CN113491658A - Preparation method and application of coffee seed powder-containing scrub cream - Google Patents

Preparation method and application of coffee seed powder-containing scrub cream Download PDF

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CN113491658A
CN113491658A CN202110858784.1A CN202110858784A CN113491658A CN 113491658 A CN113491658 A CN 113491658A CN 202110858784 A CN202110858784 A CN 202110858784A CN 113491658 A CN113491658 A CN 113491658A
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seed powder
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coffee seed
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曹远超
罗文辉
崔朝容
梁碧仪
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Guangzhou Beibi Cosmetics Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4953Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom containing pyrimidine ring derivatives, e.g. minoxidil
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P29/00Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/008Preparations for oily skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/28Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants

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Abstract

The invention discloses a preparation method and application of a frosted cream containing coffee seed powder, relating to the field of daily chemicals, wherein the raw materials comprise an A phase, a B phase, a C phase, a D phase and an E phase, and the raw materials comprise the following components in percentage by weight: phase A: 5-8% of olive fruit oil, 1-3% of ethylhexyl palmitate, 0.1-3% of polydimethylsiloxane, 1-3% of white oil, 0.1-0.8% of tocopherol acetate and 3-8% of emulsifier; phase B: 5-8% of humectant, 0.01-0.2% of methyl hydroxybenzoate, 0.01-0.2% of EDTA disodium, 0.1-0.2% of hydroxyethyl cellulose, 0.1-0.8% of carbomer, 0.01-0.2% of chlorphenesin and the balance of purified water; and C phase: 0.1-0.5% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.05-0.2% of isohexadecane and 0.01-0.1% of polysorbate; phase D: 0.1 to 0.5 percent of triethanolamine; phase E: 8-20% of small fruit coffee seed powder, 5-9% of walnut shell powder, 0.1-0.5% of phenoxyethanol and 0.01-0.3% of essence; the coffee bean can clean pore grease and soften skin, caffeine contained in the coffee grains has the effects of reducing edema and inflammation, and coffee grains can temporarily reduce orange peel tissues on the epidermis and strengthen the regeneration of skin cutin.

Description

Preparation method and application of coffee seed powder-containing scrub cream
Technical Field
The invention relates to the field of daily chemicals, in particular to a preparation method and application of a frosted cream containing coffee seed powder.
Background
The skin is outside the body, and is in direct contact with the external environment, and an organ having the functions of protecting and sensing external stimuli, etc., is the largest organ among human body organs. Cosmetics come into direct contact with the skin, and protection and modification of the skin are its most important functions. The normal skin of a human body has two barrier functions: on one hand, the loss of water, electrolyte and other substances in the body can be prevented; on the other hand, mechanical, physical, chemical and biological harmful or unwanted substances in the environment are prevented from invading. This keeps the environment in the body constant, which plays an important physiological protective role.
Most cosmetics are applied to the skin surface of a person and are in contact with the skin of the person for a long time, but the skin of many people accumulates various degrees of dirt, sebum, other secretions, and the like due to external irritation. It is difficult to achieve deep exfoliation with surface active cleansers alone. Therefore, the skin surface is periodically massaged with the exfoliating cosmetic to remove the excessive aged stratum corneum, and the skin properties can be improved.
Disclosure of Invention
The invention provides a preparation method and application of a coffee seed powder-containing scrub cream, which solves the problems in the background art, wherein the scrub cream is an emulsion type skin cleaning product containing uniform fine particles, is mainly used for removing dirt in the deep layer of skin, and can peel aged scaly cutin to remove dead skin by rubbing on the skin.
In order to achieve the purpose, the invention provides the following technical scheme:
a preparation method of a frosted cream containing coffee seed powder comprises the following raw materials in percentage by weight:
phase A: 5-8% of olive fruit oil, 1-3% of ethylhexyl palmitate, 0.1-3% of polydimethylsiloxane, 1-3% of white oil, 0.1-0.8% of tocopherol acetate and 3-8% of emulsifier;
phase B: 5-8% of humectant, 0.01-0.2% of methyl hydroxybenzoate, 0.01-0.2% of EDTA disodium, 0.1-0.2% of hydroxyethyl cellulose, 0.1-0.8% of carbomer, 0.01-0.2% of chlorphenesin and the balance of purified water;
and C phase: 0.1-0.5% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.05-0.2% of isohexadecane and 0.01-0.1% of polysorbate;
phase D: 0.1 to 0.5 percent of triethanolamine;
phase E: 8-20% of small fruit coffee seed powder, 5-9% of walnut shell powder, 0.1-0.5% of phenoxyethanol and 0.01-0.3% of essence;
wherein: the sum of the weight percentages of the phase A, the phase B, the phase C, the phase D and the phase E is 100 percent.
As a preferred technical scheme of the invention, the raw materials comprise the following components in percentage by weight:
phase A: 5.5% of olive fruit oil, 1.5% of ethylhexyl palmitate, 1.5% of polydimethylsiloxane, 1.5% of white oil, 0.3% of tocopherol acetate and 4.5% of emulsifier;
phase B: 5.2% of humectant, 0.15% of methylparaben, 0.08% of EDTA disodium, 0.1% of hydroxyethyl cellulose, 0.4% of carbomer, 0.13% of chlorphenesin and the balance of purified water;
and C phase: 0.35% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.1% of isohexadecane and 0.05% of polysorbate;
phase D: 0.4 percent of triethanolamine;
phase E: 15% of small-fruit coffee seed powder, 7% of walnut shell powder, 0.2% of phenoxyethanol and 0.1% of essence.
As a preferable technical scheme of the invention, the humectant is prepared from the following raw materials in parts by weight: 0.1-0.5% of sodium hyaluronate and 4-6% of glycerin.
As a preferable technical scheme of the invention, the humectant is prepared from the following raw materials in parts by weight: 0.2 percent of sodium hyaluronate and 5 percent of glycerin.
As a preferable technical scheme of the invention, the emulsifier is prepared from the following raw materials in parts by weight: 1-3% of cetearyl alcohol, 1-3% of cetearyl glucoside, 0.3-1% of glycerol stearate and 0.3-1% of PEG-100 stearate.
As a preferable technical scheme of the invention, the emulsifier is prepared from the following raw materials in parts by weight: cetearyl alcohol 2%, cetearyl glucoside 1.5%, glyceryl stearate 0.5%, PEG-100 stearate 0.5%.
A preparation method of a coffee seed powder-containing scrub cream comprises the following steps:
s1, weighing phase A raw materials according to the formula, putting the raw materials into a clean oil phase pot, heating to 80-85 ℃, and uniformly stirring to obtain a phase A mixture I;
s2, weighing the phase B raw materials according to the formula, putting the raw materials into a clean emulsifying pot, heating to 80-85 ℃, uniformly stirring, homogenizing, and keeping the temperature for 15-30 min;
s3, slowly pouring the mixture of the phase A into an emulsifying pot, and homogenizing for 3-5 min; adding the phase C raw material, carrying out secondary homogenization until the sample is in a uniform and fine state, carrying out heat preservation and stirring for 10-30min, and carrying out vacuum defoaming to obtain a mixture II;
s4, cooling the mixture II in a water bath, adding the D-phase raw material when the temperature is reduced to 60 ℃, and uniformly stirring; cooling to 38-42 ℃, adding the E-phase raw material, and uniformly stirring to obtain a mixture III;
and S5, filtering the mixture and discharging to obtain a finished product.
Use of the coffee seed powder-containing scrub cream of claims 1-7 in cosmetics.
The invention has the following advantages:
(1) cleaning follicular orifice oil, removing dirt on deep layer of skin, and restoring skin tightness and permeability;
(2) softening skin, peeling aged squamous cutin, removing dead skin cells, and keeping skin soft and delicate;
(3) the caffeine contained in the coffee granules has the effects of reducing edema and inflammation;
(4) the coffee grains can temporarily reduce the orange peel tissues on the epidermis and strengthen the skin cutin renewal.
Detailed Description
The following description of the preferred embodiments of the present invention is provided for the purpose of illustration and description, and is in no way intended to limit the invention.
The coffee-containing scrub cream of the following examples was used in cosmetics.
Example 1
The coffee seed powder-containing scrub cream is prepared from the following raw materials in parts by weight:
phase A: olive oil 5.5%, ethylhexyl palmitate 1.5%, dimethicone 1.5%, white oil 1.5%, tocopherol acetate 0.3%, cetearyl alcohol 2%, cetearyl glucoside 1.5%, glyceryl stearate 0.5%, PEG-100 stearate 0.5%;
phase B: 0.2% of sodium hyaluronate, 5% of glycerol, 0.15% of methylparaben, 0.08% of EDTA disodium, 0.1% of hydroxyethyl cellulose, 0.4% of carbomer, 0.13% of chlorphenesin and the balance of purified water;
and C phase: 0.35% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.1% of isohexadecane and-800.05% of polysorbate;
phase D: 0.4 percent of triethanolamine;
phase E: 8% of small fruit coffee seed powder, 7% of walnut shell powder, 0.2% of phenoxyethanol and 0.1% of essence;
wherein the sum of the weight percentages of the phase A, the phase B, the phase C, the phase D and the phase E is 100 percent.
The preparation method of the coffee seed powder-containing scrub cream comprises the following steps:
s1, weighing phase A raw materials according to a formula ratio, putting the raw materials into a clean oil phase pot, heating to 82 ℃, and uniformly stirring to obtain a phase A mixture I;
s2, weighing the phase B raw materials according to the formula, putting the raw materials into a clean emulsifying pot, heating to 82 ℃, uniformly stirring and homogenizing, and keeping the temperature for 22 min;
s3, slowly pouring the phase A mixture into an emulsifying pot, and homogenizing for 4 min; adding the phase C raw material, carrying out secondary homogenization until the sample is in a uniform and fine state, carrying out heat preservation and stirring for 20min, and carrying out vacuum defoaming to obtain a mixture II;
s4, cooling the mixture II in a water bath, adding the D-phase raw material when the temperature is reduced to 60 ℃, and uniformly stirring; cooling to 40 ℃, adding the E-phase raw material, and uniformly stirring to obtain a mixture III;
and S5, filtering the mixture and discharging to obtain a finished product.
Example 2
The coffee seed powder-containing scrub cream is prepared from the following raw materials in parts by weight:
phase A: olive oil 5.5%, ethylhexyl palmitate 1.5%, dimethicone 1.5%, white oil 1.5%, tocopherol acetate 0.3%, cetearyl alcohol 2%, cetearyl glucoside 1.5%, glyceryl stearate 0.5%, PEG-100 stearate 0.5%;
phase B: 0.2% of sodium hyaluronate, 5% of glycerol, 0.15% of methylparaben, 0.08% of EDTA disodium, 0.1% of hydroxyethyl cellulose, 0.4% of carbomer, 0.13% of chlorphenesin and the balance of purified water;
and C phase: 0.35% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.1% of isohexadecane and-800.05% of polysorbate;
phase D: 0.4 percent of triethanolamine;
phase E: 12% of small-fruit coffee seed powder, 7% of walnut shell powder, 0.2% of phenoxyethanol and 0.1% of essence;
wherein: the sum of the weight percentages of the phase A, the phase B, the phase C, the phase D and the phase E is 100 percent.
The preparation method of the coffee seed powder-containing scrub cream comprises the following steps:
s1, weighing phase A raw materials according to a formula ratio, putting the raw materials into a clean oil phase pot, heating to 82 ℃, and uniformly stirring to obtain a phase A mixture I;
s2, weighing the phase B raw materials according to the formula, putting the raw materials into a clean emulsifying pot, heating to 82 ℃, uniformly stirring and homogenizing, and keeping the temperature for 22 min;
s3, slowly pouring the phase A mixture into an emulsifying pot, and homogenizing for 4 min; adding the phase C raw material, carrying out secondary homogenization until the sample is in a uniform and fine state, carrying out heat preservation and stirring for 20min, and carrying out vacuum defoaming to obtain a mixture II;
s4, cooling the mixture II in a water bath, adding the D-phase raw material when the temperature is reduced to 60 ℃, and uniformly stirring; cooling to 40 ℃, adding the E-phase raw material, and uniformly stirring to obtain a mixture III;
and S5, filtering the mixture and discharging to obtain a finished product.
Example 3
The coffee seed powder-containing scrub cream is prepared from the following raw materials in parts by weight:
phase A: olive oil 5.5%, ethylhexyl palmitate 1.5%, dimethicone 1.5%, white oil 1.5%, tocopherol acetate 0.3%, cetearyl alcohol 2%, cetearyl glucoside 1.5%, glyceryl stearate 0.5%, PEG-100 stearate 0.5%;
phase B: 0.2% of sodium hyaluronate, 5% of glycerol, 0.15% of methylparaben, 0.08% of EDTA disodium, 0.1% of hydroxyethyl cellulose, 0.4% of carbomer, 0.13% of chlorphenesin and the balance of purified water;
and C phase: 0.35% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.1% of isohexadecane and-800.05% of polysorbate;
phase D: 0.4 percent of triethanolamine;
phase E: 16% of small-fruit coffee seed powder, 7% of walnut shell powder, 0.2% of phenoxyethanol and 0.1% of essence;
wherein: the sum of the weight percentages of the phase A, the phase B, the phase C, the phase D and the phase E is 100 percent.
The preparation method of the coffee seed powder-containing scrub cream comprises the following steps:
s1, weighing phase A raw materials according to a formula ratio, putting the raw materials into a clean oil phase pot, heating to 82 ℃, and uniformly stirring to obtain a phase A mixture I;
s2, weighing the phase B raw materials according to the formula, putting the raw materials into a clean emulsifying pot, heating to 82 ℃, uniformly stirring and homogenizing, and keeping the temperature for 22 min;
s3, slowly pouring the phase A mixture into an emulsifying pot, and homogenizing for 4 min; adding the phase C raw material, carrying out secondary homogenization until the sample is in a uniform and fine state, carrying out heat preservation and stirring for 20min, and carrying out vacuum defoaming to obtain a mixture II;
s4, cooling the mixture II in a water bath, adding the D-phase raw material when the temperature is reduced to 60 ℃, and uniformly stirring; cooling to 40 ℃, adding the E-phase raw material, and uniformly stirring to obtain a mixture III;
and S5, filtering the mixture and discharging to obtain a finished product.
Example 4
The coffee seed powder-containing scrub cream is prepared from the following raw materials in parts by weight:
phase A: olive oil 5.5%, ethylhexyl palmitate 1.5%, dimethicone 1.5%, white oil 1.5%, tocopherol acetate 0.3%, cetearyl alcohol 2%, cetearyl glucoside 1.5%, glyceryl stearate 0.5%, PEG-100 stearate 0.5%;
phase B: 0.2% of sodium hyaluronate, 5% of glycerol, 0.15% of methylparaben, 0.08% of EDTA disodium, 0.1% of hydroxyethyl cellulose, 0.4% of carbomer, 0.13% of chlorphenesin and the balance of purified water;
and C phase: 0.35% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.1% of isohexadecane and-800.05% of polysorbate;
phase D: 0.4 percent of triethanolamine;
phase E: 20% of small-fruit coffee seed powder, 7% of walnut shell powder, 0.2% of phenoxyethanol and 0.1% of essence;
wherein the sum of the weight percentages of the phase A, the phase B, the phase C, the phase D and the phase E is 100 percent.
The preparation method of the coffee seed powder-containing scrub cream comprises the following steps:
s1, weighing phase A raw materials according to a formula ratio, putting the raw materials into a clean oil phase pot, heating to 82 ℃, and uniformly stirring to obtain a phase A mixture I;
s2, weighing the phase B raw materials according to the formula, putting the raw materials into a clean emulsifying pot, heating to 82 ℃, uniformly stirring and homogenizing, and keeping the temperature for 22 min;
s3, slowly pouring the phase A mixture into an emulsifying pot, and homogenizing for 4 min; adding the phase C raw material, carrying out secondary homogenization until the sample is in a uniform and fine state, carrying out heat preservation and stirring for 20min, and carrying out vacuum defoaming to obtain a mixture II;
s4, cooling the mixture II in a water bath, adding the D-phase raw material when the temperature is reduced to 60 ℃, and uniformly stirring; cooling to 40 ℃, adding the E-phase raw material, and uniformly stirring to obtain a mixture III;
and S5, filtering the mixture and discharging to obtain a finished product.
Example 5
The coffee seed powder-containing scrub cream is prepared from the following raw materials in parts by weight:
phase A: olive oil 5.5%, ethylhexyl palmitate 1.5%, dimethicone 1.5%, white oil 1.5%, tocopherol acetate 0.3%, cetearyl alcohol 2%, cetearyl glucoside 1.5%, glyceryl stearate 0.5%, PEG-100 stearate 0.5%;
phase B: 0.2% of sodium hyaluronate, 5% of glycerol, 0.15% of methylparaben, 0.08% of EDTA disodium, 0.1% of hydroxyethyl cellulose, 0.4% of carbomer, 0.13% of chlorphenesin and the balance of purified water;
and C phase: 0.35% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.1% of isohexadecane and-800.05% of polysorbate;
phase D: 0.4 percent of triethanolamine;
phase E: 16% of small-fruit coffee seed powder, 5% of walnut shell powder, 0.2% of phenoxyethanol and 0.1% of essence;
wherein the sum of the weight percentages of the phase A, the phase B, the phase C, the phase D and the phase E is 100 percent.
S1, weighing phase A raw materials according to a formula ratio, putting the raw materials into a clean oil phase pot, heating to 82 ℃, and uniformly stirring to obtain a phase A mixture I;
s2, weighing the phase B raw materials according to the formula, putting the raw materials into a clean emulsifying pot, heating to 82 ℃, uniformly stirring and homogenizing, and keeping the temperature for 22 min;
s3, slowly pouring the phase A mixture into an emulsifying pot, and homogenizing for 4 min; adding the phase C raw material, carrying out secondary homogenization until the sample is in a uniform and fine state, carrying out heat preservation and stirring for 20min, and carrying out vacuum defoaming to obtain a mixture II;
s4, cooling the mixture II in a water bath, adding the D-phase raw material when the temperature is reduced to 60 ℃, and uniformly stirring; cooling to 40 ℃, adding the E-phase raw material, and uniformly stirring to obtain a mixture III;
and S5, filtering the mixture and discharging to obtain a finished product.
Example 6
The coffee seed powder-containing scrub cream is prepared from the following raw materials in parts by weight:
phase A: olive oil 5.5%, ethylhexyl palmitate 1.5%, dimethicone 1.5%, white oil 1.5%, tocopherol acetate 0.3%, cetearyl alcohol 2%, cetearyl glucoside 1.5%, glyceryl stearate 0.5%, PEG-100 stearate 0.5%;
phase B: 0.2% of sodium hyaluronate, 5% of glycerol, 0.15% of methylparaben, 0.08% of EDTA disodium, 0.1% of hydroxyethyl cellulose, 0.4% of carbomer, 0.13% of chlorphenesin and the balance of purified water;
and C phase: 0.35% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.1% of isohexadecane and-800.05% of polysorbate;
phase D: 0.4 percent of triethanolamine;
phase E: 16% of small-fruit coffee seed powder, 9% of walnut shell powder, 0.2% of phenoxyethanol and 0.1% of essence;
wherein the sum of the weight percentages of the phase A, the phase B, the phase C, the phase D and the phase E is 100 percent.
The preparation method of the coffee seed powder scrub cream comprises the following steps:
s1, weighing phase A raw materials according to the formula, putting the raw materials into a clean oil phase pot, heating to 80-85 ℃, and uniformly stirring to obtain a phase A mixture;
s2, weighing the phase B raw materials according to the formula, putting the raw materials into a clean emulsifying pot, heating to 80-85 ℃, uniformly stirring, homogenizing, and keeping the temperature for 15-30 min;
s3, slowly pouring the mixture of the phase A into an emulsifying pot, and homogenizing for 3-5 min; adding the phase C raw material, carrying out secondary homogenization until the sample is in a uniform and fine state, carrying out heat preservation and stirring for 10-30min, and carrying out vacuum defoaming to obtain a mixture II;
s4, cooling the mixture II in a water bath, adding the D-phase raw material when the temperature is reduced to 60 ℃, and uniformly stirring; cooling to 38-42 ℃, adding the E-phase raw material, and uniformly stirring to obtain a mixture III;
and S5, filtering the mixture III, and discharging to obtain a finished product.
Example 7
The coffee seed powder-containing scrub cream is prepared from the following raw materials in parts by weight:
phase A: olive oil 5.5%, ethylhexyl palmitate 1.5%, dimethicone 1.5%, white oil 1.5%, tocopherol acetate 0.3%, cetearyl alcohol 2%, cetearyl glucoside 1.5%, glyceryl stearate 0.5%, PEG-100 stearate 0.5%;
phase B: 0.2% of sodium hyaluronate, 5% of glycerol, 0.15% of methylparaben, 0.08% of EDTA disodium, 0.1% of hydroxyethyl cellulose, 0.4% of carbomer, 0.13% of chlorphenesin and the balance of purified water;
and C phase: 0.35% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.1% of isohexadecane and-800.05% of polysorbate;
phase D: 0.4 percent of triethanolamine;
phase E: 20% of small-fruit coffee seed powder, 9% of walnut shell powder, 0.2% of phenoxyethanol and 0.1% of essence;
wherein the sum of the weight percentages of the phase A, the phase B, the phase C, the phase D and the phase E is 100 percent.
The preparation method of the coffee seed powder scrub cream comprises the following steps:
s1, weighing phase A raw materials according to the formula, putting the raw materials into a clean oil phase pot, heating to 80-85 ℃, and uniformly stirring to obtain a phase A mixture;
s2, weighing the phase B raw materials according to the formula, putting the raw materials into a clean emulsifying pot, heating to 80-85 ℃, uniformly stirring, homogenizing, and keeping the temperature for 15-30 min;
s3, slowly pouring the mixture of the phase A into an emulsifying pot, and homogenizing for 3-5 min; adding the phase C raw material, carrying out secondary homogenization until the sample is in a uniform and fine state, carrying out heat preservation and stirring for 10-30min, and carrying out vacuum defoaming to obtain a mixture II;
s4, cooling the mixture II in a water bath, adding the D-phase raw material when the temperature is reduced to 60 ℃, and uniformly stirring; cooling to 38-42 ℃, adding the E-phase raw material, and uniformly stirring to obtain a mixture III;
and S5, filtering the mixture III, and discharging to obtain a finished product.
Comparative example 1
A preparation method of a frosted cream containing coffee seed powder comprises the following raw materials in percentage by weight:
phase A: olive oil 5.5%, ethylhexyl palmitate 1.5%, dimethicone 1.5%, white oil 1.5%, tocopherol acetate 0.3%, cetearyl alcohol 2%, cetearyl glucoside 1.5%, glyceryl stearate 0.5%, PEG-100 stearate 0.5%;
phase B: 0.15% of methylparaben, 0.08% of EDTA disodium, 0.1% of hydroxyethyl cellulose, 0.4% of carbomer, 0.13% of chlorphenesin and the balance of purified water;
and C phase: 0.35% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.1% of isohexadecane and-800.05% of polysorbate;
phase D: 0.4 percent of triethanolamine;
phase E: 16% of small-fruit coffee seed powder, 7% of walnut shell powder, 0.2% of phenoxyethanol and 0.1% of essence;
wherein the sum of the weight percentages of the phase A, the phase B, the phase C, the phase D and the phase E is 100 percent.
The control example 1 did not contain a humectant.
The preparation method of the coffee seed powder-containing scrub cream comprises the following steps:
s1, weighing phase A raw materials according to a formula ratio, putting the raw materials into a clean oil phase pot, heating to 82 ℃, and uniformly stirring to obtain a phase A mixture I;
s2, weighing the phase B raw materials according to the formula, putting the raw materials into a clean emulsifying pot, heating to 82 ℃, uniformly stirring and homogenizing, and keeping the temperature for 22 min;
s3, slowly pouring the phase A mixture into an emulsifying pot, and homogenizing for 4 min; adding the phase C raw material, carrying out secondary homogenization until the sample is in a uniform and fine state, carrying out heat preservation and stirring for 20min, and carrying out vacuum defoaming to obtain a mixture II;
s4, cooling the mixture II in a water bath, adding the D-phase raw material when the temperature is reduced to 60 ℃, and uniformly stirring; cooling to 40 ℃, adding the E-phase raw material, and uniformly stirring to obtain a mixture III;
and S5, filtering the mixture and discharging to obtain a finished product.
Comparative example 2
A preparation method of a frosted cream containing coffee seed powder comprises the following raw materials in percentage by weight:
phase A: olive oil 5.5%, ethylhexyl palmitate 1.5%, dimethicone 1.5%, white oil 1.5%, tocopherol acetate 0.3%, cetearyl alcohol 2%, cetearyl glucoside 1.5%, glyceryl stearate 0.5%, PEG-100 stearate 0.5%;
phase B: 0.2% of sodium hyaluronate, 5% of glycerol, 0.15% of methylparaben, 0.08% of EDTA disodium, 0.1% of hydroxyethyl cellulose, 0.4% of carbomer, 0.13% of chlorphenesin and the balance of purified water;
and C phase: 0.35% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.1% of isohexadecane and-800.05% of polysorbate;
phase D: 0.4 percent of triethanolamine;
phase E: 0.2 percent of phenoxyethanol and 0.1 percent of essence;
wherein the sum of the weight percentages of the phase A, the phase B, the phase C, the phase D and the phase E is 100 percent.
Comparative example 2 no cappuccino seed powder and walnut shell powder were added.
The preparation method of the coffee seed powder-containing scrub cream comprises the following steps:
s1, weighing phase A raw materials according to a formula ratio, putting the raw materials into a clean oil phase pot, heating to 82 ℃, and uniformly stirring to obtain a phase A mixture I;
s2, weighing the phase B raw materials according to the formula, putting the raw materials into a clean emulsifying pot, heating to 82 ℃, uniformly stirring and homogenizing, and keeping the temperature for 22 min;
s3, slowly pouring the phase A mixture into an emulsifying pot, and homogenizing for 4 min; adding the phase C raw material, carrying out secondary homogenization until the sample is in a uniform and fine state, carrying out heat preservation and stirring for 20min, and carrying out vacuum defoaming to obtain a mixture II;
s4, cooling the mixture II in a water bath, adding the D-phase raw material when the temperature is reduced to 60 ℃, and uniformly stirring; cooling to 40 ℃, adding the E-phase raw material, and uniformly stirring to obtain a mixture III;
and S5, filtering the mixture and discharging to obtain a finished product.
To further demonstrate the effect of the present invention, the following test methods were provided:
test for removing cutin and controlling oil
The cuticle removal can be favorable for the penetration of the humectant, and the cuticle removal effect is better and the moisturizing effect is better under the condition that the content ratio of the humectant is the same. The exfoliating effect is reflected by a moisturizing effect, and the cutin effect can be seen through the moisturizing effect.
The water and the pH value of the skin oil are monitored by a tester for the volunteer, and the water content and the oil content of the face of the volunteer are detected before use. That is, 90 volunteers, male and female, aged 18-25 years, were divided into 9 groups, 10 persons were tested with the coffee seed powder scrubs described in examples 1 to 7 and examples 1 to 2, respectively, and after using the scrubs for 2 hours, facial moisture content and oil content were again measured, and the test results are shown in table 1.
TABLE 1
Figure BDA0003185083210000121
Analysis of experiments
As can be seen from Table 1, the coffee seed powder scrub cream of the present invention has good exfoliating and oil control effects, and the following experimental analysis can be obtained:
analysis 1: it can be seen from comparative examples 1, 2 and 3 that the moisturizing effect is improved as the proportion of the small fruit coffee seed powder is increased under the conditions of the same proportion of walnut shell powder and different proportions of the small fruit coffee seed powder.
Analysis 2: comparative examples 3, 5 and 6 show that the moisturizing effect is improved as the proportion of the walnut shell powder is increased under the condition of the same proportion of the small fruit coffee seed powder and different proportions of the walnut shell powder.
Analysis 3: as can be seen from comparative experiment example 3 and comparative examples 1 and 2, the cappuccino seed powder and the walnut shell powder had good moisture absorption promoting and oil removing effects.
Analysis 4: compared with experiments 3, 4 and 7, the use amount of the small fruit coffee seed powder has a limit value, and the excessive addition of the small fruit coffee seed powder has little influence on the skin moisturizing and oil control effects.
Consumer sensory evaluation
The coffee-containing ground cream prepared according to the formulations of examples 1 to 7 were distributed to 90 volunteers mentioned above for comparison. The tester test bottles were used according to the same method, one sample was used for one week, the volunteer sensory scores were collected in this experiment, and the test results are shown in table 2. (the scoring criteria used were 10 points, 1 point being the worst and 10 points being the best.)
TABLE 2 evaluation of Using effects of coffee-containing seed powder scrub
Figure BDA0003185083210000131
Evaluation analysis
As can be seen from Table 2, the exfoliating effect of the samples with a small amount of coffee seed powder was correspondingly reduced, and the comfort in use was reduced due to the large amount of coffee seed powder, and it was found from the data that example 3 is the best combination of the effects in use.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (8)

1. The coffee seed powder-containing scrub cream is characterized by comprising a phase A, a phase B, a phase C, a phase D and a phase E, wherein the raw materials comprise the following components in percentage by weight:
phase A: 5-8% of olive fruit oil, 1-3% of ethylhexyl palmitate, 0.1-3% of polydimethylsiloxane, 1-3% of white oil, 0.1-0.8% of tocopherol acetate and 3-8% of emulsifier;
phase B: 5-8% of humectant, 0.01-0.2% of methyl hydroxybenzoate, 0.01-0.2% of EDTA disodium, 0.1-0.2% of hydroxyethyl cellulose, 0.1-0.8% of carbomer, 0.01-0.2% of chlorphenesin and the balance of purified water;
and C phase: 0.1-0.5% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.05-0.2% of isohexadecane and 0.01-0.1% of polysorbate;
phase D: 0.1 to 0.5 percent of triethanolamine;
phase E: 8-20% of small fruit coffee seed powder, 5-9% of walnut shell powder, 0.1-0.5% of phenoxyethanol and 0.01-0.3% of essence;
wherein: the sum of the weight percentages of the phase A, the phase B, the phase C, the phase D and the phase E is 100 percent.
2. The coffee seed powder-containing scrub cream of claim 1, wherein the raw materials comprise, by weight:
phase A: 5.5% of olive fruit oil, 1.5% of ethylhexyl palmitate, 1.5% of polydimethylsiloxane, 1.5% of white oil, 0.3% of tocopherol acetate and 4.5% of emulsifier;
phase B: 5.2% of humectant, 0.15% of methylparaben, 0.08% of EDTA disodium, 0.1% of hydroxyethyl cellulose, 0.4% of carbomer, 0.13% of chlorphenesin and the balance of purified water;
and C phase: 0.35% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.1% of isohexadecane and 0.05% of polysorbate;
phase D: 0.4 percent of triethanolamine;
phase E: 15% of small-fruit coffee seed powder, 7% of walnut shell powder, 0.2% of phenoxyethanol and 0.1% of essence.
3. The coffee seed powder-containing scrub cream of claim 1, wherein the humectant is comprised of, by weight: 0.1-0.5% of sodium hyaluronate and 4-6% of glycerin.
4. The coffee seed powder-containing scrub cream of claim 1, wherein the humectant is comprised of, by weight: 0.2 percent of sodium hyaluronate and 5 percent of glycerin.
5. The coffee seed powder-containing scrub cream of claim 1, wherein said emulsifier is comprised of, by weight: 1-3% of cetearyl alcohol, 1-3% of cetearyl glucoside, 0.3-1% of glycerol stearate and 0.3-1% of PEG-100 stearate.
6. The coffee seed powder-containing scrub cream of claim 1, wherein said emulsifier is comprised of, by weight: cetearyl alcohol 2%, cetearyl glucoside 1.5%, glyceryl stearate 0.5%, PEG-100 stearate 0.5%.
7. A method of making a coffee seed powder-containing scrub cream as claimed in claims 1 to 6 comprising the steps of:
s1, weighing phase A raw materials according to the formula, putting the raw materials into a clean oil phase pot, heating to 80-85 ℃, and uniformly stirring to obtain a phase A mixture I;
s2, weighing the phase B raw materials according to the formula, putting the raw materials into a clean emulsifying pot, heating to 80-85 ℃, uniformly stirring, homogenizing, and keeping the temperature for 15-30 min;
s3, slowly pouring the mixture of the phase A into an emulsifying pot, and homogenizing for 3-5 min; adding the phase C raw material, carrying out secondary homogenization until the sample is in a uniform and fine state, carrying out heat preservation and stirring for 10-30min, and carrying out vacuum defoaming to obtain a mixture II;
s4, cooling the mixture II in a water bath, adding the D-phase raw material when the temperature is reduced to 60 ℃, and uniformly stirring; cooling to 38-42 ℃, adding the E-phase raw material, and uniformly stirring to obtain a mixture III;
and S5, filtering the mixture and discharging to obtain a finished product.
8. Use of the coffee seed powder-containing scrub cream of claims 1-7 in cosmetics.
CN202110858784.1A 2021-07-28 2021-07-28 Preparation method and application of coffee seed powder-containing scrub cream Pending CN113491658A (en)

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CN114983899A (en) * 2022-07-05 2022-09-02 陇南市祥宇油橄榄开发有限责任公司 Plant type scrub cream and preparation method thereof

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CN106727090A (en) * 2015-11-19 2017-05-31 周丽 A kind of scrub cream being made of walnut
RU2680831C1 (en) * 2018-01-17 2019-02-28 Талагаева Елена Владимировна Body sugar scrubs (options)

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CN106727090A (en) * 2015-11-19 2017-05-31 周丽 A kind of scrub cream being made of walnut
RU2680831C1 (en) * 2018-01-17 2019-02-28 Талагаева Елена Владимировна Body sugar scrubs (options)

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CN114983899A (en) * 2022-07-05 2022-09-02 陇南市祥宇油橄榄开发有限责任公司 Plant type scrub cream and preparation method thereof

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