CN111567575A - Environment-friendly sterilizing and mite-killing agent and preparation method thereof - Google Patents
Environment-friendly sterilizing and mite-killing agent and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
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- A—HUMAN NECESSITIES
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/28—Myrtaceae [Myrtle family], e.g. teatree or clove
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- A—HUMAN NECESSITIES
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
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Abstract
The invention discloses an environment-friendly sterilization and mite removal agent, and particularly relates to the technical field of daily chemical sterilization and killing, and the agent comprises the following raw materials: eucalyptus leaf essential oil, folium artemisiae argyi essential oil, citronella essential oil, lemon essential oil, mint essential oil, orange essential oil, rosemary extract, fructus cnidii extract, radix sophorae flavescentis extract, sweet orange flower extract, lavender extract, small molecular alcohol, deionized water, sorbitan monolaurate polyoxyethylene (20) ether and water-soluble polymer slow-release agent starch. The invention can guarantee the product to apply medicine fast, sterilize and remove the mite and improve the durability of the product at the same time, the main active substance in the product is natural plant extract, the product has good environmental protection performance, is fresh, natural, has no toxic or side effect, is mild and non-irritant to human skin, has no harm to infants and good experience, and the drug effect is more durable, the combination effect of the raw materials is better, and the shelf life is longer by adopting magnetic stirring and ultrasonic oscillator ultrasonic treatment in the preparation process and carrying out repeated circulation staggered operation.
Description
Technical Field
The invention relates to the technical field of daily chemical industry killing, in particular to an environment-friendly sterilizing and mite-killing agent and a preparation method thereof.
Background
The mite removal is to remove mites. Mites are widely distributed in dark corners of a room, carpets, mattresses, pillows, sofas, air conditioners, summer sleeping mats and the like, wherein the mattresses are most suitable for the growth and propagation of the mites. Bedding in the home should be cleaned frequently. The acarid belongs to a tiny animal, the size of the acarid is about 0.5 mm generally, the body and the feet of the acarid have a plurality of hairs, the front end of the acarid is provided with a mouth organ, the acarid is addicted to scurf, the life span is 3 months generally, but the reproduction capability is extremely strong. The mites are in a large variety, different varieties and different in harm to human bodies, can be in a large family, are in 50 thousands of varieties, are generally divided into several categories including dust mites, powder mites, sweet mites, leather mites, chiggers and the like, and are most widely distributed and influenced. At present, some sterilizing and mite-killing agents exist, and indoor sterilizing and mite-killing treatment can be carried out.
The existing sterilization and mite removal agent has poor environmental protection performance, causes more or less harm to body health, and has large use limitation and poor experience feeling especially for users with children at home.
Disclosure of Invention
In order to overcome the defects of the prior art, the embodiment of the invention provides an environment-friendly sterilization and mite killing agent and a preparation method thereof, and the environment-friendly sterilization and mite killing agent provided by the invention aims to solve the following problems: how to improve the environmental protection performance of the sterilization and mite killing agent, reduce the harm to the body, avoid causing the harm to the infant and improve the user experience.
In order to achieve the purpose, the invention provides the following technical scheme: an environment-friendly sterilizing and mite-killing agent comprises the following raw materials in parts by weight: 10-20 parts of eucalyptus leaf essential oil, 10-20 parts of argy wormwood leaf essential oil, 10-20 parts of citronella essential oil, 10-20 parts of lemon essential oil, 10-20 parts of mint essential oil, 10-20 parts of orange essential oil, 20-30 parts of rosemary extract, 10-20 parts of fructus cnidii extract, 10-20 parts of radix sophorae flavescentis extract, 10-20 parts of sweet orange flower extract, 10-20 parts of lavender extract, 30-50 parts of small molecular alcohol, 100 parts of deionized water, 200 parts of 100 parts of sorbitan monolaurate polyoxyethylene (20) ether and 5-10 parts of water-soluble polymer slow-release agent starch;
in a preferred embodiment, the feed comprises the following raw materials in parts by weight: 10 parts of eucalyptus leaf essential oil, 10 parts of argy wormwood leaf essential oil, 10 parts of citronella essential oil, 10 parts of lemon essential oil, 10 parts of mint essential oil, 10 parts of orange essential oil, 20 parts of rosemary extract, 10 parts of common cnidium fruit extract, 10 parts of sophora flavescens extract, 10 parts of sweet orange flower extract, 10 parts of lavender extract, 30 parts of small molecular alcohol, 100 parts of deionized water, 10 parts of sorbitan monolaurate polyoxyethylene (20) ether and 5 parts of water-soluble polymer slow-release agent starch.
In a preferred embodiment, the feed comprises the following raw materials in parts by weight: 20 parts of eucalyptus leaf essential oil, 20 parts of folium artemisiae argyi essential oil, 20 parts of citronella essential oil, 20 parts of lemon essential oil, 20 parts of mint essential oil, 20 parts of orange essential oil, 30 parts of rosemary extract, 20 parts of fructus cnidii extract, 20 parts of radix sophorae flavescentis extract, 20 parts of sweet orange flower extract, 20 parts of lavender extract, 50 parts of small molecular alcohol, 200 parts of deionized water, 20 parts of sorbitan monolaurate polyoxyethylene (20) ether and 10 parts of water-soluble polymer slow-release agent starch.
In a preferred embodiment, the feed comprises the following raw materials in parts by weight: 10 parts of eucalyptus leaf essential oil, 10 parts of argy wormwood leaf essential oil, 10 parts of citronella essential oil, 10 parts of lemon essential oil, 10 parts of mint essential oil, 10 parts of orange essential oil, 30 parts of rosemary extract, 10 parts of common cnidium fruit extract, 10 parts of sophora flavescens extract, 10 parts of sweet orange flower extract, 10 parts of lavender extract, 30 parts of small molecular alcohol, 100 parts of deionized water, 10 parts of sorbitan monolaurate polyoxyethylene (20) ether and 5 parts of water-soluble polymer slow-release agent starch.
In a preferred embodiment, the rosemary, the common cnidium fruit, the lightyellow sophora root, the sweet orange flower and the lavender are all fresh products without plant diseases and insect pests.
In a preferred embodiment, the small molecule alcohol is compounded by one or more of ethanol, propylene glycol or isopropanol.
In a preferred embodiment, the small molecular alcohol is prepared by compounding ethanol and propylene glycol according to the weight ratio of 1: 1.
The invention also provides a preparation method of the environment-friendly sterilization and mite killing agent, which comprises the following specific preparation steps:
the method comprises the following steps: respectively preparing rosemary, common cnidium fruit, lightyellow sophora root, sweet orange flower and lavender alkaloid alcohol extract by adopting a 95% ethanol reflux method;
step two: weighing eucalyptus leaf essential oil, folium artemisiae argyi essential oil, citronella essential oil, lemon essential oil, mint essential oil, orange essential oil, small molecular alcohol, deionized water, sorbitan monolaurate polyoxyethylene (20) ether, water-soluble polymer slow-release agent starch and rosemary, fructus cnidii, radix sophorae flavescentis, sweet orange flower and lavender alkaloid alcohol extract in parts by weight;
step three: adding the micromolecule alcohol and the sorbitan monolaurate polyoxyethylene (20) ether into the first container, and then performing magnetic stirring and ultrasonic treatment for 20-30min by using an ultrasonic oscillator to prepare an emulsification solubilization system;
step four: adding the eucalyptus essential oil, the argy wormwood leaf essential oil, the citronella essential oil, the lemon essential oil, the mint essential oil and the orange essential oil in the second container, and then performing magnetic stirring and ultrasonic treatment for 20-30min by using an ultrasonic oscillator to obtain a compound essential oil system;
step five: adding the compound essential oil system in the fourth step into the emulsifying and dissolving system in the third step, and then performing magnetic stirring and ultrasonic treatment for 30-40min by using an ultrasonic oscillator to obtain a compound oil phase;
step six: mixing the water-soluble polymer slow-release agent starch in the step two with deionized water, and then performing magnetic stirring and ultrasonic treatment for 20-30min by using an ultrasonic oscillator to prepare a dissolution assisting system;
step seven: slowly adding the alkaloid alcohol extract of rosemary, common cnidium fruit, lightyellow sophora root, sweet orange flower and lavender in the second step into the cosolvent system in the sixth step, carrying out magnetic stirring and ultrasonic treatment by an ultrasonic oscillator in the adding process, and continuing the magnetic stirring and ultrasonic treatment by the ultrasonic oscillator for 30-50min after all the extract is added to prepare a compound liquid phase;
step eight: and (4) adding the compound liquid phase in the seventh step into the compound oil phase in the fifth step, and then performing magnetic stirring and ultrasonic treatment for 30-40min by using an ultrasonic oscillator to prepare the environment-friendly sterilizing and mite-killing agent.
In a preferred embodiment, the magnetic stirring and ultrasonic oscillator ultrasonic treatment in the third step, the fourth step, the fifth step, the sixth step, the seventh step and the eighth step are all performed by a repeated cycle staggered operation, and each cycle period is 5min, wherein the magnetic stirring is performed for 3min and the ultrasonic oscillator is performed for 2 min.
The invention has the technical effects and advantages that:
1. the environment-friendly sterilization and mite removal agent prepared by the raw material formula can ensure that the product can be quickly applied to sterilize and remove mites, meanwhile, the durability of the product is improved, the drug effect action time is longer, main active substances in the product are natural plant extracts, the environment-friendly performance is good, the product is fresh, natural and free of toxic and side effects, the fabric structure cannot be damaged, the skin of a human body is mild and non-irritant, the product is harmless to infants, and the experience feeling is good;
2. according to the invention, magnetic stirring and ultrasonic treatment by the ultrasonic oscillator are adopted in the preparation process, and repeated circulating staggered operation is carried out, so that the sterilizing and mite removing agent has better and more lasting drug effect, more uniform raw material mixing, better raw material combination effect and longer quality guarantee period.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1:
the invention provides an environment-friendly sterilizing and mite-killing agent which comprises the following raw materials in parts by weight: 10 parts of eucalyptus leaf essential oil, 10 parts of argy wormwood leaf essential oil, 10 parts of citronella essential oil, 10 parts of lemon essential oil, 10 parts of mint essential oil, 10 parts of orange essential oil, 20 parts of rosemary extract, 10 parts of common cnidium fruit extract, 10 parts of sophora flavescens extract, 10 parts of sweet orange flower extract, 10 parts of lavender extract, 30 parts of small molecular alcohol, 100 parts of deionized water, 10 parts of sorbitan monolaurate polyoxyethylene (20) ether and 5 parts of water-soluble polymer slow-release agent starch;
the rosemary, the common cnidium fruit, the lightyellow sophora root, the sweet orange flower and the lavender are all fresh products without diseases and insect pests.
The micromolecule alcohol is compounded by one or more of ethanol, propylene glycol or isopropanol, and is compounded by the weight part ratio of the ethanol to the propylene glycol of 1: 1.
The invention also provides a preparation method of the environment-friendly sterilization and mite killing agent, which comprises the following specific preparation steps:
the method comprises the following steps: respectively preparing rosemary, common cnidium fruit, lightyellow sophora root, sweet orange flower and lavender alkaloid alcohol extract by adopting a 95% ethanol reflux method;
step two: weighing eucalyptus leaf essential oil, folium artemisiae argyi essential oil, citronella essential oil, lemon essential oil, mint essential oil, orange essential oil, small molecular alcohol, deionized water, sorbitan monolaurate polyoxyethylene (20) ether, water-soluble polymer slow-release agent starch and rosemary, fructus cnidii, radix sophorae flavescentis, sweet orange flower and lavender alkaloid alcohol extract in parts by weight;
step three: adding the micromolecule alcohol and the sorbitan monolaurate polyoxyethylene (20) ether into the first container, and then performing magnetic stirring and ultrasonic treatment for 20-30min by using an ultrasonic oscillator to prepare an emulsification solubilization system;
step four: adding the eucalyptus essential oil, the argy wormwood leaf essential oil, the citronella essential oil, the lemon essential oil, the mint essential oil and the orange essential oil in the second container, and then performing magnetic stirring and ultrasonic treatment for 20-30min by using an ultrasonic oscillator to obtain a compound essential oil system;
step five: adding the compound essential oil system in the fourth step into the emulsifying and dissolving system in the third step, and then performing magnetic stirring and ultrasonic treatment for 30-40min by using an ultrasonic oscillator to obtain a compound oil phase;
step six: mixing the water-soluble polymer slow-release agent starch in the step two with deionized water, and then performing magnetic stirring and ultrasonic treatment for 20-30min by using an ultrasonic oscillator to prepare a dissolution assisting system;
step seven: slowly adding the alkaloid alcohol extract of rosemary, common cnidium fruit, lightyellow sophora root, sweet orange flower and lavender in the second step into the cosolvent system in the sixth step, carrying out magnetic stirring and ultrasonic treatment by an ultrasonic oscillator in the adding process, and continuing the magnetic stirring and ultrasonic treatment by the ultrasonic oscillator for 30-50min after all the extract is added to prepare a compound liquid phase;
step eight: and (4) adding the compound liquid phase in the seventh step into the compound oil phase in the fifth step, and then performing magnetic stirring and ultrasonic treatment for 30-40min by using an ultrasonic oscillator to prepare the environment-friendly sterilizing and mite-killing agent.
And the magnetic stirring and ultrasonic oscillator ultrasonic treatment in the third step, the fourth step, the fifth step, the sixth step, the seventh step and the eighth step all adopt repeated cycle staggered operation, each cycle period is 5min, wherein the magnetic stirring is performed for 3min, and the ultrasonic oscillator ultrasonic treatment is performed for 2 min.
Example 2:
different from the embodiment 1, the material comprises the following raw materials in parts by weight: 20 parts of eucalyptus leaf essential oil, 20 parts of folium artemisiae argyi essential oil, 20 parts of citronella essential oil, 20 parts of lemon essential oil, 20 parts of mint essential oil, 20 parts of orange essential oil, 30 parts of rosemary extract, 20 parts of fructus cnidii extract, 20 parts of radix sophorae flavescentis extract, 20 parts of sweet orange flower extract, 20 parts of lavender extract, 50 parts of small molecular alcohol, 200 parts of deionized water, 20 parts of sorbitan monolaurate polyoxyethylene (20) ether and 10 parts of water-soluble polymer slow-release agent starch.
Example 3:
different from the examples 1-2, the material comprises the following raw materials in parts by weight: 10 parts of eucalyptus leaf essential oil, 10 parts of argy wormwood leaf essential oil, 10 parts of citronella essential oil, 10 parts of lemon essential oil, 10 parts of mint essential oil, 10 parts of orange essential oil, 30 parts of rosemary extract, 10 parts of common cnidium fruit extract, 10 parts of sophora flavescens extract, 10 parts of sweet orange flower extract, 10 parts of lavender extract, 30 parts of small molecular alcohol, 100 parts of deionized water, 10 parts of sorbitan monolaurate polyoxyethylene (20) ether and 5 parts of water-soluble polymer slow-release agent starch.
The environment-friendly bactericidal and acaricidal agent prepared in the above examples 1 to 3 and a control group acaricidal agent are respectively provided for the trial of families voluntarily participating in product experience, the control group acaricidal agent is a common product, every 20 families are a group, the environment-friendly bactericidal and acaricidal agent prepared in the three examples and the control group acaricidal agent are respectively tried in four groups, a plurality of experiments are carried out and the detection is carried out, the following data are obtained, and the test results are shown in the first table and the second table:
table one:
in table one, the survival rate calculation method is: the survival amount of the bacterial mites after spraying the sterilization mite-killing agent/the survival amount of the bacterial mites between the spraying of the sterilization mite-killing agent and the spraying of the non-sterilization mite-killing agent;
table two:
| control group one | Example one | Example two | EXAMPLE III | |
| Smell(s) | Rich in flavor | Fresh and elegant | Fresh and elegant | Fresh and elegant |
| Allergy (S) | Slight allergy | Is free of | Is free of | Is free of |
| Discomfort of inhalation | Slight discomfort | Is free of | Is free of | Is free of |
| Experience feeling | In general | Superior food | Superior food | Superior food |
As can be seen from the table I and the table II, the raw materials of the environment-friendly sterilizing and mite-killing agent are as follows: the formula comprises, by weight, 10 parts of eucalyptus leaf essential oil, 10 parts of argy wormwood leaf essential oil, 10 parts of citronella essential oil, 10 parts of lemon essential oil, 10 parts of mint essential oil, 10 parts of orange essential oil, 30 parts of rosemary extract, 10 parts of common cnidium fruit extract, 10 parts of sophora flavescens extract, 10 parts of sweet orange flower extract, 10 parts of lavender extract, 30 parts of small molecular alcohol, 100 parts of deionized water, 10 parts of sorbitan monolaurate polyoxyethylene (20) ether and 5 parts of water-soluble polymer slow-release agent starch, and has the advantages of good user experience, mildness, no stimulation, no adverse effect on body health and no harm to infants, so that the raw materials in the embodiment 3 are combined into the preferable scheme of the invention, the eucalyptus leaf essential oil, the argy wormwood leaf essential oil and the citronella essential oil in the formula have high-efficiency sterilization and mite removal performance, the mixed compounding of the three can further improve the sterilization and mite removal effects, the odor is fresh and natural, and the lemon essential oil and the mint essential oil can enhance the insect expelling capability of, the fragrant citrus essential oil is used for blending fragrance, so that the smell of a product is fresher, natural and non-irritant, rosemary has the capabilities of sterilizing, removing mites and expelling insects, the sterilization and mite removal effects of the product can be effectively guaranteed, common cnidium fruit and radix sophorae flavescentis can be effectively sterilized and relieved, sweet orange flowers and lavender can effectively enhance the mite removal effect, most of the plants have the effects of soothing the nerves and restoring consciousness, the sleep quality can be effectively improved, the water-soluble polymer slow-release agent starch is combined with effective substances in raw materials, the stability of the product can be guaranteed, the durability of the product can be improved while the product is rapidly applied, the drug effect action time is longer, the proportion of the components of the water-soluble polymer slow-release agent starch in the total amount of the raw materials is smaller, the water-soluble polymer slow-release agent starch is only combined with the effective substances in one part of the raw materials, and thus the finished product contains, the main active substances in the product are natural plant extracts, so that the environment-friendly effect is good, the effects of killing, removing mites and repelling mosquitoes of the rosemary extract can be preferentially exerted, other active substances are combined with the rosemary extract, the effects and the persistence of killing, removing mites and repelling mosquitoes of the rosemary can be effectively enhanced, the main active substances in the product are natural plant extracts, the environment-friendly effect is good, the fabric structure can not be damaged, the skin of a human body is mild and non-irritant, the fabric is harmless to infants, and the experience feeling is good.
Example 4
In the preferable technical scheme, the invention provides an environment-friendly sterilizing and mite-killing agent, wherein the sock body comprises the following raw materials in parts by weight: 10 parts of eucalyptus leaf essential oil, 10 parts of argy wormwood leaf essential oil, 10 parts of citronella essential oil, 10 parts of lemon essential oil, 10 parts of mint essential oil, 10 parts of orange essential oil, 30 parts of rosemary extract, 10 parts of common cnidium fruit extract, 10 parts of sophora flavescens extract, 10 parts of sweet orange flower extract, 10 parts of lavender extract, 30 parts of small molecular alcohol, 100 parts of deionized water, 10 parts of sorbitan monolaurate polyoxyethylene (20) ether and 5 parts of water-soluble polymer slow-release agent starch.
The rosemary, the common cnidium fruit, the lightyellow sophora root, the sweet orange flower and the lavender are all fresh products without diseases and insect pests.
The micromolecule alcohol is compounded by one or more of ethanol, propylene glycol or isopropanol, and is compounded by the weight part ratio of the ethanol to the propylene glycol of 1: 1.
The invention also provides a preparation method of the environment-friendly sterilization and mite killing agent, which comprises the following specific preparation steps:
the method comprises the following steps: respectively preparing rosemary, common cnidium fruit, lightyellow sophora root, sweet orange flower and lavender alkaloid alcohol extract by adopting a 95% ethanol reflux method;
step two: weighing eucalyptus leaf essential oil, folium artemisiae argyi essential oil, citronella essential oil, lemon essential oil, mint essential oil, orange essential oil, small molecular alcohol, deionized water, sorbitan monolaurate polyoxyethylene (20) ether, water-soluble polymer slow-release agent starch and rosemary, fructus cnidii, radix sophorae flavescentis, sweet orange flower and lavender alkaloid alcohol extract in parts by weight;
step three: adding the micromolecule alcohol and the sorbitan monolaurate polyoxyethylene (20) ether into the first container, and then performing magnetic stirring and ultrasonic treatment for 30min by using an ultrasonic oscillator to prepare an emulsification solubilization system;
step four: adding the eucalyptus essential oil, the argy wormwood leaf essential oil, the citronella essential oil, the lemon essential oil, the mint essential oil and the orange essential oil in the second container, and then carrying out magnetic stirring and ultrasonic treatment for 30min by an ultrasonic oscillator to obtain a compound essential oil system;
step five: adding the compound essential oil system in the fourth step into the emulsifying and dissolving system in the third step, and then performing magnetic stirring and ultrasonic treatment for 40min by using an ultrasonic oscillator to prepare a compound oil phase;
step six: mixing the water-soluble polymer slow-release agent starch in the step two with deionized water, and then performing magnetic stirring and ultrasonic treatment for 30min by using an ultrasonic oscillator to prepare a dissolution assisting system;
step seven: slowly adding the alkaloid alcohol extract of rosemary, common cnidium fruit, lightyellow sophora root, sweet orange flower and lavender in the second step into the cosolvent system in the sixth step, carrying out magnetic stirring and ultrasonic treatment by an ultrasonic oscillator in the adding process, and continuing the magnetic stirring and ultrasonic treatment by the ultrasonic oscillator for 50min after all the extract is added to prepare a compound liquid phase;
step eight: and (4) adding the compound liquid phase in the seventh step into the compound oil phase in the fifth step, and then performing magnetic stirring and ultrasonic treatment for 40min by using an ultrasonic oscillator to prepare the environment-friendly sterilizing and mite-killing agent.
And the magnetic stirring and ultrasonic oscillator ultrasonic treatment in the third step, the fourth step, the fifth step, the sixth step, the seventh step and the eighth step all adopt repeated cycle staggered operation, each cycle period is 5min, wherein the magnetic stirring is performed for 3min, and the ultrasonic oscillator ultrasonic treatment is performed for 2 min.
Example 5
Different from the embodiment 4, the third step: adding the micromolecule alcohol and the sorbitan monolaurate polyoxyethylene (20) ether into the first container, and then carrying out magnetic stirring and ultrasonic treatment for 20min by an ultrasonic oscillator to prepare an emulsification solubilization system;
step four: adding the eucalyptus essential oil, the argy wormwood leaf essential oil, the citronella essential oil, the lemon essential oil, the mint essential oil and the orange essential oil in the second container, and then carrying out magnetic stirring and ultrasonic treatment for 20min by an ultrasonic oscillator to obtain a compound essential oil system;
step five: adding the compound essential oil system in the fourth step into the emulsifying and dissolving system in the third step, and then performing magnetic stirring and ultrasonic treatment for 30min by using an ultrasonic oscillator to obtain a compound oil phase;
step six: mixing the water-soluble polymer slow-release agent starch in the step two with deionized water, and then performing magnetic stirring and ultrasonic treatment for 20min by using an ultrasonic oscillator to prepare a dissolution assisting system;
step seven: slowly adding the alkaloid alcohol extract of rosemary, common cnidium fruit, lightyellow sophora root, sweet orange flower and lavender in the second step into the cosolvent system in the sixth step, carrying out magnetic stirring and ultrasonic treatment by an ultrasonic oscillator in the adding process, and continuing the magnetic stirring and ultrasonic treatment by the ultrasonic oscillator for 30min after all the extract is added to prepare a compound liquid phase;
step eight: and (4) adding the compound liquid phase in the seventh step into the compound oil phase in the fifth step, and then performing magnetic stirring and ultrasonic treatment for 30min by using an ultrasonic oscillator to prepare the environment-friendly sterilization and mite removal agent.
Example 6
Unlike examples 4-5, step three: adding the micromolecule alcohol and the sorbitan monolaurate polyoxyethylene (20) ether into the first container, and then carrying out magnetic stirring and ultrasonic treatment for 25min by an ultrasonic oscillator to prepare an emulsification solubilization system;
step four: adding the eucalyptus essential oil, the argy wormwood leaf essential oil, the citronella essential oil, the lemon essential oil, the mint essential oil and the orange essential oil in the second container, and then carrying out magnetic stirring and ultrasonic treatment for 25min by an ultrasonic oscillator to obtain a compound essential oil system;
step five: adding the compound essential oil system in the fourth step into the emulsifying and dissolving system in the third step, and then carrying out magnetic stirring and ultrasonic treatment for 25min by using an ultrasonic oscillator to obtain a compound oil phase;
step six: mixing the water-soluble polymer slow-release agent starch in the step two with deionized water, and then carrying out magnetic stirring and ultrasonic treatment for 25min by an ultrasonic oscillator to prepare a dissolution assisting system;
step seven: slowly adding the alkaloid alcohol extract of rosemary, common cnidium fruit, lightyellow sophora root, sweet orange flower and lavender in the second step into the cosolvent system in the sixth step, carrying out magnetic stirring and ultrasonic treatment by an ultrasonic oscillator in the adding process, and continuing the magnetic stirring and ultrasonic treatment by the ultrasonic oscillator for 40min after all the extract is added to prepare a compound liquid phase;
step eight: and (4) adding the compound liquid phase in the seventh step into the compound oil phase in the fifth step, and then performing magnetic stirring and ultrasonic treatment for 35min by using an ultrasonic oscillator to prepare the environment-friendly sterilizing and mite-killing agent.
The environment-friendly bactericidal and acaricidal agent prepared in the above examples 4-6 and the second control group acaricidal agent are provided for the trial of families voluntarily participating in product experience, the second control group acaricidal agent has the same formula as the examples, only the magnetic stirring is used for mixing the raw materials in the preparation method, every 20 families are one group, the environment-friendly bactericidal and acaricidal agent prepared in the three examples and the second control group acaricidal agent are tried in four groups respectively, and a plurality of experiments and detections are carried out, so that the following data are obtained, and the test results are shown in the following table:
from the above table, in the process of preparing the environment-friendly mite killing agent, when magnetic stirring and ultrasonic oscillator ultrasonic treatment are adopted in the preparation process, the drug effect of the mite killing agent is better, the drug effect is more durable, the raw materials are more uniformly mixed, meanwhile, when the raw materials are treated for 25 or 30 minutes in the third step, the fourth step and the sixth step, the raw materials are treated for 35 or 40 minutes in the fifth step and the eighth step, and the raw materials are treated for 40 or 50 minutes in the seventh step, the drug effect is better, the drug effect is more durable, the raw materials are more uniformly mixed, the data show that the preparation time in the sixth example is shorter than that in the fourth example, and the preparation efficiency is higher, therefore, the sixth example is a preferable scheme of the invention, the magnetic stirring and ultrasonic oscillator ultrasonic treatment in the third step is 30 minutes, the micromolecule alcohol and the sorbitan monolaurate polyoxyethylene (20) ether can be effectively uniformly mixed and diffused, the substances in the emulsification solubilization system are distributed more uniformly, the eucalyptus essential oil, the argy wormwood leaf essential oil, the citronella essential oil, the lemon essential oil, the mint essential oil and the orange essential oil can be effectively and uniformly mixed and diffused by magnetic stirring and ultrasonic oscillator ultrasonic treatment for 30min in the fourth step, the substances in the compound essential oil system are distributed more uniformly, the substances in the compound essential oil system and the emulsification compatibilization system can be uniformly mixed and diffused by magnetic stirring and ultrasonic oscillator ultrasonic treatment for 40min in the fifth step, the substances in the compound oil phase are distributed more uniformly, the substances in the compound oil phase are uniformly mixed and diffused by magnetic stirring and ultrasonic oscillator ultrasonic treatment for 30min in the sixth step, the water-soluble polymer slow-release agent starch and the deionized water can be uniformly mixed and diffused, the substances in the solubilization system are distributed more uniformly, and the magnetic stirring and ultrasonic oscillator ultrasonic treatment are carried out in the raw material adding process, after the addition is finished, magnetic stirring and ultrasonic treatment of an ultrasonic oscillator are carried out for 50min, rosemary, common cnidium fruit, radix sophorae flavescentis, sweet orange flowers and lavender alkaloid extract and a dissolution assisting system can be uniformly mixed and diffused, so that the distribution of substances in the compound liquid phase is more uniform, and in the step eight, the magnetic stirring and ultrasonic treatment of the ultrasonic oscillator are carried out for 40min, so that the compound liquid phase and the compound oil phase can be effectively uniformly mixed and diffused, and the substances in the environment-friendly sterilization mite removing agent and the like are not more uniform; can effectively strengthen the mixed effect between the raw materials, the raw materials mixes more evenly, and the medicine performance effect is better, and magnetic stirring and ultrasonic oscillator ultrasonic treatment all adopt the operation of recirculation alternating expression simultaneously, and every cycle period is 5min, and wherein magnetic stirring 3min, ultrasonic oscillator ultrasonic treatment 2min carry out the multiple circulation in the raw materials mixing process, and the raw materials combines the effect better, and the drug effect is more lasting, and the shelf life is longer.
And finally: the above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that are within the spirit and principle of the present invention are intended to be included in the scope of the present invention.
Claims (10)
1. An environment-friendly sterilization and mite-killing agent is characterized in that: the feed comprises the following raw materials in parts by weight: 10-20 parts of eucalyptus leaf essential oil, 10-20 parts of folium artemisiae argyi essential oil, 10-20 parts of citronella essential oil, 10-20 parts of lemon essential oil, 10-20 parts of mint essential oil, 10-20 parts of orange essential oil, 20-30 parts of rosemary extract, 10-20 parts of fructus cnidii extract, 10-20 parts of radix sophorae flavescentis extract, 10-20 parts of sweet orange flower extract, 10-20 parts of lavender extract, 30-50 parts of small molecular alcohol, 100 parts of deionized water, 200 parts of 100-one-month laurate polyoxyethylene (20) ether and 5-10 parts of water-soluble polymer slow-release agent starch.
2. The environment-friendly sterilizing and mite-killing agent as claimed in claim 1, wherein: the feed comprises the following raw materials in parts by weight: 10 parts of eucalyptus leaf essential oil, 10 parts of argy wormwood leaf essential oil, 10 parts of citronella essential oil, 10 parts of lemon essential oil, 10 parts of mint essential oil, 10 parts of orange essential oil, 20 parts of rosemary extract, 10 parts of common cnidium fruit extract, 10 parts of sophora flavescens extract, 10 parts of sweet orange flower extract, 10 parts of lavender extract, 30 parts of small molecular alcohol, 100 parts of deionized water, 10 parts of sorbitan monolaurate polyoxyethylene (20) ether and 5 parts of water-soluble polymer slow-release agent starch.
3. The environment-friendly sterilizing and mite-killing agent as claimed in claim 1, wherein: the feed comprises the following raw materials in parts by weight: 20 parts of eucalyptus leaf essential oil, 20 parts of folium artemisiae argyi essential oil, 20 parts of citronella essential oil, 20 parts of lemon essential oil, 20 parts of mint essential oil, 20 parts of orange essential oil, 30 parts of rosemary extract, 20 parts of fructus cnidii extract, 20 parts of radix sophorae flavescentis extract, 20 parts of sweet orange flower extract, 20 parts of lavender extract, 50 parts of small molecular alcohol, 200 parts of deionized water, 20 parts of sorbitan monolaurate polyoxyethylene (20) ether and 10 parts of water-soluble polymer slow-release agent starch.
4. The environment-friendly sterilizing and mite-killing agent as claimed in claim 1, wherein: the feed comprises the following raw materials in parts by weight: 10 parts of eucalyptus leaf essential oil, 10 parts of argy wormwood leaf essential oil, 10 parts of citronella essential oil, 10 parts of lemon essential oil, 10 parts of mint essential oil, 10 parts of orange essential oil, 30 parts of rosemary extract, 10 parts of common cnidium fruit extract, 10 parts of sophora flavescens extract, 10 parts of sweet orange flower extract, 10 parts of lavender extract, 30 parts of small molecular alcohol, 100 parts of deionized water, 10 parts of sorbitan monolaurate polyoxyethylene (20) ether and 5 parts of water-soluble polymer slow-release agent starch.
5. The environment-friendly sterilizing and mite-killing agent as claimed in claim 1, wherein: the rosemary, the common cnidium fruit, the lightyellow sophora root, the sweet orange flower and the lavender are all fresh products without diseases and insect pests.
6. The environment-friendly sterilizing and mite-killing agent as claimed in claim 1, wherein: the micromolecular alcohol is compounded by one or more of ethanol, propylene glycol or isopropanol.
7. The environment-friendly sterilizing and mite-killing agent as claimed in claim 6, wherein: the micromolecular alcohol is formed by compounding ethanol and propylene glycol according to the weight part ratio of 1: 1.
8. The preparation method of the environment-friendly sterilizing and mite-killing agent according to any one of claims 1 to 7, characterized in that: the preparation method comprises the following specific steps:
the method comprises the following steps: respectively preparing rosemary, common cnidium fruit, lightyellow sophora root, sweet orange flower and lavender alkaloid alcohol extract by adopting a 95% ethanol reflux method;
step two: weighing eucalyptus leaf essential oil, folium artemisiae argyi essential oil, citronella essential oil, lemon essential oil, mint essential oil, orange essential oil, small molecular alcohol, deionized water, sorbitan monolaurate polyoxyethylene (20) ether, water-soluble polymer slow-release agent starch and rosemary, fructus cnidii, radix sophorae flavescentis, sweet orange flower and lavender alkaloid alcohol extract in parts by weight;
step three: adding the micromolecule alcohol and the sorbitan monolaurate polyoxyethylene (20) ether into the first container, and then performing magnetic stirring and ultrasonic treatment for 20-30min by using an ultrasonic oscillator to prepare an emulsification solubilization system;
step four: adding the eucalyptus essential oil, the argy wormwood leaf essential oil, the citronella essential oil, the lemon essential oil, the mint essential oil and the orange essential oil in the second container, and then performing magnetic stirring and ultrasonic treatment for 20-30min by using an ultrasonic oscillator to obtain a compound essential oil system;
step five: adding the compound essential oil system in the fourth step into the emulsifying and dissolving system in the third step, and then performing magnetic stirring and ultrasonic treatment for 30-40min by using an ultrasonic oscillator to obtain a compound oil phase;
step six: mixing the water-soluble polymer slow-release agent starch in the step two with deionized water, and then performing magnetic stirring and ultrasonic treatment for 20-30min by using an ultrasonic oscillator to prepare a dissolution assisting system;
step seven: slowly adding the alkaloid alcohol extract of rosemary, common cnidium fruit, lightyellow sophora root, sweet orange flower and lavender in the second step into the cosolvent system in the sixth step, carrying out magnetic stirring and ultrasonic treatment by an ultrasonic oscillator in the adding process, and continuing the magnetic stirring and ultrasonic treatment by the ultrasonic oscillator for 30-50min after all the extract is added to prepare a compound liquid phase;
step eight: and (4) adding the compound liquid phase in the seventh step into the compound oil phase in the fifth step, and then performing magnetic stirring and ultrasonic treatment for 30-40min by using an ultrasonic oscillator to prepare the environment-friendly sterilizing and mite-killing agent.
9. The preparation method of the environment-friendly sterilizing and mite-killing agent according to claim 8, wherein the preparation method comprises the following steps: the magnetic stirring and ultrasonic oscillator ultrasonic treatment in the third step, the fourth step, the fifth step, the sixth step, the seventh step and the eighth step all adopt repeated circulation staggered operation.
10. The preparation method of the environment-friendly sterilizing and mite-killing agent according to claim 9, characterized in that: each cycle period is 5min, wherein the magnetic stirring is 3min, and the ultrasonic oscillator is used for ultrasonic treatment for 2 min.
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| CN112335691A (en) * | 2020-10-23 | 2021-02-09 | 北京茂思商贸有限公司 | Antibacterial and acarid-removing composite essential oil |
| CN112625812A (en) * | 2021-01-04 | 2021-04-09 | 合创博远(北京)科技有限公司 | Antibacterial and acarid-removing laundry detergent and preparation method thereof |
| CN112868678A (en) * | 2021-01-14 | 2021-06-01 | 广东迪美新材料科技有限公司 | Plant antibacterial mite-killing agent, preparation method thereof and daily necessities containing plant antibacterial mite-killing agent |
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| CN115039796A (en) * | 2022-05-16 | 2022-09-13 | 皖南医学院 | Acaricidal bacteriostatic agent containing plant essential oil and preparation method and application thereof |
| CN115500361A (en) * | 2022-09-27 | 2022-12-23 | 上海家化联合股份有限公司 | Water-based product containing peppermint leaf oil and mite killing application thereof |
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