CN111759753A - Mild amino acid facial cleanser and preparation method thereof - Google Patents
Mild amino acid facial cleanser and preparation method thereof Download PDFInfo
- Publication number
- CN111759753A CN111759753A CN202010800083.8A CN202010800083A CN111759753A CN 111759753 A CN111759753 A CN 111759753A CN 202010800083 A CN202010800083 A CN 202010800083A CN 111759753 A CN111759753 A CN 111759753A
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- China
- Prior art keywords
- parts
- amino acid
- facial cleanser
- sodium glutamate
- mild
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- 230000001815 facial effect Effects 0.000 title claims abstract description 43
- 150000001413 amino acids Chemical class 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 235000013923 monosodium glutamate Nutrition 0.000 claims abstract description 61
- 229940073490 sodium glutamate Drugs 0.000 claims abstract description 58
- 229940024606 amino acid Drugs 0.000 claims abstract description 40
- POULHZVOKOAJMA-UHFFFAOYSA-M dodecanoate Chemical compound CCCCCCCCCCCC([O-])=O POULHZVOKOAJMA-UHFFFAOYSA-M 0.000 claims abstract description 26
- 229940070765 laurate Drugs 0.000 claims abstract description 26
- 229940044591 methyl glucose dioleate Drugs 0.000 claims abstract description 24
- FPVVYTCTZKCSOJ-UHFFFAOYSA-N Ethylene glycol distearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCOC(=O)CCCCCCCCCCCCCCCCC FPVVYTCTZKCSOJ-UHFFFAOYSA-N 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 20
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 20
- 150000005846 sugar alcohols Polymers 0.000 claims abstract description 20
- ZAKOWWREFLAJOT-CEFNRUSXSA-N D-alpha-tocopherylacetate Chemical compound CC(=O)OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-CEFNRUSXSA-N 0.000 claims abstract description 18
- 239000000194 fatty acid Substances 0.000 claims abstract description 17
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 16
- 229930195729 fatty acid Natural products 0.000 claims abstract description 16
- 150000004665 fatty acids Chemical class 0.000 claims abstract description 16
- 229940042585 tocopherol acetate Drugs 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 14
- 239000002562 thickening agent Substances 0.000 claims abstract description 14
- 239000002738 chelating agent Substances 0.000 claims abstract description 9
- 229940104256 sodium taurate Drugs 0.000 claims abstract description 7
- GWLWWNLFFNJPDP-UHFFFAOYSA-M sodium;2-aminoethanesulfonate Chemical compound [Na+].NCCS([O-])(=O)=O GWLWWNLFFNJPDP-UHFFFAOYSA-M 0.000 claims abstract description 7
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims description 35
- 229920001577 copolymer Polymers 0.000 claims description 34
- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 claims description 34
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims description 26
- 238000010438 heat treatment Methods 0.000 claims description 26
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 19
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 18
- 150000002148 esters Chemical class 0.000 claims description 18
- YPFDHNVEDLHUCE-UHFFFAOYSA-N 1,3-propanediol Substances OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 claims description 17
- 229940048109 sodium methyl cocoyl taurate Drugs 0.000 claims description 16
- 239000004698 Polyethylene Substances 0.000 claims description 15
- -1 polyethylene Polymers 0.000 claims description 15
- 229920000573 polyethylene Polymers 0.000 claims description 15
- 238000002156 mixing Methods 0.000 claims description 14
- 239000005639 Lauric acid Substances 0.000 claims description 13
- 229940073743 steareth-20 methacrylate Drugs 0.000 claims description 13
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 12
- 239000003755 preservative agent Substances 0.000 claims description 11
- 238000001816 cooling Methods 0.000 claims description 10
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 8
- 230000002335 preservative effect Effects 0.000 claims description 8
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 6
- 235000019437 butane-1,3-diol Nutrition 0.000 claims description 6
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 6
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 claims description 6
- DNIAPMSPPWPWGF-VKHMYHEASA-N (+)-propylene glycol Chemical compound C[C@H](O)CO DNIAPMSPPWPWGF-VKHMYHEASA-N 0.000 claims description 5
- 229940035437 1,3-propanediol Drugs 0.000 claims description 5
- 229920000166 polytrimethylene carbonate Polymers 0.000 claims description 5
- DNIAPMSPPWPWGF-UHFFFAOYSA-N monopropylene glycol Natural products CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 4
- 229920005862 polyol Polymers 0.000 claims description 4
- 150000003077 polyols Chemical class 0.000 claims description 4
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 3
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 3
- 235000021314 Palmitic acid Nutrition 0.000 claims description 3
- 235000021355 Stearic acid Nutrition 0.000 claims description 3
- 229940110830 beheneth-25 methacrylate Drugs 0.000 claims description 3
- 239000003205 fragrance Substances 0.000 claims description 3
- 239000004223 monosodium glutamate Substances 0.000 claims description 3
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 claims description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 3
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 3
- 229960004063 propylene glycol Drugs 0.000 claims description 3
- 239000000600 sorbitol Substances 0.000 claims description 3
- 239000008117 stearic acid Substances 0.000 claims description 3
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 claims description 3
- UEUXEKPTXMALOB-UHFFFAOYSA-J tetrasodium;2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxylatomethyl)amino]acetate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O UEUXEKPTXMALOB-UHFFFAOYSA-J 0.000 claims description 3
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 235000013772 propylene glycol Nutrition 0.000 claims description 2
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims 1
- 235000011187 glycerol Nutrition 0.000 claims 1
- 239000006071 cream Substances 0.000 abstract description 32
- 239000006260 foam Substances 0.000 abstract description 13
- 238000004140 cleaning Methods 0.000 abstract description 6
- 239000002085 irritant Substances 0.000 abstract description 4
- 231100000021 irritant Toxicity 0.000 abstract description 4
- 230000036555 skin type Effects 0.000 abstract description 3
- PXEDJBXQKAGXNJ-QTNFYWBSSA-L disodium L-glutamate Chemical compound [Na+].[Na+].[O-]C(=O)[C@@H](N)CCC([O-])=O PXEDJBXQKAGXNJ-QTNFYWBSSA-L 0.000 abstract 1
- 239000008367 deionised water Substances 0.000 description 12
- 229910021641 deionized water Inorganic materials 0.000 description 12
- 230000000052 comparative effect Effects 0.000 description 10
- 230000006872 improvement Effects 0.000 description 10
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- 239000004094 surface-active agent Substances 0.000 description 5
- 230000009044 synergistic interaction Effects 0.000 description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 3
- 239000002537 cosmetic Substances 0.000 description 3
- 238000005187 foaming Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 230000008719 thickening Effects 0.000 description 3
- LXAHHHIGZXPRKQ-UHFFFAOYSA-N 5-fluoro-2-methylpyridine Chemical compound CC1=CC=C(F)C=N1 LXAHHHIGZXPRKQ-UHFFFAOYSA-N 0.000 description 2
- 239000013531 ACULYN rheology modifier Substances 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- ZAKOWWREFLAJOT-UHFFFAOYSA-N d-alpha-Tocopheryl acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-UHFFFAOYSA-N 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- FOYKKGHVWRFIBD-UHFFFAOYSA-N gamma-tocopherol acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 FOYKKGHVWRFIBD-UHFFFAOYSA-N 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- IWIUXJGIDSGWDN-UQKRIMTDSA-M sodium;(2s)-2-(dodecanoylamino)pentanedioate;hydron Chemical compound [Na+].CCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CCC(O)=O IWIUXJGIDSGWDN-UQKRIMTDSA-M 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- 238000004383 yellowing Methods 0.000 description 2
- 229940058015 1,3-butylene glycol Drugs 0.000 description 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical group OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 229960001484 edetic acid Drugs 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 238000006864 oxidative decomposition reaction Methods 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 210000002374 sebum Anatomy 0.000 description 1
- 238000011895 specific detection Methods 0.000 description 1
- 238000007619 statistical method Methods 0.000 description 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a mild amino acid cleansing cream and a preparation method thereof, and the mild amino acid cleansing cream comprises the following raw materials in parts by weight: 15-35 parts of N-lauroyl sodium glutamate, 10-40 parts of polyhydric alcohol, 1-10 parts of methyl cocoyl sodium taurate, 2-10 parts of sodium glutamate, 1-5 parts of polyethylene glycol, 1-5 parts of thickening agent, 1-5 parts of fatty acid, 1-5 parts of ethylene glycol distearate, 1-5 parts of polyglycerol-10 laurate, 0.1-1 part of PEG-120 methyl glucose dioleate, 0.1-1 part of tocopherol acetate, 0.1-0.5 part of chelating agent and 10-70 parts of water. The amino acid facial cleanser disclosed by the invention is fine and smooth in cream body, rich in smooth foam, excellent in stability, mild in use, safe and non-irritant, suitable for various skin types and strong in cleaning performance, and the pH value is 5.3-5.8 and is close to that of human skin.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a mild amino acid facial cleansing cream and a preparation method thereof.
Background
Skin cleansing is a necessary process for skin care, and is mainly aimed at removing dust, residues of cosmetic, sebum, cuticle fragments and their oxidative decomposition products, etc. from the surface of skin, and maintaining the normal physiological state of skin. With the improvement of the living standard of people and the progress of modern cosmetic science and technology, more efficient, safe and mild facial cleanser products gradually enter the mass market, and amino acid type facial cleansers are the most representative products.
At present, the products of the amino acid facial cleanser sold in the market are mostly milky or cream-shaped, are prepared by compounding N-fatty acid amino acid with other conventional surfactants, have small and unstable foam amount and are not mild enough to be used, and cannot be suitable for all skin types.
Disclosure of Invention
In view of the above, the invention aims to provide a mild amino acid facial cleanser and a preparation method thereof, and the mild amino acid facial cleanser is prepared by compounding and synergizing N-lauroyl sodium glutamate, polyhydric alcohol, methyl cocoyl sodium taurate, sodium glutamate, polyethylene glycol, a thickening agent, fatty acid, ethylene glycol distearate, polyglycerol-10 laurate, PEG-120 methyl glucose dioleate and tocopherol acetate, so that the obtained amino acid facial cleanser is fine and smooth in cream body, rich in smooth foam and excellent in stability, the pH value is 5.3-5.8, is close to the pH value of human skin, is mild in use, safe and non-irritant, is suitable for various skin types, and is strong in cleaning performance.
In order to achieve the above purpose, the invention provides the following technical scheme:
the mild amino acid facial cleanser comprises the following raw materials in parts by weight: 15-35 parts of N-lauroyl sodium glutamate, 10-40 parts of polyhydric alcohol, 1-10 parts of methyl cocoyl sodium taurate, 2-10 parts of sodium glutamate, 1-5 parts of polyethylene glycol, 1-5 parts of thickening agent, 1-5 parts of fatty acid, 1-5 parts of ethylene glycol distearate, 1-5 parts of polyglycerol-10 laurate, 0.1-1 part of PEG-120 methyl glucose dioleate, 0.1-1 part of tocopherol acetate, 0.1-0.5 part of chelating agent and 10-70 parts of water.
As a further improvement of the above technical solution, the polyhydric alcohol comprises at least one of glycerol, 1, 2-propylene glycol, 70% sorbitol, 1, 3-butylene glycol and 1, 3-propylene glycol;
preferably, the polyol is 1, 3-butanediol and/or 1, 3-propanediol.
As a further improvement of the above technical solution, the thickener comprises an acrylate copolymer;
preferably, the acrylate copolymer comprises at least one of an acrylic acid (ester)/steareth-20 methacrylate copolymer, an acrylic acid (ester)/palmitoeth-25 acrylate copolymer, and an acrylic acid (ester)/beheneth-25 methacrylate copolymer.
As a further improvement of the above technical solution, the polyethylene glycol comprises at least one of polyethylene glycol-6, polyethylene glycol-8 and polyethylene glycol-32;
as a further improvement of the technical scheme, the sodium glutamate comprises at least one of anhydrous sodium glutamate and monosodium glutamate.
As a further improvement of the above technical solution, the chelating agent comprises at least one of disodium EDTA and tetrasodium EDTA;
as a further improvement of the above technical solution, the fatty acid includes at least one of lauric acid, myristic acid, palmitic acid, and stearic acid.
As a further improvement of the above technical solution, the raw materials further comprise: preservatives and/or fragrances.
As a further improvement of the technical scheme, the using amount of the preservative is 0.1-1 part, and the using amount of the essence is 0.1-1 part.
A preparation method of a mild amino acid facial cleanser is disclosed, wherein the mild amino acid facial cleanser is the mild amino acid facial cleanser; the preparation method comprises the following steps:
mixing N-lauroyl sodium glutamate, polyhydric alcohol and water, and heating to 70-85 ℃ to obtain solution A;
mixing the solution A, sodium methyl cocoyl taurate, sodium glutamate, polyethylene glycol, fatty acid, ethylene glycol distearate, polyglycerol-10 laurate and PEG-120 methyl glucose dioleate, heating to 70-85 ℃, then cooling to 4555 ℃, adding the rest of the components and mixing.
As a further improvement of the above technical solution, the preparation method further comprises: and keeping the temperature of the solution A at 70-85 ℃, and stirring until the solution surface is free from bubbles.
The invention has the beneficial effects that:
(1) the invention compounds N-lauroyl sodium glutamate, polyalcohol, methyl cocoyl sodium taurate, sodium glutamate, polyethylene glycol, acrylate copolymer thickener, fatty acid, ethylene glycol distearate, polyglycerol-10 laurate, PEG-120 methyl glucose dioleate and tocopherol acetate for synergistic interaction, specifically utilizes the synergistic interaction of amino acid surfactant N-lauroyl sodium glutamate and sodium glutamate to form a stable crystalline thickening system, combines with acrylate copolymer and PEG-120 methyl glucose dioleate to further increase the heat resistance stability of the formula, adds polyglycerol-10 laurate to make up the defects of unstable foam and quick defoaming of the N-lauroyl sodium glutamate, ensures that the product foam is more durable and soft, adds tocopherol acetate, the yellowing phenomenon of the formula due to high temperature or long-term storage is obviously improved; the obtained amino acid facial cleanser is mild in use, fine and smooth in cream body, smooth and rich in foam, excellent in stability, safe and non-irritant, and strong in cleaning performance, and the pH value of the amino acid facial cleanser is 5.3-5.8 and is close to that of human skin.
(2) The composition disclosed by the invention is simple in preparation method, low in preparation cost, wide in market prospect and suitable for large-scale production.
In order to make the aforementioned and other objects, features and advantages of the invention more comprehensible, preferred embodiments accompanied with figures are described in detail below.
Detailed Description
In the following description, numerous specific details are set forth in order to provide a thorough understanding of the present invention.
This invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein, but rather should be construed as broadly as the present invention is capable of modification in various respects, all without departing from the spirit and scope of the present invention.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. In case of conflict, the present specification, including definitions, will control.
The terms as used herein:
"prepared from … …" is synonymous with "comprising". The terms "comprises," "comprising," "includes," "including," "has," "having," "contains," "containing," or any other variation thereof, as used herein, are intended to cover a non-exclusive inclusion. For example, a composition, process, method, article, or apparatus that comprises a list of elements is not necessarily limited to only those elements but may include other elements not expressly listed or inherent to such composition, process, method, article, or apparatus.
The conjunction "consisting of … …" excludes any unspecified elements, steps or components. If used in a claim, the phrase is intended to claim as closed, meaning that it does not contain materials other than those described, except for the conventional impurities associated therewith. When the phrase "consisting of … …" appears in a clause of the subject matter of the claims rather than immediately after the subject matter, it defines only the elements described in the clause; other elements are not excluded from the claims as a whole.
When an amount, concentration, or other value or parameter is expressed as a range, preferred range, or as a range of upper preferable values and lower preferable values, this is to be understood as specifically disclosing all ranges formed from any pair of any upper range limit or preferred value and any lower range limit or preferred value, regardless of whether ranges are separately disclosed. For example, when the range "1 ~ 5" is disclosed, the ranges described should be construed to include the ranges "1 ~ 4", "1 ~ 3", "1 ~ 2 and 4 ~ 5", "1 ~ 3 and 5", and the like. When a range of values is described herein, unless otherwise stated, the range is intended to include the endpoints thereof and all integers and fractions within the range.
In these examples, the parts and percentages are by mass unless otherwise indicated.
"part by mass" means a basic unit of measure indicating a mass ratio of a plurality of components, and 1 part may represent any unit mass, for example, 1g or 2.689 g. If we say that the part by mass of the component A is a part by mass and the part by mass of the component B is B part by mass, the ratio of the part by mass of the component A to the part by mass of the component B is a: b. alternatively, the mass of the A component is aK and the mass of the B component is bK (K is an arbitrary number, and represents a multiple factor). It is unmistakable that, unlike the parts by mass, the sum of the parts by mass of all the components is not limited to 100 parts.
"and/or" is used to indicate that one or both of the illustrated conditions may occur, e.g., a and/or B includes (a and B) and (a or B).
The invention provides mild amino acid facial cleansing cream which comprises the following raw materials: sodium N-lauroyl glutamate, polyhydric alcohol, sodium methylcocoyltaurate, sodium glutamate, polyethylene glycol, thickener, fatty acid, ethylene glycol distearate, polyglycerol-10 laurate, PEG-120 methylglucdioleate, tocopheryl acetate, chelating agent, and water.
Further, the dosage of each raw material is as follows: 15-35 parts of N-lauroyl sodium glutamate, 10-40 parts of polyhydric alcohol, 1-10 parts of methyl cocoyl sodium taurate, 2-10 parts of sodium glutamate, 1-5 parts of polyethylene glycol, 1-5 parts of thickening agent, 1-5 parts of fatty acid, 1-5 parts of ethylene glycol distearate, 1-5 parts of polyglycerol-10 laurate, 0.1-1 part of PEG-120 methyl glucose dioleate, 0.1-1 part of tocopherol acetate, 0.1-0.5 part of chelating agent and 10-70 parts of water.
The sodium N-lauroyl glutamate has foaming and cleaning effects; the invention mainly forms the cleansing cream by crystallization of the amino acid surfactant, and better separates out crystals of the N-lauroyl sodium glutamate by adding the sodium glutamate.
The polyhydric alcohol mainly plays a role in moisturizing in the invention; optionally, the polyol comprises at least one of glycerol, 1, 2-propanediol, 70% sorbitol, 1, 3-butanediol, and 1, 3-propanediol; preferably, the 1, 3-butanediol and/or 1, 3-propanediol is selected as the polyhydric alcohol, so that the prepared cleansing cream has the advantages of optimal cleansing cream temperature and stability, lowest requirements on production equipment and best stability.
The heat resistance of the cleansing cream can be improved by adding polyethylene glycol; preferably, the polyethylene glycol comprises at least one of polyethylene glycol-6, polyethylene glycol-8 and polyethylene glycol-32.
The sodium methyl cocoyl taurate can effectively assist the forming of the cleansing cream and increase the foam quantity.
The above fatty acids are effective in the present invention to synergistically contribute to an increase in the amount and the feeling of softness of the foam of the resulting cleansing cream.
The ethylene glycol distearate can effectively improve the appearance of the paste in a synergistic manner and also has the function of increasing the consistency;
the polyglycerol-10 laurate is effective in synergistically improving the dry and astringent feeling of the skin after washing and reducing the irritation of the surfactant.
Further, the thickener includes an acrylate copolymer thickener, which is weakly acidic, preferably, the acrylate copolymer includes at least one of an acrylate/steareth-20 methacrylate copolymer (e.g., ACULYN 88POLMER, available from dow chemical), an acrylate/palmitoeth-25 acrylate copolymer (e.g., Synthalen W2000, available from 3V sigma s.p.a, italy), and an acrylate/beheneth-25 methacrylate copolymer (e.g., noveth L-10, available from luobu); the three acrylic acid (ester) copolymers have better thickening performance in the formula than the common acrylic acid (ester) copolymers, and have better matching performance with the whole formula system.
The invention compounds N-lauroyl sodium glutamate, polyalcohol, methyl cocoyl sodium taurate, sodium glutamate, polyethylene glycol, acrylate copolymer thickener, fatty acid, ethylene glycol distearate, polyglycerol-10 laurate, PEG-120 methyl glucose dioleate and tocopherol acetate for synergistic interaction, specifically utilizes the synergistic interaction of amino acid surfactant N-lauroyl sodium glutamate and sodium glutamate to form a stable crystalline thickening system, combines with acrylate copolymer and PEG-120 methyl glucose dioleate to further increase the heat resistance stability of the formula, adds polyglycerol-10 laurate to make up the defects of unstable foam and quick defoaming of the N-lauroyl sodium glutamate, ensures that the foam of the product is more durable and softer, adds the tocopherol acetate, the yellowing phenomenon of the formula due to high temperature or long-term storage is obviously improved; the obtained amino acid facial cleanser is mild in use, fine in cream body, smooth and rich in foam, excellent in stability, safe, free of stimulation and strong in cleaning performance, and the pH value is 5.3-5.8 and is close to that of human skin.
Furthermore, the inventor obtains through a large number of research statistical analyses that the N-lauroyl sodium glutamate, the polyhydric alcohol, the sodium methyl cocoyl taurate, the sodium glutamate, the polyethylene glycol, the acrylate copolymer thickener, the fatty acid, the ethylene glycol distearate, the polyglycerol-10 laurate, the PEG-120 methyl glucose dioleate and the tocopherol acetate are proportioned according to the parts by weight, can exert good synergistic effect and do not generate any side effect.
Preferably, the sodium glutamate comprises at least one of anhydrous sodium glutamate and monosodium glutamate.
Preferably, the chelating agent comprises at least one of disodium EDTA and tetrasodium EDTA.
Preferably, the fatty acid includes at least one of lauric acid, myristic acid, palmitic acid, and stearic acid.
Preferably, the mild amino acid facial cleansing cream of the present application further comprises: preservatives and/or fragrances.
Preferably, the preservative is used in an amount of 0.1-1 part, and the essence is used in an amount of 0.1-1 part.
A preparation method of a mild amino acid facial cleanser is disclosed, wherein the mild amino acid facial cleanser is the mild amino acid facial cleanser; the preparation method comprises the following steps:
(1) mixing N-lauroyl sodium glutamate, polyhydric alcohol and water, and heating to 70-85 ℃ to obtain solution A.
(2) Mixing the solution A, sodium methyl cocoyl taurate, sodium glutamate, polyethylene glycol, fatty acid, ethylene glycol distearate, polyglycerol-10 laurate and PEG-120 methyl glucose dioleate, heating to 70-85 ℃, then cooling to 45-55 ℃, adding the rest of the components, and mixing.
Preferably, the preparation method further comprises: and keeping the temperature of the solution A at 70-85 ℃, and stirring until the solution surface is free from bubbles.
Preferably, in step (2) of the above preparation method: and (3) after cooling to 45-55 ℃, adding an acrylate copolymer thickener, homogenizing and stirring uniformly at a low speed, adding other residual components such as tocopherol acetate, a chelating agent and the like, stirring and cooling to 40-42 ℃ to obtain the amino acid facial cleanser.
The water may be pure water, distilled water or deionized water, preferably deionized water.
Embodiments of the present invention will be described in detail below with reference to specific examples, but those skilled in the art will appreciate that the following examples are only illustrative of the present invention and should not be construed as limiting the scope of the present invention. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available commercially.
Example 1
The cleansing cream comprises the following raw materials in parts by weight: 67 parts of deionized water, 15 parts of N-lauroyl sodium glutamate, 10 parts of 1, 3-propylene glycol, 3 parts of sodium methyl cocoyl taurate, 2 parts of sodium glutamate, 81 parts of polyethylene glycol, 1 part of lauric acid, 1 part of ethylene glycol distearate, 1 part of polyglycerol-10 laurate, 0.1 part of PEG-120 methyl glucose dioleate, 1 part of acrylic acid (ester)/steareth-20 methacrylate copolymer, 0.5 part of preservative, 0.1 part of tocopherol acetate, 0.1 part of disodium EDTA (ethylene diamine tetraacetic acid) and 0.2 part of essence.
The preparation process of the facial cleansing cream comprises the following steps:
(1) adding N-lauroyl sodium glutamate and polyalcohol into deionized water, heating to 70 deg.C while stirring to dissolve to obtain solution A, stirring at 70 deg.C while maintaining the temperature until the solution surface is free of bubbles, and stopping heating;
(2) adding sodium methyl cocoyl taurate, sodium glutamate, polyethylene glycol-8, lauric acid, ethylene glycol distearate, polyglycerol-10 laurate and PEG-120 methyl glucose dioleate into the solution A obtained in the step (1), uniformly stirring and mixing, heating to 75 ℃ to dissolve, stopping heating, then stirring until the temperature is reduced to about 45 ℃, adding acrylic acid (ester)/steareth-20 methacrylate copolymer, uniformly stirring at low speed, adding the rest components, stirring and cooling to 40 ℃ to obtain the cleansing cream.
Example 2
The cleansing cream comprises the following raw materials in parts by weight: 40.8 parts of deionized water, 20 parts of N-lauroyl sodium glutamate, 20 parts of 1, 3-propylene glycol, 5 parts of sodium methyl cocoyl taurate, 3 parts of sodium glutamate, 82 parts of polyethylene glycol-82 parts of lauric acid, 1.5 parts of ethylene glycol distearate, 1.5 parts of polyglycerol-10 laurate, 0.3 part of PEG-120 methyl glucose dioleate, 2 parts of acrylic acid (ester)/stearyl polyether-20 methacrylate copolymer, 0.5 part of preservative, 0.1 part of tocopherol acetate, 0.3 part of disodium EDTA and 0.9 part of essence.
The preparation process of the facial cleansing cream comprises the following steps:
(1) adding N-lauroyl sodium glutamate and polyalcohol into deionized water, heating to 70 deg.C while stirring to dissolve to obtain solution A, stirring at 70 deg.C while maintaining the temperature until the solution surface is free of bubbles, and stopping heating;
(2) adding sodium methyl cocoyl taurate, sodium glutamate, polyethylene glycol-8, lauric acid, ethylene glycol distearate, polyglycerol-10 laurate and PEG-120 methyl glucose dioleate into the solution A obtained in the step (1), uniformly stirring and mixing, heating to 75 ℃ to dissolve, stopping heating, then stirring until the temperature is reduced to about 45 ℃, adding acrylic acid (ester)/steareth-20 methacrylate copolymer, uniformly stirring at low speed, adding the rest components, stirring and cooling to 40 ℃ to obtain the cleansing cream.
Example 3
The cleansing cream comprises the following raw materials in parts by weight: 29 parts of deionized water, 19 parts of N-lauroyl sodium glutamate, 25 parts of 1, 3-propylene glycol, 8 parts of sodium methyl cocoyl taurate, 5 parts of sodium glutamate, 83 parts of polyethylene glycol, 2.5 parts of lauric acid, 2 parts of ethylene glycol distearate, 2 parts of polyglycerol-10 laurate, 0.5 part of PEG-120 methyl glucose dioleate, 2 parts of acrylic acid (ester)/steareth-20 methacrylate copolymer, 0.8 part of preservative, 0.8 part of tocopherol acetate, 0.1 part of disodium EDTA and 0.2 part of essence.
The preparation process of the facial cleansing cream comprises the following steps:
(1) adding N-lauroyl sodium glutamate and polyalcohol into deionized water, heating to 70 deg.C while stirring to dissolve to obtain solution A, stirring at 70 deg.C while maintaining the temperature until the solution surface is free of bubbles, and stopping heating;
(2) adding sodium methyl cocoyl taurate, sodium glutamate, polyethylene glycol-8, lauric acid, ethylene glycol distearate, polyglycerol-10 laurate and PEG-120 methyl glucose dioleate into the solution A obtained in the step (1), uniformly stirring and mixing, heating to 75 ℃ to dissolve, stopping heating, then stirring until the temperature is reduced to about 45 ℃, adding acrylic acid (ester)/steareth-20 methacrylate copolymer, uniformly stirring at low speed, adding the rest components, stirring and cooling to 40 ℃ to obtain the cleansing cream.
Example 4
The cleansing cream comprises the following raw materials in parts by weight: 18 parts of deionized water, 15 parts of N-lauroyl sodium glutamate, 30 parts of 1, 3-propylene glycol, 10 parts of sodium methyl cocoyl taurate, 5 parts of sodium glutamate, 85 parts of polyethylene glycol, 3 parts of lauric acid, 2 parts of ethylene glycol distearate, 5 parts of polyglycerol-10 laurate, 1 part of PEG-120 methyl glucose dioleate, 5 parts of acrylic acid (ester)/steareth-20 methacrylate copolymer, 0.1 part of preservative, 0.3 part of tocopherol acetate, 0.3 part of EDTA disodium and 0.2 part of essence.
The preparation process of the facial cleansing cream comprises the following steps:
(1) adding N-lauroyl sodium glutamate and polyalcohol into deionized water, heating to 70 deg.C while stirring to dissolve to obtain solution A, stirring at 70 deg.C while maintaining the temperature until the solution surface is free of bubbles, and stopping heating;
(2) adding sodium methyl cocoyl taurate, sodium glutamate, polyethylene glycol-8, lauric acid, ethylene glycol distearate, polyglycerol-10 laurate and PEG-120 methyl glucose dioleate into the solution A obtained in the step (1), uniformly stirring and mixing, heating to 75 ℃ to dissolve, stopping heating, then stirring until the temperature is reduced to about 45 ℃, adding acrylic acid (ester)/steareth-20 methacrylate copolymer, uniformly stirring at low speed, adding the rest components, stirring and cooling to 40 ℃ to obtain the cleansing cream.
Example 5
The cleansing cream comprises the following raw materials in parts by weight: 24 parts of deionized water, 30 parts of N-lauroyl sodium glutamate, 30 parts of 1, 3-propylene glycol, 1 part of sodium methyl cocoyl taurate, 1 part of sodium glutamate, 85 parts of polyethylene glycol, 3 parts of lauric acid, 2 parts of ethylene glycol distearate, 1 part of polyglycerol-10 laurate, 0.1 part of PEG-120 methyl glucose dioleate, 1 part of acrylic acid (ester)/steareth-20 methacrylate copolymer, 0.1 part of preservative, 1 part of tocopherol acetate, 0.5 part of EDTA disodium and 0.2 part of essence.
The preparation process of the facial cleansing cream comprises the following steps:
(1) adding N-lauroyl sodium glutamate and polyalcohol into deionized water, heating to 70 deg.C while stirring to dissolve to obtain solution A, stirring at 70 deg.C while maintaining the temperature until the solution surface is free of bubbles, and stopping heating;
(2) adding sodium methyl cocoyl taurate, sodium glutamate, polyethylene glycol-8, lauric acid, ethylene glycol distearate, polyglycerol-10 laurate and PEG-120 methyl glucose dioleate into the solution A obtained in the step (1), uniformly stirring and mixing, heating to 75 ℃ to dissolve, stopping heating, then stirring until the temperature is reduced to about 45 ℃, adding acrylic acid (ester)/steareth-20 methacrylate copolymer, uniformly stirring at low speed, adding the rest components, stirring and cooling to 40 ℃ to obtain the cleansing cream.
Comparative example 1
This comparative example differs from example 1 in that: the raw material component, sodium glutamate, in example 1 was removed.
Comparative example 2
This comparative example differs from example 1 in that: the starting material, PEG-120 methyl glucose dioleate, in example 1 was removed.
Comparative example 3
This comparative example differs from example 3 in that: the starting material component, tocopheryl acetate, in example 1 was removed.
Comparative example 4
This comparative example differs from example 3 in that: the raw material component, polyglycerol-10 laurate, of example 1 was removed.
Comparative example 5
The amino acid facial cleanser sold in the market is adopted.
The acrylic/steareth-20 methacrylate copolymer was ACULYN 88POLMER available from Dow chemical.
The performance indexes of the cleansing creams prepared in the embodiments 1-5 and the comparative examples 1-5 of the invention are detected, and the specific detection results are shown in the following table 1.
TABLE 1
The measurement method of the foam (i.e., foaming power) in Table 1 is specifically described in GB/T13173.6-2000.
In conclusion, the facial cleanser prepared by the invention is mild in use, fine in cream body, good in foaming power, rich in foam, excellent in heat-resistant and cold-resistant stability, safe and non-irritant, and strong in cleaning performance, and the pH value of the facial cleanser is 5.3-5.8 and is close to that of human skin.
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; and the modifications or the substitutions do not make the essence of the corresponding technical solutions depart from the scope of the technical solutions of the embodiments of the present invention. Furthermore, those skilled in the art will appreciate that while some embodiments herein include some features included in other embodiments, rather than other features, combinations of features of different embodiments are meant to be within the scope of the invention and form different embodiments. For example, in the claims above, any of the claimed embodiments may be used in any combination. The information disclosed in this background section is only for enhancement of understanding of the general background of the invention and should not be taken as an acknowledgement or any form of suggestion that this information forms the prior art already known to a person skilled in the art.
Claims (10)
1. The mild amino acid facial cleanser is characterized by comprising the following raw materials in parts by weight: 15-35 parts of N-lauroyl sodium glutamate, 10-40 parts of polyhydric alcohol, 1-10 parts of methyl cocoyl sodium taurate, 2-10 parts of sodium glutamate, 1-5 parts of polyethylene glycol, 1-5 parts of thickening agent, 1-5 parts of fatty acid, 1-5 parts of ethylene glycol distearate, 1-5 parts of polyglycerol-10 laurate, 0.1-1 part of PEG-120 methyl glucose dioleate, 0.1-1 part of tocopherol acetate, 0.1-0.5 part of chelating agent and 10-70 parts of water.
2. The mild amino acid facial cleanser of claim 1, wherein said polyol comprises at least one of glycerin, 1, 2-propanediol, 70% sorbitol, 1, 3-butanediol, and 1, 3-propanediol;
preferably, the polyol is 1, 3-butanediol and/or 1, 3-propanediol.
3. The mild amino acid facial cleanser of claim 1, wherein said thickening agent comprises an acrylate copolymer;
preferably, the acrylate copolymer comprises at least one of an acrylic acid (ester)/steareth-20 methacrylate copolymer, an acrylic acid (ester)/palmitoeth-25 acrylate copolymer, and an acrylic acid (ester)/beheneth-25 methacrylate copolymer.
4. The mild amino acid facial cleanser of claim 1, wherein said polyethylene glycol comprises at least one of polyethylene glycol-6, polyethylene glycol-8, and polyethylene glycol-32.
5. The mild amino acid facial cleanser of claim 1, wherein said sodium glutamate comprises at least one of anhydrous sodium glutamate and monosodium glutamate.
6. The mild amino acid facial cleanser of claim 1, wherein said chelating agent comprises at least one of disodium EDTA and tetrasodium EDTA;
preferably, the fatty acid includes at least one of lauric acid, myristic acid, palmitic acid, and stearic acid.
7. The mild amino acid facial cleanser of claim 1, wherein said raw materials further comprise: preservatives and/or fragrances.
8. The mild amino acid facial cleanser of claim 7, wherein the preservative is used in an amount of 0.1 to 1 part, and the essence is used in an amount of 0.1 to 1 part.
9. A preparation method of a mild amino acid facial cleanser is characterized in that the mild amino acid facial cleanser is the mild amino acid facial cleanser of any one of claims 1-8; the preparation method comprises the following steps:
mixing N-lauroyl sodium glutamate, polyhydric alcohol and water, and heating to 70-85 ℃ to obtain solution A;
mixing the solution A, sodium methyl cocoyl taurate, sodium glutamate, polyethylene glycol, fatty acid, ethylene glycol distearate, polyglycerol-10 laurate and PEG-120 methyl glucose dioleate, heating to 70-85 ℃, then cooling to 45-55 ℃, adding the rest of the components, and mixing.
10. The method of making a mild amino acid facial cleanser of claim 9, further comprising: and keeping the temperature of the solution A at 70-85 ℃, and stirring until the solution surface is free from bubbles.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112957302A (en) * | 2021-02-08 | 2021-06-15 | 福建片仔癀化妆品有限公司 | Amino acid facial cleanser and preparation method thereof |
| WO2024104026A1 (en) * | 2022-11-16 | 2024-05-23 | 上海家化联合股份有限公司 | Self-thickening composition of amino acid surfactant |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107137245A (en) * | 2017-04-01 | 2017-09-08 | 广州天玺生物科技有限公司 | A kind of amino acid cleansing cream and its preparation technology |
| CN107349121A (en) * | 2017-07-19 | 2017-11-17 | 广州众乐生物科技有限公司 | A kind of amino acid mildy wash that sebum film ability is protected by Balancing and preparation method thereof |
| CN110812261A (en) * | 2018-08-14 | 2020-02-21 | 完美（中国）有限公司 | Crystalline amino acid facial cleanser and preparation method thereof |
| CN111419736A (en) * | 2020-04-03 | 2020-07-17 | 陈宇航 | Skin cleaning composition with high sodium lauroyl isethionate content |
-
2020
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107137245A (en) * | 2017-04-01 | 2017-09-08 | 广州天玺生物科技有限公司 | A kind of amino acid cleansing cream and its preparation technology |
| CN107349121A (en) * | 2017-07-19 | 2017-11-17 | 广州众乐生物科技有限公司 | A kind of amino acid mildy wash that sebum film ability is protected by Balancing and preparation method thereof |
| CN110812261A (en) * | 2018-08-14 | 2020-02-21 | 完美（中国）有限公司 | Crystalline amino acid facial cleanser and preparation method thereof |
| CN111419736A (en) * | 2020-04-03 | 2020-07-17 | 陈宇航 | Skin cleaning composition with high sodium lauroyl isethionate content |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112957302A (en) * | 2021-02-08 | 2021-06-15 | 福建片仔癀化妆品有限公司 | Amino acid facial cleanser and preparation method thereof |
| WO2024104026A1 (en) * | 2022-11-16 | 2024-05-23 | 上海家化联合股份有限公司 | Self-thickening composition of amino acid surfactant |
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Effective date of registration: 20231107 Address after: Room 203, Building B, No. 620 Huangbian North Road, Helong Street, Baiyun District, Guangzhou City, Guangdong Province, 510080 Patentee after: Guangzhou Haiya Supply Chain Technology Co.,Ltd. Address before: 510800 No.4, no.4-1, no.4-2 and no.4-3, Qiyuan Avenue, Huashan Town, Huadu District, Guangzhou, Guangdong Patentee before: Guangzhou Meixi Biotechnology Co.,Ltd. |