CN112175243A - 一种高性能醋酸纤维素复合材料及其制备方法 - Google Patents
一种高性能醋酸纤维素复合材料及其制备方法 Download PDFInfo
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- CN112175243A CN112175243A CN202010996269.5A CN202010996269A CN112175243A CN 112175243 A CN112175243 A CN 112175243A CN 202010996269 A CN202010996269 A CN 202010996269A CN 112175243 A CN112175243 A CN 112175243A
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- Prior art keywords
- cellulose acetate
- parts
- performance
- composite material
- halloysite
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- 229920002301 cellulose acetate Polymers 0.000 title claims abstract description 75
- 239000002131 composite material Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title abstract description 15
- HPTYUNKZVDYXLP-UHFFFAOYSA-N aluminum;trihydroxy(trihydroxysilyloxy)silane;hydrate Chemical compound O.[Al].[Al].O[Si](O)(O)O[Si](O)(O)O HPTYUNKZVDYXLP-UHFFFAOYSA-N 0.000 claims abstract description 33
- 229910052621 halloysite Inorganic materials 0.000 claims abstract description 33
- BTXXTMOWISPQSJ-UHFFFAOYSA-N 4,4,4-trifluorobutan-2-one Chemical compound CC(=O)CC(F)(F)F BTXXTMOWISPQSJ-UHFFFAOYSA-N 0.000 claims abstract description 32
- BQACOLQNOUYJCE-FYZZASKESA-N Abietic acid Natural products CC(C)C1=CC2=CC[C@]3(C)[C@](C)(CCC[C@@]3(C)C(=O)O)[C@H]2CC1 BQACOLQNOUYJCE-FYZZASKESA-N 0.000 claims abstract description 32
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims abstract description 32
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 42
- 238000003756 stirring Methods 0.000 claims description 29
- 239000006185 dispersion Substances 0.000 claims description 12
- 238000001035 drying Methods 0.000 claims description 9
- 239000011521 glass Substances 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 7
- 238000009210 therapy by ultrasound Methods 0.000 claims description 6
- 125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 claims description 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 7
- 230000003078 antioxidant effect Effects 0.000 abstract description 6
- 230000004888 barrier function Effects 0.000 abstract description 6
- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 abstract description 5
- 230000007760 free radical scavenging Effects 0.000 abstract description 5
- 230000003287 optical effect Effects 0.000 abstract description 4
- 230000003321 amplification Effects 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000003199 nucleic acid amplification method Methods 0.000 abstract description 2
- 238000004806 packaging method and process Methods 0.000 abstract description 2
- 230000006750 UV protection Effects 0.000 abstract 1
- 239000003607 modifier Substances 0.000 abstract 1
- 239000000463 material Substances 0.000 description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000012528 membrane Substances 0.000 description 3
- 238000011056 performance test Methods 0.000 description 3
- 230000002292 Radical scavenging effect Effects 0.000 description 2
- 238000002835 absorbance Methods 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- MGJZITXUQXWAKY-UHFFFAOYSA-N diphenyl-(2,4,6-trinitrophenyl)iminoazanium Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1N=[N+](C=1C=CC=CC=1)C1=CC=CC=C1 MGJZITXUQXWAKY-UHFFFAOYSA-N 0.000 description 2
- 239000002105 nanoparticle Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000002791 soaking Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000006228 supernatant Substances 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000005284 excitation Effects 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012599 radical scavenging assay Methods 0.000 description 1
- 238000001878 scanning electron micrograph Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000002834 transmittance Methods 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
Images
Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/09—Carboxylic acids; Metal salts thereof; Anhydrides thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/002—Physical properties
- C08K2201/003—Additives being defined by their diameter
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/002—Physical properties
- C08K2201/004—Additives being defined by their length
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/10—Transparent films; Clear coatings; Transparent materials
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
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CN202010996269.5A CN112175243B (zh) | 2020-09-21 | 2020-09-21 | 一种高性能醋酸纤维素复合材料及其制备方法 |
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Citations (9)
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CN104334153A (zh) * | 2012-05-24 | 2015-02-04 | 株式会社爱茉莉太平洋 | 含有脱氢松香酸作为有效成分的抗老化用组合物 |
CN104611990A (zh) * | 2014-12-18 | 2015-05-13 | 瑞辰星生物技术(广州)有限公司 | 用于造纸的表面施胶剂和改善纸张强度、抗水性的造纸方法 |
CN106621857A (zh) * | 2017-02-21 | 2017-05-10 | 北京理工大学 | 一种醋酸纤维素基纳米材料复合超滤膜及其制备方法 |
JP2019094482A (ja) * | 2017-10-27 | 2019-06-20 | 日本製紙株式会社 | セルロースナノファイバー及びハロイサイトナノチューブを含む組成物、それを含むフィルム及び複合体 |
CN110204720A (zh) * | 2019-04-28 | 2019-09-06 | 南京岳子化工有限公司 | 一种聚酰亚胺树脂的绿色生产工艺 |
CN110240723A (zh) * | 2019-07-17 | 2019-09-17 | 华南协同创新研究院 | 一种紫外高屏蔽纤维素膜及其制备方法与应用 |
CN110337451A (zh) * | 2017-01-25 | 2019-10-15 | 株式会社大赛璐 | 乙酸纤维素、乙酸纤维素组合物、成型体及膜 |
CN110343292A (zh) * | 2018-04-02 | 2019-10-18 | 广西大学 | 一种纤维素纳米纤维/埃洛石纳米管增强淀粉膜及其制备方法 |
CN111655736A (zh) * | 2018-02-01 | 2020-09-11 | 日产化学株式会社 | 功能性多糖粒子 |
-
2020
- 2020-09-21 CN CN202010996269.5A patent/CN112175243B/zh active Active
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104334153A (zh) * | 2012-05-24 | 2015-02-04 | 株式会社爱茉莉太平洋 | 含有脱氢松香酸作为有效成分的抗老化用组合物 |
CN104611990A (zh) * | 2014-12-18 | 2015-05-13 | 瑞辰星生物技术(广州)有限公司 | 用于造纸的表面施胶剂和改善纸张强度、抗水性的造纸方法 |
CN110337451A (zh) * | 2017-01-25 | 2019-10-15 | 株式会社大赛璐 | 乙酸纤维素、乙酸纤维素组合物、成型体及膜 |
CN106621857A (zh) * | 2017-02-21 | 2017-05-10 | 北京理工大学 | 一种醋酸纤维素基纳米材料复合超滤膜及其制备方法 |
JP2019094482A (ja) * | 2017-10-27 | 2019-06-20 | 日本製紙株式会社 | セルロースナノファイバー及びハロイサイトナノチューブを含む組成物、それを含むフィルム及び複合体 |
CN111655736A (zh) * | 2018-02-01 | 2020-09-11 | 日产化学株式会社 | 功能性多糖粒子 |
CN110343292A (zh) * | 2018-04-02 | 2019-10-18 | 广西大学 | 一种纤维素纳米纤维/埃洛石纳米管增强淀粉膜及其制备方法 |
CN110204720A (zh) * | 2019-04-28 | 2019-09-06 | 南京岳子化工有限公司 | 一种聚酰亚胺树脂的绿色生产工艺 |
CN110240723A (zh) * | 2019-07-17 | 2019-09-17 | 华南协同创新研究院 | 一种紫外高屏蔽纤维素膜及其制备方法与应用 |
Non-Patent Citations (3)
Title |
---|
MIKKO KANERVA 等: ""Comparison of rosin and propolis antimicrobials in cellulose acetate fibers against staphylococcus aureus"", 《BIORESOURCES》 * |
刘莹等: "醋酸纤维素复合膜的改性及应用进展", 《塑料》 * |
王松 等: ""埃洛石纳米管/聚乙烯醇-淀粉复合膜的结构与性能"", 《复合材料学报》 * |
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Application publication date: 20210105 Assignee: GUILIN XINYU GE INDUSTRY Co.,Ltd. Assignor: GUILIN University OF TECHNOLOGY Contract record no.: X2023980044200 Denomination of invention: A high-performance cellulose acetate composite material and its preparation method Granted publication date: 20230505 License type: Common License Record date: 20231025 |
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Application publication date: 20210105 Assignee: Guangxi Zaifa Energy Technology Co.,Ltd. Assignor: GUILIN University OF TECHNOLOGY Contract record no.: X2023980045075 Denomination of invention: A high-performance cellulose acetate composite material and its preparation method Granted publication date: 20230505 License type: Common License Record date: 20231031 Application publication date: 20210105 Assignee: GUANGXI HEYANG ENERGY LTD. Assignor: GUILIN University OF TECHNOLOGY Contract record no.: X2023980045074 Denomination of invention: A high-performance cellulose acetate composite material and its preparation method Granted publication date: 20230505 License type: Common License Record date: 20231031 Application publication date: 20210105 Assignee: Guangxi Wokang Medical Technology Co.,Ltd. Assignor: GUILIN University OF TECHNOLOGY Contract record no.: X2023980045070 Denomination of invention: A high-performance cellulose acetate composite material and its preparation method Granted publication date: 20230505 License type: Common License Record date: 20231101 |
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Application publication date: 20210105 Assignee: Guangxi manjin Energy Saving Technology Co.,Ltd. Assignor: GUILIN University OF TECHNOLOGY Contract record no.: X2023980045248 Denomination of invention: A high-performance cellulose acetate composite material and its preparation method Granted publication date: 20230505 License type: Common License Record date: 20231103 |