CN111067853A - Mild and foamy skin cleaning composition and preparation method and application thereof - Google Patents
Mild and foamy skin cleaning composition and preparation method and application thereof Download PDFInfo
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- CN111067853A CN111067853A CN202010070445.2A CN202010070445A CN111067853A CN 111067853 A CN111067853 A CN 111067853A CN 202010070445 A CN202010070445 A CN 202010070445A CN 111067853 A CN111067853 A CN 111067853A
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- mild
- laurate
- skin
- polyquaternium
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- 239000000203 mixture Substances 0.000 title claims abstract description 78
- 238000004140 cleaning Methods 0.000 title claims abstract description 56
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- -1 acyl potassium glycinate Chemical compound 0.000 claims abstract description 49
- POULHZVOKOAJMA-UHFFFAOYSA-M dodecanoate Chemical compound CCCCCCCCCCCC([O-])=O POULHZVOKOAJMA-UHFFFAOYSA-M 0.000 claims abstract description 36
- 229940070765 laurate Drugs 0.000 claims abstract description 36
- POULHZVOKOAJMA-UHFFFAOYSA-N methyl undecanoic acid Natural products CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims abstract description 36
- 239000005639 Lauric acid Substances 0.000 claims abstract description 34
- 235000013162 Cocos nucifera Nutrition 0.000 claims abstract description 19
- 244000060011 Cocos nucifera Species 0.000 claims abstract description 19
- 229920000289 Polyquaternium Polymers 0.000 claims abstract description 15
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 54
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 23
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims description 22
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims description 22
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 19
- 239000011734 sodium Substances 0.000 claims description 19
- 229910052708 sodium Inorganic materials 0.000 claims description 19
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims description 18
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 18
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 18
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims description 18
- LXAHHHIGZXPRKQ-UHFFFAOYSA-N 5-fluoro-2-methylpyridine Chemical compound CC1=CC=C(F)C=N1 LXAHHHIGZXPRKQ-UHFFFAOYSA-N 0.000 claims description 17
- 239000002537 cosmetic Substances 0.000 claims description 11
- 229940079988 potassium cocoyl glycinate Drugs 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 4
- 238000007599 discharging Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 229940083542 sodium Drugs 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 2
- 239000006260 foam Substances 0.000 abstract description 22
- 230000007794 irritation Effects 0.000 abstract description 20
- 239000004094 surface-active agent Substances 0.000 abstract description 14
- 238000005406 washing Methods 0.000 abstract description 8
- GZWNUORNEQHOAW-UHFFFAOYSA-M potassium;2-aminoacetate Chemical compound [K+].NCC([O-])=O GZWNUORNEQHOAW-UHFFFAOYSA-M 0.000 abstract description 3
- 238000013329 compounding Methods 0.000 abstract description 2
- 244000075850 Avena orientalis Species 0.000 description 30
- 235000007319 Avena orientalis Nutrition 0.000 description 30
- 230000000694 effects Effects 0.000 description 16
- 239000002994 raw material Substances 0.000 description 14
- 230000000052 comparative effect Effects 0.000 description 10
- 238000012360 testing method Methods 0.000 description 9
- OSCJHTSDLYVCQC-UHFFFAOYSA-N 2-ethylhexyl 4-[[4-[4-(tert-butylcarbamoyl)anilino]-6-[4-(2-ethylhexoxycarbonyl)anilino]-1,3,5-triazin-2-yl]amino]benzoate Chemical compound C1=CC(C(=O)OCC(CC)CCCC)=CC=C1NC1=NC(NC=2C=CC(=CC=2)C(=O)NC(C)(C)C)=NC(NC=2C=CC(=CC=2)C(=O)OCC(CC)CCCC)=N1 OSCJHTSDLYVCQC-UHFFFAOYSA-N 0.000 description 6
- 235000014113 dietary fatty acids Nutrition 0.000 description 4
- 239000000194 fatty acid Substances 0.000 description 4
- 229930195729 fatty acid Natural products 0.000 description 4
- 238000005187 foaming Methods 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- 235000019198 oils Nutrition 0.000 description 4
- DXDTUQXKMVJYAM-UHFFFAOYSA-N 2-aminoacetic acid;potassium Chemical compound [K].NCC(O)=O DXDTUQXKMVJYAM-UHFFFAOYSA-N 0.000 description 3
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 3
- 206010067482 No adverse event Diseases 0.000 description 3
- 208000003251 Pruritus Diseases 0.000 description 3
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical class OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 3
- 239000003945 anionic surfactant Substances 0.000 description 3
- 239000006071 cream Substances 0.000 description 3
- 230000001815 facial effect Effects 0.000 description 3
- 239000002736 nonionic surfactant Substances 0.000 description 3
- 239000004471 Glycine Substances 0.000 description 2
- 206010040914 Skin reaction Diseases 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- 239000002280 amphoteric surfactant Substances 0.000 description 2
- 230000002421 anti-septic effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 125000002091 cationic group Chemical group 0.000 description 2
- 239000003093 cationic surfactant Substances 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- GLSRFBDXBWZNLH-UHFFFAOYSA-L disodium;2-chloroacetate;2-(4,5-dihydroimidazol-1-yl)ethanol;hydroxide Chemical compound [OH-].[Na+].[Na+].[O-]C(=O)CCl.OCCN1CCN=C1 GLSRFBDXBWZNLH-UHFFFAOYSA-L 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 230000003020 moisturizing effect Effects 0.000 description 2
- 230000037307 sensitive skin Effects 0.000 description 2
- 230000035483 skin reaction Effects 0.000 description 2
- 231100000430 skin reaction Toxicity 0.000 description 2
- 229940096501 sodium cocoamphoacetate Drugs 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- 230000008719 thickening Effects 0.000 description 2
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 description 1
- IDUUXROOZBOOPH-QHHAFSJGSA-N 2-{[(2E)-3-(3,4-dihydroxyphenyl)-1-hydroxyprop-2-en-1-ylidene]amino}-5-hydroxybenzoic acid Chemical compound OC(=O)C1=CC(O)=CC=C1NC(=O)\C=C\C1=CC=C(O)C(O)=C1 IDUUXROOZBOOPH-QHHAFSJGSA-N 0.000 description 1
- FRPAVHFNOFSNDR-UHFFFAOYSA-N 3-(2,4-dioxo-1,3-thiazolidin-3-yl)propanoic acid Chemical compound OC(=O)CCN1C(=O)CSC1=O FRPAVHFNOFSNDR-UHFFFAOYSA-N 0.000 description 1
- WOKDXPHSIQRTJF-UHFFFAOYSA-N 3-[3-[3-[3-[3-[3-[3-[3-[3-(2,3-dihydroxypropoxy)-2-hydroxypropoxy]-2-hydroxypropoxy]-2-hydroxypropoxy]-2-hydroxypropoxy]-2-hydroxypropoxy]-2-hydroxypropoxy]-2-hydroxypropoxy]-2-hydroxypropoxy]propane-1,2-diol Chemical compound OCC(O)COCC(O)COCC(O)COCC(O)COCC(O)COCC(O)COCC(O)COCC(O)COCC(O)COCC(O)CO WOKDXPHSIQRTJF-UHFFFAOYSA-N 0.000 description 1
- 206010067484 Adverse reaction Diseases 0.000 description 1
- 229930190481 Avenanthramide Natural products 0.000 description 1
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 description 1
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 description 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 229920006322 acrylamide copolymer Polymers 0.000 description 1
- 239000002390 adhesive tape Substances 0.000 description 1
- 230000006838 adverse reaction Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical class [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 238000005238 degreasing Methods 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- YIOJGTBNHQAVBO-UHFFFAOYSA-N dimethyl-bis(prop-2-enyl)azanium Chemical compound C=CC[N+](C)(C)CC=C YIOJGTBNHQAVBO-UHFFFAOYSA-N 0.000 description 1
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 210000000245 forearm Anatomy 0.000 description 1
- 239000008233 hard water Substances 0.000 description 1
- 230000000774 hypoallergenic effect Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 230000007803 itching Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- FJWSMXKFXFFEPV-UHFFFAOYSA-N prop-2-enamide;hydrochloride Chemical compound Cl.NC(=O)C=C FJWSMXKFXFFEPV-UHFFFAOYSA-N 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
Abstract
The invention discloses a mild and foamy skin cleaning composition and a preparation method and application thereof, and the skin cleaning composition comprises the following components in parts by weight: 25-65 parts of coconut acyl potassium glycinate; 5-30 parts of lauric acid TEA salt; 70.1-2 parts of polyquaternium; 0.1-3 parts of polyglycerol-10 laurate; 0.1 to 1 portion of oat kernel extract. The mild and multi-foam skin cleaning composition is prepared by compounding surfactant which takes cocoyl potassium glycinate and lauric acid TEA salt as main bodies with components such as polyquaternium-7, polyglycerol-10 laurate, oat kernel extract and the like, on one hand, the mild and multi-foam skin cleaning composition provides rich and dense foam for the product, on the other hand, the smoothness and softness of the skin after the product is used are improved, the problems of tightness, dryness and the like are avoided after the product is used, and the mild and multi-foam skin cleaning composition has the characteristics of rich foam, pleasant washing feeling, mildness, low irritation, strong cleaning capability and the like.
Description
Technical Field
The invention relates to the technical field of daily chemical cosmetics, in particular to a mild and foamy skin cleaning composition (RX-C) and a preparation method and application thereof.
Background
More and more consumers begin to favor healthy products, cleaning products gradually change from the past simple cleaning to the directions of mildness, moisture retention and protection, and more consumers do not want to have the problems of dryness, itch and the like during cleaning; with the increasing standard of living, mild, low-irritation cleansing products will gradually gain market acceptance.
The traditional skin cleaning products usually focus on rich foam to achieve a refreshing face cleaning effect, most of the adopted surfactants are components mainly comprising fatty acid salts or fatty acid salts and some surfactants, and the products have the advantages of rich foam, capability of meeting the requirements of consumers on facial cleaning and refreshing face cleaning feeling, however, the products have the defects of too strong degreasing power, high irritation and dry and itchy conditions after washing.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention provides a mild and foamy skin cleaning composition (RX-C) which has the characteristics of abundant foam, pleasant washing feeling, mildness, low irritation and the like.
The invention also provides a preparation method of the mild and foamy skin cleaning composition.
The invention also provides application of the mild and foamy skin cleaning composition.
The invention is realized by adopting the following technical scheme:
the invention provides a mild and foamy skin cleaning composition which comprises the following components in parts by weight:
25-65 parts of coconut acyl potassium glycinate;
5-30 parts of lauric acid TEA salt;
70.1-2 parts of polyquaternium;
0.1-3 parts of polyglycerol-10 laurate;
0.1 to 1 portion of oat kernel extract.
The mild and multi-foam skin cleaning composition is a surfactant taking cocoyl potassium glycinate and lauric acid TEA salt (triethanolamine laurate) as main bodies, and the surfactant provides rich and dense foam for the product, so that the product has the effects of refreshing fine feeling and good cleaning capability; the polyquaternium-7 is matched with a surfactant, so that the smoothness and the softness of the skin after use can be improved; the polyglycerol-10 laurate (decaglycerol monolaurate) has mild property and strong cleaning capability, and after being compounded with the surfactant, the polyglycerol-10 laurate plays a role in balancing skin oil ester in the product, and is beneficial to preventing the problems of tightness, dryness, itching and the like after washing; the oat kernel extract is added to the composition to help reduce the irritation of the surfactant to the skin during the washing process.
Further, the skin cleaning composition comprises the following components in parts by weight:
30-65 parts of coconut acyl potassium glycinate;
5-30 parts of lauric acid TEA salt;
70.5-2 parts of polyquaternium;
0.5-3 parts of polyglycerol-10 laurate;
0.1 to 1 portion of oat kernel extract.
Further, the skin cleaning composition also comprises the following components in parts by weight:
1-3 parts of propylene glycol;
0.05 part to 0.4 part of hydroxypropyl methyl cellulose;
0.05 part to 0.2 part of EDTA disodium.
The propylene glycol has the moisturizing effect and the antiseptic effect, and can help the penetration of active ingredients and improve the water-holding capacity of the skin by combining with moisture; the aqueous solution of hydroxypropyl methyl cellulose has the advantages of good surface activity, thickening, water retention, film forming property and the like, and can improve the dispersibility of other components of the product in water; the disodium EDTA has mineral chelating effect and synergistic antiseptic effect, and can regulate pH value of the product to protect skin from strong irritation.
Further, the skin cleaning composition also comprises the following components in parts by weight:
1-6 parts of cocoyl amphoacetate;
1-6 parts of cocamidopropyl betaine;
0.5 to 2 portions of cocamide MEA.
The cocoyl amphoacetate and the cocamidopropyl betaine are amphoteric surfactants, the cocoyl amphoacetate is mild and low in irritation, and has the effect of effectively reducing irritation of other surfactants, the foam is rich and fine, and the foam state of a formula system can be obviously improved; the cocamidopropyl betaine is usually used together with anionic, cationic and nonionic surfactants, has good compatibility, small irritation, easy water solubility, acid and alkali stability, good foaming effect, strong detergency, excellent thickening property, softness, bactericidal property, antistatic property and hard water resistance; cocoamide MEA (cocoyl monoethanolamine) is a nonionic surfactant, can thicken a formula, can enhance the cleaning capability of a main cleaning component in the surfactant, and provides excellent moisturizing and conditioning effects for skin.
The invention also provides a mild and foamy skin cleaning composition which comprises the following components in parts by weight:
30-65 parts of coconut acyl potassium glycinate;
1-6 parts of cocoyl amphoacetate;
1-6 parts of cocamidopropyl betaine;
0.5-2 parts of cocamide MEA;
5-30 parts of lauric acid TEA salt;
70.5-2 parts of polyquaternium;
0.5-3 parts of polyglycerol-10 laurate;
0.1 to 1 portion of oat kernel extract;
1-3 parts of propylene glycol;
0.05 part to 0.4 part of hydroxypropyl methyl cellulose;
0.05 part to 0.2 part of EDTA disodium;
5-65 parts of water.
The mild and foamy skin cleaning composition can be directly used for cleaning facial skin, has the characteristics of rich foam, pleasant washing feeling, mildness, low irritation and the like, and enables the skin to have better skin feeling and smooth feeling.
Further, the mass ratio of the potassium cocoyl glycinate, the sodium cocoyl amphoacetate, the polyquaternium-7, the oat kernel extract, the TEA salt of lauric acid and the polyglycerol-10 laurate is 55: 5: 1.5: 0.5: 12-20: 2. the raw materials are reasonably proportioned, so that the foam of the product is more abundant and dense, the delicate feeling is fresh and better, and the cleaning capability is stronger.
Further, the sodium cocoyl amphoacetate: cocamidopropyl betaine: the mass ratio of the cocamide MEA is 5: 3: 1-2. The surfactant is reasonably proportioned, so that the irritation of the product can be effectively reduced, and the cleaning capability of the product is improved.
Further, the mass ratio of the potassium cocoyl glycinate, the polyquaternium-7, the lauric acid TEA salt and the water is 55: 1-2: 15: 20. the raw materials and water are reasonably proportioned, so that the bubble effect of the product can be effectively improved.
The invention also provides a preparation method of the mild and foamy skin cleaning composition, which comprises the following steps:
mixing polyglycerol-10 laurate, potassium cocoyl glycinate, sodium cocoyl amphoacetate, cocamidopropyl betaine, cocamide MEA, lauric acid TEA salt, polyquaternium-7, propylene glycol and water, heating to 55-70 ℃ in a vacuum state, and stirring until the mixture is completely dissolved to obtain a mixture;
sequentially adding oat kernel extract, hydroxypropyl methylcellulose and EDTA disodium into the mixture, controlling the temperature at 50-60 ℃, stirring and preserving the temperature for 20-30 min, observing that the mixture is completely transparent, cooling, and discharging to obtain the mild and foamy skin cleaning composition.
The invention also provides application of the mild and foamy skin cleaning composition in preparation of cosmetics for cleaning skin. The skin-cleaning cosmetic comprises body wash, hand sanitizer, face cleanser, scrub, skin cleaning cream, bubble bath, bath oil, etc.
Compared with the prior art, the invention has the beneficial effects that:
the mild and multi-foam skin cleaning composition disclosed by the invention is prepared by compounding surfactants which take cocoyl glycine potassium and lauric acid TEA salt as main bodies with components such as polyquaternium-7, polyglycerol-10 laurate, oat kernel extract and the like, on one hand, rich and dense foam can be provided for the product, so that the product has the effects of refreshing thin feeling and good cleaning capability, on the other hand, the smoothness and softness of the skin after the product is used can be improved, the problems of tightness, dryness and the like are avoided after the product is used, and the mild and multi-foam skin cleaning composition has the characteristics of rich foam, pleasant washing feeling, mildness, low irritation, strong cleaning capability and the like.
The mild, foamy skin cleansing composition of the present invention can be added to most skin cleansing products, including direct application type skin cleansing liquids or masks, etc., which have a better hydrophilic-lipophilic system and better compatibility with other care ingredients.
The mild and foamy skin cleansing composition of the present invention can form an aqueous emulsion system with uniform texture and stable system, which has better stability and is not easy to precipitate for a long time.
Detailed Description
The present invention is further described below with reference to specific embodiments, and it should be noted that, without conflict, any combination between the embodiments or technical features described below may form a new embodiment.
The invention provides a mild and foamy skin cleaning composition which comprises the following components in parts by weight:
25-65 parts of coconut acyl potassium glycinate; 5-30 parts of lauric acid TEA salt; 70.1-2 parts of polyquaternium; 0.1-3 parts of polyglycerol-10 laurate; 0.1 to 1 portion of oat kernel extract.
Further, the skin cleaning composition also comprises the following components in parts by weight:
1-3 parts of propylene glycol; 0.05 part to 0.4 part of hydroxypropyl methyl cellulose; 0.05 part to 0.2 part of EDTA disodium; 1-6 parts of sodium cocoyl amphoacetate; 1-6 parts of cocamidopropyl betaine; 0.5 to 2 portions of cocamide MEA.
Preferably, the skin cleansing composition comprises the following components in parts by weight:
30-65 parts of coconut acyl potassium glycinate; 1-6 parts of sodium cocoyl amphoacetate; 1-6 parts of cocamidopropyl betaine; 0.5-2 parts of cocamide MEA; 5-30 parts of lauric acid TEA salt; 70.5-2 parts of polyquaternium; 0.5-3 parts of polyglycerol-10 laurate; 0.1 to 1 portion of oat kernel extract; 1-3 parts of propylene glycol; 0.05 part to 0.4 part of hydroxypropyl methyl cellulose; 0.05 part to 0.2 part of EDTA disodium; 5-65 parts of water.
Wherein, the cocoyl glycine potassium has the INCI name: coconut acyl potassium glycinate, numbered (07561) in the catalogue of used cosmetic raw materials (2015 edition) in china, contains coconut acyl potassium glycinate, which is an anionic surfactant synthesized from coconut oil fatty acid and glycine (one of 28 amino acids necessary for human bodies), has smooth and elastic foam, is different from the traditional soap-based products, and has the effects of cleaning and not tightening after being washed by coconut acyl glycine, smooth and refreshing feeling, mildness and the like.
The sodium cocoyl amphoacetate has the INCI name: sodium cocoyl amphoacetate, which is contained in the catalog of names of used cosmetic raw materials (2015 edition) in China as No. (07586). Sodium cocoyl amphoacetate is a type of amphoteric surfactant, has a group of positive charges and a group of negative charges, and exhibits anionic surfactant properties under alkaline conditions and cationic surfactant properties under acidic conditions. The cocoyl amphoacetate is mild and low in irritation, and has the effect of effectively reducing irritation of other surfactants. Can be widely applied to personal cleaning products, especially sensitive skin or products requiring low irritation.
The polyquaternium-7, INCI name: polyquaternium-7, numbered (03946) in catalog of names of used cosmetic raw materials (2015) in China contains Polyquaternium-7. Polyquaternium-7, alias M550, chinese name: dimethyldiallylammonium chloride-acrylamide copolymers. Polyquaternium-7 is a cationic high-molecular polymer, and has effects of reducing surface activity irritation, enhancing foam, and improving smoothness and softness of skin after use.
The oat (AVENA SATIVA) kernel extract, INCI name: oat (AVENA SATIVA) kernel extract, serial number (07404) in the catalogue of used cosmetic raw materials (2015 edition) in china contains oat (AVENA SATIVA) kernel extract. The oat (AVENA SATIVA) kernel extract is derived from natural active ingredients of oat kernel, has remarkable improvement effect on sensitive skin, can reduce external irritation and adverse effect of adverse environment on skin, and can remarkably reduce irritation of surfactant on skin and eyes.
The lauric acid TEA salt, INCI name: lauric acid TEA salt, No. (08382) in the catalog of names of used cosmetic raw materials in china (2015 edition), contains lauric acid TEA salt. The lauric acid TEA salt is prepared by reacting lauric acid and triethanolamine, and has soft and dense foam.
The polyglycerol-10 laurate, INCI name: polyglycerol-10 laurate, numbered (03800) in the catalogue of used cosmetic raw materials (2015) in china, contains polyglycerol-10 laurate. The polyglycerol-10 laurate is prepared by the reaction of polyglycerol-10 and laurate, has mild property and strong cleaning capability, can be used as a nonionic surfactant and has the fat-endowing effect when being added into washing products, and has lower irritation than the polyoxyethylene fatty acid ester products.
Preferably, the mass ratio of the potassium cocoyl glycinate to the sodium cocoyl amphoacetate to the polyquaternium-7 to the oat kernel extract to the TEA laurate to the polyglycerol-10 laurate is 55: 5: 1.5: 0.5: 12-20: 2. the sodium cocoamphoacetate: cocamidopropyl betaine: the mass ratio of the cocamide MEA is 5: 3: 1-2. The mass ratio of the cocoyl glycine potassium, the polyquaternium-7, the lauric acid TEA salt and the water is 55: 1-2: 15: 20.
the invention also provides a preparation method of the mild and foamy skin cleaning composition, which comprises the following steps:
mixing polyglycerol-10 laurate, potassium cocoyl glycinate, sodium cocoyl amphoacetate, cocamidopropyl betaine, cocamide MEA, lauric acid TEA salt, polyquaternium-7, propylene glycol and water, heating to 55-70 ℃ in a vacuum state, and stirring until the mixture is completely dissolved to obtain a mixture;
sequentially adding oat kernel extract, hydroxypropyl methylcellulose and EDTA disodium into the mixture, controlling the temperature at 50-60 ℃, stirring and preserving the temperature for 20-30 min, observing that the mixture is completely transparent, cooling, and discharging to obtain the mild and foamy skin cleaning composition.
Because the mild and foamy skin cleansing composition has a better hydrophilic-lipophilic system, the mild and foamy skin cleansing composition can be added into most skin cleansing products and has better compatibility with other care ingredients, and the skin cleansing cosmetics comprise shower gel, hand sanitizer, facial cleanser, scrub cream, skin cleansing cream, bubble bath, bath oil and the like.
The following are specific examples of the present invention, and raw materials, equipment, and the like used in the following examples can be obtained by purchasing, unless otherwise specified.
In the following embodiments, the water is pure water or deionized water, unless otherwise specified.
Wherein, the cocoyl potassium glycinate is purchased from the Kesi company with the model number: AMILITE GCK-12/GCK-12K (potassium cocoyl glycinate);
sodium cocoyl amphoacetate purchased from winning companies and having the following model: REWOTERIC AMC (sodium cocoamphoacetate);
polyquaternary ammonium salt-7, available from Luborun corporation, of the type: merquatTM550Polymer；
Oat kernel extract, which is purchased from the raw materials of a gathering company and is named as avenanthramide;
lauric acid TEA salt, available from Synf under the product name lauric acid TEA salt;
polyglycerol-10 laurate, available from nippon oil & fat company, model number: ML-10.
Example 1
The mild and foamy skin cleaning composition comprises the following components in parts by weight:
30 parts of coconut acyl potassium glycinate; 1 part of sodium cocoyl amphoacetate; 1 part of cocamidopropyl betaine; 0.5 part of cocamide MEA; 5 parts of lauric acid TEA salt; 70.5 parts of polyquaternium; 0.5 part of polyglycerol-10 laurate; 0.1 part of oat kernel extract; 1 part of propylene glycol; 0.05 part of hydroxypropyl methyl cellulose; 0.05 part of EDTA disodium; and 5 parts of water.
The mild and foamy skin cleaning composition comprises the following preparation steps:
mixing polyglycerol-10 laurate, potassium cocoyl glycinate, sodium cocoyl amphoacetate, cocamidopropyl betaine, cocamide MEA, lauric acid TEA salt, polyquaternium-7, propylene glycol and water, heating to 65 ℃ in a vacuum state, and stirring until the mixture is completely dissolved to obtain a mixture;
and sequentially adding the oat kernel extract, hydroxypropyl methylcellulose and EDTA disodium into the mixture, controlling the temperature at 60 ℃, stirring and preserving the temperature for 30min, observing that the mixture is completely transparent, cooling, and discharging to obtain the mild and foamy skin cleaning composition.
Example 2
Example 2 unlike example 1, the mild, lathering skin cleansing composition comprises the following components in parts by weight:
30 parts of coconut acyl potassium glycinate; 1 part of sodium cocoyl amphoacetate; 1 part of cocamidopropyl betaine; 0.5 part of cocamide MEA; 5 parts of lauric acid TEA salt; 70.5 parts of polyquaternium; 0.5 part of polyglycerol-10 laurate; 0.1 part of oat kernel extract; 1 part of propylene glycol; 0.05 part of hydroxypropyl methyl cellulose; 0.05 part of EDTA disodium; 60.3 parts of water.
Example 3
Example 3 unlike example 1, the mild, lathering skin cleansing composition comprises the following components in parts by weight:
40 parts of coconut acyl potassium glycinate; 3 parts of cocoyl amphoacetate; 3 parts of cocamidopropyl betaine; 2 parts of cocamide MEA; 30 parts of lauric acid TEA salt; 72 parts of polyquaternium; 3 parts of polyglycerol-10 laurate; 1 part of oat kernel extract; 3 parts of propylene glycol; 0.4 part of hydroxypropyl methyl cellulose; 0.2 part of EDTA disodium; 12.4 parts of water.
Example 4
Example 4 unlike example 1, the mild, lathering skin cleansing composition comprises the following components in parts by weight:
45 parts of coconut acyl potassium glycinate; 3 parts of cocoyl amphoacetate; 3 parts of cocamidopropyl betaine; 1 parts of cocamide MEA; 20 parts of lauric acid TEA salt; polyquaternium-71 parts; 2 parts of polyglycerol-10 laurate; 0.5 part of oat kernel extract; 2 parts of propylene glycol; 0.2 part of hydroxypropyl methyl cellulose; 0.1 part of EDTA disodium; and 30 parts of water.
Example 5
Example 5 unlike example 1, the mild, lathering skin cleansing composition comprises the following components in parts by weight:
55 parts of coconut acyl potassium glycinate; 5 parts of cocoyl amphoacetate; 3 parts of cocamidopropyl betaine; 1 parts of cocamide MEA; 15 parts of lauric acid TEA salt; 71.5 parts of polyquaternium; 2 parts of polyglycerol-10 laurate; 0.5 part of oat kernel extract; 2 parts of propylene glycol; 0.2 part of hydroxypropyl methyl cellulose; 0.1 part of EDTA disodium; and 20 parts of water.
Example 6
Example 6 unlike example 1, the mild, lathering skin cleansing composition comprises the following components in parts by weight:
65 parts of coconut acyl potassium glycinate; 6 parts of cocoyl amphoacetate; 6 parts of cocamidopropyl betaine; 2 parts of cocamide MEA; 10 parts of lauric acid TEA salt; 72 parts of polyquaternium; 1 part of polyglycerol-10 laurate; 0.3 part of oat kernel extract; 2 parts of propylene glycol; 0.1 part of hydroxypropyl methyl cellulose; 0.1 part of EDTA disodium; and 5.5 parts of water.
Example 7
Example 7 unlike example 1, the mild, lathering skin cleansing composition comprises the following components in parts by weight:
65 parts of coconut acyl potassium glycinate; 6 parts of cocoyl amphoacetate; 6 parts of cocamidopropyl betaine; 2 parts of cocamide MEA; 30 parts of lauric acid TEA salt; 72 parts of polyquaternium; 3 parts of polyglycerol-10 laurate; 1 part of oat kernel extract; 3 parts of propylene glycol; 0.4 part of hydroxypropyl methyl cellulose; 0.2 part of EDTA disodium; and 65 parts of water.
Comparative example 1
Comparative example 1 is a skin cleansing composition, which is different from example 1 in that no potassium cocoyl glycinate was used as the raw material of comparative example 1.
Comparative example 2
Comparative example 2 is a skin cleansing composition, which is different from example 1 in that the raw material of comparative example 1 does not use lauric acid TEA salt.
Comparative example 3
Comparative example 3 is a skin cleansing composition, which is different from example 1 in that the raw material of comparative example 1 does not use oat kernel extract.
And (3) performance detection:
first, Mild Effect determination
1. The experimental method comprises the following steps: each example selected 30 eligible subjects for testing.
Adopting skin closed patch test, selecting patch with area not more than 50mm2And qualified spot test equipment with the depth of about 1 mm.
Placing the experimental product into a spot tester chamber, wherein the dosage is about 0.020mL-0.025mL, applying the spot tester with the tested object to the curved side of the forearm of the tested object by using hypoallergenic adhesive tape, slightly pressing the spot tester with the palm to uniformly apply the spot tester to the skin for 24 hours, and observing the skin reaction for 24 hours according to the skin reaction grading standard of the skin-closed spot test.
2. The results of the tests, are given in table 1 below:
TABLE 1
Note: + represents no adverse reaction; + represents that a small amount of irritation can be felt but no adverse reaction occurs; the + and + indicates that strong stimulation can be felt, but no adverse reaction occurs; the sign of +++ indicates that strong irritation is felt and adverse reaction occurs.
As can be seen from table 1, the skin cleansing composition provided by the present invention has a synergistic effect between the raw materials, and the composition is a mild and safe composition.
Second, testing foaming ability
1. The test method comprises the following steps: the foaming force was measured by reference to the ROSS-Miles method, and the foam height was read immediately after the test, 5 minutes after the test, and the average of three readings was taken.
2. The results of the tests, are given in table 2 below:
TABLE 2
As can be seen from Table 2, the compositions of examples 1 to 7 of the present invention have a strong foaming power, particularly the compositions of example 5, as compared with those of comparative examples 1 to 3.
The above embodiments are only preferred embodiments of the present invention, and the protection scope of the present invention is not limited thereby, and any insubstantial changes and substitutions made by those skilled in the art based on the present invention are within the protection scope of the present invention.
Claims (10)
1. The mild and foamy skin cleaning composition is characterized by comprising the following components in parts by weight:
25-65 parts of coconut acyl potassium glycinate;
5-30 parts of lauric acid TEA salt;
70.1-2 parts of polyquaternium;
0.1-3 parts of polyglycerol-10 laurate;
0.1 to 1 portion of oat kernel extract.
2. The mild, lathering skin cleansing composition according to claim 1 wherein said skin cleansing composition comprises the following components in parts by weight:
30-65 parts of coconut acyl potassium glycinate;
5-30 parts of lauric acid TEA salt;
70.5-2 parts of polyquaternium;
0.5-3 parts of polyglycerol-10 laurate;
0.1 to 1 portion of oat kernel extract.
3. The mild, lathering skin cleansing composition according to claim 2 further comprising the following components in parts by weight:
1-3 parts of propylene glycol;
0.05 part to 0.4 part of hydroxypropyl methyl cellulose;
0.05 part to 0.2 part of EDTA disodium.
4. The mild, lathering skin cleansing composition according to claim 2 further comprising the following components in parts by weight:
1-6 parts of sodium cocoyl amphoacetate;
1-6 parts of cocamidopropyl betaine;
0.5 to 2 portions of cocamide MEA.
5. The mild and foamy skin cleaning composition is characterized by comprising the following components in parts by weight:
30-65 parts of coconut acyl potassium glycinate;
1-6 parts of sodium cocoyl amphoacetate;
1-6 parts of cocamidopropyl betaine;
0.5-2 parts of cocamide MEA;
5-30 parts of lauric acid TEA salt;
70.5-2 parts of polyquaternium;
0.5-3 parts of polyglycerol-10 laurate;
0.1 to 1 portion of oat kernel extract;
1-3 parts of propylene glycol;
0.05 part to 0.4 part of hydroxypropyl methyl cellulose;
0.05 part to 0.2 part of EDTA disodium;
5-65 parts of water.
6. The mild, lathering skin cleansing composition according to claim 5 wherein the ratio by mass of potassium cocoyl glycinate, sodium cocoyl amphoacetate, polyquaternium-7, oat kernel extract, TEA laurate, polyglycerol-10 laurate is 55: 5: 1.5: 0.5: 12-20: 2.
7. the mild, lathering skin cleansing composition according to claim 5 wherein said sodium cocoyl amphoacetate: cocamidopropyl betaine: the mass ratio of the cocamide MEA is 5: 3: 1-2.
8. The mild, multivesicular skin cleansing composition according to claim 5, wherein the mass ratio of potassium cocoyl glycinate, polyquaternium-7, TEA laurate, and water is 55: 1-2: 15: 20.
9. a method for preparing a mild, lathering skin cleansing composition comprising the steps of:
mixing polyglycerol-10 laurate, potassium cocoyl glycinate, sodium cocoyl amphoacetate, cocamidopropyl betaine, cocamide MEA, lauric acid TEA salt, polyquaternium-7, propylene glycol and water, heating to 55-70 ℃ in a vacuum state, and stirring until the mixture is completely dissolved to obtain a mixture;
sequentially adding oat kernel extract, hydroxypropyl methylcellulose and EDTA disodium into the mixture, controlling the temperature at 50-60 ℃, stirring and preserving the temperature for 20-30 min, observing that the mixture is completely transparent, cooling, and discharging to obtain the mild and foamy skin cleaning composition.
10. Use of a mild, lathering skin cleansing composition according to any one of claims 1 to 8 in the preparation of a cosmetic product for cleansing the skin.
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