CN112656715A - Artemisia argyi skin-moistening antibacterial hand cream and preparation method thereof - Google Patents
Artemisia argyi skin-moistening antibacterial hand cream and preparation method thereof Download PDFInfo
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Abstract
The wormwood skin-moistening antibacterial hand cream comprises the following raw materials in parts by weight: 3-10 parts of wormwood plant essential oil, 8-15 parts of sweet almond oil, 8-20 parts of shea butter, 2-8 parts of vitamin E, 3-10 parts of nicotinamide, 3-10 parts of amino acid humectant, 5-12 parts of glycerol, 3-10 parts of cosmetic grade urea, 3-8 parts of plant emulsifier and the balance of deionized water. The preparation method comprises the following steps: mixing sweet almond oil, shea butter and vitamin E, adding an emulsifier, and stirring until the mixture is melted to obtain an oil phase mixture; mixing nicotinamide, amino acid humectant, glycerol, urea and deionized water to obtain a water phase mixture; slowly adding the water phase mixture into the oil phase mixture, mixing until the mixture is a uniform white milky matrix, stopping stirring, naturally cooling to room temperature, and adding folium Artemisiae Argyi plant essential oil to obtain the folium Artemisiae Argyi skin-moistening antibacterial hand-protecting cream. The hand cream contains antibacterial and anti-inflammatory components accounting for more than 50% of the essential oil content, and has the effects of resisting bacteria and diminishing inflammation and deeply moistening skin.
Description
Technical Field
The invention relates to the field of skin care products, and in particular relates to a wormwood skin-moistening antibacterial hand cream and a preparation method thereof.
Background
In daily life, hands are in contact with various substances in the nature, including daily contact with detergents and use of various tools, so that the skin on the hands is most susceptible to damage, becomes dry and rough, or is allergic to the skin of the hands due to ultraviolet irradiation or the like, the skin color becomes dark, and the hands are also susceptible to frost cracking in severe cold winter. At present, a plurality of hand cream products exist in the market, but the problems of poor transdermal property and difficult absorption exist mostly, and in addition, as the raw materials of a plurality of hand creams contain odors with different degrees, chemical essences can be added into the hand creams sold in order to cover the odors of the raw materials and attract consumers. The chemical essence is a product simulating natural fragrance in a laboratory, smells fragrance all around, and substantially damages health, and the chemical essence generally contains a large amount of benzene and formaldehyde, which can cause carcinogenesis and cause direct harm to the body and mind if entering the human body and passing through the five viscera and six entrails.
Aiming at the market disorder, a series of skin care products containing the efficacy of natural products are preferred or favored by consumers. The mugwort is also called mugwort, borneol, medicinals, etc., belongs to a perennial herb of the compositae, and the plant has strong fragrance. The wormwood is a plant which is recognized and used by people in labor in China earlier, and is commonly used by people in the first year of West. The production places of the wormwood are widely distributed, the wormwood is almost spread throughout the whole country except for extremely arid and alpine regions, and northeast, east, south and southwest of China, Shaanxi, Gansu and the like are distributed. Moxa has a close relationship with the life of Chinese people, and people always keep moxa at home to avoid pathogens every morning. Folium Artemisiae Argyi is bitter, pungent and warm in nature, enters spleen, liver and kidney, and whole herbs are used as herbs, and has the effects of removing dampness, dispelling cold, stopping bleeding, diminishing inflammation, relieving asthma, relieving cough, preventing miscarriage, and resisting allergy, so it is also called as "Yi Cao". The main component of the wormwood is volatile oil which is grass green or light yellow clear oily liquid, has special fragrance, and has pharmacological activities of resisting bacteria, diminishing inflammation, resisting allergy, resisting oxidation and the like.
Disclosure of Invention
In view of the above, in order to solve the defects of the prior art, the invention aims to provide a wormwood skin-moistening antibacterial hand cream and a preparation method thereof, so as to solve the problems in the prior art, the wormwood skin-moistening antibacterial hand cream has the dual effects of moisturizing, resisting bacteria and resisting oxidation, has an obvious whitening effect, is fragrant and pleasant, does not contain a chemical preservative, is safe and effective, and can be applied to all people.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
the wormwood skin-moistening antibacterial hand cream is characterized in that: the composite material comprises the following raw materials in parts by weight: 3-10 parts of wormwood plant essential oil, 8-15 parts of sweet almond oil, 8-20 parts of shea butter, 2-8 parts of vitamin E, 3-10 parts of nicotinamide, 3-10 parts of amino acid humectant, 5-12 parts of glycerol, 3-10 parts of urea, 3-8 parts of emulsifier and the balance of deionized water.
A preparation method of a wormwood skin-moistening antibacterial hand cream comprises the following specific steps:
mixing sweet almond oil, shea butter and vitamin E, adding an emulsifier in a water bath at 40-70 ℃, and stirring until the materials are completely melted to obtain an oil phase mixture for later use;
step two, mixing nicotinamide, amino acid humectant, glycerol, urea and a proper amount of deionized water together, and uniformly stirring in a water bath at 40-70 ℃ to obtain a water phase mixture for later use;
step three, slowly adding the water phase mixture into the oil phase mixture, mixing until a uniform white milky matrix is formed, stopping stirring, and naturally cooling to room temperature;
and step four, adding the wormwood plant essential oil into the mixture obtained in the step three, and uniformly stirring to obtain the wormwood skin-moistening antibacterial hand cream.
Further optimizing, the method for extracting the wormwood plant essential oil in the fourth step comprises the following steps:
weighing stems and leaves of overground parts of wormwood which is dried in the shade as wormwood raw materials, and spraying cellulase aqueous solution on the wormwood raw materials after crushing;
step two, placing the wormwood raw material treated in the step one into a distillation flask, and carrying out steam distillation for 3-5 hours at the distillation speed of 1-2 drops per second to obtain wormwood volatile oil for later use;
and step three, extracting the wormwood volatile oil obtained in the step two by using ethyl acetate, collecting upper-layer extract liquor, then adding anhydrous magnesium sulfate for drying, standing overnight, filtering, collecting filtrate, and evaporating the filtrate under reduced pressure to remove the solvent to obtain the natural wormwood essential oil.
Further optimization, the mass concentration of the cellulase aqueous solution in the step one is 0.15%.
Further optimizing, the vacuum degree of the reduced pressure distillation in the third step is 0.090-0.095Mpa, and the water bath temperature is 45-52 ℃.
Further optimizing, the dosage of the ethyl acetate in the third step is 1/3 of the weight of the wormwood volatile oil.
The invention has the beneficial effects that:
1. the antibacterial and anti-inflammatory components marked by eucalyptol, camphor, borneol, alpha-phellandrene, camphene, linalool, eugenol, limonene and the like contained in the wormwood skin-moistening antibacterial hand cream disclosed by the invention account for more than 50% of the content of the essential oil, have the effects of resisting bacteria, diminishing inflammation and protecting the skin, moisten and preserve moisture, have aromatic odor, and can be suitable for all people, wherein the antibacterial components can also be used as natural preservatives, and are safe and effective;
2. the volatile oil in the folium artemisiae argyi has an inhibiting or killing effect on various pathogenic bacteria and viruses, the main components of the volatile oil of the folium artemisiae argyi are monoterpene and derivatives thereof, sesquiterpenes and derivatives thereof, ketones, alcohols, acids and alkane compounds, and the volatile oil has wide pharmacological activity, wherein the antibacterial components comprise eucalyptol, camphor, borneol, alpha-phellandrene, camphene, linalool, eugenol, limonene and the like, in addition, the folium artemisiae argyi has the special effects of activating blood and resisting oxidation, can promote the blood circulation of hand skin, particularly can activate blood and dispel cold in winter, prevent freezing and cracking, can also lighten hand wrinkles and keep the hand skin tender and compact;
3. the wormwood skin-moistening antibacterial hand cream provided by the invention is converted into the current antibacterial hand cream urgently needed for epidemic prevention based on the scientific research achievements of wormwood research, the preparation method is simple, the raw material sources are wide, the prepared hand cream is good in antibacterial and bacteriostatic effects, natural and mild in use feeling and has good antioxidant and whitening health-care effects, compared with the prior art, the prepared hand cream is suitable in viscosity, good in transdermal property, fine and smooth in skin, fresh and mild in taste, whitening and antioxidant, and has high-efficiency antibacterial and bacteriostatic effects, the raw material sources are wide, and the preparation method is simple;
4. the hand cream prepared by the invention adopts sweet almond oil, shea butter, amino acid humectant, glycerin and urea as moisturizing and moisturizing components, adopts vitamin E as an antioxidant component, adopts nicotinamide as a whitening component and also comprises 3-8 parts of emulsifier, the formula highlights the compatibility of the physicochemical and medicinal effects of various components and the wormwood essential oil, the prepared wormwood moisturizing and antibacterial hand cream product is unique in use, the detection indexes all reach the quality standard, the melting point reaches 45-55 ℃, and the volatile oil amount is more than or equal to 3.0 percent, and the formula and the preparation method process thereof can reduce the product cost and ensure the product quality and also accord with the quality standard.
Detailed Description
The following specific examples are given to further clarify, complete and detailed the technical solution of the present invention. The present embodiment is a preferred embodiment based on the technical solution of the present invention, but the scope of the present invention is not limited to the following embodiments.
Example 1
The wormwood skin-moistening antibacterial hand cream comprises the following raw materials in parts by weight: 3 parts of wormwood plant essential oil, 8 parts of sweet almond oil, 8 parts of shea butter, 2 parts of vitamin E, 3 parts of nicotinamide, 3 parts of amino acid humectant, 5 parts of glycerol, 3 parts of urea, 3 parts of emulsifier and the balance of deionized water.
The specific preparation method of the hand cream comprises the following steps:
mixing sweet almond oil, shea butter and vitamin E, adding an emulsifier under the condition of water bath at 40 ℃, and stirring until the materials are completely melted to obtain an oil phase mixture; mixing nicotinamide, amino acid humectant, glycerol, urea and a proper amount of deionized water together, and stirring uniformly under the condition of water bath at 40 ℃ to obtain a water phase mixture; slowly adding the water phase mixture into the oil phase mixture, mixing until the mixture is a uniform white milky matrix, stopping stirring, naturally cooling to room temperature, adding the wormwood plant essential oil, and continuously stirring uniformly to obtain the wormwood skin-moistening antibacterial hand cream.
The method for extracting the wormwood plant essential oil comprises the following steps:
collecting wormwood from a Zhenshan Xiandan moxa base of Funiu mountain range, weighing stems and leaves of overground parts of the wormwood as wormwood raw materials after drying in the shade, and spraying cellulase aqueous solution on the wormwood raw materials after crushing, wherein the mass concentration of the cellulase aqueous solution is 0.15%;
step two, placing the wormwood raw material treated in the step one into a distillation flask, and carrying out steam distillation for 3 hours at the distillation speed of 1-2 drops per second to obtain wormwood volatile oil for later use;
and step three, extracting the wormwood volatile oil obtained in the step two by using ethyl acetate, wherein the using amount of the ethyl acetate is 1/3 of the weight of the wormwood volatile oil, collecting upper-layer extract liquor, then adding anhydrous magnesium sulfate for drying, standing overnight, filtering, collecting filtrate, removing a solvent from the filtrate through reduced pressure evaporation, and obtaining the wormwood natural essential oil, wherein the vacuum degree of the reduced pressure distillation is 0.095Mpa, and the water bath temperature is 45 ℃.
Example 2
The wormwood skin-moistening antibacterial hand cream is prepared from the following raw materials in parts by weight: 5 parts of wormwood plant essential oil, 10 parts of sweet almond oil, 15 parts of shea butter, 4 parts of vitamin E, 5 parts of nicotinamide, 5 parts of amino acid humectant, 10 parts of glycerol, 5 parts of urea, 5 parts of emulsifier and the balance of deionized water;
the specific preparation method of the hand cream comprises the following steps:
mixing sweet almond oil, shea butter and vitamin E, adding an emulsifier under the condition of 50 ℃ water bath, and stirring until the materials are completely melted to obtain an oil phase mixture; mixing nicotinamide, amino acid humectant, glycerol, urea and a proper amount of deionized water, and uniformly stirring in a water bath at 50 ℃ to obtain a water phase mixture; slowly adding the water phase mixture into the oil phase mixture, mixing until the mixture is a uniform white milky matrix, stopping stirring, naturally cooling to room temperature, adding the wormwood plant essential oil, and continuously stirring uniformly to obtain the wormwood skin-moistening antibacterial hand cream.
The method for extracting the wormwood plant essential oil comprises the following steps:
collecting wormwood from a Zhenshan Xiandan moxa base of Funiu mountain range, weighing stems and leaves of overground parts of the wormwood as wormwood raw materials after drying in the shade, and spraying cellulase aqueous solution on the wormwood raw materials after crushing, wherein the mass concentration of the cellulase aqueous solution is 0.15%;
step two, placing the wormwood raw material treated in the step one into a distillation flask, and carrying out steam distillation for 5 hours at the distillation speed of 1-2 drops per second to obtain wormwood volatile oil for later use;
and step three, extracting the wormwood volatile oil obtained in the step two by using ethyl acetate, wherein the using amount of the ethyl acetate is 1/3 of the weight of the wormwood volatile oil, collecting upper layer extract, then adding anhydrous magnesium sulfate for drying, standing overnight, filtering, collecting filtrate, removing the solvent from the filtrate through reduced pressure evaporation, and obtaining the wormwood natural essential oil, wherein the vacuum degree of the reduced pressure distillation is 0.092Mpa, and the water bath temperature is 50 ℃.
Example 3
The wormwood skin-moistening antibacterial hand cream is prepared from the following raw materials in parts by weight: 10 parts of wormwood plant essential oil, 15 parts of sweet almond oil, 20 parts of shea butter, 8 parts of vitamin E, 10 parts of nicotinamide, 10 parts of amino acid humectant, 12 parts of glycerol, 10 parts of urea, 8 parts of emulsifier and the balance of deionized water;
the specific preparation method of the hand cream comprises the following steps:
mixing sweet almond oil, shea butter and vitamin E, adding an emulsifier under the condition of 70 ℃ water bath, and stirring until the materials are completely melted to obtain an oil phase mixture; mixing nicotinamide, amino acid humectant, glycerol, urea and a proper amount of deionized water together, and stirring uniformly under the condition of 70 ℃ water bath to obtain a water phase mixture; slowly adding the water phase mixture into the oil phase mixture, mixing until the mixture is a uniform white milky matrix, stopping stirring, naturally cooling to room temperature, adding the wormwood plant essential oil, and continuously stirring uniformly to obtain the wormwood skin-moistening antibacterial hand cream.
The method for extracting the wormwood plant essential oil comprises the following steps:
collecting wormwood from a Zhenshan Xiandan moxa base of Funiu mountain range, weighing stems and leaves of overground parts of the wormwood as wormwood raw materials after drying in the shade, and spraying cellulase aqueous solution on the wormwood raw materials after crushing, wherein the mass concentration of the cellulase aqueous solution is 0.15%;
step two, putting the wormwood raw material processed in the step one into a distillation flask, and carrying out steam distillation for 4 hours at the distillation speed of 1-2 drops per second to obtain wormwood volatile oil for later use;
and step three, extracting the wormwood volatile oil obtained in the step two by using ethyl acetate, wherein the using amount of the ethyl acetate is 1/3 of the weight of the wormwood volatile oil, collecting upper-layer extract liquor, then adding anhydrous magnesium sulfate for drying, standing overnight, filtering, collecting filtrate, removing a solvent from the filtrate through reduced pressure distillation, and obtaining the wormwood natural essential oil, wherein the vacuum degree of the reduced pressure distillation is 0.090Mpa, and the water bath temperature is 52 ℃.
The total identification of 24 effective components in the volatile oil of folium Artemisiae Argyi by GC-MS analysis is shown in Table 1 below, wherein the GC-MS analysis instrument adopts US HP6890 gas phase
HP5973N mass spectrum is used together with the Nist98 data system, a capillary column adopts a model DB-35MS, 30.0m is multiplied by 250 m is multiplied by 0.30 m, carrier gas is helium, the flow rate is 1.0ml/min, the split ratio is 5:1, EI voltage is 70ev, the scanning mass range is 40-400, the temperature rise program is that 80 ℃ is kept for 1min, 4 ℃/min is kept for 5min when the temperature rises to 120 ℃, 3 ℃/min is kept for 2min when the temperature rises to 170 ℃, and then 10 ℃/min is kept for 5min when the temperature rises to 280 ℃.
TABLE 1 analysis table of volatile oil components of wormwood
The prepared wormwood skin-moistening antibacterial hand cream contains eucalyptol, camphor, borneol, alpha-phellandrene, camphene, linalool, eugenol and limonene, and has the antibacterial and anti-inflammatory components accounting for 55.66% of the content of wormwood essential oil, has double effects of resisting bacteria, diminishing inflammation and protecting skin, and has the detection indexes of the hand cream reaching the quality standard, the melting point reaching the high-grade standard, namely the melting point of 45-55 ℃, and the volatile oil content of more than or equal to 3.0%.
The principal features, principles and advantages of the invention have been shown and described above. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to explain the principles of the invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the invention as expressed in the following claims. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (6)
1. The wormwood skin-moistening antibacterial hand cream is characterized in that: the composite material comprises the following raw materials in parts by weight: 3-10 parts of wormwood plant essential oil, 8-15 parts of sweet almond oil, 8-20 parts of shea butter, 2-8 parts of vitamin E, 3-10 parts of nicotinamide, 3-10 parts of amino acid humectant, 5-12 parts of glycerol, 3-10 parts of urea, 3-8 parts of emulsifier and the balance of deionized water.
2. A preparation method of a wormwood skin-moistening antibacterial hand cream is characterized by comprising the following steps: the method comprises the following specific steps:
mixing sweet almond oil, shea butter and vitamin E, adding an emulsifier in a water bath at 40-70 ℃, and stirring until the materials are completely melted to obtain an oil phase mixture for later use;
step two, mixing nicotinamide, amino acid humectant, glycerol, urea and a proper amount of deionized water together, and uniformly stirring in a water bath at 40-70 ℃ to obtain a water phase mixture for later use;
step three, slowly adding the water phase mixture into the oil phase mixture, mixing until a uniform white milky matrix is formed, stopping stirring, and naturally cooling to room temperature;
and step four, adding the wormwood plant essential oil into the mixture obtained in the step three, and uniformly stirring to obtain the wormwood skin-moistening antibacterial hand protector.
3. The preparation method of the wormwood skin-moistening antibacterial hand cream as claimed in claim 2, wherein the preparation method comprises the following steps: the method for extracting the wormwood plant essential oil in the fourth step comprises the following steps:
weighing stems and leaves of overground parts of wormwood which is dried in the shade as wormwood raw materials, and spraying cellulase aqueous solution on the wormwood raw materials after crushing;
step two, placing the wormwood raw material treated in the step one into a distillation flask, and carrying out steam distillation for 3-5 hours at the distillation speed of 1-2 drops per second to obtain wormwood volatile oil for later use;
and step three, extracting the wormwood volatile oil obtained in the step two by using ethyl acetate, collecting upper-layer extract liquor, then adding anhydrous magnesium sulfate for drying, standing overnight, filtering, collecting filtrate, and evaporating the filtrate under reduced pressure to remove the solvent to obtain the natural wormwood essential oil.
4. The preparation method of the wormwood skin-moistening antibacterial hand cream as claimed in claim 3, wherein the preparation method comprises the following steps: the mass concentration of the cellulase aqueous solution in the step one is 0.15%.
5. The preparation method of the wormwood skin-moistening antibacterial hand cream as claimed in claim 3, wherein the preparation method comprises the following steps: the vacuum degree of the reduced pressure distillation in the third step is 0.090-0.095Mpa, and the water bath temperature is 45-52 ℃.
6. The preparation method of the wormwood skin-moistening antibacterial hand cream as claimed in claim 3, wherein the preparation method comprises the following steps: the dosage of the ethyl acetate in the third step is 1/3 based on the weight of the wormwood volatile oil.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114903818A (en) * | 2021-07-12 | 2022-08-16 | 河北翰林生物科技有限公司 | Hand repairing nutritional composition and preparation method thereof |
| CN115670982A (en) * | 2022-11-25 | 2023-02-03 | 南京科技职业学院 | Essential oil-containing liquid crystal hand cream and preparation method thereof |
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| CN103536485A (en) * | 2013-10-18 | 2014-01-29 | 桂林雪芙莲日化有限公司 | Hand cream for preventing chapped skin |
| CN107669501A (en) * | 2017-11-15 | 2018-02-09 | 陈荷芬 | A kind of anti-cracking type plant nourishes hand lotion |
| CN107822962A (en) * | 2017-10-31 | 2018-03-23 | 董嘉丽 | The Anti-bacterium hand cream that a kind of baby is applicable |
| CN109453353A (en) * | 2018-12-21 | 2019-03-12 | 卢照宇 | A kind of moxa-moxibustion essential oil and preparation method thereof |
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2021
- 2021-02-05 CN CN202110161453.2A patent/CN112656715A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103536485A (en) * | 2013-10-18 | 2014-01-29 | 桂林雪芙莲日化有限公司 | Hand cream for preventing chapped skin |
| CN107822962A (en) * | 2017-10-31 | 2018-03-23 | 董嘉丽 | The Anti-bacterium hand cream that a kind of baby is applicable |
| CN107669501A (en) * | 2017-11-15 | 2018-02-09 | 陈荷芬 | A kind of anti-cracking type plant nourishes hand lotion |
| CN109453353A (en) * | 2018-12-21 | 2019-03-12 | 卢照宇 | A kind of moxa-moxibustion essential oil and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114903818A (en) * | 2021-07-12 | 2022-08-16 | 河北翰林生物科技有限公司 | Hand repairing nutritional composition and preparation method thereof |
| CN115670982A (en) * | 2022-11-25 | 2023-02-03 | 南京科技职业学院 | Essential oil-containing liquid crystal hand cream and preparation method thereof |
| CN115670982B (en) * | 2022-11-25 | 2024-03-12 | 南京科技职业学院 | Liquid crystal hand cream containing essential oil and preparation method thereof |
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