CN111910448A - 一种梭织布染料配方及其印染工艺 - Google Patents

一种梭织布染料配方及其印染工艺 Download PDF

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CN111910448A
CN111910448A CN202010742894.7A CN202010742894A CN111910448A CN 111910448 A CN111910448 A CN 111910448A CN 202010742894 A CN202010742894 A CN 202010742894A CN 111910448 A CN111910448 A CN 111910448A
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dye
fabric
anhydrous potassium
potassium sulfite
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冯永芳
施国琴
金水祥
祝吉琴
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Shaoxing Textile Lianma Textile Co ltd
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Abstract

本发明公开了一种梭织布染料配方，包括以下质量份数的原料：邻苯二甲酸二丁酯2‑5份、着色剂5‑8份、匀染剂8‑10份、聚乙烯醇6‑10份、丙烯酰胺2‑6份、海藻酸3‑7份、过氧化苯甲酸六丁酯10‑15份、环氟化活性染料30‑40份、无水亚硫酸钾5‑9份、甲基硅油1‑4份、去离子水8‑16份、无水亚硫酸钾3‑8份、天然染料20‑30份。本发明还提供了一种梭织布印染工艺，其特征在于，包括以下步骤：S1，放缝；S2，烧毛；S3，煮练；S4，定型丝光；S5，热熔搅拌；S6，浸染；S7，拉幅。本发明制备方法简单，制备的梭织布不掉色，且能够严格的控制印染温度，提高印染效果。

Description

一种梭织布染料配方及其印染工艺
技术领域
本发明涉及梭织布生产技术领域，尤其涉及一种梭织布染料配方及其印染工艺。
背景技术
梭织布：是将纱线由经纬两个方向相互垂直交织而成的布，纵向的纱线叫经纱，横向的纱线叫纬纱。
但是现有的梭织布容易出现掉色的问题，其跟采用的原料息息相关，并且影响染色效果的因素有很多，主要有染液温度、浓度、时间等。其中，温度是影响染色效果的最重要因素之一，一般来说，温度高，染料的动能增加，同时因纤维膨胀，其内部空隙增大，便于吸附扩散，从而使上染加快，但是温度过高时，由于纤维空隙过大，染料粒子动能过大，反而会使染上纤维的部分重新溶入染液中，影响染色效果。
发明内容
基于背景技术存在的技术问题，本发明提出了一种梭织布染料配方及其印染工艺。
本发明提出的一种梭织布染料配方，包括以下质量份数的原料：邻苯二甲酸二丁酯2-5份、着色剂5-8份、匀染剂8-10份、聚乙烯醇6-10份、丙烯酰胺2-6份、海藻酸3-7份、过氧化苯甲酸六丁酯10-15份、环氟化活性染料30-40份、无水亚硫酸钾5-9份、甲基硅油1-4份、去离子水8-16份、无水亚硫酸钾3-8份、天然染料20-30份。
优选地，所述匀染剂由2-4份聚乙烯吡咯烷酮，3-8份亚甲基双萘磺酸盐，5-10份十二烷基二苯醚二磺酸钠组成。
优选地，所述天然染料为靛蓝、茜草、紫草、红花、桑、茶中的一种。
本发明还公开了一种梭织布印染工艺，包括以下步骤：
S1，放缝：采用延长需要缝合的净缝线，与另一毛缝线相交，过交点作缝线延长线的垂直线，即可按缝份画出四边形进行缝制；
S2，烧毛：加热金属辊至700-800℃，将梭织布在放卷辊与收卷辊的作用下，快速的经过金属辊，除去织物表面上的绒毛，并尽可能不引起织物的损伤；
S3，煮练：将布料经过煮练炉，加入50-80ml的煮练剂烧碱以及20-50ml的煮练助剂，杂质通过溶解、降解、乳化作用，部分直接溶解在煮练液中，部分从织物上脱落下来，部分通过表面活性剂的乳化作用从织物上剥离下来；
S4，定型丝光：将布料通过定型机定型，再用浓的烧碱液处理，使布料任意收缩，最后洗去烧碱；
S5，热熔搅拌：将邻苯二甲酸二丁酯2-5份、着色剂5-8份、匀染剂8-10份、聚乙烯醇6-10份、丙烯酰胺2-6份、海藻酸3-7份、过氧化苯甲酸六丁酯10-15份、环氟化活性染料30-40份、无水亚硫酸钾5-9份、甲基硅油1-4份、去离子水8-16份、无水亚硫酸钾3-8份、天然染料20-30份加热至200-300℃，搅拌40-60min得到染料；
S6，浸染：将布料先用清水浸泡10-20min，再经过S5制得的染料中浸泡30-40min，浸染过程中，先对染料进行预加热至100-300℃，使用温度计实时监控染缸内的温度，在染缸的侧壁安装多个加热器，及时对温度进行调控，浸染结束使用清水冲去多余染料，最后使用烘干机烘干即可；
S7，拉幅：将S6得到的布料经过布铗拉幅机拉幅处理，可将植物拉至需要的宽度，同时进行热成型，最终得到梭织布。
优选地，在S5中，所述搅拌的转速控制在30r/s。
优选地，所述热熔搅拌过程中，原料的放入顺序为：先放入邻苯二甲酸二丁酯、聚乙烯醇、丙烯酰胺、海藻酸、过氧化苯甲酸六丁酯、无水亚硫酸钾、甲基硅油、去离子水、无水亚硫酸钾、天然染料，再注入环氟化活性染料，最终再注入着色剂与匀染剂。
本发明中，原料采用邻苯二甲酸二丁酯、聚乙烯醇、丙烯酰胺、海藻酸、过氧化苯甲酸六丁酯、无水亚硫酸钾、甲基硅油、去离子水、无水亚硫酸钾、天然染料、环氟化活性染料、着色剂与匀染剂，能够大大减少梭织布的掉色问题；将布料先用清水浸泡10-20min，再经过S5制得的染料中浸泡30-40min，浸染过程中，先对染料进行预加热至100-300℃，使用温度计实时监控染缸内的温度，在染缸的侧壁安装多个加热器，及时对温度进行调控，能够精确的控制侵染的温度，从而提高印染效果。
具体实施方式
下面结合具体实施例对本发明作进一步解说。
实施例1
本发明提出的一种梭织布染料配方，包括以下质量份数的原料：邻苯二甲酸二丁酯2份、着色剂5份、匀染剂8份、聚乙烯醇6份、丙烯酰胺2份、海藻酸3份、过氧化苯甲酸六丁酯10份、环氟化活性染料30份、无水亚硫酸钾5份、甲基硅油1份、去离子水8份、无水亚硫酸钾3份、天然染料20份。
具体的，所述匀染剂由2份聚乙烯吡咯烷酮，3份亚甲基双萘磺酸盐，5份十二烷基二苯醚二磺酸钠组成。
具体的，所述天然染料为靛蓝。
本发明还公开了一种梭织布印染工艺，包括以下步骤：
S1，放缝：采用延长需要缝合的净缝线，与另一毛缝线相交，过交点作缝线延长线的垂直线，即可按缝份画出四边形进行缝制；
S2，烧毛：加热金属辊至700℃，将梭织布在放卷辊与收卷辊的作用下，快速的经过金属辊，除去织物表面上的绒毛，并尽可能不引起织物的损伤；
S3，煮练：将布料经过煮练炉，加入50ml的煮练剂烧碱以及20ml的煮练助剂，杂质通过溶解、降解、乳化作用，部分直接溶解在煮练液中，部分从织物上脱落下来，部分通过表面活性剂的乳化作用从织物上剥离下来；
S4，定型丝光：将布料通过定型机定型，再用浓的烧碱液处理，使布料任意收缩，最后洗去烧碱；
S5，热熔搅拌：将邻苯二甲酸二丁酯2份、着色剂5份、匀染剂8份、聚乙烯醇6份、丙烯酰胺2份、海藻酸3份、过氧化苯甲酸六丁酯10份、环氟化活性染料30份、无水亚硫酸钾5份、甲基硅油1份、去离子水8份、无水亚硫酸钾3份、天然染料20份加热至200℃，搅拌40min得到染料；
S6，浸染：将布料先用清水浸泡10min，再经过S5制得的染料中浸泡30min，浸染过程中，先对染料进行预加热至100℃，使用温度计实时监控染缸内的温度，在染缸的侧壁安装多个加热器，及时对温度进行调控，浸染结束使用清水冲去多余染料，最后使用烘干机烘干即可；
S7，拉幅：将S6得到的布料经过布铗拉幅机拉幅处理，可将植物拉至需要的宽度，同时进行热成型，最终得到梭织布。
具体的，在S5中，所述搅拌的转速控制在30r/s。
具体的，所述热熔搅拌过程中，原料的放入顺序为：先放入邻苯二甲酸二丁酯、聚乙烯醇、丙烯酰胺、海藻酸、过氧化苯甲酸六丁酯、无水亚硫酸钾、甲基硅油、去离子水、无水亚硫酸钾、天然染料，再注入环氟化活性染料，最终再注入着色剂与匀染剂。
实施例2
本发明提出的一种梭织布染料配方，包括以下质量份数的原料：邻苯二甲酸二丁酯4份、着色剂6份、匀染剂9份、聚乙烯醇8份、丙烯酰胺4份、海藻酸5份、过氧化苯甲酸六丁酯12份、环氟化活性染料35份、无水亚硫酸钾7份、甲基硅油3份、去离子水10份、无水亚硫酸钾7份、天然染料25份。
具体的，所述匀染剂由3份聚乙烯吡咯烷酮，6份亚甲基双萘磺酸盐，7份十二烷基二苯醚二磺酸钠组成。
具体的，所述天然染料为靛蓝、茜草、紫草、红花、桑、茶中的一种。
本发明还公开了一种梭织布印染工艺，包括以下步骤：
S1，放缝：采用延长需要缝合的净缝线，与另一毛缝线相交，过交点作缝线延长线的垂直线，即可按缝份画出四边形进行缝制；
S2，烧毛：加热金属辊至750℃，将梭织布在放卷辊与收卷辊的作用下，快速的经过金属辊，除去织物表面上的绒毛，并尽可能不引起织物的损伤；
S3，煮练：将布料经过煮练炉，加入70ml的煮练剂烧碱以及30ml的煮练助剂，杂质通过溶解、降解、乳化作用，部分直接溶解在煮练液中，部分从织物上脱落下来，部分通过表面活性剂的乳化作用从织物上剥离下来；
S4，定型丝光：将布料通过定型机定型，再用浓的烧碱液处理，使布料任意收缩，最后洗去烧碱；
S5，热熔搅拌：邻苯二甲酸二丁酯4份、着色剂6份、匀染剂9份、聚乙烯醇8份、丙烯酰胺4份、海藻酸5份、过氧化苯甲酸六丁酯12份、环氟化活性染料35份、无水亚硫酸钾7份、甲基硅油3份、去离子水10份、无水亚硫酸钾7份、天然染料25份加热至250℃，搅拌50min得到染料；
S6，浸染：将布料先用清水浸泡15min，再经过S5制得的染料中浸泡35min，浸染过程中，先对染料进行预加热至200℃，使用温度计实时监控染缸内的温度，在染缸的侧壁安装多个加热器，及时对温度进行调控，浸染结束使用清水冲去多余染料，最后使用烘干机烘干即可；
S7，拉幅：将S6得到的布料经过布铗拉幅机拉幅处理，可将植物拉至需要的宽度，同时进行热成型，最终得到梭织布。
具体的，在S5中，所述搅拌的转速控制在30r/s。
具体的，所述热熔搅拌过程中，原料的放入顺序为：先放入邻苯二甲酸二丁酯、聚乙烯醇、丙烯酰胺、海藻酸、过氧化苯甲酸六丁酯、无水亚硫酸钾、甲基硅油、去离子水、无水亚硫酸钾、天然染料，再注入环氟化活性染料，最终再注入着色剂与匀染剂。
实施例3
本发明提出的一种梭织布染料配方，包括以下质量份数的原料：邻苯二甲酸二丁酯5份、着色剂8份、匀染剂10份、聚乙烯醇10份、丙烯酰胺6份、海藻酸7份、过氧化苯甲酸六丁酯15份、环氟化活性染料40份、无水亚硫酸钾9份、甲基硅油4份、去离子水16份、无水亚硫酸钾8份、天然染料30份。
具体的，所述匀染剂由4份聚乙烯吡咯烷酮，8份亚甲基双萘磺酸盐，10份十二烷基二苯醚二磺酸钠组成。
具体的，所述天然染料为靛蓝、茜草、紫草、红花、桑、茶中的一种。
本发明还公开了一种梭织布印染工艺，包括以下步骤：
S1，放缝：采用延长需要缝合的净缝线，与另一毛缝线相交，过交点作缝线延长线的垂直线，即可按缝份画出四边形进行缝制；
S2，烧毛：加热金属辊至800℃，将梭织布在放卷辊与收卷辊的作用下，快速的经过金属辊，除去织物表面上的绒毛，并尽可能不引起织物的损伤；
S3，煮练：将布料经过煮练炉，加入80ml的煮练剂烧碱以及50ml的煮练助剂，杂质通过溶解、降解、乳化作用，部分直接溶解在煮练液中，部分从织物上脱落下来，部分通过表面活性剂的乳化作用从织物上剥离下来；
S4，定型丝光：将布料通过定型机定型，再用浓的烧碱液处理，使布料任意收缩，最后洗去烧碱；
S5，热熔搅拌：将邻苯二甲酸二丁酯5份、着色剂8份、匀染剂10份、聚乙烯醇10份、丙烯酰胺6份、海藻酸7份、过氧化苯甲酸六丁酯15份、环氟化活性染料40份、无水亚硫酸钾9份、甲基硅油4份、去离子水16份、无水亚硫酸钾8份、天然染料30份加热至300℃，搅拌60min得到染料；
S6，浸染：将布料先用清水浸泡20min，再经过S5制得的染料中浸泡40min，浸染过程中，先对染料进行预加热至300℃，使用温度计实时监控染缸内的温度，在染缸的侧壁安装多个加热器，及时对温度进行调控，浸染结束使用清水冲去多余染料，最后使用烘干机烘干即可；
S7，拉幅：将S6得到的布料经过布铗拉幅机拉幅处理，可将植物拉至需要的宽度，同时进行热成型，最终得到梭织布。
具体的，在S5中，所述搅拌的转速控制在30r/s。
具体的，所述热熔搅拌过程中，原料的放入顺序为：先放入邻苯二甲酸二丁酯、聚乙烯醇、丙烯酰胺、海藻酸、过氧化苯甲酸六丁酯、无水亚硫酸钾、甲基硅油、去离子水、无水亚硫酸钾、天然染料，再注入环氟化活性染料，最终再注入着色剂与匀染剂。
本发明中，原料采用邻苯二甲酸二丁酯、聚乙烯醇、丙烯酰胺、海藻酸、过氧化苯甲酸六丁酯、无水亚硫酸钾、甲基硅油、去离子水、无水亚硫酸钾、天然染料、环氟化活性染料、着色剂与匀染剂，能够大大减少梭织布的掉色问题；将布料先用清水浸泡10-20min，再经过S5制得的染料中浸泡30-40min，浸染过程中，先对染料进行预加热至100-300℃，使用温度计实时监控染缸内的温度，在染缸的侧壁安装多个加热器，及时对温度进行调控，能够精确的控制侵染的温度，从而提高印染效果。
以上所述，仅为本发明较佳的具体实施方式，但本发明的保护范围并不局限于此，任何熟悉本技术领域的技术人员在本发明揭露的技术范围内，根据本发明的技术方案及其发明构思加以等同替换或改变，都应涵盖在本发明的保护范围之内。

Claims (6)

1.一种梭织布染料配方，其特征在于，包括以下质量份数的原料：邻苯二甲酸二丁酯2-5份、着色剂5-8份、匀染剂8-10份、聚乙烯醇6-10份、丙烯酰胺2-6份、海藻酸3-7份、过氧化苯甲酸六丁酯10-15份、环氟化活性染料30-40份、无水亚硫酸钾5-9份、甲基硅油1-4份、去离子水8-16份、无水亚硫酸钾3-8份、天然染料20-30份。
2.根据权利要求1所述的一种梭织布染料配方，其特征在于，所述匀染剂由2-4份聚乙烯吡咯烷酮，3-8份亚甲基双萘磺酸盐，5-10份十二烷基二苯醚二磺酸钠组成。
3.根据权利要求1所述的一种梭织布染料配方，其特征在于，所述天然染料为靛蓝、茜草、紫草、红花、桑、茶中的一种。
4.一种梭织布印染工艺，其特征在于，包括以下步骤：
S1，放缝：采用延长需要缝合的净缝线，与另一毛缝线相交，过交点作缝线延长线的垂直线，即可按缝份画出四边形进行缝制；
S2，烧毛：加热金属辊至700-800℃，将梭织布在放卷辊与收卷辊的作用下，快速的经过金属辊，除去织物表面上的绒毛，并尽可能不引起织物的损伤；
S3，煮练：将布料经过煮练炉，加入50-80ml的煮练剂烧碱以及20-50ml的煮练助剂，杂质通过溶解、降解、乳化作用，部分直接溶解在煮练液中，部分从织物上脱落下来，部分通过表面活性剂的乳化作用从织物上剥离下来；
S4，定型丝光：将布料通过定型机定型，再用浓的烧碱液处理，使布料任意收缩，最后洗去烧碱；
S5，热熔搅拌：将邻苯二甲酸二丁酯2-5份、着色剂5-8份、匀染剂8-10份、聚乙烯醇6-10份、丙烯酰胺2-6份、海藻酸3-7份、过氧化苯甲酸六丁酯10-15份、环氟化活性染料30-40份、无水亚硫酸钾5-9份、甲基硅油1-4份、去离子水8-16份、无水亚硫酸钾3-8份、天然染料20-30份加热至200-300℃，搅拌40-60min得到染料；
S6，浸染：将布料先用清水浸泡10-20min，再经过S5制得的染料中浸泡30-40min，浸染过程中，先对染料进行预加热至100-300℃，使用温度计实时监控染缸内的温度，在染缸的侧壁安装多个加热器，及时对温度进行调控，浸染结束使用清水冲去多余染料，最后使用烘干机烘干即可；
S7，拉幅：将S6得到的布料经过布铗拉幅机拉幅处理，可将植物拉至需要的宽度，同时进行热成型，最终得到梭织布。
5.根据权利要求4所述的一种梭织布印染工艺，其特征在于，在S5中，所述搅拌的转速控制在30r/s。
6.根据权利要求4所述的一种梭织布印染工艺，其特征在于，所述热熔搅拌过程中，原料的放入顺序为：先放入邻苯二甲酸二丁酯、聚乙烯醇、丙烯酰胺、海藻酸、过氧化苯甲酸六丁酯、无水亚硫酸钾、甲基硅油、去离子水、无水亚硫酸钾、天然染料，再注入环氟化活性染料，最终再注入着色剂与匀染剂。
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CN104358000A (zh) * 2014-09-30 2015-02-18 福建泉州市健凯服饰有限公司 一种竹炭纤维纺织面料的加工方法
CN104452349A (zh) * 2014-12-24 2015-03-25 常熟市淼泉盛达助剂厂 高温匀染剂
CN105603776A (zh) * 2015-10-30 2016-05-25 无锡市长安曙光手套厂 一种活性染料的配方
CN106884342A (zh) * 2017-03-24 2017-06-23 合肥云都棉花有限公司 一种纺织面料用染色剂及其染色方法
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CN101082154A (zh) * 2006-05-31 2007-12-05 山东理工大学 聚乳酸纤维/棉混纺梭织布的染色工艺
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