CN1120049A - 聚异丁烯的生产方法 - Google Patents
聚异丁烯的生产方法 Download PDFInfo
- Publication number
- CN1120049A CN1120049A CN95104053A CN95104053A CN1120049A CN 1120049 A CN1120049 A CN 1120049A CN 95104053 A CN95104053 A CN 95104053A CN 95104053 A CN95104053 A CN 95104053A CN 1120049 A CN1120049 A CN 1120049A
- Authority
- CN
- China
- Prior art keywords
- butylene
- raw material
- aforesaid right
- require
- ether
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/06—Metallic compounds other than hydrides and other than metallo-organic compounds; Boron halide or aluminium halide complexes with organic compounds containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F210/00—Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F210/04—Monomers containing three or four carbon atoms
- C08F210/08—Butenes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F210/00—Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F210/04—Monomers containing three or four carbon atoms
- C08F210/08—Butenes
- C08F210/10—Isobutene
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polymerization Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Description
批号 | 原料 组成 | ||||||
异丁烯% | 正丁烷% | 异丁烷% | 1-丁烯% | 反式-2-丁烯% | 顺式-2-丁烯% | 1,3-丁二烯% | |
1 | 42.33 | 17.52 | 5.59 | 21.68 | 7.35 | 5.34 | 660 |
2 | 46.06 | 53.68 | 0.00 | 0.00 | 0.00 | 0.00 | 0 |
3 | 45.23 | 25.89 | 0.16 | 4.38 | 14.39 | 9.90 | 36 |
批号 | 每公斤C4混合物中BF3乙醇络合物的浓度(g) | C4混合物的重量(g) | 起始温度℃ | 最高温度℃ | 反应时间(分) |
1 | 1.900 | 358.1 | -15.4 | -1.5 | 20 |
2 | 1.725 | 307.2 | -11.5 | 2.5 | 21 |
3 | 1.825 | 306.8 | -15.3 | 1.4 | 20 |
批号 | 亚乙烯基含量(由I.R.) | 由GPC测的Mn | 有机氟(ppm) |
1 | 75.3 | 1001 | 62.0 |
2 | 82.3 | 1220 | 3.5 |
3 | 79.3 | 942 | 17.0 |
批号 | 原料 组成K | ||||||
异丁烯% | 正丁烷% | 异丁烷% | 1-丁烯% | 反式-2-丁烯% | 顺式-2-丁烯% | 1,3-丁二烯% | |
4 | 42.50 | 16.20 | 5.00 | 22.10 | 8.60 | 5.50 | 400 |
5 | 46.06 | 53.68 | 0.00 | 0.00 | 0.00 | 0.00 | 0 |
6 | 45.23 | 25.89 | 0.16 | 4.38 | 14.39 | 9.90 | 36 |
7 | 42.50 | 16.20 | 5.00 | 22.10 | 8.60 | 5.50 | 400 |
8 | 40.13 | 59.52 | 0.32 | 0.00 | 0.00 | 0.00 | 0 |
9 | 45.23 | 25.89 | 0.16 | 4.38 | 14.39 | 9.90 | 36 |
批号 | 每公斤C4混合物引发剂浓度(g) | C4混合物重量(g) | 起始温度℃ | 最高温度℃ | 反应时间(分) |
4* | 1 35 | 229.3 | -10.0 | -3.0 | 30 |
5* | 1.24 | 258.2 | -12.9 | -1.4 | 30 |
6* | 1.23 | 333.2 | -14.5 | -0.2 | 20 |
7** | 1.59 | 207.5 | -10.8 | -7.5 | 20 |
8** | 1 44 | 332.6 | -13.7 | -8.2 | 20 |
9** | 1.41 | 424.3 | -13.2 | -7.5 | 20 |
批号 | 亚乙烯基浓度%(由I.R.) | 由GPC测的Mn | 有机氟(PPm) |
4* | 74.0 | 1203 | 99 |
5* | 85.0 | 1049 | 2 |
6* | 82.0 | 866 | 32 |
7** | 59.0 | 671 | 280 |
8** | 80.0 | 743 | 7 |
9** | 69.0 | 637 | 23 |
原料 反应时间(分) 反应温度 催化剂浓度 产物的Mn 亚乙烯基含量 氟浓度g/Kg C4(℃) 混合物 (由GPC) (由IR) (ppm) | ||||||
IB | 15 | -10 | 1.31 | 721 | 84 | <10 |
HI | 14 | -10 | 1.82 | 791 | 86 | 34 |
RI | 18 | -13 | 0.98 | 812 | 77 | 81 |
IB | 15 | -13 | 0.98 | 969 | 88 | <10 |
HI | 15 | -15 | 1.53 | 1063 | 81 | 23 |
RI | 10 | -10 | 0.98 | 910 | 75 | 58 |
IB | 18 | -13 | 0.98 | 1376 | 85 | <10 |
HI | 18 | -13 | 1.26 | 1414 | 80 | 14 |
RI | 15 | -13 | 0.98 | 1302 | 75 | 61 |
IB | 20 | -15 | 0.79 | 1586 | 85 | <10 |
HI | 27 | -13 | 1.41 | 1510 | 83 | 22 |
RI | 15 | -10 | 1.64 | 1429 | 78 | 58 |
Claims (21)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB9404368A GB9404368D0 (en) | 1994-03-07 | 1994-03-07 | Production of polyisobutenes |
GB9404368.4 | 1994-03-07 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1120049A true CN1120049A (zh) | 1996-04-10 |
CN1178967C CN1178967C (zh) | 2004-12-08 |
Family
ID=10751418
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB951040537A Expired - Lifetime CN1178967C (zh) | 1994-03-07 | 1995-03-07 | 聚异丁烯的生产方法 |
Country Status (11)
Country | Link |
---|---|
US (1) | US5674955A (zh) |
EP (1) | EP0671419B1 (zh) |
JP (1) | JP3942655B2 (zh) |
KR (1) | KR100362545B1 (zh) |
CN (1) | CN1178967C (zh) |
BR (1) | BR9500835A (zh) |
DE (2) | DE69502425T2 (zh) |
GB (1) | GB9404368D0 (zh) |
HU (1) | HU218306B (zh) |
IN (1) | IN190180B (zh) |
MY (1) | MY115946A (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105324399A (zh) * | 2013-06-05 | 2016-02-10 | 大林产业株式会社 | 制备具有多种分子量的聚丁烯的装置和方法 |
CN106604936A (zh) * | 2014-08-22 | 2017-04-26 | 大林产业株式会社 | 聚丁烯制备方法 |
US9683060B2 (en) | 2013-01-17 | 2017-06-20 | Daelim Industrial Co., Ltd. | Method for preparing polybutene |
CN113366027A (zh) * | 2018-12-17 | 2021-09-07 | 阿朗新科新加坡私人有限公司 | 使用叔醚生产异烯烃聚合物的方法 |
Families Citing this family (43)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19619267A1 (de) * | 1996-05-13 | 1997-11-20 | Basf Ag | Verfahren zur Herstellung von mittelmolekularem, hochreaktivem Polyisobuten |
FR2749015B1 (fr) * | 1996-05-24 | 1998-07-03 | Bp Chemicals Snc | Procede de polymerisation d'olefine(s) |
DE19646405A1 (de) * | 1996-11-11 | 1998-05-14 | Erdoelchemie Gmbh | Verfahren zur Oligomerisierung von i-Buten |
FR2757505B1 (fr) * | 1996-12-23 | 1999-02-19 | Inst Francais Du Petrole | Procede de production d'isobutene de haute purete combinant une distillation reactive d'hydroisomerisation, une distillation et une isomerisation squelettale |
FR2757506B1 (fr) * | 1996-12-23 | 1999-02-19 | Inst Francais Du Petrole | Procede de production d'isobutene de haute purete combinant une distillation reactive d'hydroisomerisation et une isomerisation squelettale |
KR20010031186A (ko) | 1998-08-25 | 2001-04-16 | 사이카와 겐조오 | 부텐중합체의 제조 방법 |
KR100639611B1 (ko) * | 1999-02-23 | 2006-10-27 | 니뽄 세키유 가가쿠 가부시키가이샤 | 탄소-탄소 이중결합을 포함하는 탄화수소의 탈할로겐방법 |
US6884858B2 (en) | 1999-10-19 | 2005-04-26 | Texas Petrochemicals Lp | Process for preparing polyolefin products |
EP1242464B1 (en) | 1999-09-16 | 2011-04-27 | TPC Group LLC | Process for preparing polyolefin products |
US6562913B1 (en) | 1999-09-16 | 2003-05-13 | Texas Petrochemicals Lp | Process for producing high vinylidene polyisobutylene |
US6992152B2 (en) | 1999-10-19 | 2006-01-31 | Texas Petrochemicals Lp | Apparatus and method for controlling olefin polymerization process |
US7037999B2 (en) | 2001-03-28 | 2006-05-02 | Texas Petrochemicals Lp | Mid-range vinylidene content polyisobutylene polymer product and process for producing the same |
US6858188B2 (en) | 2003-05-09 | 2005-02-22 | Texas Petrochemicals, Lp | Apparatus for preparing polyolefin products and methodology for using the same |
KR100486044B1 (ko) * | 2000-11-13 | 2005-04-29 | 대림산업 주식회사 | 폴리부텐의 제조방법 |
DE10061727A1 (de) | 2000-12-12 | 2002-06-13 | Basf Ag | Verfahren zur Herstellung von Polyisobutenen |
DE10061715A1 (de) | 2000-12-12 | 2002-06-13 | Basf Ag | Verfahren zur Herstellung von Homo- und Copolymeren des Isobutens |
DE10125583A1 (de) | 2001-05-25 | 2002-11-28 | Basf Ag | Verfahren zur Herstellung von Homo- und Copolymeren des Isobutens |
DE10162567A1 (de) | 2001-12-19 | 2003-07-03 | Basf Ag | Polyisobutene und Polyisobutenderivate für Schmierstoffzusammensetzungen |
DE10215108A1 (de) * | 2002-04-05 | 2003-10-16 | Basf Ag | Polyisobutenamine |
US6933351B2 (en) * | 2003-06-20 | 2005-08-23 | Infineum International Limited | Process for forming polyalkenyl acylating agents |
US7339007B2 (en) * | 2003-06-20 | 2008-03-04 | Infineum International Limited | Low sediment process for thermally reacting highly reactive polymers and enophiles |
WO2007096296A1 (de) * | 2006-02-23 | 2007-08-30 | Basf Se | Verfahren zur herstellung von polyisobutylen mit einem gehalt an endständigen doppelbindungen von mehr als 50% aus einem technischen 1-buten-, 2-buten- und isobuten-haltigen c4-kohlenwasserstoffstrom |
CN101460530A (zh) * | 2006-06-06 | 2009-06-17 | 巴斯夫欧洲公司 | 由低异丁烯的c4烃混合物制备反应性且基本上无卤聚异丁烯的方法 |
EP2099731A1 (de) | 2006-11-30 | 2009-09-16 | Basf Se | Verfahren zur hydroformylierung von olefinen |
KR100851639B1 (ko) | 2007-03-22 | 2008-08-13 | 대림산업 주식회사 | 고농도 이소부텐을 이용한 고반응성 폴리이소부텐의제조방법 |
US20100298507A1 (en) | 2009-05-19 | 2010-11-25 | Menschig Klaus R | Polyisobutylene Production Process With Improved Efficiencies And/Or For Forming Products Having Improved Characteristics And Polyisobutylene Products Produced Thereby |
CA2784549C (en) | 2009-12-18 | 2018-01-23 | Chevron Oronite Company Llc | Carbonyl-ene functionalized polyolefins |
JP2013521363A (ja) | 2010-03-02 | 2013-06-10 | ビーエイエスエフ・ソシエタス・エウロパエア | ブロックコポリマーおよびその使用 |
US8673275B2 (en) | 2010-03-02 | 2014-03-18 | Basf Se | Block copolymers and their use |
JP5343041B2 (ja) * | 2010-06-18 | 2013-11-13 | Jx日鉱日石エネルギー株式会社 | オレフィン重合体の製造方法 |
US11072570B2 (en) | 2012-01-09 | 2021-07-27 | Basf Se | Process for continuously preparing polyisobutylene |
EP2802610B1 (de) | 2012-01-09 | 2018-11-07 | Basf Se | Verfahren zur kontinuierlichen herstellung von polyisobutylen |
WO2014070354A1 (en) * | 2012-10-31 | 2014-05-08 | Washington State University | Stable mixed oxide catalysts for direct conversion of ethanol to isobutene and process for making |
KR101511701B1 (ko) * | 2013-07-30 | 2015-04-13 | 대림산업 주식회사 | 폴리부텐 제조 시 사용되는 원료의 재순환 장치 및 방법 |
KR101511708B1 (ko) * | 2013-08-28 | 2015-04-13 | 대림산업 주식회사 | 폴리부텐 제조 시 발생되는 할로겐의 제거 장치 및 방법 |
US9617366B1 (en) | 2016-03-03 | 2017-04-11 | Tpc Group Llc | Low-fluoride, reactive polyisobutylene |
WO2017151341A1 (en) | 2016-03-03 | 2017-09-08 | Tpc Group Llc | Low-fluoride, reactive polyisobutylene |
US9617363B1 (en) | 2016-03-03 | 2017-04-11 | Tpc Group Llc | Low-fluoride, reactive polyisobutylene |
JP7216826B2 (ja) | 2018-12-21 | 2023-02-01 | アランセオ・シンガポール・プライヴェート・リミテッド | ハロゲン化イソオレフィンコポリマーの連続製造方法 |
CA3122591A1 (en) | 2018-12-27 | 2020-07-02 | Arlanxeo Singapore Pte. Ltd. | Process for producing chlorinated butyl rubber |
EP3943518A1 (en) | 2020-07-22 | 2022-01-26 | Indian Oil Corporation Limited | Polymerization catalyst system and process to produce highly reactive polyisobutylene |
US11845705B2 (en) * | 2021-08-17 | 2023-12-19 | Saudi Arabian Oil Company | Processes integrating hydrocarbon cracking with metathesis for producing propene |
US20230167208A1 (en) * | 2021-11-30 | 2023-06-01 | Braskem S.A. | Heterogeneous catalyst for highly-reactive polyisobutylene |
Family Cites Families (9)
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US2775577A (en) * | 1952-12-23 | 1956-12-25 | Exxon Research Engineering Co | Controlled isobutylene polymerization |
DE2702604C2 (de) * | 1977-01-22 | 1984-08-30 | Basf Ag, 6700 Ludwigshafen | Polyisobutene |
FR2463802A1 (fr) * | 1979-08-21 | 1981-02-27 | Inst Francais Du Petrole | Procede de valorisation des coupes c4 olefiniques |
US4358574A (en) * | 1981-01-19 | 1982-11-09 | Exxon Research & Engineering Co. | Production of hydrocarbon resins and products resulting therefrom |
GB8329082D0 (en) * | 1983-11-01 | 1983-12-07 | Bp Chem Int Ltd | Low molecular weight polymers of 1-olefins |
US5068490A (en) * | 1989-08-18 | 1991-11-26 | Amoco Corporation | BF3-tertiary etherate complexes for isobutylene polymerization |
US5254649A (en) * | 1990-11-28 | 1993-10-19 | Bp Chemicals Limited | Cationic polymerization of 1-olefins |
US5286823A (en) * | 1991-06-22 | 1994-02-15 | Basf Aktiengesellschaft | Preparation of highly reactive polyisobutenes |
US5416176A (en) * | 1994-06-16 | 1995-05-16 | Phillips Petroleum Company | Method for controlling the feed composition to a process for polymerizing isobutylene |
-
1994
- 1994-03-07 GB GB9404368A patent/GB9404368D0/en active Pending
-
1995
- 1995-02-28 DE DE69502425T patent/DE69502425T2/de not_active Expired - Lifetime
- 1995-02-28 DE DE0671419T patent/DE671419T1/de active Pending
- 1995-02-28 EP EP95301302A patent/EP0671419B1/en not_active Expired - Lifetime
- 1995-03-01 US US08/396,674 patent/US5674955A/en not_active Expired - Lifetime
- 1995-03-02 IN IN351DE1995 patent/IN190180B/en unknown
- 1995-03-06 MY MYPI95000551A patent/MY115946A/en unknown
- 1995-03-07 JP JP04761495A patent/JP3942655B2/ja not_active Expired - Lifetime
- 1995-03-07 HU HU9500686A patent/HU218306B/hu unknown
- 1995-03-07 CN CNB951040537A patent/CN1178967C/zh not_active Expired - Lifetime
- 1995-03-07 BR BR9500835A patent/BR9500835A/pt not_active IP Right Cessation
- 1995-03-07 KR KR1019950004640A patent/KR100362545B1/ko not_active IP Right Cessation
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9683060B2 (en) | 2013-01-17 | 2017-06-20 | Daelim Industrial Co., Ltd. | Method for preparing polybutene |
CN105324399A (zh) * | 2013-06-05 | 2016-02-10 | 大林产业株式会社 | 制备具有多种分子量的聚丁烯的装置和方法 |
CN105324399B (zh) * | 2013-06-05 | 2017-09-08 | 大林产业株式会社 | 制备具有多种分子量的聚丁烯的装置和方法 |
CN106604936A (zh) * | 2014-08-22 | 2017-04-26 | 大林产业株式会社 | 聚丁烯制备方法 |
CN113366027A (zh) * | 2018-12-17 | 2021-09-07 | 阿朗新科新加坡私人有限公司 | 使用叔醚生产异烯烃聚合物的方法 |
Also Published As
Publication number | Publication date |
---|---|
US5674955A (en) | 1997-10-07 |
HU218306B (en) | 2000-07-28 |
CN1178967C (zh) | 2004-12-08 |
EP0671419A1 (en) | 1995-09-13 |
EP0671419B1 (en) | 1998-05-13 |
MY115946A (en) | 2003-10-31 |
IN190180B (zh) | 2003-06-28 |
JPH07268033A (ja) | 1995-10-17 |
BR9500835A (pt) | 1995-10-31 |
DE69502425D1 (de) | 1998-06-18 |
JP3942655B2 (ja) | 2007-07-11 |
GB9404368D0 (en) | 1994-04-20 |
KR950032300A (ko) | 1995-12-20 |
KR100362545B1 (ko) | 2003-02-07 |
DE69502425T2 (de) | 1998-09-03 |
HU9500686D0 (en) | 1995-04-28 |
DE671419T1 (de) | 1996-09-19 |
HUT71633A (en) | 1996-01-29 |
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Effective date of registration: 20111205 Address after: England Hampshire Patentee after: INEOS COMMERCIAL SERVICES UK Ltd. Address before: The Middlesex County Patentee before: INEOS EUROPE LTD. Effective date of registration: 20111205 Address after: The Middlesex County Patentee after: INEOS EUROPE LTD. Address before: The Middlesex County Patentee before: INNOVENE EUROPE LTD. Effective date of registration: 20111205 Address after: The Middlesex County Patentee after: INNOVENE EUROPE LTD. Address before: The Middlesex County Patentee before: O and D Trading Co.,Ltd. Effective date of registration: 20111205 Address after: The Middlesex County Patentee after: O and D Trading Co.,Ltd. Address before: London, England, England Patentee before: BP Chemicals Ltd. |
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Owner name: INEOS SALES (UK) LIMITED Free format text: FORMER OWNER: INEOS COMMERCIAL SERVICES UK LIMITED Effective date: 20140718 |
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Effective date of registration: 20140718 Address after: England Hampshire Patentee after: Ineos sales (UK) Ltd. Address before: England Hampshire Patentee before: INEOS COMMERCIAL SERVICES UK Ltd. |
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