CN106580795A - Extraction method of Tuwei flower extract having effects of moisture retention and whitening - Google Patents
Extraction method of Tuwei flower extract having effects of moisture retention and whitening Download PDFInfo
- Publication number
- CN106580795A CN106580795A CN201611237548.3A CN201611237548A CN106580795A CN 106580795 A CN106580795 A CN 106580795A CN 201611237548 A CN201611237548 A CN 201611237548A CN 106580795 A CN106580795 A CN 106580795A
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- China
- Prior art keywords
- common vetch
- edible plant
- bitter edible
- plant common
- boiler
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
Abstract
The invention discloses an extraction method of Tuwei flower extract having effects of moisture retention and whitening. The extraction method comprises (1) removing receptacles of fresh Tuwei flowers, retaining petals, chopping the petals and adding the chopped petals into a distillation pot prepared from a specific material, (2) adding a plant-derived phenol substance and a hydroalcoholic solution into the distillation pot and controlling the temperature and pressure in the distillation pot, (3) collecting the volatile low-boiling point Tuwei flower essence/water solution by condensing, (4) filtering the materials in the distillation pot, removing flower dregs and collecting a high-boiling point Tuwei flower original color essence/alcohol solution, and (5) mixing the low-boiling point Tuwei flower essence/water solution and high-boiling point Tuwei flower original color essence/alcohol solution to obtain Tuwei flower essence extract. The Tuwei flower essence extract can be used for preparation of cosmetics such as shampoo, shower gel, hand cream, toner, cream and lotion and has good effects of moisturizing and whitening skin.
Description
Technical field
The present invention relates to a kind of extracting method of natural plants, and in particular to a kind of bitter edible plant common vetch with moisturizing and white-skinned face function
The extracting method of flower extract.
Background technology
Bitter edible plant common vetch flower is a kind of peculiar Flos Rosae Rugosae flower variety of the little olive area plantation in Zhongshan City, Guangdong Province, is that Rosaceae Rosa is planted
The pale reddish brown polyphyll Flos Rosae Rugosae of thing.Bitter edible plant common vetch flower is applied to food (such as drinks, cookiess) industry very long history, but it is applied
It is not yet reported on personal care articles.
The extraction of flower elite, at present frequently with hydrodistillation or vegetable oil solvent extraction or supercritical CO2Extraction.
Hydrodistillation is together to distill flower and water, the flower elite obtained after collection.This flower elite is lower boiling part,
Although the method is simple to operate, have the disadvantage, substantial amounts of high boiling flower elite and the basic nothing of water-fast flower elite
Method is extracted.Vegetable oil solvent extraction is, by flower and some vegetable oil mixing, to contact through long-term immersion, flower essence
China is lentamente dissolved in oil phase.But time-consuming for the method, and vegetable oil is apt to deteriorate, corruption, some water miscible flowers
Elite still cannot be extracted.Supercritical CO2Extraction is to utilize CO2As solvent, flower oiliness elite, but this are extracted
Method equipment is very expensive, and conditional parameter when extracting is complicated, it is not easy to control, so not being used widely.
The content of the invention
For the problem that prior art is present, it is an object of the invention to provide a kind of bitter edible plant common vetch with moisturizing and white-skinned face function
The extracting method of flower extract.
To achieve these goals, the present invention is employed the following technical solutions：
A kind of extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function, comprises the following steps：
(1) holder of fresh bitter edible plant common vetch flower is extractd, after remaining bitter edible plant common vetch flower petal is shredded, is added in boiler；
(2) aldehydes matter of plant origin is added toward in boiler；
(3) 0.1-20 times of bitter edible plant common vetch is added to spend the pure water of petal weight toward in boiler；It is further preferably 0.2-15
Times；More preferably 0.5-10 times；
(4) 0.1-20 times of bitter edible plant common vetch is added to spend the alcohol of petal weight toward in boiler；It is further preferably 0.2-15 times；More
Preferably 0.5-10 times；
(5) by the material stirring in boiler it is uniform after, heated, steam through condenser cool down, received with catcher
Collection low boiling bitter edible plant common vetch flower essence/aqueous solution, after moisture all volatilization heating is stopped；
(6) material in boiler is filtered, bitter edible plant common vetch flower residue is removed, high boiling bitter edible plant common vetch flower primary colors essence/alcohol is obtained molten
Liquid；
(7) spend essence/aqueous solution and high boiling bitter edible plant common vetch flower primary colors essence/alcoholic solution mixing equal low boiling bitter edible plant common vetch
It is even, obtain bitter edible plant common vetch flower extract.
Preferably, the material of the boiler is the one kind in 304 rustless steels, 316 rustless steels, 316L rustless steels, copper, aluminum
Or it is various；Preferred material is 316L rustless steels and copper.
Preferably, the aldehydes matter of plant origin described in step (2) includes in chamenol, totarol, magnolol
Plant or various.
Preferably, the addition of the aldehydes matter of plant origin described in step (2) is that bitter edible plant common vetch spends petal weight
0.000001-1 times；It is further preferably 0.000002-0.5 times；More preferably 0.00001-0.2 times.
Preferably, alcohol described in step (4) is 1 for the ratio of dihydroxylic alcohols and/or polyhydric alcohol, dihydroxylic alcohols and polyhydric alcohol：20
To 20：1, more preferably 1：10 to 10：1.
Preferably, the dihydroxylic alcohols are one or more in Propylene Glycol, butanediol, pentanediol, hexanediol, ethohexadiol.
Preferably, the polyhydric alcohol is in glycerol, Sorbitol, maltol, mannitol, glucitol, dipropylene glycol
One or more.
Preferably, vapo(u)rizing temperature described in step (5) is 80-120 DEG C；More preferably 95-110 DEG C.
Preferably, the pressure described in step (5) in boiler is 0.90-1.08 normal atmosphere；More preferably
0.95-1.05 normal atmosphere.
The technical problem to be solved is to provide a kind of bitter edible plant common vetch flower extract with moisturizing and white-skinned face function
Extracting method, the method does not use organic/toxic solvent, does not use putrefactive vegetable oil, safe and simple to operate, is not required to
The fund for wanting both expensive buys supercritical CO2Extraction equipment, it is not only economical and practical, and compare supercritical CO2Extraction is extracted
The elite of more water alcohol dissolvings, such as Air Bladder pseudosciaenae seu Acipenser matter, polysaccharide, aminoacid etc..
Present invention incorporates hydrodistillation, is creatively introduced into alcoholic solution in water phase, the alcoholic solution of the present invention is in high temperature
Under, good stability, and the property with vegetable oil, bitter edible plant common vetch can be dissolved and spend oil-soluble elite.Inventor is surprised to find that
Through catalysis extract abnormal smells from the patient can be allowed purer by being used in combination the boiler of special substance and the aldehydes matter of plant origin, and
With significant moisturizing and white-skinned face function.This extracting method farthest extract the bitter edible plant common vetch flower extract, including volatilization
Low boiling bitter edible plant common vetch HUAJING China, high boiling point bitter edible plant common vetch flower extract in non-volatile alcoholic solution phase in water-soluble liquid phase.This extracting method operation
Simple easy, convenient and swift, economy, it is important that retain in bitter edible plant common vetch flower extraction process a large amount of bitter edible plant common vetch spend natural aromatic substance and
Active component.The bitter edible plant common vetch flower extract of the present invention is catalyzed in the boiler of specific materials through aldehydes matter, and uses water alcohol
System comprehensively extracts the effective ingredient that bitter edible plant common vetch is spent, with good moisturizing and white-skinned face function.
Beneficial effects of the present invention：
(1) alcoholic solution of present invention addition is the natural material of ECO certifications, does not add the biologies such as glycosidase, cellulase
Enzyme and other industrial chemicals, so bitter edible plant common vetch flower extract is natural safe；
(2) extracting method of the invention is simple to operate, and low cost, efficiency high can more effectively extract bitter edible plant common vetch and spend middle day
Right aromatic substance and active component；
(3) bitter edible plant common vetch flower extract of the invention has extensive use, can be used to prepare article of everyday use, cosmetics, for example, take a shower
Dew, shampoo, cosmetic water, hand cream etc..
Specific embodiment
In order to preferably explain the present invention, it is described further in conjunction with specific examples below, but the present invention is not limited
In specific embodiment.
Embodiment 1
A kind of extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function, comprises the following steps：
(1) the fresh bitter edible plant common vetch flower that 1000g has removed holder is weighed, after petal is shredded, the steaming of fine copper material is added to
In evaporating pot；
(2) 0.01g chamenols are added toward in boiler；
(3) 3000g pure water is added toward in boiler；
(4) 500g1,2- Propylene Glycol are added toward in boiler；
(5) by the material stirring in boiler it is uniform after, it is that 95 DEG C and pressure are to heat and control to distill kettle temperature
0.98 normal atmosphere, when vapor is after condenser cooling, with catcher low boiling bitter edible plant common vetch flower essence/water-soluble is collected
Liquid, when moisture content all volatilizees, and there was only 1,2-PD solution in boiler, stops heating；
(6) filter the material in boiler and remove bitter edible plant common vetch flower residue, it is molten that collection obtains high boiling point bitter edible plant common vetch flower primary colors essence/alcohol
Liquid；
(7) spend essence/aqueous solution and high boiling bitter edible plant common vetch flower primary colors essence/alcoholic solution mixing equal low boiling bitter edible plant common vetch
It is even, obtain the bitter edible plant common vetch HUAJING China extract 3517g of the present invention.
Embodiment 2
A kind of extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function, comprises the following steps：
(1) the fresh bitter edible plant common vetch flower that 1000g has removed holder is weighed, after petal is shredded, 316L stainless steels is added to
In the boiler of matter；
(2) 0.015g totarols are added toward in boiler；
(3) 2000g pure water is added toward in boiler；
(4) 800g dipropylene glycol and 1200g glycerol are added toward in boiler；
(5) by the material stirring in boiler it is uniform after, it is that 100 DEG C and pressure are to heat and control to distill kettle temperature
0.98 normal atmosphere, when vapor is after condenser cooling, with catcher low boiling bitter edible plant common vetch flower essence/water-soluble is collected
Liquid, when moisture content all volatilizees, and there was only dipropylene glycol and glycerite in boiler, stops heating；
(6) filter the material in boiler and remove bitter edible plant common vetch flower residue, it is molten that collection obtains high boiling point bitter edible plant common vetch flower primary colors essence/alcohol
Liquid；
(7) spend essence/aqueous solution and high boiling bitter edible plant common vetch flower primary colors essence/alcoholic solution mixing equal low boiling bitter edible plant common vetch
It is even, obtain the bitter edible plant common vetch HUAJING China extract 4020g of the present invention.
Embodiment 3
A kind of extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function, comprises the following steps：
(1) the fresh bitter edible plant common vetch flower that 1000g has removed holder is weighed, after petal is shredded, 316L stainless steels is added to
In the boiler of matter；
(2) 0.02g totarols are added toward in boiler；
(3) 4000g pure water is added toward in boiler；
(4) 2000g butanediols are added toward in boiler；
(5) by the material stirring in boiler it is uniform after, it is that 103 DEG C and pressure are to heat and control to distill kettle temperature
1.03 normal atmospheres, when vapor is after condenser cooling, with catcher low boiling bitter edible plant common vetch flower essence/water-soluble are collected
Liquid, when moisture content all volatilizees, and there was only butanediol solution in boiler, stops heating；
(6) filter the material in boiler and remove bitter edible plant common vetch flower residue, it is molten that collection obtains high boiling point bitter edible plant common vetch flower primary colors essence/alcohol
Liquid；
(7) spend essence/aqueous solution and high boiling bitter edible plant common vetch flower primary colors essence/alcoholic solution mixing equal low boiling bitter edible plant common vetch
It is even, obtain the bitter edible plant common vetch HUAJING China extract 6024g of the present invention.
Embodiment 4
A kind of extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function, comprises the following steps：
(1) the fresh bitter edible plant common vetch flower that 1000g has removed holder is weighed, after petal is shredded, the steaming of fine copper material is added to
In evaporating pot；
(2) 0.015g chamenols are added toward in boiler；
(3) 1000g pure water is added toward in boiler；
(4) 1500g glycerol is added toward in boiler；
(5) by the material stirring in boiler it is uniform after, heat and control to distill kettle temperature be 103 DEG C and pressure be 1
Individual normal atmosphere, when vapor is after condenser cooling, with catcher low boiling bitter edible plant common vetch flower essence/aqueous solution is collected,
When moisture content all volatilizees, and there was only glycerite in boiler, stop heating；
(6) filter the material in boiler and remove bitter edible plant common vetch flower residue, it is molten that collection obtains high boiling point bitter edible plant common vetch flower primary colors essence/alcohol
Liquid；
(7) spend essence/aqueous solution and high boiling bitter edible plant common vetch flower primary colors essence/alcoholic solution mixing equal low boiling bitter edible plant common vetch
It is even, obtain the bitter edible plant common vetch HUAJING China extract 2525g of the present invention.
Comparative example 1
A kind of extracting method of bitter edible plant common vetch flower extract, comprises the following steps：
(1) the fresh bitter edible plant common vetch flower that 1000g has removed holder is weighed, after petal is shredded, the steaming of enamel material is added to
In evaporating pot；
(2) 3000g pure water is added toward in boiler；
(3) 500g1,2- Propylene Glycol are added toward in boiler；
(4) by the material stirring in boiler it is uniform after, it is that 95 DEG C and pressure are to heat and control to distill kettle temperature
0.98 normal atmosphere, when vapor is after condenser cooling, with catcher low boiling bitter edible plant common vetch flower essence/water-soluble is collected
Liquid, when moisture content all volatilizees, and there was only 1,2-PD solution in boiler, stops heating；
(5) filter the material in boiler and remove bitter edible plant common vetch flower residue, it is molten that collection obtains high boiling point bitter edible plant common vetch flower primary colors essence/alcohol
Liquid；
(6) spend essence/aqueous solution and high boiling bitter edible plant common vetch flower primary colors essence/alcoholic solution mixing equal low boiling bitter edible plant common vetch
It is even, obtain bitter edible plant common vetch flower extract 3520g.
Comparative example 2
A kind of extracting method of bitter edible plant common vetch flower extract, comprises the following steps：
(1) the fresh bitter edible plant common vetch flower that 1000g has removed holder is weighed, after petal is shredded, 316L stainless steels is added to
In the boiler of matter；
(2) 4000g pure water is added toward in boiler；
(3) 2000g butanediols are added toward in boiler；
(4) by the material stirring in boiler it is uniform after, it is that 103 DEG C and pressure are to heat and control to distill kettle temperature
1.03 normal atmospheres, when vapor is after condenser cooling, with catcher low boiling bitter edible plant common vetch flower essence/water-soluble are collected
Liquid, when moisture content all volatilizees, and there was only butanediol solution in boiler, stops heating；
(5) filter the material in boiler and remove bitter edible plant common vetch flower residue, it is molten that collection obtains high boiling point bitter edible plant common vetch flower primary colors essence/alcohol
Liquid；
(6) spend essence/aqueous solution and high boiling bitter edible plant common vetch flower primary colors essence/alcoholic solution mixing equal low boiling bitter edible plant common vetch
It is even, obtain bitter edible plant common vetch flower extract 6020g.
Moistening effect is tested
According to QB/T4256《Cosmetics moisture-keeping efficacy evaluation guide》Method, with capacitance method determine keratodermatitis moisture content
Content.
25 effective volunteers in 25 DEG C of temperature, humidity be 50% environment in tested.In volunteer's both hands forearm
The region of difference 13 × 3cm of labelling, then with the bitter edible plant common vetch flower extract single application of the present invention.With the CM825 skins of CK companies
Humidity measurements (MMV before the test volunteer's forearm marked region coating of skin water tester0) and coating after 1 hour humidity survey
Value (MMV1).Moistening effect assessment result is shown in Table 1.
Skin moisture content rate of increase %=(MMV1-MMV0)/MMV0 × 100%
Evaluation criteria is：
A：Skin moisture content rate of increase %≤0
B:0 ＜ skin moisture content rate of increase %≤15%
C:15% ＜ skin moisture content rate of increase %≤30%
D:30% ＜ skin moisture content rate of increase %≤50%
E:50% ＜ skin moisture content rate of increase %
Table 1
The boiler using special substance is can be seen that from the test result of table 1 and add the phenolic material of plant origin
After matter, then there is significant moistening effect through 2 sections of bitter edible plant common vetch flower extracts for extracting.
Whitening effect is tested
25 effective volunteers smear bitter edible plant common vetch flower the continuous morning and evening daily in 1 month in the region of one 2*2CM of left forearm
Do reference in extract, right arm corresponding region.After 1 month, using Lab colorimeter system colour difference meters (CM-2000D) measurement assessments area
The L-value (brightness) in domain is calculating Δ L-value.The results are shown in Table 2 (Δ L-value is bigger to represent that whitening effect is better).
Table 2
The boiler with special substance is can be seen that from the test result of table 2 and add the aldehydes matter of plant origin
Afterwards, than only through 2 sections extraction bitter edible plant common vetch flower extracts have significant whitening effect.
Claims (9)
1. a kind of extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function, it is characterised in that comprise the following steps：
（1）The holder of fresh bitter edible plant common vetch flower is extractd, after remaining bitter edible plant common vetch flower petal is shredded, is added in boiler；
（2）The aldehydes matter of plant origin is added toward in boiler；
（3）0.1-20 times of bitter edible plant common vetch is added to spend the pure water of petal weight toward in boiler；
（4）0.1-20 times of bitter edible plant common vetch is added to spend the alcohol of petal weight toward in boiler；
（5）By the material stirring in boiler it is uniform after, begin to warm up, steam through condenser cool down, with catcher collect it is low
Boiling point bitter edible plant common vetch spends essence/aqueous solution, and after moisture all volatilization heating is stopped；
（6）The material in boiler is filtered, bitter edible plant common vetch flower residue is removed, high boiling bitter edible plant common vetch flower primary colors essence/alcoholic solution is obtained；
（7）Low boiling bitter edible plant common vetch is spent into essence/aqueous solution and high boiling bitter edible plant common vetch flower primary colors essence/alcoholic solution mix homogeneously, is obtained
To bitter edible plant common vetch flower extract.
2. the extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function according to claim 1, its feature exists
In step（1）Described in boiler material be one kind in 304 rustless steels, 316 rustless steels, 316L rustless steels, copper, aluminum or
It is various.
3. the extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function according to claim 1, its feature exists
In step（2）Described in plant origin aldehydes matter include chamenol, totarol, magnolol in one or more.
4. the extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function according to claim 1 or 3, its feature
It is, step（2）Described in the addition of aldehydes matter of plant origin be that bitter edible plant common vetch spends 0.000001-1 times of petal weight.
5. the extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function according to claim 1, its feature exists
In step（4）Described in alcohol be dihydroxylic alcohols and/or polyhydric alcohol.
6. the extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function according to claim 5, its feature exists
In the dihydroxylic alcohols are one or more in Propylene Glycol, butanediol, pentanediol, hexanediol, ethohexadiol.
7. the extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function according to claim 5, its feature exists
In the polyhydric alcohol is one or more in glycerol, Sorbitol, maltol, mannitol, glucitol, dipropylene glycol.
8. the extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function according to claim 1, its feature exists
In step（5）Middle vapo(u)rizing temperature is 80-120 DEG C.
9. the extracting method with moisturizing and the bitter edible plant common vetch flower extract of white-skinned face function according to claim 1, its feature exists
In step（5）Pressure in middle boiler is 0.90-1.08 normal atmosphere.
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|---|---|---|---|
| CN201611237548.3A CN106580795A (en) | 2016-12-28 | 2016-12-28 | Extraction method of Tuwei flower extract having effects of moisture retention and whitening |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611237548.3A CN106580795A (en) | 2016-12-28 | 2016-12-28 | Extraction method of Tuwei flower extract having effects of moisture retention and whitening |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109966211A (en) * | 2019-05-05 | 2019-07-05 | 上海悦目化妆品有限公司 | A kind of fresh extraction technology of plant and its application in cosmetic mask |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101282708A (en) * | 2005-10-05 | 2008-10-08 | 江崎格力高株式会社 | External preparation for skin containing a phosphorlated saccharide |
| CN105853271A (en) * | 2016-04-11 | 2016-08-17 | 中山市荼薇化妆品有限公司 | Personnel cleaning composition containing Tuwei rose flower extract |
| CN106176480A (en) * | 2016-08-30 | 2016-12-07 | 广州品赫化妆品有限公司 | A kind of food grade compositions with antiseptic activity and the application in cosmetics thereof |
-
2016
- 2016-12-28 CN CN201611237548.3A patent/CN106580795A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101282708A (en) * | 2005-10-05 | 2008-10-08 | 江崎格力高株式会社 | External preparation for skin containing a phosphorlated saccharide |
| CN105853271A (en) * | 2016-04-11 | 2016-08-17 | 中山市荼薇化妆品有限公司 | Personnel cleaning composition containing Tuwei rose flower extract |
| CN106176480A (en) * | 2016-08-30 | 2016-12-07 | 广州品赫化妆品有限公司 | A kind of food grade compositions with antiseptic activity and the application in cosmetics thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109966211A (en) * | 2019-05-05 | 2019-07-05 | 上海悦目化妆品有限公司 | A kind of fresh extraction technology of plant and its application in cosmetic mask |
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Application publication date: 20170426 |