CN115282070A - Cleaning composition with temperature sensation and preparation method and application thereof - Google Patents
Cleaning composition with temperature sensation and preparation method and application thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
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Abstract
The invention provides a cleaning composition with temperature sensation, which comprises, by mass, 25-35 parts of aluminum silicate potassium salt, 25-35 parts of grease, 13-25 parts of surfactant, 11-25 parts of thickener and 3.1-7.5 parts of abrasive agent. The composition provides a cleaning composition containing aluminum silicate potassium salt with temperature for the first time, the composition can generate heat release effect and adsorption effect when meeting water, the surface temperature of the skin is improved, the cutin is softened, the microcirculation and metabolism speed of the skin are promoted, the composition is convenient to remove dirt which is difficult to remove on the surface of the skin, aged cuticle cells and aged squamous cutin which are accumulated on the surface of the skin, and the skin is thoroughly cleaned; the cleaning composition has strong cleaning power and high moisturizing performance, so that the skin is moistened and not tight after being cleaned, is safe and mild, and is suitable for various skins; the composition adopts one of ethylhexyl palmitate, caprylic/capric triglyceride or shea butter extract as basic oil, and has skin caring effect.
Description
Technical Field
The application relates to the technical field of cosmetic production, in particular to a cleaning composition with temperature sensation and a preparation method and application thereof.
Background
The horny layer is positioned on the outermost layer of the skin, and under normal conditions, the epidermis carries out self-renewal in about 28 days as a period, and old and waste horny layers can automatically fall off without human intervention. Skin metabolism is affected by many factors such as aging, changes in work and rest, and changes in weather. The skin is dark and rough and has no elasticity due to the fact that the skin cutin is slowly renewed, and the skin is blocked, the skin grows pox and the skin grows chicken for a long time. Therefore, proper exfoliation is critical in order to improve the skin and keep the skin healthy.
Scrub cream, a skin cleanser with uniform particle size. The main functions are to remove aged cutin and indirectly assist deep cleaning. When in use, the ointment is properly massaged on the skin, and the friction effect of the abrasive materials such as plant particles, chemical particles and the like can remove dirt which is difficult to remove, aged stratum corneum cells and aged squamous cutin which are accumulated on the surface of the skin while playing the cleaning effect of oil, moisture and surfactant in the preparation, so that the skin is soft and fine.
However, when the temperature is low, the metabolism speed of human skin becomes slow, which causes serious accumulation of old and waste cutin, and in this case, the cleaning effect of the common scrub is not good enough. Therefore, there is a need for a scrub cream that can achieve a better cleansing effect even when the skin temperature of the human body is low.
CN 113662893A discloses a warm feeling facial mask, wherein ginger root oil, pepper seed extract and evodia fruit extract are used for permeating into skin to bring heat sensation and induce vasodilatation. The safety and heating effect of the heating device are improved. At present, no temperature-sensitive cosmetic using aluminum silicate potassium salt as a heating component is available.
Disclosure of Invention
The invention aims to provide a cleaning composition containing aluminum silicate potassium salt and having a temperature feeling, which can generate heat when meeting water, effectively improve the surface temperature of skin, achieve a better cleaning effect, and simultaneously have excellent moisturizing performance, so that the skin is moistened and not tight after being cleaned.
On one hand, the application provides a cleaning composition with temperature sensation, and the cleaning composition comprises, by mass, 25-35 parts of aluminum silicate potassium salt, 25-35 parts of grease, 13-25 parts of surfactant, 11-25 parts of thickener and 3.1-7.5 parts of abrasive.
Furthermore, the particle size of the aluminum silicate potassium salt is 0.4-0.5mm.
The application selects the aluminum silicate potassium salt as a main heating component to obtain the cleaning composition with the temperature feeling. Potassium aluminosilicate is a generic term for minerals of the zeolite family, a hydrous alkali or alkaline earth aluminosilicate mineral. The potassium aluminum silicate is a new material, is used as an ion exchanger, an adsorption separating agent, a drying agent, a catalyst and a cement mixed material, and is widely applied to the departments of industry, agriculture, national defense and the like. The potassium aluminum silicate has various microporous structures, can adsorb water, and the adsorption process when meeting water is a heat release process. There is no prior art prior use of such materials in scrub creams.
This application uses it in scrub cream, on the one hand, makes it meet water and release heat, effectively improves the real temperature of skin surface, softens cutin. On the other hand, the cleansing power of the scrub cream is improved by utilizing the adsorption property of the aluminum silicate potassium salt.
Further, the grease is selected from one or more of ethylhexyl palmitate, caprylic capric triglyceride, shea butter extract, cetyl polydimethylsiloxane, dioctyl carbonate and oleyl erucate; preferably, the oil and fat is ethylhexyl palmitate, caprylic capric triglyceride or shea butter extract.
In one embodiment, ethylhexyl palmitate is selected as the oil component, and the oil is a very light and comfortable skin moistening oil, has good air permeability and good spreadability, is a dry breathable oil and is an excellent skin softening agent. This application adopts the ethylhexyl palmitate as basic component, and the nature of ethylhexyl palmitate is close to human skin, changes and is absorbed by skin to can reach the effect that oil was nourished the skin, can effectively improve user's skin state.
In one embodiment, caprylic capric triglyceride is selected as the oil component, and the caprylic capric triglyceride is a high-cleanness odorless vegetable oil and belongs to cottonseed oil or coconut oil compounds. It has high skin-friendly property, is not greasy, has skin lubricating effect, and has good spreadability, so that skin has smooth but not greasy feeling, and is easily absorbed by skin.
In one embodiment, the present application selects shea butter extract as the lipid component. The shea butter is a pure natural substance extracted from plants, and has the effects of moisturizing and nourishing, because the shea butter extract is rich in various unsaturated fatty acids and the like, is easy to be absorbed by the skin, and can nourish the skin. The shea butter can also be used as emollient to provide additional fat to the skin, reduce the evaporation of water from the skin, and restore the luster, softness, and elasticity of the skin.
In addition, ethylhexyl palmitate, caprylic/capric triglyceride and shea butter extract can form a stable system with aluminum silicate potassium salt, and are suitable for the composition.
Further, the surfactant is fatty alcohol-polyoxyethylene ether and/or glycerol triisostearate; preferably, the surfactant is 5-10 parts by mass of fatty alcohol-polyoxyethylene ether and 8-15 parts by mass of glycerol triisostearate.
The surfactant of the application selects fatty alcohol-polyoxyethylene ether and glycerol triisostearate (PEG-20). The fatty alcohol-polyoxyethylene ether is light yellow viscous liquid, has rich foam, strong detergency, good emulsifying power and solubility, lower skin irritation and good biodegradability, and can be compatible with various surfactants. Glycerol triisostearate (PEG-20) has mild properties, low irritation to skin, and good cleansing effect.
Further, the thickening agent comprises, by mass, 5-10 parts of MIGLYOL 840Gel B, 1-5 parts of polyethylene and 5-10 parts of beeswax.
Wherein MIGLYOL 840Gel B is provided by Guangzhou Qijia chemical industry Co., ltd840Gel B, whose main components are propylene glycol dicaprylate/dicaprate, and selelammonium hectorite and propylene carbonate.
Further, the abrasive agent comprises, by mass, 3-7 parts of hydrated silica and 0.1-0.5 part of olive shell particles.
In a preferable embodiment, the composition comprises 25-35 parts by mass of aluminum silicate potassium salt with the particle size of 0.4-0.5mm, 25-35 parts by mass of ethylhexyl palmitate or caprylic/capric triglyceride or shea butter fruit resin extract, 5-10 parts by mass of fatty alcohol polyoxyethylene ether, 8-15 parts by mass of glycerol triisostearate, 5-10 parts by mass of MIGLYOL 840gel B, 1-5 parts by mass of polyethylene, 5-10 parts by mass of beeswax, 3-7 parts by mass of hydrated silica and 0.1-0.5 part by mass of olive shell particles.
In another aspect, the present application also provides a method for preparing the above cleaning composition having a temperature sensation, the method comprising the steps of:
step one, mixing oil and a surfactant, and homogenizing until the oil and the surfactant are completely dispersed;
step two, continuously adding the thickening agent, heating to 88-90 ℃, reacting for 10-20min, and stirring at the speed of 30-50r/min until the thickening agent is completely dissolved; preferably, the reaction is carried out for 15min;
step three, stirring and cooling to 60-70 ℃, adding aluminum silicate potassium salt, stirring and dispersing, adding a grinding agent, and continuously stirring uniformly; preferably, the temperature is reduced to 65 ℃.
Further, the method also comprises the steps of filling at the temperature of 40-50 ℃, and standing for 10-24 hours at normal temperature; preferably, the mixture is placed at normal temperature for 12 hours.
In a preferred embodiment, a manufacturing process of a scrub cream with temperature sensation comprises the following steps:
step 1, mixing oil, fatty alcohol-polyoxyethylene ether and glycerol triisostearate (PEG-20), and homogenizing until the mixed raw materials are uniformly dispersed at a homogenizing speed of 600-800r/min;
2, continuously adding MIGLYOL 840Gel B, polyethylene and beeswax into the mixed raw materials, heating to 88-90 ℃ in an emulsifying pot, preserving the heat for 15 minutes, and stirring at the speed of 30-50r/min until the MIGLYOL 840Gel B, the polyethylene and the beeswax are completely dissolved;
step 3, stirring until the temperature is reduced to 65 ℃, adding aluminum silicate potassium salt after uniformly mixing, stirring and dispersing, adding hydrated silica and olive shell particles after uniformly dispersing, and continuously stirring uniformly;
and 4, filling while stirring under the condition that the temperature is controlled to be 40-50 ℃, standing at normal temperature for 12 hours, and forming solid paste.
Wherein the oil can be ethylhexyl palmitate, caprylic capric triglyceride or shea butter fruit resin extract, all of which can achieve the same technical effect.
In another aspect, the present application also provides a cosmetic containing the above cleansing composition with a warm feeling, wherein the cosmetic is a scrub, a soap, a cleansing cream and/or a cleanser.
Further, the cosmetic is scrub cream.
The invention has the following beneficial effects:
1. the application provides a cleaning composition containing aluminum silicate potassium salt and having temperature sensation for the first time, the cleaning composition can generate a heat release effect when meeting water, the surface temperature of the skin can be improved, the microcirculation and the metabolism speed of the skin are further promoted, the cutin can be effectively softened, dirt which is difficult to remove on the surface of the skin, aged cuticle cells accumulated on the surface of the skin and aged scaly cutin can be conveniently removed by the composition, and the skin is thoroughly cleaned;
2. the cleaning composition containing the potassium aluminosilicate and having the temperature sense can be used for mildly and efficiently adsorbing dirt on the surface of the skin and efficiently cleaning the skin by utilizing the adsorption effect of the potassium aluminosilicate and matching with other components of the composition while warming and releasing heat;
3. the cleaning composition has strong cleaning power and high moisturizing performance, so that the skin is moistened and not tight after being cleaned, the skin is prevented from being damaged by excessive cleaning, and the cleaning composition is safe and mild, is suitable for various skins, and can be widely applied and popularized;
4. in the application, ethylhexyl palmitate, caprylic capric triglyceride or shea butter fruit resin extract is used as basic grease, and the basic grease, aluminum silicate potassium salt and other components jointly form a stable system of the cleaning composition, so that the effect of nourishing skin by oil can be achieved, and the skin state of a user can be effectively improved.
Detailed Description
In order to more clearly explain the overall concept of the present application, the following detailed description is given by way of example. In the following description, numerous specific details are set forth in order to provide a more thorough understanding of the present invention. It will be apparent, however, to one skilled in the art, that the present invention may be practiced without one or more of these specific details. In other instances, well-known features have not been described in order to avoid obscuring the invention.
The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer.
Wherein, the cocamidopropyl betaine and the aluminum silicate potassium salt are provided by Shanghai Maxin Biochemical technology Co., ltd, wherein the particle size of the aluminum silicate potassium salt is 0.4-0.5mm; ethylhexyl palmitate, cetyl dimethicone, fatty alcohol polyoxyethylene ether, hydrated silica, glycerin, sorbitol, sodium lauroyl glutamate, and sodium chloride were provided by Shanghai Aladdin Biotechnology Ltd; caprylic/capric triglyceride and shea butter extract are provided by Beijing Lingbao science and technology Limited; the glycerol triisostearate is provided by a Heian petrochemical plant in Jiangsu province; polyethylene has limited chemical industryCompany offerings; propylene carbonate, MIGLYOL 840Gel B, is available from Kyoja chemical Co., ltd, where MIGLYOL 840Gel B is840Gel B, whose main components are propylene glycol dicaprylate/dicaprate, and seleonium hectorite and propylene carbonate; beeswax is supplied by western chemicals, ltd; olive shell particles, having a particle size of 40-80 mesh, provided by the environmental protection technologies ltd, weibang, he; disodium lauryl sulfosuccinate is available from new materials, ltd, guangda, guangzhou; sodium lauroyl isethionate was supplied by the readily available chemical company, limited of north lake; the plant frosted particles and the fine silica frosted particles are provided by a processing plant of the ore products of Saint Pont, lingshou; the grafted starch is acrylic acid grafted starch 300 provided by east commercial company Limited of Beijing next juniper; water-soluble jojoba ester waxes are available from baylon international trade ltd, guangzhou; the antiseptic is antiseptic EG5, provided by Guangzhou simple Caica Biotechnology Inc.; the skin moisture tester is a MoistureMeter SC, supplied by Shanghai Yiwidi industries, inc.
In the following embodiments, reagents or instruments used are not indicated by manufacturers, and are all conventional products available by commercial purchase, unless otherwise specified.
EXAMPLE 1 composition component screening test
In this example, a suspension experiment was performed on potassium aluminum silicate, and complexes thereof were screened.
The specific experimental method comprises the following steps: step 1, adding different oils, 7 parts of MIGLYOL 840Gel B, 2 parts of polyethylene and 8 parts of beeswax into an emulsifying pot, heating to 88-90 ℃, preserving heat for 15 minutes, and stirring at the speed of 30-50r/min until the oils are completely dissolved; step 2, stirring until the temperature is reduced to 65 ℃, adding 30 parts of aluminum silicate potassium salt after uniformly stirring and mixing, adding 5 parts of hydrated silica and 0.1 part of olive shell particles after uniformly stirring and dispersing, and uniformly stirring; and 3, filling while stirring under the condition that the temperature is controlled to be 40-50 ℃, and standing at normal temperature for 12 hours to form solid paste.
After the paste was prepared, the state was observed to determine whether the potassium aluminum salt was uniformly suspended in the system, and the results of the observation are shown in table 1.
TABLE 1
Composition comprising a metal oxide and a metal oxide | Ratio of parts by mass | Stability of |
Aluminum silicate potassium salt + ethylhexyl palmitate | 30:32 | Slightly yielding water |
Aluminum silicate potassium salt + caprylic capric triglyceride | 30:32 | Slightly yielding water |
Aluminum silicate potassium salt + shea butter fruit resin extract | 30:32 | Slightly yielding water |
Potassium aluminosilicate + cetyl dimethicone | 30:32 | Severe stratification |
The grease can be ethylhexyl palmitate, caprylic acid capric acid triglyceride or shea butter fruit resin extract, but has little water yielding phenomenon, and different surfactants are further adopted to be compounded with the preferable grease for further improving the long-term storage stability of the system. The optimized grease and different surfactants are mixed and homogenized at the homogenizing speed of 600-800r/min, and the observation results are shown in table 2.
TABLE 2
Make up of | Ratio of parts by mass | Stability of |
Ethylhexyl palmitate and fatty alcohol polyoxyethylene ether | 32:5 | Stabilization |
Ethylhexyl palmitate + glycerol triisostearate | 32:5 | Stabilization of |
Ethylhexyl palmitate + Cocoaminyl Glycerol | 32:5 | Delamination of layers |
Caprylic capric acid triglyceride and fatty alcohol polyoxyethylene ether | 32:5 | Stabilization |
Caprylic capric triglyceride + Glycerol Triisostearate | 32:5 | Stabilization |
Octanoic acid decanoic acidTriglyceride + glyceryl cocoate | 32:5 | Layering |
Butyrospermum parkii fruit resin extract and fatty alcohol-polyoxyethylene ether | 32:5 | Stabilization of |
Butyrospermum parkii fruit resin extract and glycerol triisostearate | 32:5 | Stabilization |
Butyrospermum parkii fruit fat extract + Glycerol cocoate | 32:5 | Layering |
Ethylhexyl palmitate, fatty alcohol polyoxyethylene ether and glycerol triisostearate | 32:6:10 | Stabilization |
Caprylic/capric triglyceride, fatty alcohol polyoxyethylene ether and glycerol triisostearate | 32:6:10 | Stabilization of |
Butyrospermum parkii fruit resin extract, fatty alcohol-polyoxyethylene ether and glycerol triisostearate | 32:6:10 | Stabilization |
Ethylhexyl palmitate, fatty alcohol polyoxyethylene ether and glycerol triisostearate | 32:6:6 | Slightly delaminated |
Caprylic capric acid triglyceride, fatty alcohol polyoxyethylene ether and glycerol triisostearate | 32:6:6 | Slightly delaminated |
Butyrospermum parkii fruit resin extract, fatty alcohol-polyoxyethylene ether and glycerol triisostearate | 32:6:6 | Slightly delaminated |
As shown in the results of Table 2, the test proves that the components of the composition are preferably 25-35 parts of aluminum silicate potassium salt, 25-35 parts of grease, 5-10 parts of fatty alcohol-polyoxyethylene ether and 8-15 parts of glycerol triisostearate. Wherein, the components have coordination, and in the mass ratio range of the embodiment, the components jointly form a stable system.
Example 2
The embodiment provides a frosted cream with temperature sensation, which comprises the following components in parts by weight: 30 parts of aluminum silicate potassium salt with the particle size of 0.4-0.5mm, 32 parts of ethylhexyl palmitate, 6 parts of fatty alcohol-polyoxyethylene ether, 10 parts of glycerol triisostearate (PEG-20), 7 parts of MIGLYOL 840gel B, 2 parts of polyethylene, 8 parts of beeswax, 5 parts of hydrated silica and 0.1 part of olive shell particles.
The embodiment provides a manufacturing process of a frosted cream with temperature sensation, which comprises the following steps:
step 1, mixing ethylhexyl palmitate, fatty alcohol-polyoxyethylene ether and glycerol triisostearate (PEG-20), and homogenizing until the mixed raw materials are uniformly dispersed at the homogenizing speed of 600-800r/min;
2, continuously adding MIGLYOL 840Gel B, polyethylene and beeswax into the mixed raw materials, heating to 88-90 ℃ in an emulsifying pot, preserving heat for 15 minutes, and stirring at the speed of 30-50r/min until the mixture is completely dissolved;
step 3, stirring until the temperature is reduced to 65 ℃, adding aluminum silicate potassium salt after uniformly mixing, stirring and dispersing, adding hydrated silica and olive shell particles after uniformly dispersing, and continuously stirring uniformly;
and 4, stirring and filling under the condition that the temperature is controlled to be 40-50 ℃, standing for 12 hours at normal temperature, and forming solid paste.
Example 3
The embodiment provides a frosted cream with temperature sensation, which comprises the following components in parts by weight: 30 parts of aluminum silicate potassium salt with the particle size of 0.4-0.5mm, 32 parts of caprylic/capric triglyceride, 6 parts of fatty alcohol-polyoxyethylene ether, 10 parts of glycerol triisostearate (PEG-20), 7 parts of MIGLYOL 840gel B, 2 parts of polyethylene, 8 parts of beeswax, 5 parts of hydrated silica and 0.1 part of olive shell particles.
The embodiment provides a manufacturing process of a frosted cream with temperature sensation, which comprises the following steps:
step 1, mixing caprylic/capric triglyceride, fatty alcohol-polyoxyethylene ether and glycerol triisostearate (PEG-20), and homogenizing until the mixed raw materials are uniformly dispersed at the homogenizing speed of 600-800r/min;
2, continuously adding MIGLYOL 840Gel B, polyethylene and beeswax into the mixed raw materials, heating to 88-90 ℃ in an emulsifying pot, preserving the heat for 15 minutes, and stirring at the speed of 30-50r/min until the MIGLYOL 840Gel B, the polyethylene and the beeswax are completely dissolved;
step 3, stirring until the temperature is reduced to 65 ℃, adding aluminum silicate potassium salt after uniformly mixing, stirring and dispersing, adding hydrated silica and olive shell particles after uniformly dispersing, and continuously stirring uniformly;
and 4, filling while stirring under the condition that the temperature is controlled to be 40-50 ℃, standing at normal temperature for 12 hours, and forming solid paste.
Example 4
The embodiment provides a frosted cream with temperature sensation, which comprises the following components in parts by weight: 30 parts of aluminum silicate potassium salt with the particle size of 0.4-0.5mm, 32 parts of shea butter fruit resin extract, 6 parts of fatty alcohol-polyoxyethylene ether, 10 parts of glycerol triisostearate (PEG-20), 7 parts of MIGLYOL 840gel B, 2 parts of polyethylene, 8 parts of beeswax, 5 parts of hydrated silica and 0.1 part of olive shell particles.
The embodiment provides a manufacturing process of a frosted cream with temperature sensation, which comprises the following steps:
step 1, mixing the shea butter extract, fatty alcohol-polyoxyethylene ether and glycerol triisostearate (PEG-20), and homogenizing until the mixed raw materials are uniformly dispersed at the homogenizing speed of 600-800r/min;
2, continuously adding MIGLYOL 840Gel B, polyethylene and beeswax into the mixed raw materials, heating to 88-90 ℃ in an emulsifying pot, preserving the heat for 15 minutes, and stirring at the speed of 30-50r/min until the MIGLYOL 840Gel B, the polyethylene and the beeswax are completely dissolved;
step 3, stirring until the temperature is reduced to 65 ℃, adding aluminum silicate potassium salt after uniform mixing, stirring and dispersing, adding hydrated silica and olive shell particles after uniform dispersing, and continuously stirring uniformly;
and 4, stirring and filling under the condition that the temperature is controlled to be 40-50 ℃, standing for 12 hours at normal temperature, and forming solid paste.
Example 5
This example differs from example 1 only in that no potassium aluminosilicate is present.
Comparative example
The comparison example provides a full-surface-active-system scrub cream which comprises the following components in parts by weight: 15 parts of glycerin, 30 parts of disodium lauryl sulfosuccinate, 10 parts of sodium lauroyl isethionate, 0.5 part of plant frosted particles, 5 parts of fine silica frosted particles, 4 parts of sorbitol, 6 parts of cocamidopropyl betaine, 2.5 parts of grafted starch, 1 part of sodium lauroyl glutamate, 2 parts of sodium chloride, 0.5 part of water-soluble jojoba ester wax, 1 part of preservative and the balance of water.
The components are prepared according to the following steps:
step 1, preparation: cleaning equipment for later use, mixing glycerol and grafted starch together, and uniformly dispersing;
step 2, adding sodium lauroyl isethionate, disodium lauryl sulfosuccinate, sodium lauroyl glutamate, sorbitol, water-soluble jojoba ester wax and water into a main emulsifying pot, heating to 88-90 ℃, preserving heat for 15 minutes, and slowly stirring until the sodium lauroyl isethionate, disodium lauryl sulfosuccinate, sodium lauroyl glutamate, sorbitol, water-soluble jojoba ester wax and water are completely dissolved (proper low-speed homogenization is performed);
step 3, taking a small amount of liquid, observing no particles, adding sodium chloride, stirring and mixing uniformly, adding fine silica sand particles and plant sand particles, stirring and dispersing uniformly, adding the mixed glycerol, grafted starch and cocamidopropyl betaine, stirring uniformly, keeping the temperature at 88-90 ℃ for 10 minutes, and cooling;
step 4, stirring until the temperature is reduced to 65 ℃, adding the preservative, and uniformly stirring;
and 5, discharging after the inspection is qualified, stirring and filling under the condition of heat preservation (the temperature is controlled to be 56-60 ℃), standing for 12 hours at normal temperature, and forming solid paste, namely the all-surface living scrub paste.
Example 6 scrub cream feel in use survey
In this example, a cleaning force test was performed for the above-described example 2 to 5 and comparative scrub.
The specific experimental method comprises the following steps: 50 consumers in the age range of 18-30 years are randomly selected, the sex is randomly determined, the consumers are randomly divided into five groups, the scrub creams of the examples 2-5 and the comparison example are respectively used for bathing for 1 month and once every two days, the use feelings of the consumers for the examples 2, 3, 4 and 5 and the comparison example are investigated, and the results are evaluated, and the specific results are shown in the table 3.
TABLE 3
As can be seen from Table 3, the products of examples 2-4 in this application are considered by 100% of the consumers to have good cleaning power, the application process is considered by 100% of the consumers to be mild and not irritating, the application process is considered by 100% of the consumers to be hot, and the moisturizing property is considered to be good by 83.33% of the consumers and not to be tight after washing.
In the application, the potassium aluminum silicate salt is in a porous structure and strong in adsorption capacity, can effectively adsorb impurities on skin when generating heat when meeting water, and is matched with PEG-20 surfactant, so that the scrub cream of the embodiment 2-4 has a better cleaning effect compared with the scrub cream of a full surfactant system. The frosted paste system has the advantages of ensuring high cleaning force, simultaneously having mildness and moisture retention, and bringing good use feeling to consumers.
EXAMPLE 7 scrub moisturizing test
The moisturizing ability test was continued on the scrub creams using the above comparative examples and examples 2-4.
The specific experimental method comprises the following steps: 40 consumers in the age range of 18-60 years are randomly selected, the sex is randomly determined, the consumers are divided into four groups at random, the scrub cream in the examples 2-4 and the arms in the comparative example are used for massaging and applying, and the scrub cream is cleaned after being applied for one time, wherein the applying amount is 4cm x 5cm and is about 300mg. Under the condition of constant temperature (21 +/-1 ℃,50 +/-10% humidity), taking 0h, 1h and 2h after cleaning as nodes, using a skin moisture tester to measure the CAP value of the stratum corneum hydration content of the arm skin, and calculating the CAP reduction rate based on the 0h CAP value, wherein the specific results are shown in Table 4.
CAP decline rate = (CAP) 0h -CAP x h )/CAP 0h
CAP 0h The CAP value was measured for 0h, and X is the corresponding time (1 h or 2 h), CAP x h CAP values were measured for X h.
TABLE 4
As can be seen from Table 4, in the moisturizing force test of the scrub cream, after the scrub cream in examples 2-4 is used for 1 hour and 2 hours, the hydration content CAP value of the horny layer of the arm skin is reduced compared with that T0, but the CAP value reduction rate is smaller than that of the comparative example, namely the moisturizing performance of the scrub cream in examples 2-4 in the application is better than that of the comparative example.
In the application, ethylhexyl palmitate, caprylic capric triglyceride or shea butter fruit resin extract is used as a basic oil component, so that the function of caring a skin fat membrane is achieved, and after the product is used, the water dispersion loss of the skin is small, so that the moisturizing effect of the scrub cream is better than that of other products.
The above description is only an example of the present application and is not intended to limit the present application. Various modifications and changes may occur to those skilled in the art. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present application should be included in the scope of the claims of the present application.
Claims (10)
1. The cleaning composition with the temperature sense is characterized by comprising, by mass, 25-35 parts of aluminum silicate potassium salt, 25-35 parts of grease, 13-25 parts of surfactant, 11-25 parts of thickener and 3.1-7.5 parts of abrasive agent.
2. The cleansing composition with temperature sensation of claim 1, wherein the particle size of the aluminum silicate potassium salt is 0.4-0.5mm.
3. The cleansing composition with the temperature feeling as claimed in claim 1, wherein the oil and fat is selected from one or more of ethylhexyl palmitate, caprylic capric triglyceride, shea butter extract, cetyl dimethicone, dioctyl carbonate, oleyl erucate; preferably, the oil and fat is ethylhexyl palmitate, caprylic capric triglyceride or shea butter extract.
4. The cleansing composition with temperature feel according to claim 1, characterized in that said surfactant is fatty alcohol polyoxyethylene ether and/or glycerol triisostearate; preferably, the surfactant is 5-10 parts by mass of fatty alcohol-polyoxyethylene ether and 8-15 parts by mass of glycerol triisostearate.
5. The cleansing composition with temperature sensation according to claim 1, characterized in that the thickening agent comprises 5-10 parts of MIGLYOL 840Gel B, 1-5 parts of polyethylene and 5-10 parts of beeswax in parts by mass.
6. The cleansing composition with temperature sensation as claimed in claim 1, characterized in that the abrasive is 3-7 parts of hydrated silica, 0.1-0.5 parts of olive shell particles by mass parts.
7. A process for the preparation of a cleaning composition having a temperature sensation according to any one of claims 1 to 6, characterized in that it comprises the following steps:
step one, mixing grease and a surfactant, and homogenizing until the grease and the surfactant are completely dispersed;
step two, continuously adding the thickening agent, heating to 88-90 ℃, reacting for 10-20min, and stirring at the speed of 30-50r/min until the thickening agent is completely dissolved; preferably, the reaction is carried out for 15min;
step three, stirring and cooling to 60-70 ℃, adding aluminum silicate potassium salt, stirring and dispersing, adding the grinding agent, and continuously stirring uniformly; preferably, the temperature is reduced to 65 ℃.
8. The method according to claim 7, further comprising filling at 40-50 ℃, standing at normal temperature for 10-24h; preferably, the mixture is placed at normal temperature for 12 hours.
9. A cosmetic product comprising the cleansing composition with a warm feeling as claimed in any one of claims 1 to 6, which is a scrub, soap, cleansing cream and/or cleanser.
10. The cosmetic of claim 9, wherein said cosmetic is a scrub.
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CN115737456A (en) * | 2022-11-22 | 2023-03-07 | 宁波子沐新材料科技有限公司 | Skin cleaning scrub cream and preparation method thereof |
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EP2082722A2 (en) * | 2008-01-17 | 2009-07-29 | Beiersdorf AG | Foaming self-warming cosmetic preparations |
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DE10253304A1 (en) * | 2002-11-15 | 2004-05-27 | Beiersdorf Ag | Self-warming cosmetic or dermatological composition, useful as mask for cleaning face, neck and decolletage, comprises emulsion of polyol, oil and emulsifier, plus zeolite |
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CN115737456B (en) * | 2022-11-22 | 2024-05-17 | 宁波子沐新材料科技有限公司 | Skin cleansing scrub and preparation method thereof |
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