CN106389175B - A kind of nourishing and moisturizing lotion containing Rosa Damascana - Google Patents
A kind of nourishing and moisturizing lotion containing Rosa Damascana Download PDFInfo
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- CN106389175B CN106389175B CN201610808019.8A CN201610808019A CN106389175B CN 106389175 B CN106389175 B CN 106389175B CN 201610808019 A CN201610808019 A CN 201610808019A CN 106389175 B CN106389175 B CN 106389175B
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Abstract
The invention discloses a kind of nourishing and moisturizing lotion containing Rosa Damascana.Contain Rosa Damascana, plant extracts and a variety of natural moisture preserving ingredients in nourishing and moisturizing lotion of the present invention containing Rosa Damascana, without ingredients such as heavy metal, alcohol, hormone, mineral oil, pigments, formula is soft, will not generate stimulation and burden to skin.The ingredients such as lotion at present on the market generally existing heavy metal, alcohol, hormone add and lead to skin allergy, rubescent, ulceration problem, the nourishing and moisturizing lotion can be very good to avoid the above problem through the invention, and nourishing and moisturizing lotion of the present invention is homogeneous mild, rich in active components of plants, by adding Rosa Damascana, there is the distinctive aromatic fragrance of rose.
Description
Technical field
The present invention relates to cosmetic fields, and in particular to a kind of nourishing and moisturizing lotion containing Rosa Damascana.
Background technique
Lotion is a kind of low viscosity, the extremely runny liquid skin care cosmetics as water, by it after facial cleansing
It adds on skin, moisturizing, moisturizing can be played, moisturize the skin, promote a kind of beauty and skin care of the effect of skin physiology function
Product.
Essential oil, person " liquid golden ", due to its distinctive natural characteristic and efficacy effect, in cosmetics field,
Obtain the favor of numerous consumers.Rosa Damascana is one kind volatilization that is safe and nontoxic, having peat-reek extracted from rose
Property substance.Rosa Damascana is the essential oil of most expensive in the world, referred to as " after essential oil ".Rosa Damascana is protected with good beauty
Skin acts on, and outer Kohakuhi is supported within energy, and melanin is promoted to decompose, and improves and has dry skin, and restores skin elasticity, consumer is allowed to gather around
There is healthy skin pale and full of elasticity, is the volatile oil for being suitable for female health.
Summary of the invention
It is an object of the invention to the generally existing heavy metal of the lotion according to current market, hormone, alcohol, pigments etc.
Addition and caused by skin easy allergy the problems such as, a kind of nourishing and moisturizing lotion containing Rosa Damascana is provided, the lotion at
It is divided into pure natural raw material, without heavy metal, alcohol, hormone, pigment, mineral oil etc., formula is soft, non-stimulated to skin.
Above-mentioned purpose of the present invention is achieved by the following technical programs:
A kind of nourishing and moisturizing lotion containing Rosa Damascana, it is characterised in that by as follows according to the group of mass percentage
It is grouped as: Rosa Damascana 0.5~1%, moisturizer 10.05~16%, avenabeta glucosan 0.5~1%, plant extracts 0.1
~0.2%, vitamin E 0.05~0.1% and deionized water 81.7~88.8%；
Wherein, the Rosa Damascana is to be prepared as follows to obtain:
(1) pre-process: roseleaf handles 15~20h through vacuum freeze drying, crushes, and crosses 40~60 meshes；By true
Sky is dry, directly will can obtain moisture in rose and rose is dried by solid state sublimation to gaseous state, the fragrance in rose
Ingredient and functional component are able to maintain best；
(2) it digests: step (1) products therefrom is sufficiently mixed with complex enzyme hydrolysis liquid according to the mass ratio of 1:1~1:6,
10~30min is digested at 30~60 DEG C；Cellulase, polygalacturonase, beta-glucosidase, Endo-β-glucanase
It is that the carbohydrate to macromolecular, cellulose family and pectin class are hydrolyzed, rhizomucor miehei lipase mainly carries out water to fat
Solution, mainly resolves into small-molecule substance for macromolecular carbohydrate, cellulose family, the fat etc. in plant material, can thus make
The plant extracts fragrance component of preparation increases, and fragrance is stronger；
(3) rose crude oil is extracted: step (2) products therefrom being filtered, the side of accelerated solvent extraction is used after removing filter residue
Formula is extracted；Accelerated solvent extraction is one kind under conditions of improving temperature and pressure, extracts mesh with organic solvent
The method for marking ingredient.The advantages of this method is that consumption of organic solvent is few；Extraction is quickly, general only to need 15~20min；To extraction
The influence of raw material is small, and different raw material volumes can select identical extraction conditions, and the high-efficient of extraction, selectivity are good, operation is simple
It is single；
(4) it purifies: the resulting rose crude oil of step (3) being isolated and purified using wiped-film still, is obtained
Rosa Damascana；Wiped-film still is mainly the process purified to the coarse-fine oil of extraction.Molecular distillation mainly exists
The technology of Liquid liquid Separation is carried out under conditions of high vacuum, its advantage is that the temperature of distillation is low, the heated time of material is short and separates
Degree height etc., particularly suitable for isolating and purifying for higher boiling, thermal sensitivity and oxidizable substance.Rosa Damascana is thermal sensitivity object
Matter is retained preferably using fragrance component of the molecular distillation to essential oil, while removing removal of impurities gas, keeps the fragrance of Rosa Damascana purer
Just, fragrance is stronger；
The complex enzyme hydrolysis liquid is by cellulase, polygalacturonase, beta-glucosidase, inscribe beta glucan
Enzyme, rhizomucor miehei lipase are mixed according to the mass ratio of 2:1:1:1:1~5:4:1:1:1, and water is added to be configured to mass percent
For 0.3~0.9% complex enzyme hydrolysis liquid, and its pH is adjusted to 4.0~6.0.
As a kind of perferred technical scheme, the moisturizer is hyaluronic acid, serine and glycerine.
As a kind of further optimal technical scheme, in the moisturizer, the additive amount of hyaluronic acid is 2~3%,
The additive amount of serine is 0.05~1%, and the additive amount of glycerine is 8~12%.
As a kind of perferred technical scheme, the plant extracts is marine algae extract, green-tea extract, wheat or rice
Rice germ extracts, grape seed extract.The marine algae extract, green-tea extract, wheat or aid from rice germ extract, grape
The preparation method of seed extract is that seaweed, green tea, wheat embryo or aid from rice germ, grape pip are dried to perseverance at 50 DEG C respectively
Weight, smashes it through 40~60 meshes, obtains raw material, be then uniformly mixed respectively with water according to the mass ratio of 1:10~20, through super
Sound is uniformly mixed, and filters to take supernatant through precipitating, 5 times of weight of raw material are concentrated at 40~50 DEG C, seaweed is respectively obtained and mentions
Take object, green-tea extract, wheat or aid from rice germ extract, grape seed extract.
As a kind of optimal technical scheme, the extraction of the step (3) is using accelerated solvent extraction, and extractant is
Dehydrated alcohol, extracting pressure are 8~10MPa, and extraction temperature is 40~60 DEG C, and solid-liquid ratio is 1:10~1:20, and extraction time is
10~20min.
As a kind of optimal technical scheme, when being purified in the step (4) using wiped-film still, distillation
Temperature be 60~70 DEG C, distillation pressure be 18~25Pa, feed rate be 1.0~2.0ml/min, scrape diaphragm plate revolving speed be 25~
40r/min。
As a kind of optimal technical scheme, the pH adjusting of the complex enzyme hydrolysis liquid is slow using citrate-phosphate disodium hydrogen
Fliud flushing is adjusted, and the concentration of citric acid solution is 0.1mol/L, and the concentration of disodium phosphate soln is 0.2mol/L.
As a kind of perferred technical scheme, the nourishing and moisturizing lotion of the present invention containing Rosa Damascana by pressing as follows
It is grouped as according to the group of mass percentage: Rosa Damascana 0.8%, moisturizer 13%, avenabeta glucosan 0.8%, plant extract
Object 0.15%, vitamin E 0.08% and deionized water 85.17%.
Compared with prior art, the invention has the following beneficial effects:
(1) lotion of the present invention is homogeneous, mildly, has no stimulation of the skin, and is rich in active components of plants, formula choosing
The raw material taken is food grade materials and its extract, and product is pure natural, is free of heavy metal, alcohol, hormone, mineral oil and color
The substances such as element, formula is soft, without any stimulation；
(2) present invention, which combines biological enzyme-accelerated solvent extraction-molecular distillation technique, is applied to mentioning for Rosa Damascana
In taking, extraction time is short, and the yield of Rosa Damascana is high, and Rosa Damascana quality obtained is good, and fragrance component dramatically increases；
(3) present invention addition Rosa Damascana has good beautifying skin-protection function, supports outer Kohakuhi within energy, promote
Melanin decomposes, and improves dry skin, restores skin elasticity, and consumer is allowed to possess healthy skin pale and full of elasticity；
(4) present invention is added to hyaluronic acid, and hyaluronic acid (HA) has special water retention, be it is presently found from
The best substance of moisture retention, referred to as ideal natural moisturizing factor in right boundary.HA has high molecular weight and macromolecular volume
Characteristic, HA numberator height stretches in aqueous solution, as " molecule sponge ", can be absorbed and keep thousands of times of its own weight
Moisture content.When this molecular network for being full of moisture content or " molecule sponge " are coated on skin surface, then one layer of aquation is formed
Film, moment Stratum Corneum keep humidification, prevent from having dry skin, enable skin emolliency smooth.In all water associativity moisturizings
In agent, this film forming characteristics of HA is unique, so it all has than any other natural or synthesis polymer
Stronger water holding capacity is moisturizer best recognized by cosmetic industry in the world；
(5) present invention is added to serine, and serine is important one of nature moisturizing factor (NMF), keratoderma
Keep the dominant role of moisture, the crucial additive in superior cosmetics；
(6) present invention is added to glycerol, it is glycerine from structure, is colourless, odorless, tasteless, sticky good
Liquid, it is inexpensive, stable, it is common moisturizer, has very strong hygroscopicity, be fully soluble in water and alcohol.It can be from humid air
Moisture is absorbed, has soft lubricating action to skin, the evaporation of product moisture can also be delayed by being added in cosmetics；
(7) marine algae extract is a kind of natural marine organism extract, it contains phycocolloid acid, multivitamin, enzyme, thick
Albumen and microelement can reduce the blood lipid of skin surface, promote dermal erythropoiesis function after skin absorbs.Secondly, in seaweed
Containing a large amount of anion, it can stimulate fibrocyte to generate collagen and elastin laminin, promote skin metabolism, have anti-
The function of wrinkle and anti-aging；
(8) main composition in green-tea extract is tea polyphenols.Tea polyphenols are the general names of Polyphenols of Tea.
Tea polyphenols are a kind of new type natural antioxidants, have inhibiting effect to clostridiopetidase A and elastoser, can prevent elastin laminin matter
Content decline or denaturation, maintain skin elasticity, reach anti-wrinkle effect.In addition, tea polyphenols also have resisting age of skin, can hinder
It keeps off ultraviolet light and removes the free radical of ultraviolet induction, reduce the generation of melanin, while can inhibit tyrosinase and peroxidating
The activity of hydrogen enzyme, to achieve the effect that whitening；
(9) natural tocopherol level that wheat or aid from rice germ extract contain is very high, it is good antioxidant
And emollient.Studies have shown that natural VE can promote the normal development of muscle and the metabolism of skin, make to keep skin
Elasticity enables skin and body maintain vigour；Meanwhile vitamin E can directly help skin to free radical resisting, ultraviolet light and pollution
The infringement of object prevents pigementation, resisting age of skin.In addition, vitamin E can extend cosmetics use as antioxidant
Time；
(10) contain several functions composition in grape seed extract, including procyanidine, grape seed oil, resveratrol,
Vitamin, tannin etc., these ingredients all have higher nutritive value and beauty and health care functions.Wherein with procyanidine most by special
Family payes attention to because its small molecule structure can penetrating blood-brain barrier, provide and reinforce the oxidation resistant function of intracerebral, at the same it
Anti-oxidant efficiency is 18 times higher than vitamin C；It is 50 times higher than vitamin E.It and 95% is exactly procyanidine contained by grape pip.For
Skin, grape pip can protect skin from the degeneration of ultraviolet light afflicted with great suffering torment, prevent collagenous fibres and elastomer, protect skin
Hold it is due elasticity and tension, and can pre- anti-melanin hoard, skin whitening；
(11) vitamin E is considered as " the most direct captor of free radical ", has powerful antioxidation, to skin
The maximum effect of skin is exactly vitamin E anti-aging, it can slow down cell proliferation and the speed of division plays extension cell senescence
Purpose；Vitamin E can inhibit the activity of promise propylhomoserin enzyme, reduce the formation of melanin, meanwhile, it is micro- that it can also improve blood vessel
Circulation promotes the conveying and the excretion of metabolism rubbish in vivo of nutritional ingredient, plays certain freckle effect；Vitamin E can
Inhibit the peroxidization of lipid, keeps contacting between tissue, make skin smooth, flexible；Vitamin E can also make cell membrane from
The oxidation of free radical can help the natural protective barrier for repairing and consolidating skin along upper, lock the moisture in skin；Vitamin E
Skin can also be helped preferably to absorb the nutritional ingredient of external skin care item, make skin effect more preferably；
(12) present invention is added to oat-beta glucan.Avenabeta glucosan has good senile-resistant efficacy, can comfort
The fine wrinkles of flat skin surface improve skin elasticity, improve dermatoglyph degree；Meanwhile oat-beta glucan is only due to having
Special straight-chain molecular structure, makes it have good Transdermal absorption performance, can be used as the release carrier of active ingredient, give skin
Smooth sense of touch is moistened such as silk；Beta glucan has film forming, and skin can be helped to keep moisture；Protect the skin from purple
The injury of outside line, skin resist the tolerance of environmental stimuli.
Specific embodiment
The invention will be further described with reference to embodiments, but embodiment the present invention is not done it is any type of
It limits.
In following embodiment, unless otherwise instructed, used raw material is raw material on sale on the market, used side
Method is method well known to those skilled in the art.
Embodiment 1
A kind of nourishing and moisturizing lotion containing Rosa Damascana, is grouped as: rose by the group as follows according to mass percentage
Rare essential oil 0.5%, hyaluronic acid 2%, serine 0.05%, glycerine 8%, oat-beta glucan 0.5%, grape pip extract
Object 0.1%, vitamin E 0.05%, deionized water 88.8%；
Wherein the extracting method of the Rosa Damascana includes the following steps: that roseleaf is handled through vacuum freeze drying
15h is crushed, and crosses 40 meshes；By cellulase, polygalacturonase, beta-glucosidase, Endo-β-glucanase, rice
Rhizomocur miehei lipase is mixed according to the mass ratio of 2:1:1:1:1, is formulated as the complex enzyme hydrolysis that mass percent is 0.3% with water
Liquid, using citrate-phosphate disodium hydrogen buffer to adjust enzyme solution pH is 4.0, and the concentration of citric acid solution is 0.1mol/L, phosphoric acid
The concentration of disodium hydrogen solution is 0.2mol/L.Roseleaf powder is sufficiently mixed with complex enzyme hydrolysis liquid according to the mass ratio of 1:1,
30min is digested at 30 DEG C；By the mixture filtering after enzymatic hydrolysis, the extraction of progress Rosa Damascana after filter residue is removed.Rosa Damascana
It is extracted using accelerated solvent extraction, selected equipment is accelerated solvent extraction, and extractant is dehydrated alcohol, tool
Body extraction process are as follows: extracting pressure 8MPa, extraction temperature are 40 DEG C, solid-liquid ratio 1:10, extraction time 20min.Using molecule
Distillation technique isolates and purifies rose crude oil obtained, and selected equipment is wiped-film still.Molecular distillation
Process conditions are as follows: distilled temperature 60 C, feed rate 1.0ml/min, scrapes diaphragm plate revolving speed 25r/min at distillation pressure 18Pa.Examination
Test the result shows that, preparing is 1.5h the time required to Rosa Damascana, compared with the prior art in Rosa Damascana extraction time be 3~
5h substantially reduces the extraction time of Rosa Damascana, meanwhile, the dried flower yield for measuring Rosa Damascana is 1.58%, and yield is high；It is right
The physical and chemical index of Rosa Damascana obtained is detected, and the results are shown in Table 1, by table 1 it is found that rose fragrant prepared by embodiment 1
Essence complies with standard；It is detected using fragrance component of the GC-MS method to Rosa Damascana obtained, the results are shown in Table 2, the results showed that
The fragrance component of preparation up to 60 kinds, illustrate using this method preparation Rosa Damascana remain in maximum its fragrance at
Point, fragrance is richer, harmonious.Rosa Damascana made from the method for the present invention is mainly by alcohol, alkene, ester, ketone, aldehyde, ether, alkane, phenol
The compounds such as class, acids composition, mainly based on the higher alcohol of low molecular weight, wherein up to 21 kinds of alcohol compound, including
Citronellol, geraniol, benzyl carbinol, linalool etc.；11 kinds of alkenes substance；9 kinds of esters；6 kinds of ketone；3 kinds of ethers；3 kinds of phenols；Acid
3 kinds of class；2 kinds of aldehydes；2 kinds of alkanes.
Table 1
Table 2
Embodiment 2
A kind of nourishing and moisturizing lotion containing Rosa Damascana, is grouped as: rose by the group as follows according to mass percentage
It is rare essential oil 1%, hyaluronic acid 3%, serine 1%, glycerine 12%, avenabeta glucosan 1%, marine algae extract 0.2%, micro-
Raw element E0.1%, deionized water 81.7%；
Wherein the extracting method of the Rosa Damascana includes the following steps: that roseleaf handles 20h, powder through vacuum freeze drying
It is broken, cross 60 meshes；By cellulase, polygalacturonase, beta-glucosidase, Endo-β-glucanase, rhizomucor miehei fat
Enzyme is mixed according to the mass ratio of 5:4:1:1:1, the complex enzyme hydrolysis liquid that mass percent is 0.9% is formulated as with water, using citrate-phosphate
It is 6.0 that disodium hydrogen buffer, which adjusts enzyme solution pH, and the concentration of citric acid solution is 0.1mol/L, and the concentration of disodium phosphate soln is
0.2mol/L.Roseleaf powder is sufficiently mixed with complex enzyme hydrolysis liquid according to the mass ratio of 1:6, digests 10min at 60 DEG C；It will enzymatic hydrolysis
Mixture filtering afterwards, removes the extraction of progress Rosa Damascana after filter residue.Rosa Damascana is extracted using accelerated solvent extraction,
Selected equipment is accelerated solvent extraction, and extractant is dehydrated alcohol, specific extraction process are as follows: extracting pressure 10MPa, extraction temperature
Degree is 60 DEG C, solid-liquid ratio 1:20, extraction time 10min.Rose crude oil obtained is isolated and purified using molecular distillation technique,
Selected equipment is wiped-film still.The process conditions of molecular distillation are as follows: distilled temperature 70 C, distillation pressure 25Pa, into
Material rate 2.0ml/min, diaphragm plate revolving speed 40r/min is scraped.Test result shows that preparing Rosa Damascana required time is 1.2h, compared to
Rosa Damascana extraction time in the prior art is 3~5h, substantially reduces the extraction time of Rosa Damascana, meanwhile, measure rhodamine toner
The dried flower yield of oil is 1.45%, and yield is high；The physical and chemical index of Rosa Damascana obtained is detected, the results are shown in Table 3, shows to make
Standby flavoring rose essence complies with standard；It is detected using fragrance component of the GC-MS method to Rosa Damascana obtained, the results are shown in Table 4, as a result
Show: the fragrance component of preparation up to 60 kinds, illustrate using this method preparation Rosa Damascana largely remain its fragrance at
Point, the richer harmony of fragrance.Rosa Damascana is mainly made of compounds such as alcohol, alkene, ester, ketone, aldehyde, ether, alkane, phenols, acids, main
If based on the higher alcohol of low molecular weight, wherein up to 21 kinds of alcohol compound, including citronellol, geraniol, benzyl carbinol, fragrant camphor tree
Alcohol etc.；11 kinds of alkenes substance；9 kinds of esters；6 kinds of ketone；3 kinds of ethers；3 kinds of phenols；3 kinds of acids；2 kinds of aldehydes；2 kinds of alkanes.
Table 3
Table 4
Embodiment 3
A kind of nourishing and moisturizing lotion containing Rosa Damascana, is grouped as: rose by the group as follows according to mass percentage
Rare essential oil 0.8%, hyaluronic acid 2.5%, serine 0.5%, glycerine 10%, avenabeta glucosan 0.8%, green-tea extract
0.15%, vitamin E 0.08%, deionized water 85.17%；
It includes such as that wherein the preparation method of Rosa Damascana nanoemulsions, which includes: the extracting method of the wherein described Rosa Damascana,
Lower step: roseleaf handles 18h through vacuum freeze drying, crushes, and crosses 50 meshes；It will be by cellulase, poly galacturonic
Sour enzyme, beta-glucosidase, Endo-β-glucanase, rhizomucor miehei lipase are mixed according to the mass ratio of 5:3:1:1:1, are used
Water be formulated as mass percent be 0.7% complex enzyme hydrolysis liquid, use citrate-phosphate disodium hydrogen buffer adjust enzyme solution pH for
5.0, the concentration of citric acid solution is 0.1mol/L, and the concentration of disodium phosphate soln is 0.2mol/L.By roseleaf powder
It is sufficiently mixed with complex enzyme hydrolysis liquid according to the mass ratio of 1:3, digests 20min at 45 DEG C；By the mixture filtering after enzymatic hydrolysis, remove
It goes after filter residue to carry out the extraction of Rosa Damascana.Rosa Damascana is extracted using accelerated solvent extraction, and selected equipment is
Accelerated solvent extraction, extractant are dehydrated alcohol, specific extraction process are as follows: extracting pressure 9MPa, extraction temperature are 50 DEG C,
Solid-liquid ratio is 1:15, extraction time 15min.Rose crude oil obtained is isolated and purified using molecular distillation technique, it is selected
Equipment is wiped-film still.The process conditions of molecular distillation are as follows: 65 DEG C of distilled temperature, distillation pressure 22Pa, into
Material rate 1.5ml/min, diaphragm plate revolving speed 32r/min is scraped.Test result shows the time required to preparing Rosa Damascana to be 1.3h, phase
Than in Rosa Damascana extraction time in the prior art be 3~5h, substantially reduce the extraction time of Rosa Damascana, meanwhile, survey
The dried flower yield for obtaining Rosa Damascana is 1.52%, and yield is high；；The physical and chemical index of Rosa Damascana obtained is detected, is tied
Fruit is shown in Table 5, shows that the flavoring rose essence of preparation complies with standard；It is carried out using fragrance component of the GC-MS method to Rosa Damascana obtained
Detection, the results are shown in Table 6, the results showed that the fragrance component of preparation illustrates using the Rosa Damascana of this method preparation up to 60 kinds very
Its fragrance component, the richer harmony of fragrance are remained in big degree.Rosa Damascana is mainly by alcohol, alkene, ester, ketone, aldehyde, ether, alkane
The compounds such as hydrocarbon, phenols, acids composition, mainly based on the higher alcohol of low molecular weight, wherein up to 21 kinds of alcohol compound,
Including citronellol, geraniol, benzyl carbinol, linalool etc.；11 kinds of alkenes substance；9 kinds of esters；6 kinds of ketone；3 kinds of ethers；Phenols 3
Kind；3 kinds of acids；2 kinds of aldehydes；2 kinds of alkanes.
Table 5
Table 6
Comparative example 1
The patent of invention institute of the Rosa Damascana and Patent No. 201210235667.0 that are prepared this patent using GC-MS method
Rosa Damascana fragrance component made from disclosed method compares.It the results are shown in Table 7.
It can be seen from the test results that the main component for the Rosa Damascana that two kinds of extracting methods obtain all be citronellol and its
Esters, geraniol and its esters, benzyl carbinol, nerol, linalool, eugenol and its esters, but the content presence of ingredient is very big
Difference.The invention patent to Rosa Damascana ingredient up to 60 kinds, mainly based on the higher alcohols of low molecular weight, Patent No.
201210235667.0 patent of invention disclosed in its ingredient of Rosa Damascana made from method only have 43 kinds.Intuitively show as this
Fuller, harmonious, the non-stimulated smell of its fragrance of Rosa Damascana of patent of invention preparation, Patent No. 201210235667.0
Rosa Damascana fragrance made from method disclosed in patent of invention is relatively thin, sense of being slightly discord.
Table 7
Comparative example 2
The nourishing and moisturizing lotion containing Rosa Damascana is prepared, is grouped as by the group as follows according to mass percentage: rose
Rare essential oil 0.8%, hyaluronic acid 2.5%, serine 0.5%, glycerine 10%, avenabeta glucosan 0.8%, green-tea extract
0.15%, vitamin E 0.08%, deionized water 85.17%.
Comparison: by Rosa Damascana equivalent made from method disclosed in the patent of invention of Patent No. 201210235667.0
The Rosa Damascana of the method for the present invention preparation is replaced, remaining component is constant.
Subject of 200 age brackets at 18~50 years old is chosen, the subject not tolerated to the easy allergy of cosmetics is excluded.
Firstly, 200 subjects give a mark to the organoleptic indicator of the toner of preparation.Each index is commented with 10 minute marks
Valence result is in terms of average mark.Analyses Methods for Sensory Evaluation Results is shown in Table 8.
Table 8
Then, subject is divided into 2 groups, every group of number of subjects is 100 people.A group is to smear rose moisturizing profit of the present invention
The subject of skin water, B group are that Rosa Damascana prepared by smearing Patent No. 201210235667.0 replaces rhodamine toner of the present invention
The subject of the lotion of oil production.Time using Rosa Damascana lotion is 6 months, then from the guarantor of rose lotion
Whether allergy is evaluated by wet, whitening, crease-resistant and other effects and subject.Evaluation result is shown in Table 9.
Table 9
Comparative example 3
Comparison: acidic cellulase disclosed in patent of invention of the complex enzyme using Patent No. 201210235667.0,
Pectase and compound protease are hydrolyzed, and the usage amount and enzymolysis time of enzyme are referring to the embodiment data of the patent disclosure.
Remaining step is identical as the present invention, and lotion is made.
Above-mentioned lotion is compared with 1 lotion of the embodiment of the present invention.
Subject of 200 age brackets at 18~50 years old is chosen, the subject not tolerated to the easy allergy of cosmetics is excluded.
Firstly, 200 subjects give a mark to the organoleptic indicator of the toner of preparation.Each index is commented with 10 minute marks
Valence result is in terms of average mark.Analyses Methods for Sensory Evaluation Results is shown in Table 10.
Table 10
Then, subject is divided into 2 groups, every group of number of subjects is 100 people.A group is to smear 1 gained of the embodiment of the present invention
Rose skin-moisturizing, skin water subject, B group be smearing Patent No. 201210235667.0 disclosed in compound protease
Rosa Damascana obtained replaces the subject of the lotion of Rosa Damascana production of the present invention.The time for smearing rose water is 6 months,
Then from the moisturizing of rose lotion, whitening, crease-resistant and other effects and subject, whether allergy is evaluated.Evaluation result is shown in Table
11。
Table 11
Claims (7)
1. a kind of nourishing and moisturizing lotion containing Rosa Damascana, it is characterised in that by as follows according to the component of mass percentage
Composition: Rosa Damascana 0.5~1%, moisturizer 10.05~16%, avenabeta glucosan 0.5~1%, plant extracts 0.1~
0.2%, vitamin E 0.05~0.1% and deionized water 81.7~88.8%；
Wherein, the Rosa Damascana is to be prepared as follows to obtain:
(1) pre-process: roseleaf handles 15~20h through vacuum freeze drying, crushes, and crosses 40~60 meshes；
(2) it digests: step (1) products therefrom is sufficiently mixed with complex enzyme hydrolysis liquid according to the mass ratio of 1:1~1:6,30~
10~30min is digested at 60 DEG C；
(3) rose crude oil extract: by step (2) products therefrom filter, remove filter residue after by the way of accelerated solvent extraction into
Row extraction；
(4) it purifies: the resulting rose crude oil of step (3) being isolated and purified using wiped-film still, obtains rose
Essential oil；
The complex enzyme hydrolysis liquid be by cellulase, polygalacturonase, beta-glucosidase, Endo-β-glucanase,
Rhizomucor miehei lipase is mixed according to the mass ratio of 2:1:1:1:1~5:4:1:1:1, is added water to be configured to mass percent and is
0.3~0.9% complex enzyme hydrolysis liquid, and its pH is adjusted to 4.0~6.0；
The plant extracts is marine algae extract, green-tea extract, wheat or aid from rice germ extract, grape seed extract；
The marine algae extract, green-tea extract, wheat or aid from rice germ extract, grape seed extract preparation method be will be extra large
Drying to constant weight at 50 DEG C respectively for algae, green tea, wheat embryo or aid from rice germ, grape pip, smashes it through 40~60 meshes, obtains
To raw material, then it is uniformly mixed respectively with water according to the mass ratio of 1:10~20, it is uniform through ultrasonic mixing, it is filtered to take through precipitating
Clear liquid is concentrated into 5 times of weight of raw material at 40~50 DEG C, respectively obtains marine algae extract, green-tea extract, wheat or rice
Germ extracts, grape seed extract.
2. the nourishing and moisturizing lotion according to claim 1 containing Rosa Damascana, it is characterised in that by as follows according to matter
The group of amount percentage meter is grouped as: Rosa Damascana 0.8%, moisturizer 13%, avenabeta glucosan 0.8%, plant extracts
0.15%, vitamin E 0.08% and deionized water 85.17%.
3. the nourishing and moisturizing lotion according to claim 1 containing Rosa Damascana, it is characterised in that the moisturizer is
Hyaluronic acid, serine and glycerine.
4. the nourishing and moisturizing lotion according to claim 3 containing Rosa Damascana, it is characterised in that in the moisturizer,
The additive amount of hyaluronic acid is 2~3%, and the additive amount of serine is 0.05~1%, and the additive amount of glycerine is 8~12%.
5. the nourishing and moisturizing lotion according to claim 1 containing Rosa Damascana, it is characterised in that the step (3)
Extraction is using accelerated solvent extraction, and extractant is dehydrated alcohol, and extracting pressure is 8~10MPa, extraction temperature is 40~
60 DEG C, solid-liquid ratio is 1:10~1:20, and extraction time is 10~20min.
6. the nourishing and moisturizing lotion according to claim 1 containing Rosa Damascana, it is characterised in that in the step (4)
When being purified using wiped-film still, vapo(u)rizing temperature is 60~70 DEG C, and distillation pressure is 18~25Pa, feed rate
For 1.0~2.0mL/min, scraping diaphragm plate revolving speed is 25~40r/min.
7. the nourishing and moisturizing lotion containing Rosa Damascana according to claim 1, it is characterised in that the complex enzyme hydrolysis liquid
PH adjusting be to be adjusted using citrate-phosphate disodium hydrogen buffer, the concentration of citric acid solution is 0.1mol/L, phosphoric acid
The concentration of disodium hydrogen solution is 0.2mol/L.
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