thereof, scalp nourishing and moisturizing composition and scalp anti-dandruff oil-control deodorizing composition |
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Citations (5)
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|---|---|---|---|---|
| CN103520019A (en) * | 2013-09-27 | 2014-01-22 | 华南理工大学 | Preparation method of beautifying, sun-blocking and isolating emulsion containing hexagonal meso-porous silicon |
| CN103816084A (en) * | 2014-02-28 | 2014-05-28 | 华南理工大学 | Slow- release lotion carrier for whitening and spot removing, and preparation method thereof |
| CN107184455A (en) * | 2017-05-18 | 2017-09-22 | 上海伊匠生物科技有限公司 | A kind of natural organic face cream |
| CN112587434A (en) * | 2021-01-05 | 2021-04-02 | 石远琳 | Hair blackening agent, preparation method of hair blackening agent and washing and caring liquid |
| CN113230157A (en) * | 2021-04-07 | 2021-08-10 | 欧众联合(广州)科技有限公司 | Refreshing oil-control shampoo composition and preparation method thereof |
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- 2022-02-23 CN CN202210169611.3A patent/CN114557921A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103520019A (en) * | 2013-09-27 | 2014-01-22 | 华南理工大学 | Preparation method of beautifying, sun-blocking and isolating emulsion containing hexagonal meso-porous silicon |
| CN103816084A (en) * | 2014-02-28 | 2014-05-28 | 华南理工大学 | Slow- release lotion carrier for whitening and spot removing, and preparation method thereof |
| CN107184455A (en) * | 2017-05-18 | 2017-09-22 | 上海伊匠生物科技有限公司 | A kind of natural organic face cream |
| CN112587434A (en) * | 2021-01-05 | 2021-04-02 | 石远琳 | Hair blackening agent, preparation method of hair blackening agent and washing and caring liquid |
| CN113230157A (en) * | 2021-04-07 | 2021-08-10 | 欧众联合(广州)科技有限公司 | Refreshing oil-control shampoo composition and preparation method thereof |
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