CN112335691A - Antibacterial and acarid-removing composite essential oil - Google Patents
Antibacterial and acarid-removing composite essential oil Download PDFInfo
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Abstract
The invention discloses a sterilization and mite removal compound essential oil, which comprises a solvent and essential oil, wherein the essential oil comprises: 0.02-0.04% essential oil of fructus Citri Sarcodactylis; 0.04-0.06% of lemon essential oil; 0.01-0.03% rosemary essential oil; 0.01-0.02% essential oil of peppermint; 0.01-0.02% of eucalyptus oil by mass. The solvent comprises: 80-90% water; 2.0-5.0% of PPG-26-butanol polyether-26; 2.0-5.0% propylene glycol; 1.0-2.0% PEG-40 hydrogenated castor oil; 2.0-5.0% of 1, 2-hexanediol; 2.0-5.0% 1, 3-propanediol; 0.01-0.05% of caprylyl hydroximic acid. The sterilization and mite-killing compound essential oil disclosed by the invention can be used for effectively removing mites, is good in killing effect, is non-toxic and harmless, and has no side effect on environment and human bodies.
Description
Technical Field
The invention belongs to the technical field of household mite killing and antibiosis, and particularly relates to antibacterial and mite killing composite essential oil.
Background
With the increase of industrialization and the increase of environmental pollution, allergic diseases tend to increase year by year around the world, and become a worldwide health problem. According to one survey, the Chinese children asthma prevalence rate is 64.84% increased in ten years, and the onset age is 80% before 5 years, and the trend is gradually advanced. Generally, mites in the domestic environment, mainly dust mites, which belong to the class of arachnids, are effective against pyrethrins. Pyrethroids, which are pyrethroid-like drugs, are compounds that mimic the synthesis of pyrethrin. Among them, dimethyl propane carboxylate, commonly known as bifenthrin, has good mite killing effect. Some common household insecticides contain pyrethroid type ingredients and can also be used to kill mites. In addition, avermectins (commonly known as "avermectin") and carboxylic acid derivatives have also been used in mite control products. Although the chemical insecticide has a good mite killing effect, the pyrethrin has certain harm to human bodies, the harm is mainly reflected in the mucous membranes of skin, eyes, nose and throat, even influences on the nerves of the human bodies, and the human bodies have dizziness and uncomfortable feelings after being used by some people.
In order to reduce discomfort symptoms caused by other potential hazards of the mite killing agent to human bodies or spray residues, the development of the sterilizing and mite killing compound essential oil is urgently needed, can effectively remove and kill mites, is non-toxic and harmless, and has no side effects on the environment and human bodies.
Disclosure of Invention
The present invention is based on the discovery and recognition by the inventors of the following facts and problems: some plants contain biologically active chemicals, volatile plant extracts and essential oils consisting of alkanes, alcohols, aldehydes and terpenoids, especially monoterpenes, the fumigant activity of butanediamine, cinnamaldehyde, cinnamyl alcohol and salicylaldehyde, eugenol, benzoic acid and paeonol against mealybug and pteropiptosis adults, certain monoterpenes and sesquiterpene alcohols extracted from the volatile oils of the genus Mentha species competitively inhibit AChE-acetylcholinesterase in vitro and thereby exert neurotoxicity to living organisms. Extracts of some plants are selective, and are usually biodegradable into non-toxic products with little or no deleterious effect on non-target organisms. The acaricide can be used for dust mite nests such as mattresses, carpets, sofas and the like the traditional acaricide. The current commercial acaricide basically has contact toxicity, and can cause harm to human body and environment after long-term use.
The present invention is directed to solving, at least to some extent, one of the technical problems in the related art.
Therefore, the embodiment of the invention provides the sterilization and mite killing compound essential oil which can effectively remove mites, has a good killing effect, is non-toxic and harmless, and has no side effect on the environment and human bodies.
The sterilization and mite removal compound essential oil comprises a solvent and essential oil, wherein the essential oil comprises:
according to the advantages and the technical effects brought by the independent claims, 1, the composite essential oil disclosed by the embodiment of the invention has the advantages that the high inhibition rate on mites and bacteria can be realized under the condition that the whole addition amount of the essential oil is very low by carefully selecting the components and the proportion of each essential oil, the total addition amount of the essential oil is lower than 0.2%, the production cost is reduced, and the composite essential oil is suitable for industrial application; 2. the composite essential oil provided by the embodiment of the invention can obtain a good bacteriostatic effect while efficiently removing mites, has a good inhibitory effect on common domestic bacteria such as Escherichia coli, Staphylococcus aureus and Candida albicans, has a bacteriostatic rate of over 90%, and has broad-spectrum protection; 3. the compound essential oil provided by the embodiment of the invention is compounded from natural plant essential oil, is non-toxic and harmless, and has no side effect on environment and human body; 4. the compound essential oil provided by the embodiment of the invention can be used for home environments such as home textiles, bedding articles, pet articles and wet garbage storage barrels.
The sterilization and mite removal compound essential oil provided by the embodiment of the invention comprises the following solvents:
the sterilization and mite removal compound essential oil provided by the embodiment of the invention further comprises 0.02-0.03% of essence.
The sterilization and mite removal compound essential oil provided by the embodiment of the invention further comprises 0.01-0.02% of bitter orange leaf essential oil.
The sterilization and mite removal compound essential oil provided by the embodiment of the invention further comprises 0.01-0.02% of marjoram essential oil.
The sterilization and mite removal compound essential oil provided by the embodiment of the invention comprises the following components:
the sterilization and mite removal compound essential oil provided by the embodiment of the invention further comprises 0.01% of bitter orange leaf essential oil.
The sterilization and mite removal compound essential oil provided by the embodiment of the invention further comprises 0.01% of marjoram essential oil.
Detailed Description
The following detailed description of embodiments of the invention is intended to be illustrative, and not to be construed as limiting the invention.
The sterilization and mite removal compound essential oil comprises a solvent and essential oil, wherein the essential oil comprises:
the essential oil used in the examples of the present invention has the following effects:
bergamot essential oil: the bergamot has an antibacterial effect, and the composite essential oil provided by the embodiment of the invention can play a mite removing effect and also has an antibacterial effect.
Rosemary essential oil: rosemary is one of the earliest plants used in medicine, rosemary essential oil contains aromatic hydrocarbon B-2 which can rapidly kill mites, and the rosemary essential oil in the compound essential oil provided by the embodiment of the invention is mainly used for killing mites.
Peppermint essential oil: the peppermint is one of a few medicinal plants with high cure efficiency molecules capable of being completely converted into essential oil, the menthol with the proportion of 50-90% enables the peppermint to have fresh smell, and the peppermint essential oil is mainly used for removing mites and killing mites in the compound essential oil of the embodiment of the invention.
Lemon essential oil: the lemon has fresh fragrance, can refresh and restore consciousness, revivify spirit, relieve dysphoria, purify air and have good antifungal activity, the terpenes in the lemon essential oil can enable mites to be in a paralytic state after being used for 30 minutes, and the mites can be killed after being used for 2 hours. The lemon essential oil in the compound essential oil provided by the embodiment of the invention can play a mite removing role and also has an antibacterial effect.
Eucalyptus essential oil: especially, the main component of the composition is eucalyptol which is a good immunity stimulant and is suitable for people who feel tired frequently and are easy to catch a cold. Eucalyptus has very strong bactericidal and viricidal capabilities. The compound essential oil provided by the embodiment of the invention is mainly used as a bactericide.
According to the advantages and the technical effects brought by the independent claims, 1, the composite essential oil disclosed by the embodiment of the invention has the advantages that the high inhibition rate on mites and bacteria can be realized under the condition that the whole addition amount of the essential oil is very low by carefully selecting the components and the proportion of each essential oil, the total addition amount of the essential oil is lower than 0.2%, the production cost is reduced, and the composite essential oil is suitable for industrial application; 2. the composite essential oil provided by the embodiment of the invention can obtain a good bacteriostatic effect while efficiently removing mites, has a good inhibitory effect on common domestic bacteria such as Escherichia coli, Staphylococcus aureus and Candida albicans, has a bacteriostatic rate of over 90%, and has broad-spectrum protection; 3. the compound essential oil provided by the embodiment of the invention is compounded from natural plant essential oil, is non-toxic and harmless, and has no side effect on environment and human body; 4. the compound essential oil provided by the embodiment of the invention can be used for home environments such as home textiles, bedding articles, pet articles and wet garbage storage barrels.
The sterilization and mite removal compound essential oil provided by the embodiment of the invention comprises the following solvents:
the solvent provided by the embodiment of the invention adopts a formula combining various solvents and water, PPG-26-butanol polyether-26 is used as an emulsifier and a solubilizer and can promote the mixing of essential oil and water, propylene glycol is used as a solvent and a volatilization promoter, PEG-40 hydrogenated castor oil is used as an emulsifier and can promote the mixing of essential oil and water, 1, 2-hexanediol is a moisturizing agent with a refreshing feeling and can ensure that the compound essential oil provided by the embodiment of the invention is not sticky and sticky, 1, 3-propanediol is used as a solvent, and caprylyl hydroximic acid is used as a chelating agent.
The sterilization and mite removal compound essential oil provided by the embodiment of the invention further comprises 0.02-0.03% of essence. The solvent in the embodiment of the invention can also further comprise essence to adjust the odor of the compound essential oil.
The sterilization and mite removal compound essential oil provided by the embodiment of the invention further comprises 0.01-0.02% of bitter orange leaf essential oil, and preferably 0.01%. The bitter orange leaves are good essential oil with balanced flora, wherein linalool (linalool), limonene and terpineol have good inhibition effects on common bacteria and mold. In the embodiment of the invention, the bitter orange leaves are added to have a synergistic effect with the eucalyptus, so that the antibacterial effect is further improved.
The sterilization and mite removal compound essential oil provided by the embodiment of the invention further comprises 0.01-0.02% of origanum majorana essential oil, and preferably 0.01%. The origanum majorana essential oil is mild, wherein carvacrol and thymol have good inhibition effects on bacteria, can be used in a synergistic effect with eucalyptus, and particularly can effectively improve the inhibition effect on candida albicans after being used in combination with bitter orange leaf essential oil, and the inhibition rate on the candida albicans can reach more than 95%.
The sterilization and mite removal compound essential oil provided by the embodiment of the invention can be prepared into spray for use, about 0.2ml can be obtained after 2-3 times of pressing, and the use amount can also be adjusted according to the household environment.
The present invention will be described in detail with reference to examples.
Example 1
Essential oil: 0.03% of bergamot essential oil, 0.047% of lemon essential oil, 0.02% of rosemary essential oil, 0.01% of peppermint essential oil and 0.01% of eucalyptus essential oil.
Solvent: 3% of PPG-26-butanol polyether-26, 5% of propylene glycol, 1% of PEG-40 hydrogenated castor oil, 3% of 1, 2-hexanediol, 4% of 1, 3-propylene glycol, 0.02% of caprylyl hydroximic acid, and the balance of water.
Adding the prepared essential oil and various raw materials of the solvent into a stirring reactor one by one, and stirring for half an hour at the rotating speed of 40-60rpm to obtain the compound essential oil.
The complex essential oil of example 1 was subjected to mite-killing and bactericidal tests.
1. Mite killing and mite expelling test
The mite species were tested: dust mites, adult female and male mites and nymphs;
the test method comprises the following steps: marking a test method according to NY/T1151.2006;
the results of the mite killing test are shown in table 1, and the results of the mite repelling test are shown in table 2.
TABLE 1
| Sample (I) | Test mite number (only) | Number of dead mites (only) | Mite eradication Rate (%) | Corrected mite-killing rate (%) |
| Example 1 | 591 | 591 | 100 | 100 |
| Example 2 | 591 | 591 | 100 | 100 |
| Example 3 | 591 | 591 | 100 | 100 |
| Example 4 | 591 | 591 | 100 | 100 |
| Comparative example 1 | 591 | 569 | 96.27 | 95.72 |
| Comparative example 2 | 591 | 497 | 84.09％ | 82.06 |
| Comparative example 3 | 591 | 591 | 100 | 100 |
| Blank control group | 591 | 67 | 11.34 | ------ |
Note: correcting acarid killing rate (test group acarid killing rate-control group acarid killing rate)/(1-control group acarid killing rate)
TABLE 2
| Sample (I) | Mite number in blank control group (only) | Mite number in experimental group (only) | Deacarid Rate (%) |
| Example 1 | 366 | 6 | 98.36 |
| Example 2 | 366 | 6 | 98.36 |
| Example 3 | 366 | 6 | 98.36 |
| Example 4 | 366 | 6 | 98.36 |
| Comparative example 1 | 366 | 13 | 96.44 |
| Comparative example 2 | 366 | 37 | 89.9％ |
| Comparative example 3 | 366 | 6 | 98.36 |
Note: the number of test insects in the central culture dish is 1000.
Pc＝(1-Nt/N0) 100, wherein PcTo combat mite rate, NtNumber of test insects, N0The number of insects was tested as a control.
2. Sterilization test
Strain: 1) escherichia coli strain ATCC 25922
2) Staphylococcus aureus strain ATCC 6538
3) Candida albicans strain ATCC 10231
The test method comprises the following steps: the test method is labeled with reference to QB/T2738-2012.
The test results are shown in Table 3.
TABLE 3
Example 2
The same formula as the compound essential oil in example 1, except that the essential oil also contains 0.02% of bitter orange leaf essential oil. The method comprises the following specific steps:
essential oil: 0.03% of bergamot essential oil, 0.047% of lemon essential oil, 0.02% of rosemary essential oil, 0.01% of peppermint essential oil, 0.01% of eucalyptus essential oil and 0.02% of bitter orange leaf essential oil.
Solvent: 3% of PPG-26-butanol polyether-26, 5% of propylene glycol, 1% of PEG-40 hydrogenated castor oil, 3% of 1, 2-hexanediol, 4% of 1, 3-propylene glycol, 0.02% of caprylyl hydroximic acid, and the balance of water.
The composite essential oil of example 2 was subjected to mite-killing, mite-repelling and sterilization tests, and the results of mite-killing are shown in table 1, mite-repelling in table 2 and sterilization in table 4.
TABLE 4
Example 3
The same formula as the compound essential oil in example 1, except that the essential oil also contains 0.01% of bitter orange leaf essential oil and 0.01% of marjoram essential oil. The method comprises the following specific steps:
essential oil: 0.03 percent of bergamot essential oil, 0.047 percent of lemon essential oil, 0.02 percent of rosemary essential oil, 0.01 percent of peppermint essential oil, 0.01 percent of eucalyptus essential oil, 0.01 percent of bitter orange leaf essential oil and 0.01 percent of marjoram essential oil.
Solvent: 3% of PPG-26-butanol polyether-26, 5% of propylene glycol, 1% of PEG-40 hydrogenated castor oil, 3% of 1, 2-hexanediol, 4% of 1, 3-propylene glycol, 0.02% of caprylyl hydroximic acid, and the balance of water.
The composite essential oil of example 3 was subjected to mite-killing, mite-repelling and sterilization tests, and the results of mite-killing are shown in table 1, mite-repelling in table 2 and sterilization in table 5.
TABLE 5
Example 4
The same complex essential oil formulation as in example 1, except that the essential oil also contained 0.02% of essential oil of marjoram. The method comprises the following specific steps:
essential oil: 0.03% of bergamot essential oil, 0.047% of lemon essential oil, 0.02% of rosemary essential oil, 0.01% of peppermint essential oil, 0.01% of eucalyptus essential oil and 0.02% of marjoram essential oil.
Solvent: 3% of PPG-26-butanol polyether-26, 5% of propylene glycol, 1% of PEG-40 hydrogenated castor oil, 3% of 1, 2-hexanediol, 4% of 1, 3-propylene glycol, 0.02% of caprylyl hydroximic acid, and the balance of water.
The compound essential oil of example 4 was subjected to mite-killing, mite-repelling and sterilization tests, and the results of mite-killing are shown in table 1, mite-repelling in table 2 and sterilization in table 6.
TABLE 6
Comparative example 1
The solvent used in example 1 was the same except that the essential oil was different, as follows:
essential oil: 0.04% of bergamot essential oil, 0.06% of lemon essential oil and 0.02% of peppermint essential oil.
Solvent: 3% of PPG-26-butanol polyether-26, 5% of propylene glycol, 1% of PEG-40 hydrogenated castor oil, 3% of 1, 2-hexanediol, 4% of 1, 3-propylene glycol, 0.02% of caprylyl hydroximic acid, and the balance of water.
The compound essential oil of comparative example 1 was subjected to mite killing, mite expelling and sterilization tests, and the results of mite killing are shown in table 1, the results of mite expelling are shown in table 2 and the results of sterilization are shown in table 7.
TABLE 7
In comparative example 1, rosemary essential oil and eucalyptus essential oil are not added, the mite killing rate and the mite expelling rate of the compound essential oil in example 1 are not as good as those of the compound essential oil in example 1, and the bacteriostasis rate of candida albicans is only 86.97%, so that the requirement of sterilization cannot be met.
Comparative example 2
The solvent used in example 1 was the same except that the essential oil was different, as follows:
essential oil: 0.06% of lemon essential oil, 0.03% of lavender essential oil, 0.02% of sage essential oil and 0.02% of roman chamomile essential oil.
Solvent: 3% of PPG-26-butanol polyether-26, 5% of propylene glycol, 1% of PEG-40 hydrogenated castor oil, 3% of 1, 2-hexanediol, 4% of 1, 3-propylene glycol, 0.02% of caprylyl hydroximic acid, and the balance of water.
The compound essential oil of comparative example 2 was subjected to mite killing, mite expelling and sterilization tests, and the results of mite killing are shown in table 1, the results of mite expelling are shown in table 2 and the results of sterilization are shown in table 8.
TABLE 8
Although the compound essential oil in the comparative example 2 obviously improves the inhibition rate of candida albicans, the inhibition rate of staphylococcus aureus is very low, namely 52.38%, and the compound essential oil does not have a broad spectrum.
Comparative example 3
Comparative example 3 the same complex essential oil formulation as in example 1, except that the essential oil has a different content of eucalyptus oil. The method comprises the following specific steps:
essential oil: 0.03% of bergamot essential oil, 0.047% of lemon essential oil, 0.02% of rosemary essential oil, 0.01% of peppermint essential oil and 0.03% of eucalyptus essential oil.
Solvent: 3% of PPG-26-butanol polyether-26, 5% of propylene glycol, 1% of PEG-40 hydrogenated castor oil, 3% of 1, 2-hexanediol, 4% of 1, 3-propylene glycol, 0.02% of caprylyl hydroximic acid, and the balance of water.
The compound essential oil of example 4 was subjected to mite-killing, mite-repelling and sterilization tests, and the results of mite-killing are shown in table 1, mite-repelling in table 2 and sterilization in table 9.
TABLE 9
In comparative example 3, the addition amount of the eucalyptus essential oil is increased, and is 3 times of that in example 1, but the bacteriostatic rate of staphylococcus aureus and candida albicans is not remarkably improved.
In the present disclosure, the terms "one embodiment," "some embodiments," "an example," "a specific example," or "some examples" and the like mean that a specific feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the present disclosure. In this specification, the schematic representations of the terms used above are not necessarily intended to refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples. Furthermore, various embodiments or examples and features of different embodiments or examples described in this specification can be combined and combined by one skilled in the art without contradiction.
Although embodiments of the present invention have been shown and described above, it is understood that the above embodiments are exemplary and should not be construed as limiting the present invention, and that variations, modifications, substitutions and alterations can be made to the above embodiments by those of ordinary skill in the art within the scope of the present invention.
Claims (8)
1. The sterilization and mite removal compound essential oil is characterized by comprising a solvent and essential oil, wherein the essential oil comprises:
2. the bactericidal acaricidal composite essential oil according to claim 1, wherein the solvent comprises:
3. the compound essential oil for killing bacteria and mites as claimed in claim 1, where in the solvent further comprises 0.02-0.03% of an essence.
4. The compound essential oil for killing bacteria and mites as claimed in claim 1, which further comprises 0.01-0.02% of bitter orange leaf essential oil.
5. The bactericidal and acaricidal composite essential oil according to claim 1 or 4, which further comprises 0.01-0.02% of essential oil of origanum majorana.
6. The bactericidal and acaricidal composite essential oil according to claim 1, which comprises:
7. the sterilization and mite killing compound essential oil of claim 1 or 6, wherein the essential oil further comprises 0.01% of bitter orange leaf essential oil.
8. The bactericidal and acaricidal composite essential oil of claim 7 further comprising 0.01% of essential oil of origanum majorana.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113615717A (en) * | 2021-08-23 | 2021-11-09 | 皖南医学院 | Acaricide containing plant essential oil, and its application method and application |
| CN115039796A (en) * | 2022-05-16 | 2022-09-13 | 皖南医学院 | Acaricidal bacteriostatic agent containing plant essential oil and preparation method and application thereof |
| EP4353084A1 (en) * | 2022-10-10 | 2024-04-17 | Kimitec Biogroup S.L | Biopesticide composition with synergistic effect and method for combating and controlling pests |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1249167A1 (en) * | 2001-04-11 | 2002-10-16 | Takasago International Corporation | Miticidal essential oil mixtures and miticidal spray |
| WO2013001116A1 (en) * | 2011-06-30 | 2013-01-03 | Mieles Llovel, S.L. | Composition and method for inhibiting varroa reproduction in beehives |
| CN104923002A (en) * | 2015-06-15 | 2015-09-23 | 临沂大学 | Preparation method and application of air purification agent special for haze prevention window screen |
| CN109620757A (en) * | 2018-12-28 | 2019-04-16 | 厦门昶瀚商贸有限公司 | A kind of antiallergic perfume (or spice) atmosphere is spraying and its preparation method and application |
| CN110338197A (en) * | 2019-07-31 | 2019-10-18 | 西藏阿木达草本科技有限公司 | A kind of plant type disinfecting mite-removing element and preparation method |
| CN111195330A (en) * | 2018-11-19 | 2020-05-26 | 上海茗想健康科技有限公司 | Compound essential oil for refreshing and restoring consciousness as well as preparation method and application thereof |
| CN111388358A (en) * | 2020-05-13 | 2020-07-10 | 黄敏 | Plant essential oil composition with mite-killing and acne-removing effects, and preparation and application thereof |
| CN111567575A (en) * | 2020-05-16 | 2020-08-25 | 无锡市伙伴日化科技有限公司 | Environment-friendly sterilizing and mite-killing agent and preparation method thereof |
| CN111685134A (en) * | 2020-07-16 | 2020-09-22 | 北京美科兴业生物科技有限公司 | Mite-removing and bacterium-inhibiting composition containing plant essential oil and application thereof |
-
2020
- 2020-10-23 CN CN202011146223.0A patent/CN112335691B/en active Active
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1249167A1 (en) * | 2001-04-11 | 2002-10-16 | Takasago International Corporation | Miticidal essential oil mixtures and miticidal spray |
| WO2013001116A1 (en) * | 2011-06-30 | 2013-01-03 | Mieles Llovel, S.L. | Composition and method for inhibiting varroa reproduction in beehives |
| CN104923002A (en) * | 2015-06-15 | 2015-09-23 | 临沂大学 | Preparation method and application of air purification agent special for haze prevention window screen |
| CN111195330A (en) * | 2018-11-19 | 2020-05-26 | 上海茗想健康科技有限公司 | Compound essential oil for refreshing and restoring consciousness as well as preparation method and application thereof |
| CN109620757A (en) * | 2018-12-28 | 2019-04-16 | 厦门昶瀚商贸有限公司 | A kind of antiallergic perfume (or spice) atmosphere is spraying and its preparation method and application |
| CN110338197A (en) * | 2019-07-31 | 2019-10-18 | 西藏阿木达草本科技有限公司 | A kind of plant type disinfecting mite-removing element and preparation method |
| CN111388358A (en) * | 2020-05-13 | 2020-07-10 | 黄敏 | Plant essential oil composition with mite-killing and acne-removing effects, and preparation and application thereof |
| CN111567575A (en) * | 2020-05-16 | 2020-08-25 | 无锡市伙伴日化科技有限公司 | Environment-friendly sterilizing and mite-killing agent and preparation method thereof |
| CN111685134A (en) * | 2020-07-16 | 2020-09-22 | 北京美科兴业生物科技有限公司 | Mite-removing and bacterium-inhibiting composition containing plant essential oil and application thereof |
Non-Patent Citations (3)
| Title |
|---|
| 三采文化编著: "《精油芳疗养生事典》", 30 September 2005, 汕头大学出版社 * |
| 姚欢远: "《舌尖上的丁香 中国的外来植物 香料》", 30 April 2017, 上海咬文嚼字文化传播有限公司 * |
| 张卫明主编: "《一带一路经济植物》", 31 December 2017, 东南大学出版社 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113615717A (en) * | 2021-08-23 | 2021-11-09 | 皖南医学院 | Acaricide containing plant essential oil, and its application method and application |
| CN115039796A (en) * | 2022-05-16 | 2022-09-13 | 皖南医学院 | Acaricidal bacteriostatic agent containing plant essential oil and preparation method and application thereof |
| EP4353084A1 (en) * | 2022-10-10 | 2024-04-17 | Kimitec Biogroup S.L | Biopesticide composition with synergistic effect and method for combating and controlling pests |
| WO2024078917A1 (en) * | 2022-10-10 | 2024-04-18 | Kimitec Biogroup S.L | Biopesticide composition with synergistic effect and method for combating and controlling pests |
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