CN105853271B - The personal cleaning compositions of the flower extract of common vetch containing the bitter edible plant - Google Patents
The personal cleaning compositions of the flower extract of common vetch containing the bitter edible plant Download PDFInfo
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- CN105853271B CN105853271B CN201610223195.5A CN201610223195A CN105853271B CN 105853271 B CN105853271 B CN 105853271B CN 201610223195 A CN201610223195 A CN 201610223195A CN 105853271 B CN105853271 B CN 105853271B
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- edible plant
- common vetch
- bitter edible
- plant common
- extract
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
Abstract
The invention discloses a kind of personal cleaning compositions comprising raw material by weight percentage below：Detersive surfactant 1% 20%, bitter edible plant common vetch flower extract 0.01 15%, surplus is deionized water.Can also include other auxiliary agents.The present invention includes the personal cleaning compositions of bitter edible plant common vetch flower extract, and formula is readily produced, and has high foam volume, low irritant, increases the moisture retention of skin and with good rinsability.This cleaning compositions are particularly suitable for washing and/or improving keratin substances, such as hair or skin.
Description
Technical field
The present invention relates to personal care articles fields, especially personal cleaning compositions.
Background technology
Bitter edible plant common vetch flower is a kind of peculiar rose flower variety of the small olive area plantation in Zhongshan City, Guangdong Province, is planted for rose family Rosa
The pale reddish brown polyphyll rose of object.Bitter edible plant common vetch flower is used for food（Such as drinks, biscuit）Industry has had very long history, but it is applied
It is not yet reported on personal care articles.
Personal cleaning compositions on the market are made of surfactant and conditioner at present, during use, work as bubble
When foam is more, irritation is bigger, and is not easy to rinse.
Invention content
In order to solve the problems in the existing technology, the present invention provides a kind of personal cleanliness's group of the flower extract of common vetch containing the bitter edible plant
Close object.
To achieve the goals above, the present invention uses following technical scheme：
A kind of personal cleaning compositions, including following raw material by weight percentage：
Detersive surfactant 1%-20%,
Bitter edible plant common vetch flower extract 0.01-15%
Surplus is deionized water.
Preferably, the detersive surfactant, by the total weight of the composition, generally about 5% to about 20%,
It is preferred that 8% to about 20%, in the range of more preferably from about 10% to about 20%.
Preferably, the detersive surfactant is anion surfactant, amphoteric surfactant and nonionic
One or more of surfactant.
Suitable anion surfactant is laureth sulfuric acid in personal cleaning compositions for use in the present invention
Ester sodium, laureth sulfuric ester ammonium, sodium lauroyl sarcosine, sodium lauroyl glutamate, laureth phosphate potassium, cocounut oil
One or more of acyl sodium isethionate, cocounut oil acyl glycine potassium, potassium laurate and potassium myristate.
In personal cleaning compositions for use in the present invention, suitable amphoteric surfactant is cocamidopropyl propyl amide beet
Alkali, cocoamido betaine, coconut oleoyl amine hydroxyl sulfo betaine, sodium cocoamphoacetate, cocounut oil acyl both sexes base diethyl
One or more of acid disodium and Sodium Lauroamphoacetate.
In personal cleaning compositions for use in the present invention, suitable nonionic surfactant includes coconut oleoyl amine
MEA, coconut oleoyl amine MIPA, cocoyl glucoside, lauryl glucoside, PEG-120 methyls dioleate and PEG-200
One or more of hydrogenating glycerol palm acid ester.
Preferably, the bitter edible plant common vetch flower extract is the bitter edible plant common vetch flower extract of aqueous based systems and/or water/alcohol base system.
It is further preferred that the bitter edible plant common vetch flower extract of the aqueous based systems refers to that water is used to spend gained as solvent extraction bitter edible plant common vetch
Bitter edible plant common vetch flower extract.
It is further preferred that the bitter edible plant common vetch flower extract of the water/alcohol base system is to use water-alcohol as solvent extraction bitter edible plant common vetch
Flower, is dissolved in increase bitter edible plant common vetch anthosin essence in water/alcohol base system, the bitter edible plant common vetch flower extract of gained.Wherein, the alcohol is one
One or more of first alcohol, dihydric alcohol and polyalcohol.Monohydric alcohol is ethyl alcohol；Dihydric alcohol is 1,2- propylene glycol, 1,3- propylene glycol
Or butanediol etc.；Polyalcohol is glycerine, sorbierite or maltitol etc..
It is further preferred that the bitter edible plant common vetch flower extract of the aqueous based systems is that 500 parts of bitter edible plant common vetch is spent petal and 1500
The pure water of part, which is placed in reaction pot, to be heated to boiling, and vapor after condensation, collect oil phase, obtain aqueous based systems by separation
Bitter edible plant common vetch flower extract distills until water no longer volatilizees.
It is further preferred that the bitter edible plant common vetch flower extract of the water/alcohol base system be by 500 parts of bitter edible plant common vetch flower petal,
1500 parts of pure water and 500 parts of alcohol, which are placed in reaction pot, to be heated to boiling, and for vapor after condensation, oil is collected in separation
Phase obtains low-boiling bitter edible plant common vetch flower extract；Until water no longer volatilizees, the alcohol in reaction pot obtains height by filtering for distillation
The bitter edible plant common vetch flower extract of boiling point merges low-boiling bitter edible plant common vetch flower extract and high boiling bitter edible plant common vetch flower extract to get to this hair
The bitter edible plant common vetch flower extract of bright water/alcohol base system.
The personal cleaning compositions of the present invention can further include auxiliary agent, and the auxiliary agent is cation opsonizing agent, suspends
One or more of agent, chelating agent, colorant, opacifier, aromatic, pH buffer, vitamin and moisturizer.
In personal cleaning compositions for use in the present invention, suitable cation opsonizing agent is Polyquaternium-10, polyquaternary amine
Salt -7 etc..
In personal cleaning compositions for use in the present invention, suitable suspending agent is xanthans, acrylic acid（Ester）Class is copolymerized
Object, hydroxyethyl cellulose or hydroxypropyl methyl cellulose etc..
In personal cleaning compositions for use in the present invention, suitable chelating agent be EDTA-2 sodium, Etidronic Acid and its
Salt.
In personal cleaning compositions for use in the present invention, suitable colorant be can be used for pigment in cosmetics and
Toner etc..
In personal cleaning compositions for use in the present invention, suitable opacifier such as glycol distearate, styrene
Polymer etc..
In personal cleaning compositions for use in the present invention, suitable aromatic is essence or essential oil.
In personal cleaning compositions for use in the present invention, suitable pH buffer is citric acid, sodium bicarbonate or carbonic acid
Sodium dihydrogen etc..
In personal cleaning compositions for use in the present invention, suitable vitamin be D-pantothenyl aleohol, vitamin B3, vitamin A,
Vitamin E or vitamin e acetate etc..
In personal cleaning compositions for use in the present invention, suitable moisturizer be lactic acid, Anjidew NL50, glycerine, propylene glycol,
Butanediol, hyaluronic acid, trehalose, hydrolyzed milk protein or hydrogenated starch hydrolysate etc..
The personal cleaning compositions of the present invention can be prepared by the conventional method of this field.The composition of the present invention is preferably used
To clean skin, including hair, body, face.
Beneficial effects of the present invention
The present invention includes the personal cleaning compositions of bitter edible plant common vetch flower extract, and formula is readily produced, and has high foam
Amount, low irritant increase the moisture retention of skin and with good rinsability.This cleaning compositions are particularly suitable for washing
And/or conditioning keratin substances, such as hair or skin.Bitter edible plant common vetch flower extract is present in personal cleaning compositions, makes combination
The performance of keeping humidity of object significantly improves, and is substantially reduced the irritation of detersive surfactant.Personal cleanliness's combination of the present invention
Object can be configured to, such as shampoo, shower cream, facial cleanser, hand cleanser etc..
Specific implementation mode
The present invention will be described with embodiment below, but should not be considered as them is limitation of the present invention.
Each raw material and its weight percent of 1-5 of the embodiment of the present invention and comparative example 1-3 is as shown in table 1.
The composition of embodiment 1-5 and comparative example 1-3 in table 1 are prepared by the conventional method of this field, evaluated
The foamability of above-mentioned composition, skin moisture-keeping performance, irritation and easily it is rinsability, evaluation result is as shown in table 2.Test method
It is as follows：
The test method of foamability
Prepare 20 times of aqueous dilute solutions of composition, and by 100ml（Solution temperature:40℃）Aqueous dilute solution is poured into
Into 1000ml graduated cylinders.Then the four leaf blenders of a diameter of 5cm are put into solution, measure and stirs 30 seconds at 1,000 rpm
The volume of foam is generated later（ml）.Measurement result is as gas release（Foamability）And it evaluates with descending standard according to this.It is adjoint
Ground, the reversion of every five seconds for example blender are primary.
Evaluation criteria is：
A：200ml≤foam volume
B：150ml≤foam volume ＜ 200ml
C：Foam volume ＜ 150ml
The moisture retention test method of skin
According to QB/T4256《Cosmetics moisture-keeping efficacy evaluation guide》In method, with capacitance method measure keratoderma water
Part content.
25 effective volunteers are tested in 25 DEG C of temperature, the environment that humidity is 50%.In volunteer's both hands forearm point
Then the not region of 13 × 3cm of label is cleaned 20 seconds with the personal cleaning compositions of the present invention, is then rinsed with clear water dry
Only.Humidity measurements before being cleaned with the CM825 skin moisture testers of CK companies test volunteer's forearm marked region（MMV0）
With 1 hour after cleaning humidity measurements（MMV1）.
Calculating skin moisture content growth rate %=（MMV1-MMV0）/MMV0×100%
Evaluation criteria is：
A：Skin moisture content growth rate %≤0
B:0 ＜ skin moisture content growth rate %≤15%
C:15% ＜ skin moisture content growth rate %≤30%
D:30% ＜ skin moisture content growth rate %≤50%
E:50% ＜ skin moisture content growth rates %
Irritating test method
Using irritation testing in vitro method-erythrocyte hemolysis experimental method of cosmetic field（RBC methods）To test combination
The irritation of object.According to HD50（50% hemolytic concentration）, DI（Albuminous degeneration index）And the ratio of H/D determines the thorn of product
Swash property.
Evaluation criteria is：
A：HD50/DI ＞ 100 are nonirritant；
B：10 faint irritations of HD50/DI ＞；
C：1 slight stimulations of HD50/DI ＞；
D：0.1 medium irritations of HD50/DI ＞；
E：0.1 serious irritations of HD50/DI ＜.
Easily rinsability test method
Ten female volunteers its face of above-mentioned cleaning compositions, according to following evaluation criteria, by washing or rinsing
Feel to evaluate the easy to be rinsability of composition with the presence or absence of cunning/refreshing when its face：
Evaluation criteria is：
A：There are 8 to 10 volunteers to think dry and comfortable；And there is 1 people or less to think satiny；
B：There are 6 to 7 volunteers to think dry and comfortable；And there are 3 people or less to think satiny；
C：5 or less volunteers think dry and comfortable；And there are 5 people or more to think satiny；
D：2 or less volunteers think dry and comfortable；And there are 8 people or more to think satiny.
Each raw material and its weight percent of table 1 embodiment 1-5 and comparative example 1-3
The foamability of the composition of table 2 embodiment 1-5 and comparative example 1-3, irritation and easily rinsability evaluation result
Can be seen that addition bitter edible plant common vetch from the test result of table 2 spends water base extract or bitter edible plant common vetch to spend water/alcohol radical extract, can
To reduce the irritation of composition, raising is easily rinsability, and at the same time having high foam volume and moisture retention.
Embodiment 6
Each raw material and its weight percent of embodiment 6 are as shown in table 3, according to the known method of this field, are prepared into
Shampoo.
Each raw material and its weight percent of 3 embodiment 6 of table
| Component | Hundred parts of ratios of weight（%） |
| Deionized water | In right amount to 100 |
| Laureth sodium sulfovinate | 12 |
| Sodium lauroyl sarcosine | 3 |
| Cocoamidopropyl betaine | 2.1 |
| Propylene glycol | 3 |
| Bitter edible plant common vetch spends water/alcohol radical extract | 5 |
| Polyquaternium-10 | 0.3 |
| EDTA-2 sodium | 0.2 |
| PEG-120 methyl dioleates | 1 |
| Glycol distearate | 1 |
| Cocoyl glucoside | 1.5 |
| Citric acid | In right amount |
| Preservative | In right amount |
Embodiment 7
Each raw material and its weight percent of embodiment 7 are as shown in table 4, according to the known method of this field, are prepared into
Shower cream.
Each raw material and its weight percent of 4 embodiment 7 of table
| Component | Hundred parts of ratios of weight（%） |
| Deionized water | In right amount to 100 |
| Lauric acid | 6 |
| Myristic acid | 4 |
| Potassium hydroxide | 2.5 |
| Laureth sodium sulfovinate | 5.6 |
| Glycol distearate | 1 |
| Cocoamidopropyl betaine | 1.5 |
| Glycerine | 3 |
| Bitter edible plant common vetch spends water/alcohol radical extract | 10 |
| Hydroxypropyl methyl cellulose | 0.2 |
| EDTA-2 sodium | 0.1 |
| Preservative | In right amount |
Embodiment 8
Each raw material and its weight percent of embodiment 8 are as shown in table 5, according to the known method of this field, are prepared into
Facial cleanser.
Each raw material and its weight percent of 5 embodiment 8 of table
| Component | Hundred parts of ratios of weight（%） |
| Deionized water | In right amount to 100 |
| Lauric acid | 6 |
| Myristic acid | 4 |
| Stearic acid | 22 |
| Potassium hydroxide | 4.5 |
| Carbomer | 0.6 |
| Glycol distearate | 3 |
| Cocoamidopropyl betaine | 1.5 |
| Glycerine | 25 |
| Bitter edible plant common vetch spends water/alcohol radical extract | 8 |
| Hydroxypropyl methyl cellulose | 0.2 |
| EDTA-2 sodium | 0.1 |
| Preservative | In right amount |
The high foam volume of personal cleaning compositions of the present invention is low to skin irritation and easily rinsability good.Therefore, of the invention
Personal cleaning compositions can prepare, such as shampoo, shower cream, facial cleanser, hand cleanser etc..
Claims (7)
1. a kind of personal cleaning compositions, which is characterized in that including following raw material by weight percentage：
Lauric acid 6%,
Myristic acid 4%,
Potassium hydroxide 2.3%,
Laureth sodium sulfovinate 3.5%,
Cocoamidopropyl betaine 2.1%,
Bitter edible plant common vetch spends water base extract 3%,
Surplus is deionized water；
The bitter edible plant common vetch spends water base extract to be prepared by the following method：500 parts of bitter edible plant common vetch is spent into petal and 1500 parts of pure water
It is placed in reaction pot and is heated to boiling, for vapor after condensation, oil phase is collected in separation, and the bitter edible plant common vetch flower for obtaining aqueous based systems carries
Object is taken, is distilled until water no longer volatilizees.
2. a kind of personal cleaning compositions, which is characterized in that including following raw material by weight percentage：Lauric acid 4%,
Myristic acid 2%,
Potassium hydroxide 1.5%,
Laureth sodium sulfovinate 1.4%,
Cocounut oil acyl glycine potassium 4%,
Cocoamidopropyl betaine 2.1%,
Bitter edible plant common vetch spends water base extract 5%,
Surplus is deionized water；
The bitter edible plant common vetch spends water base extract to be prepared by the following method：500 parts of bitter edible plant common vetch is spent into petal and 1500 parts of pure water
It is placed in reaction pot and is heated to boiling, for vapor after condensation, oil phase is collected in separation, and the bitter edible plant common vetch flower for obtaining aqueous based systems carries
Object is taken, is distilled until water no longer volatilizees.
3. a kind of personal cleaning compositions, which is characterized in that including following raw material by weight percentage：
Laureth sodium sulfovinate 14%,
Cocounut oil acyl glycine potassium 3%,
Sodium lauroyl sarcosine 1.2%,
Cocoamidopropyl betaine 2.1%,
Bitter edible plant common vetch spends water/alcohol radical extract 5%,
Surplus is deionized water；
The bitter edible plant common vetch flower water/alcohol radical extract is prepared by the following method：By 500 parts of bitter edible plant common vetch flower petal, 1500 parts pure
Water and 500 parts of alcohol, which are placed in reaction pot, to be heated to boiling, and vapor after condensation, collect oil phase, obtain low boiling by separation
The bitter edible plant common vetch flower extract of point；Until water no longer volatilizees, the alcohol in reaction pot obtains high boiling bitter edible plant common vetch flower by filtering for distillation
Extract, merge low-boiling bitter edible plant common vetch flower extract and high boiling bitter edible plant common vetch flower extract to get.
4. a kind of personal cleaning compositions, which is characterized in that including following raw material by weight percentage：
Laureth sodium sulfovinate 14%,
Sodium lauroyl sarcosine 1.8%,
Cocoamidopropyl betaine 2.1%,
Bitter edible plant common vetch spends water/alcohol radical extract 10%,
Surplus is deionized water；
The bitter edible plant common vetch flower water/alcohol radical extract is prepared by the following method：By 500 parts of bitter edible plant common vetch flower petal, 1500 parts pure
Water and 500 parts of alcohol, which are placed in reaction pot, to be heated to boiling, and vapor after condensation, collect oil phase, obtain low boiling by separation
The bitter edible plant common vetch flower extract of point；Until water no longer volatilizees, the alcohol in reaction pot obtains high boiling bitter edible plant common vetch flower by filtering for distillation
Extract, merge low-boiling bitter edible plant common vetch flower extract and high boiling bitter edible plant common vetch flower extract to get.
5. a kind of personal cleaning compositions, which is characterized in that including following raw material by weight percentage：
Cocounut oil acyl glycine potassium 1.2%,
Sodium lauroyl sarcosine 14%,
Cocoamidopropyl betaine 2.1%,
Bitter edible plant common vetch spends water base extract 10%,
Surplus is deionized water；
The bitter edible plant common vetch spends water base extract to be prepared by the following method：500 parts of bitter edible plant common vetch is spent into petal and 1500 parts of pure water
It is placed in reaction pot and is heated to boiling, for vapor after condensation, oil phase is collected in separation, and the bitter edible plant common vetch flower for obtaining aqueous based systems carries
Object is taken, is distilled until water no longer volatilizees.
6. a kind of personal cleaning compositions, which is characterized in that including following raw material by weight percentage：
Lauric acid 6%,
Myristic acid 4%,
Potassium hydroxide 2.5%,
Laureth sodium sulfovinate 5.6%,
Glycol distearate 1%,
Cocoamidopropyl betaine 1.5%,
Glycerine 3%,
Bitter edible plant common vetch spends water/alcohol radical extract 10%,
Hydroxypropyl methyl cellulose 0.2%,
EDTA- disodiums 0.1%,
Preservative qs,
Surplus is deionized water；
The bitter edible plant common vetch flower water/alcohol radical extract is prepared by the following method：By 500 parts of bitter edible plant common vetch flower petal, 1500 parts pure
Water and 500 parts of alcohol, which are placed in reaction pot, to be heated to boiling, and vapor after condensation, collect oil phase, obtain low boiling by separation
The bitter edible plant common vetch flower extract of point；Until water no longer volatilizees, the alcohol in reaction pot obtains high boiling bitter edible plant common vetch flower by filtering for distillation
Extract, merge low-boiling bitter edible plant common vetch flower extract and high boiling bitter edible plant common vetch flower extract to get.
7. a kind of personal cleaning compositions, which is characterized in that including following raw material by weight percentage：
Lauric acid 6%,
Myristic acid 4%,
Stearic acid 22%,
Potassium hydroxide 4.5%,
Carbomer 0.6%,
Glycol distearate 3%,
Cocoamidopropyl betaine 1.5%,
Glycerine 25%,
Bitter edible plant common vetch spends water/alcohol radical extract 8%,
Hydroxypropyl methyl cellulose 0.2%,
EDTA- disodiums 0.1%,
Preservative qs,
Surplus is deionized water；
The bitter edible plant common vetch flower water/alcohol radical extract is prepared by the following method：By 500 parts of bitter edible plant common vetch flower petal, 1500 parts pure
Water and 500 parts of alcohol, which are placed in reaction pot, to be heated to boiling, and vapor after condensation, collect oil phase, obtain low boiling by separation
The bitter edible plant common vetch flower extract of point；Until water no longer volatilizees, the alcohol in reaction pot obtains high boiling bitter edible plant common vetch flower by filtering for distillation
Extract, merge low-boiling bitter edible plant common vetch flower extract and high boiling bitter edible plant common vetch flower extract to get.
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106580795A (en) * | 2016-12-28 | 2017-04-26 | 中山市荼薇化妆品有限公司 | Extraction method of Tuwei flower extract having effects of moisture retention and whitening |
| CN106619162A (en) * | 2017-03-10 | 2017-05-10 | 九江天赐高新材料有限公司 | Mild cleaning composition |
| CN109745236A (en) * | 2017-11-07 | 2019-05-14 | 陕西博鸿生物科技集团有限公司 | A kind of compound face cleaning cream and preparation method thereof |
| CN108066216A (en) * | 2017-12-27 | 2018-05-25 | 国东启 | A kind of antiallergic releive composition, include its cleanser and preparation method |
| CN109316369B (en) * | 2018-09-19 | 2021-09-03 | 德国欧悦安股份有限公司 | Face cleaning mousse and preparation method thereof |
| CN111067853A (en) * | 2020-01-21 | 2020-04-28 | 广州睿新生物科技有限公司 | Mild and foamy skin cleaning composition and preparation method and application thereof |
| CN111588664A (en) * | 2020-05-11 | 2020-08-28 | 广州星业科技股份有限公司 | Amino acid antibacterial hand washing bubble containing plant extract composition and preparation method thereof |
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| CN104254313A (en) * | 2012-03-19 | 2014-12-31 | 科蒂德国有限责任公司 | Cosmetic skin composition with soothing effect and its use |
| CN104906007A (en) * | 2015-06-24 | 2015-09-16 | 陈琳仁 | Method for extracting rose essential oil, pigment and flavone from roses simultaneously and application of extracts |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101781606A (en) * | 2010-03-03 | 2010-07-21 | 广东珠江桥生物科技股份有限公司 | Extraction method of rosa rugosa essential oil |
| CN104254313A (en) * | 2012-03-19 | 2014-12-31 | 科蒂德国有限责任公司 | Cosmetic skin composition with soothing effect and its use |
| CN104906007A (en) * | 2015-06-24 | 2015-09-16 | 陈琳仁 | Method for extracting rose essential oil, pigment and flavone from roses simultaneously and application of extracts |
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