CN111840124A

CN111840124A - Oligopeptide water-sensitive skin beautifying mask, essence thereof and preparation method of essence

Info

Publication number: CN111840124A
Application number: CN202010769314.3A
Authority: CN
Inventors: 邓超
Original assignee: Guangzhou Lize Cosmetics Co ltd
Current assignee: Guangzhou Lize Cosmetics Co ltd
Priority date: 2020-08-03
Filing date: 2020-08-03
Publication date: 2020-10-30

Abstract

The invention relates to the field of skin care products, in particular to an oligopeptide water-sensitive skin beautifying mask, essence thereof and a preparation method of the essence, wherein the oligopeptide water-sensitive skin beautifying mask mainly comprises the following components: including oligopeptide-1; oligopeptide-2; oligopeptide-3; magnesium gluconate; chicory extract; a thickener; the solvent is the balance, and the preparation method of the oligopeptide water-sensitive skin beautifying mask essence comprises the following steps: step 1), mixing a solvent and a thickening agent, heating to 83-88 ℃, stirring until the thickening agent is completely dissolved, and keeping the temperature at 83-88 ℃ for 28-32 minutes to obtain a first mixture; and 2) cooling the first mixture to 40 ℃ or below, adding magnesium gluconate, a chicory extract, oligopeptide-1, oligopeptide-2 and oligopeptide-5 into the first mixture, and uniformly stirring to obtain the oligopeptide water-sensitive skin beautifying mask essence. The invention has the effect of realizing multiple effects and simultaneously having lower cost.

Description

Oligopeptide water-sensitive skin beautifying mask, essence thereof and preparation method of essence

Technical Field

The invention relates to the technical field of skin care products, in particular to an oligopeptide water-sensitive skin beautifying mask, essence thereof and a preparation method of the essence.

Background

At present, with the improvement of living standard, people have higher requirements on beauty, people have higher and higher attention on skin care, and the mask has relatively excellent whitening, moisturizing and anti-aging effects as a conventional skin care product, is convenient to carry and is deeply loved by consumers.

The existing facial mask temporarily isolates the outside air and the pollution in the air by using a short time of covering the facial mask, so that the temperature of the skin is increased, pores of the skin are expanded, secretion and metabolism of sweat glands are promoted, the oxygen content of the skin is increased, metabolic products of epidermal cells and accumulated grease substances are favorably discharged, and the moisture in the facial mask permeates into the horny layer of the skin to ensure that the skin becomes soft and elastic.

The oligopeptide is one of polypeptides, is a peptide with the number of amino acids less than 10, has the molecular weight generally below 1000 daltons, is also called as small molecule active peptide, and is most different from other peptides in that the oligopeptide can be directly absorbed by a human body without digestion, can promote the rapid repair of the damaged part of the epidermis, regulate fibroblast disorder, effectively inhibit scar formation, promote the skin to restore and smooth, help to reconstruct the skin barrier, inhibit the generation of melanin, lighten pigmentation and enhance the capillary blood circulation of the skin, so that the damaged skin is restored and is in a smooth and transparent state, and therefore, the oligopeptide is very suitable for being used in skin care products.

As people are exposed to ultraviolet rays for a longer time, the skin color tends to be darker as the content of melanin in the skin is higher, but when the melanin is excessively produced, hyperpigmentation is easily caused, so that the skin is easily spotted, and therefore, the skin abnormal pigmentation and hyperpigmentation need to be improved to make the skin white and bright.

The above prior art solutions have the following drawbacks:

however, in order to make the skin care product have a whitening effect, components having a whitening effect, such as ascorbic acid, kojic acid, tartaric acid, nicotinamide, and the like, are usually added to the skin care product, however, most products having a whitening effect have a problem of great irritation, are particularly not suitable for people with sensitive skin, and limit the application range of the products, so that there is room for improvement.

Disclosure of Invention

Aiming at the defects in the prior art, the invention aims to provide the oligopeptide water-sensitive skin beautifying mask essence which has the effects of better efficacy and lower irritation.

Aiming at the defects in the prior art, the invention also aims to provide a preparation method of the oligopeptide water-sensitive skin-beautifying mask essence, which has the effect of preventing active ingredients of all components from being damaged easily.

Aiming at the defects in the prior art, the invention also aims to provide the oligopeptide water-sensitive skin-beautifying mask which has the effect of facilitating the skin to absorb the oligopeptide water-sensitive skin-beautifying mask essence.

The above object of the present invention is achieved by the following technical solutions:

the oligopeptide water-sensitive skin beautifying mask essence mainly comprises the following components in percentage by mass:

the total mass percentage is 100 percent.

By adopting the technical scheme, the chicory extract is added, so that the chicory extract can effectively remove free radicals, has a good antioxidant effect and a good anti-inflammatory effect, and can promote wound healing.

By adding the magnesium gluconate, the magnesium gluconate can supplement energy for cells, improve the cell metabolism and promote the absorption and utilization of other active substances, and is beneficial to keeping the skin healthy;

by adding oligopeptide-1, the oligopeptide-1 can not only reduce the loss of collagen, but also promote the generation of elastin and collagen, thereby improving relaxation, helping the repair of damaged cells, improving cell metabolism, helping to remove free radicals harmful to human bodies and reducing pigmentation;

by adding the oligopeptide-2, the oligopeptide-2 can easily enter a basal layer through a channel of the skin, can promote the generation of collagen and elastic fibers, help the skin to recover elasticity, improve the water retention capacity of the horny layer of the skin, increase the water content between the horny layers of the skin and further enhance the barrier function of the epidermis;

by adding oligopeptide-5, oligopeptide-5 can specifically stimulate the metabolism of epithelial cells, repair cuticle, increase the thickness of the cuticle, and enhance the activity of collagen and elastin, thereby promoting wound healing;

by adding the thickening agent, the thickening agent can effectively improve the consistency of the oligopeptide water-sensitive skin beautifying mask essence, reduce the fluidity of the product, and ensure that the product is not easy to drip, thereby reducing the waste of the product;

the chicory extract and the magnesium gluconate extract are added, so that a good whitening effect is shown after the chicory extract and the magnesium gluconate extract are mixed, the content of melanin in the skin can be reduced after the oligopeptide-1, the oligopeptide-2 and the oligopeptide-5 are used in a matching way, so that the whitening effect is further improved, and a good synergistic effect is achieved, so that the skin is white and transparent, and meanwhile, the skin is mild due to the fact that the chicory extract, the magnesium gluconate, the oligopeptide-1, the oligopeptide-2 and the oligopeptide-5 are low in irritation after being used in a matching way;

the thickening agent can adopt carbomer, xanthan gum, polyacrylic acid, cyclopentadimethylsiloxane and the like, and the carbomer, the xanthan gum, the polyacrylic acid and the cyclopentadimethylsiloxane are used as the thickening agent, so that the thickening effect of the mask essence is better, and skin irritation is not easily caused.

The present invention in a preferred example may be further configured to: the oligopeptide water-sensitive skin beautifying mask essence further comprises the following components in percentage by mass:

0.05 to 0.2 percent of the broccoli extract;

0.2% -0.8% of soluble collagen cross-linked polymer;

0.005-0.02% of dendrobium officinale stem extract;

0.01-0.03% of dendrobium officinale extract;

0.01 to 0.08 percent of the Uncaria tomentosa extract.

By adopting the technical scheme, the gelidium amansii extract is added, contains various trace elements required by a human body, has a good moisturizing effect, and can also perform effective oxidation resistance, so that the skin is cared;

by adding the soluble collagen cross-linked polymer, a layer of stable water-retaining gel film can be formed on the surface of the skin by the high molecular component of the soluble collagen cross-linked polymer, the water content of the skin can be increased, the small molecular component can penetrate below the horny layer of the skin to form a water-retaining barrier, the water loss of the dermis layer is prevented, and the dual effects of retaining moisture and retaining water are achieved;

by adding the dendrobium officinale stem extract, the dendrobium officinale stem extract contains rich dendrobium officinale polyphenol and dendrobium officinale polysaccharide, so that the hydration capability of skin can be effectively improved, the skin barrier can be repaired, free radicals can be eliminated, and the dendrobium officinale stem extract has better oxidation resistance;

by adding the dendrobium officinale extract, the dendrobium officinale extract can promote the expression of aquaporin AQP-3, so that the hydration capacity of skin is improved, the moisture of skin tissue cells is increased, and the dendrobium officinale extract has important significance for repairing and moisturizing the barrier of epidermis;

by adding the Uncaria tomentosa extract, the Uncaria tomentosa extract can reduce the content of intermediate glycosylation products and advanced glycosylation end products, thereby improving dark yellow skin color, reducing the solidification of collagen fibers and enabling cells to be rich in elasticity.

0.01-0.05% of sargassum blunt extract;

0.05% -0.2% of Fucus serratus extract;

0.02% -0.08% of Chondrus crispus extract.

By adopting the technical scheme, the sargassum blunt extract can remove free radicals, has oxidation resistance, has a good promoting effect on the activity of fibroblast cells, and can promote the synthesis of hyaluronic acid, thereby helping skin to moisturize;

by adding the fucus rudis extract, the fucus rudis extract can inhibit the activity of elastase, so that elastin is not easy to inactivate, free radicals can be removed, and a better antioxidant effect is achieved;

by adding Chondrus crispus extract, the Chondrus crispus extract can increase the amount of protein and oxygen required for synthesizing protein membranous structure on skin surface, thereby promoting the formation of membranous structure, increasing skin moisture, and improving rough skin.

0.58% -1.82% of a skin conditioner;

the skin conditioner comprises one or more of creatine, caprylyl hydroximic acid, p-hydroxyacetophenone, sclerotium rolfsii gum, 1, 2-pentanediol and glyceryl caprylate.

By adopting the technical scheme, the creatine is added, so that the skin aging and damage caused by ultraviolet irradiation can be effectively prevented and treated, the skin regeneration is promoted, the skin dryness can be prevented, the pain and the itch of sensitive skin can be relieved, and the damaged skin can be quickly repaired;

by adding the caprylyl hydroximic acid, the caprylyl hydroximic acid has better inhibition effect on the growth and reproduction of bacteria, so that the content of bacteria in a product is reduced, and the caprylyl hydroximic acid has stronger stability, can stably play the antibacterial effect and is not easily influenced by other substances;

by adding the p-hydroxyacetophenone, the p-hydroxyacetophenone has better oxidation resistance and certain inhibition effect on the growth of bacteria, thereby being beneficial to prolonging the service life of the product;

by adding the sclerotium rolfsii gum, the sclerotium rolfsii gum has good biological activity, is beneficial to promoting wound healing, can increase lipid of an epidermal barrier, promotes the integrity of a stratum corneum structure, enables the skin to be smoother, has good film forming property, is beneficial to forming a water-retaining and water-locking layer, and retains water in the skin;

through adding the 1, 2-pentanediol, the 1, 2-pentanediol can better lock water, has better moisture retention and can also inhibit the growth of bacteria to a certain extent, thereby endowing the product with an antibacterial effect;

the short lipophilic carbon chain in the glyceryl caprylate permeates into and is adsorbed on the lipid part of human, other hydrophilic groups can better preserve moisture in the stratum corneum, and the glyceryl caprylate has better esterification effect, can convey and retain oily components on the surface layer of the skin, so that the water in the skin is not easy to lose.

The present invention in a preferred example may be further configured to: the skin conditioner comprises the following components in percentage by mass:

0.2% -0.6% of creatine;

0.1% -0.3% of caprylyl hydroximic acid;

0.1 to 0.3 percent of p-hydroxyacetophenone;

sclerotium rolfsii gum 0.08% -0.12%;

0.05% -0.3% of 1, 2-pentanediol;

0.05% -0.2% of glyceryl caprylate.

By adopting the technical scheme, the components are matched in a specific proportion, so that the skin conditioning effect of the components is better, the skin is favorably cared better, and the skin is helped to recover health quickly.

6.11 to 14.6 percent of humectant;

the humectant comprises one or more of hyaluronic acid, glycerol, 1, 3-propylene glycol and butanediol.

By adopting the technical scheme, the moisturizing agent can enhance the moisturizing effect of the skin and slow down the water loss speed in the skin by adding the moisturizing agent, so that the water in the skin is not easy to lose, and the skin is kept moist.

The present invention in a preferred example may be further configured to: the humectant consists of the following components in percentage by mass:

0.01 to 0.1 percent of hyaluronic acid;

2% -6% of glycerol;

4% -8% of 1, 3-propylene glycol;

0.1 to 0.5 percent of butanediol.

The components are matched in a specific proportion, so that the moisturizing effect of the product is better, the skin can be kept in a relatively wet state within a certain time, and the skin is effectively cared.

The invention also provides an oligopeptide water-sensitive skin-beautifying mask which comprises the following components in parts by weight: the oligopeptide water-sensitive skin-beautifying facial mask essence is soaked on the facial mask paper.

By adopting the technical scheme, through above-mentioned oligopeptide water-sensitive beautiful skin facial mask essence is soaked on the facial mask paper for oligopeptide water-sensitive beautiful skin facial mask has the function of oligopeptide water-sensitive beautiful skin facial mask essence, and when oligopeptide water-sensitive beautiful skin facial mask is applied on the face, along with the temperature rise of people's face, oligopeptide water-sensitive beautiful skin facial mask essence more easily sees through the skin, makes things convenient for the absorption of skin to oligopeptide water-sensitive beautiful skin facial mask essence, makes the effect of oligopeptide water-sensitive beautiful skin facial mask essence better.

The present invention in a preferred example may be further configured to: the preparation method of the oligopeptide water-sensitive skin beautifying mask essence comprises the following steps:

step 1), mixing a solvent and a thickening agent, heating to 83-88 ℃, stirring until the thickening agent is completely dissolved, and keeping the temperature at 83-88 ℃ for 28-32 minutes to obtain a first mixture;

and 2) cooling the first mixture to 40 ℃ or below, adding magnesium gluconate, a chicory extract, oligopeptide-1, oligopeptide-2 and oligopeptide-5 into the first mixture, and uniformly stirring to obtain the oligopeptide water-sensitive skin beautifying mask essence.

By adopting the technical scheme, the solvent and the thickening agent are mixed, then heated to 83-88 ℃, and stirred until the thickening agent is completely dissolved, so that the thickening agent is gradually stirred to be dissolved in the temperature rise process of the solvent, and the thickening agent is gradually dispersed in the solvent, and the dispersing effect of the thickening agent in the solvent is better;

by keeping the temperature of 83-88 ℃ for 28-32 minutes, the thermal motion of molecules is violent at the temperature of 83-88 ℃, so that air molecules in the solvent easily overflow from the solvent, and the air content in the solvent is reduced;

the first mixture is cooled to 40 ℃ or below, then the magnesium gluconate, the chicory extract, the oligopeptide-1, the oligopeptide-2 and the oligopeptide-5 are added into the first mixture, and the mixture is uniformly stirred, so that the active ingredients of the magnesium gluconate, the chicory extract, the oligopeptide-1, the oligopeptide-2 and the oligopeptide-5 are not easily damaged, and a better effect is achieved.

The present invention in a preferred example may be further configured to: in the step 1), adding a dendrobium officinale extract, a dendrobium officinale stem extract, sclerotium rolfsii gum, p-hydroxyacetophenone, glycerol and 1, 3-propylene glycol into a solvent, heating to 83-88 ℃, then adding hyaluronic acid and creatine, and stirring until the hyaluronic acid and creatine are completely dissolved to obtain a first mixture;

in the step 2), the first mixture is also added with agar-agar extract, soluble collagen cross-linked polymer, maltose, Chondrus crispus extract, Uncaria tomentosa extract, Fucus serratus extract, Sargassum blunt extract, caprylyl hydroximic acid, glyceryl caprylate, 1, 2-pentanediol and butanediol, and is stirred uniformly.

By adopting the technical scheme, the dendrobium officinale extract, the dendrobium officinale stem extract, the sclerotium rolfsii gum, the p-hydroxyacetophenone, the glycerol and the 1, 3-propylene glycol are added into the solvent, so that the dendrobium officinale stem extract, the sclerotium rolfsii gum, the p-hydroxyacetophenone, the glycerol and the 1, 3-propylene glycol are dissolved in the solvent along with the rise of temperature, and the dispersing effect of each component is improved;

heating to 83-88 ℃, then adding hyaluronic acid and creatine, and stirring until the hyaluronic acid and creatine are completely dissolved, so that the hyaluronic acid and creatine are quickly dissolved in the solvent at 83-88 ℃, and the dispersion effect of the hyaluronic acid and creatine in the solvent is better due to more violent molecular thermal motion;

the agar-like extract, the soluble collagen cross-linked polymer, maltose, the Chondrus crispus extract, the Uncaria tomentosa extract, the Fucus serratus extract, the Sargassum blumea extract, the caprylyl hydroximic acid, the glyceryl caprylate, the 1, 2-pentanediol and the butanediol are added into the first mixture and uniformly stirred, so that the effective components of the components are not easily damaged and the components can better exert the respective effects because the agar-like extract, the soluble collagen cross-linked polymer, the maltose, the Chondrus crispus extract, the Uncaria tomentosa extract, the Fucus serratus extract, the Sargassum blumea extract, the caprylyl hydroximic acid, the glyceryl caprylate, the 1, 2-pentanediol and the butanediol are added at the temperature of 40 ℃ or below.

In summary, the invention includes at least one of the following beneficial technical effects:

1. the chicory extract, the magnesium gluconate, the oligopeptide-1, the oligopeptide-2 and the oligopeptide-5 are added, the chicory extract and the magnesium gluconate extract are mixed to show better whitening effect, the oligopeptide-1, the oligopeptide-2 and the oligopeptide-5 are used in a matching way to reduce the content of melanin in the skin, and have better synergistic effect, so that the skin is white and transparent;

2. by adding the agar-agar extract, the soluble collagen cross-linked polymer, the dendrobium officinale extract, the dendrobium officinale stem extract and the uncinata extract, the moisture content of skin can be increased, the skin moisturizing effect is good, effective antioxidation can be performed, and the skin surface barrier repair is accelerated, so that the stimulation of the external environment is resisted; thereby caring the skin;

3. by adding the skin conditioner, the skin conditioning effect of each component is better, the skin is favorably cared better, and the skin is helped to recover health quickly.

Drawings

Fig. 1 is a flow chart illustrating a preparation method of the oligopeptide water-sensitive skin beautifying mask essence.

Detailed Description

The present invention will be described in further detail with reference to the accompanying drawings.

In the following examples and comparative examples, the information on the source of each raw material is shown in Table 1.

TABLE 1

Examples 1 to 3

An oligopeptide water-sensitive skin beautifying mask essence comprises the following components:

magnesium gluconate, chicory extract, oligopeptide-1, oligopeptide-2, oligopeptide-3, thickening agent and solvent.

The thickening agent is acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer;

the solvent is water.

In examples 1-3, the amounts (in Kg) of each component added are specified in Table 2

TABLE 2

Referring to fig. 1, the method for preparing the oligopeptide water-sensitive skin beautifying mask essence of embodiments 1 to 3 includes the following steps:

step 1), adding water and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer into a first stirring kettle at a rotating speed of 60r/min, heating to 85 ℃ while stirring, continuously stirring until the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is completely dissolved, and preserving heat at the temperature of 85 ℃ for 30min to obtain a first mixture;

and 2) cooling the first mixture to 40 ℃, adding magnesium gluconate, the chicory extract, oligopeptide-1, oligopeptide-2 and oligopeptide-5 into the first mixture, stirring for 3min at the rotation speed of 60r/min, and uniformly stirring to obtain the oligopeptide water-sensitive skin beautifying mask essence.

Example 4

Compared with example 2, the difference is only that:

in the step 1), water and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer are mixed and heated to 88 ℃, the mixture is continuously stirred until the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer is completely dissolved, and then the temperature is kept at 88 ℃ for 32 min.

In step 2), the first mixture was cooled to 39 ℃.

Example 5

Compared with example 2, the difference is only that:

in the step 1), water and acrylic acid (ester)/C10-30 alkanol acrylate crosslinked polymer are mixed and heated to 83 ℃, the mixture is continuously stirred until the acrylic acid (ester)/C10-30 alkanol acrylate crosslinked polymer is completely dissolved, and the temperature is kept at 83 ℃ for 28 min.

In step 2), the first mixture was cooled to 38 ℃.

Examples 6 to 8

Compared with example 2, the difference is only that:

the oligopeptide water-sensitive skin beautifying mask essence further comprises the following components:

herba Lysimachiae, soluble collagen cross-linked polymer, caulis Dendrobii extract, herba Dendrobii extract, and herba Gelsemii Elegantis extract.

In examples 6 to 8, the amounts (in Kg) of the respective components added are specified in Table 3

TABLE 3

Adding the dendrobium officinale stem extract and the dendrobium officinale extract in the step 1), the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and water into a first stirring kettle, and uniformly stirring.

The Eucheuma Gelatinosum extract, soluble collagen cross-linked polymer, and Harpagophytum procumbens extract in step 2) are added to the first mixture together with magnesium gluconate, herba Cichorii extract, oligopeptide-1, oligopeptide-2, and oligopeptide-5, and stirred uniformly.

Examples 9 to 11

Compared with example 2, the difference is only that:

sargassum fusiforme extract, Fucus serratus extract, Chondrus crispus extract.

In examples 9 to 11, the amounts (in Kg) of the respective components added are specified in Table 4

TABLE 4

Adding the extract of Sargassum Blumeae Balsamiferae, the extract of Fucus serratus, and the extract of Chondrus crispus in step 2) together with magnesium gluconate, herba Cichorii extract, oligopeptide-1, oligopeptide-2, and oligopeptide-5 into the first mixture, and stirring.

Examples 12 to 14

Compared with example 2, the difference is only that:

a skin conditioner.

The skin conditioner is a compound of creatine, caprylyl hydroximic acid, p-hydroxyacetophenone, sclerotium rolfsii gum, 1, 2-pentanediol and glyceryl caprylate.

In examples 12 to 14, the amounts (in Kg) of the respective components added are specified in Table 5

TABLE 5

Adding the sclerotium rolfsii gum and the p-hydroxyacetophenone in the step 1) together with the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and water into a first stirring kettle, uniformly stirring, heating to 85 ℃, then adding creatine, stirring at the rotating speed of 60r/min for 3min, and uniformly stirring.

Octanoyl hydroxamic acid, 1, 2-pentanediol, glyceryl caprylate are added to the first mixture in step 2) together with magnesium gluconate, chicory extract, oligopeptide-1, oligopeptide-2 and oligopeptide-5, and stirred well.

Examples 15 to 17

Compared with example 2, the difference is only that:

a humectant.

The humectant comprises hyaluronic acid, glycerol, 1, 3-propylene glycol and butanediol.

In examples 15 to 17, the amounts (in Kg) of the respective components added are specified in Table 6

TABLE 6

Adding glycerol, 1, 3-propylene glycol, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and water into a first stirring kettle in the step 1), uniformly stirring, heating to 85 ℃, then adding hyaluronic acid, stirring for 3min at the rotating speed of 60r/min, and uniformly stirring.

Adding butanediol in step 2) together with magnesium gluconate, herba Cichorii extract, oligopeptide-1, oligopeptide-2 and oligopeptide-5 into the first mixture, and stirring.

Examples 18 to 20

Compared with example 2, the difference is only that:

pH regulator, solubilizer, chelating agent, and aromatic.

The pH regulator is arginine;

the solubilizer is PEG-40 hydrogenated castor oil;

the chelating agent is EDTA disodium;

the aromatic is essence.

In examples 18 to 20, the amounts (in Kg) of the respective components added are specified in Table 7

TABLE 7

Adding the EDTA disodium in the step 1), acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and water into a first stirring kettle, uniformly stirring, preserving heat at 85 ℃ for 30min, then adding arginine, stirring at the rotating speed of 60r/min for 3min, and uniformly stirring.

Firstly, uniformly mixing essence and PEG-40 hydrogenated castor oil, in the step 2), adding magnesium gluconate, a chicory extract, oligopeptide-1, oligopeptide-2 and oligopeptide-5 into the first mixture, uniformly stirring, then adding the mixture of essence and PEG-40 hydrogenated castor oil, rotating at the speed of 60r/min, stirring for 3min, and uniformly stirring.

Examples 21 to 23

Compared with example 2, the difference is only that:

herba Dendrobii extract, herba Dendrobii stem extract, soluble collagen cross-linked polymer, Eucheuma Gelatinosum extract, Sargassum blunt, Fucus serratus extract, Chondrus crispus extract, Hypnea charides extract, skin conditioner, humectant, pH regulator, solubilizer, thickener, chelating agent, and aromatic.

The pH regulator is arginine;

the solubilizer is PEG-40 hydrogenated castor oil;

the chelating agent is EDTA disodium;

the aromatic is essence.

In examples 18 to 20, the amounts (in Kg) of the respective components added are specified in Table 8

TABLE 8

Adding the dendrobium officinale extract, the dendrobium officinale stem extract, the sclerotium rolfsii gum, the p-hydroxyacetophenone, the glycerol, the 1, 3-propylene glycol and the EDTA disodium in the step 1) together with the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and water into a first stirring kettle, uniformly stirring, heating to 85 ℃, then adding the hyaluronic acid and the creatine at the rotating speed of 60r/min, stirring for 3min, uniformly stirring, preserving heat at 85 ℃ for 30min, then adding the arginine at the rotating speed of 60r/min, stirring for 3min, and uniformly stirring.

Firstly, uniformly mixing essence and PEG-40 hydrogenated castor oil, and in the step 2), adding the chicory extract, the gulfweed extract, maltose, the fucus extract, magnesium gluconate, the carrageen crispus extract, the Uncaria tomentosa extract, butanediol, caprylyl hydroxamic acid, 1, 2-pentanediol and glyceryl caprylate into the first mixture together with the magnesium gluconate, the chicory extract, oligopeptide-1, oligopeptide-2 and oligopeptide-5, uniformly stirring, then adding the mixture of the essence and the PEG-40 hydrogenated castor oil, rotating at the speed of 60r/min, stirring for 3min, and uniformly stirring.

Example 24

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence in embodiment 1 is adopted.

Example 25

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence in the embodiment 2 is adopted.

Example 26

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in embodiment 3.

Example 27

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence in embodiment 4 is adopted.

Example 28

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in the embodiment 5.

Example 29

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in the embodiment 6.

Example 30

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence in embodiment 7 is adopted.

Example 31

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in the embodiment 8.

Example 32

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in embodiment 9.

Example 33

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in the embodiment 10.

Example 34

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in embodiment 11.

Example 35

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in the embodiment 12.

Example 36

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in the embodiment 13.

Example 37

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in the embodiment 14.

Example 38

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in the embodiment 15.

Example 39

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in the embodiment 16.

Example 40

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in the embodiment 17.

EXAMPLE 41

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in embodiment 18.

Example 42

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in the embodiment 19.

Example 43

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in the embodiment 20.

Example 44

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in embodiment 21.

Example 45

A facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in embodiment 22.

Example 46

The facial mask comprises facial mask paper, wherein facial mask essence is soaked on the facial mask paper, and in the embodiment, the facial mask essence is the facial mask essence in embodiment 23.

Comparative example 1

Compared with example 2, the difference is only that:

in the step 2), magnesium gluconate, chicory extract, oligopeptide-1, oligopeptide-2 and oligopeptide-5 are replaced by equal amount of water.

Comparative example 2

Compared with example 2, the difference is only that:

in the step 2), magnesium gluconate and chicory extract are replaced by the same amount of water.

Comparative example 3

Compared with example 2, the difference is only that:

in step 2), chicory extract is replaced by equal amount of water.

Comparative example 4

Compared with example 2, the difference is only that:

in step 2), magnesium gluconate is replaced by an equal amount of water.

Experiment 1

Human skin irritation test

The test method comprises the following steps: a patch test method for detecting human safety adopts a 48-hour closed patch test, 135 healthy volunteers are selected and randomly and evenly divided into 27 groups, 5 persons in each group have no allergic history. After cleaning the back of a subject, a spot tester added with the oligopeptide water-sensitive skin beautifying facial mask essence prepared in each embodiment and comparative example is applied to a selected position on the back by using a non-irritating adhesive tape, the patch is uniformly applied to the skin by lightly pressing with fingers after being well adhered for 48 hours, the subject is ordered to keep the spot-adhered part dry within 48 hours, violent exercise, scratching of the spot-adhered part, long-time sunlight irradiation and the like are avoided, the spot-adhered part is removed after 48 hours and dried, the patch disappears after 30 minutes and the like, judgment is carried out under sufficient light, and revisit observation is carried out for 72 hours and 96 hours respectively.

The grading standards of adverse reactions in the skin patch test are shown in Table 9

TABLE 9

The adverse skin reaction results of the oligopeptide water-sensitive skin beautifying mask essence prepared in each example and comparative example are shown in Table 10 and Table 10

According to the data in the table, the skin reactions of all the subjects are negative, which indicates that the essence of the oligopeptide water-sensitive skin-beautifying mask prepared in each example and each comparative example is relatively mild and has small irritation.

Experiment 2

Moisturizing Performance test of facial mask

The detection method comprises the following steps:

1. the constant temperature and humidity chamber was set at 25 ℃ and 75% relative humidity and stabilized for 12 hours.

2. The beaker mouth of each 200mL beaker was sealed with a wrap film, labeled in turn, placed on an electronic balance to weigh and record the data, yielding M1.

3. And (3) removing the seal of the beaker, respectively weighing 20g of the oligopeptide water-sensitive skin beautifying mask essence prepared in the embodiment and the comparative example, uniformly coating the oligopeptide water-sensitive skin beautifying mask essence on the bottom of the beaker, weighing the oligopeptide water-sensitive skin beautifying mask essence together with the corresponding preservative film, and recording data to obtain M2.

4. Placing the beaker into a constant-temperature and constant-humidity box which is stable for 12 hours, taking out the beaker in 4 hours, 8 hours, 12 hours, 16 hours, 20 hours and 24 hours, respectively, sealing the beaker by using preservative film, recording data together with corresponding preservative film weighing capacity to obtain M3, wherein the water loss rate is calculated according to a formula which is as follows: water loss (%) - (M2-M3)/(M2-M1) × 100%. The details of the measured data are shown in Table 11

Experiment 3

Melanin content detection

The test method comprises the following steps: 135 adult volunteers of 20-50 years of age were selected and randomly divided into 27 groups of 5 individuals. The test was carried out using the melanin and heme test probe (mexametemx 18) of the multifunctional skin tester MPA9 from CK company, germany.

After cleaning face, applying the product, adjusting nose, lip, eye, etc., squeezing out air, removing facial mask paper after 15 min, and applying the rest liquid on face for absorption, without cleaning, for 3 times per week for 4 weeks.

Before testing, the tested people need to clean the faces with clean water, wipe the faces clean with facial tissues, sit still for 30 minutes in a constant temperature and humidity laboratory (the temperature is 20 +/-1 ℃ and the humidity is 55 +/-3%), then start testing, a 4 x 4cm area in the middle of the right face of each tested person is selected, the average melanin content of the four corners and the middle of the area is tested by a probe, and then the average melanin content of each group of people is tested according to the method when the oligopeptide water-sensitive skin-beautifying facial mask is used for 3 rd, 6 th, 9 th and 12 th times. A decrease in melanin content indicates efficacy, and an increase or no change in melanin content indicates ineffectiveness. The detection data are shown in Table 12

TABLE 11

TABLE 12

According to the comparison of the data of comparative example 2 and comparative example 1 in tables 11 and 12, the addition of oligopeptide-1, oligopeptide-2 and oligopeptide-5 reduces the water loss rate and melanin content, thus proving that the combination of oligopeptide-1, oligopeptide-2 and oligopeptide-5 has better moisturizing effect and certain whitening effect.

According to the comparison of the data of comparative example 3 and comparative example 2 in tables 11 and 12, the water loss is reduced after the chicory extract is added, and the results prove that the chicory extract is beneficial to improving the moisturizing effect of the product, and the melanin content is not obviously changed, which indicates that the chicory extract has little influence on the melanin content.

As can be seen from comparison of the data of comparative example 4 and comparative example 2 in tables 11 and 12, the change in the water loss ratio was not significant after the addition of the magnesium gluconate extract, which demonstrated that the moisturizing effect of magnesium gluconate was general, the change in the melanin content was small, and the influence of magnesium gluconate on melanin was small.

According to the data comparison between example 25 and comparative examples 3 and 4 in tables 11 and 12, it can be seen that the combination of magnesium gluconate and chicory extract reduces the water loss rate, further improves the moisturizing effect, and significantly reduces the melanin content, thus proving that the combination of magnesium gluconate and chicory extract further reduces the melanin content, and is beneficial to helping the skin to gradually whiten.

As can be seen from comparison of the data of example 25 with examples 27 and 28 in tables 11 and 12, the composition was mixed at a specific temperature and maintained for a specific time, so that the mixing effect of the obtained mask was relatively stable.

According to comparison of data of examples 29 to 31 and example 25 in tables 11 and 12, free radical scavenging rate and mitochondrial activity ratio are significantly improved and water loss rate is further reduced by adding the gelidium amansii extract, the soluble collagen cross-linked polymer, the dendrobium officinale extract, the dendrobium officinale stem extract and the henry sage extract, so that moisturizing capability of the product is improved and melanin content is further reduced, and the gelidium amansii extract, the soluble collagen cross-linked polymer, the dendrobium officinale extract, the dendrobium officinale stem extract and the henry sage extract are proved to have good whitening effect, and thus effects of various efficacies of the mask essence are further improved.

According to the comparison of the data of the examples 32 to 34 and the example 2 in the tables 11 and 12, the water loss rate is further reduced, the moisture retention effect of the product is enhanced, and the change of the melanin content is small by adding the sargassum obtusifolia extract, the fucus serratus extract and the carrageen crispus extract, which shows that the change of the melanin content is not greatly influenced after the sargassum obtusifolia extract, the fucus serratus extract and the carrageen crispus extract are used in combination, so that the efficacy of the mask essence is improved to a certain extent.

According to comparison of data of examples 35 to 37 and example 2 in tables 11 and 12, the radical clearance and the mitochondrial activity are improved to a certain extent by adding the skin conditioner, so that the skin conditioner can improve the antioxidant effect and promote metabolism to a certain extent, the influence of the skin conditioner on the melanin content is small, the influence of the skin conditioner on the melanin of the skin is small, and the comprehensive effect of the mask essence is further improved.

From the comparison of the data of examples 38 to 40 in tables 11 and 12 with that of example 2, it can be seen that the moisturizing effect of the product is improved by adding the moisturizing agent, the melanin content is not greatly changed, and the water loss rate is reduced, but the effect of reducing the melanin content of the skin by helping the skin antioxidant is not significant.

The embodiments of the present invention are preferred embodiments of the present invention, and the scope of the present invention is not limited by these embodiments, so: all equivalent changes made according to the structure, shape and principle of the invention are covered by the protection scope of the invention.

Claims

1. An oligopeptide water-sensitive skin beautifying mask essence is characterized in that: the paint mainly comprises the following components in percentage by mass:

oligopeptide-10.1% -0.5%;

oligopeptide-20.1% -0.3%;

oligopeptide-30.1% -0.3%;

magnesium gluconate 0.01% -0.06%;

chicory extract 0.05% -0.2%;

0.1 to 0.2 percent of thickening agent;

the balance of solvent;

the total mass percentage is 100 percent.

2. The oligopeptide water-sensitive beauty mask essence according to claim 1, which is characterized in that: the oligopeptide water-sensitive skin beautifying mask essence further comprises the following components in percentage by mass:

0.05 to 0.2 percent of the broccoli extract;

0.2% -0.8% of soluble collagen cross-linked polymer;

0.005-0.02% of dendrobium officinale stem extract;

0.01-0.03% of dendrobium officinale extract;

0.01 to 0.08 percent of the Uncaria tomentosa extract.

3. The oligopeptide water-sensitive beauty mask essence according to claim 1, which is characterized in that: the oligopeptide water-sensitive skin beautifying mask essence further comprises the following components in percentage by mass:

0.01-0.05% of sargassum blunt extract;

0.05% -0.2% of Fucus serratus extract;

0.02% -0.08% of Chondrus crispus extract.

4. The oligopeptide water-sensitive beauty mask essence according to claim 1, which is characterized in that: the oligopeptide water-sensitive skin beautifying mask essence further comprises the following components in percentage by mass:

0.58% -1.82% of a skin conditioner;

5. The oligopeptide water-sensitive beauty mask essence according to claim 4, which is characterized in that: the skin conditioner comprises the following components in percentage by mass:

0.2% -0.6% of creatine;

0.1% -0.3% of caprylyl hydroximic acid;

0.1 to 0.3 percent of p-hydroxyacetophenone;

sclerotium rolfsii gum 0.08% -0.12%;

0.05% -0.3% of 1, 2-pentanediol;

0.05% -0.2% of glyceryl caprylate.

6. The oligopeptide water-sensitive beauty mask essence according to claim 1, which is characterized in that: the oligopeptide water-sensitive skin beautifying mask essence further comprises the following components in percentage by mass:

6.11 to 14.6 percent of humectant;

7. The oligopeptide water-sensitive beauty mask essence according to claim 6, which is characterized in that: the humectant comprises the following components in percentage by mass:

0.01 to 0.1 percent of hyaluronic acid;

2% -6% of glycerol;

4% -8% of 1, 3-propylene glycol;

0.1 to 0.5 percent of butanediol.

8. An oligopeptide water-sensitive skin beautifying mask is characterized in that: the oligopeptide water-sensitive skin beautifying mask essence disclosed by any one of claims 1-7 is soaked on the mask paper.

9. The preparation method of the oligopeptide water-sensitive skin beautifying mask essence according to claim 1 is characterized by comprising the following steps: the preparation method of the oligopeptide water-sensitive skin beautifying mask essence comprises the following steps:

10. The preparation method of the oligopeptide water-sensitive beauty mask essence according to claim 8, which is characterized by comprising the following steps: in the step 1), adding a dendrobium officinale extract, a dendrobium officinale stem extract, sclerotium rolfsii gum, p-hydroxyacetophenone, glycerol and 1, 3-propylene glycol into a solvent, heating to 83-88 ℃, then adding hyaluronic acid and creatine, and stirring until the hyaluronic acid and creatine are completely dissolved to obtain a first mixture;