CN107737038B - Natural soda water rose self-emulsifying essential oil emulsion for Wudalianchi and preparation method thereof - Google Patents
Natural soda water rose self-emulsifying essential oil emulsion for Wudalianchi and preparation method thereof Download PDFInfo
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- CN107737038B CN107737038B CN201711092987.4A CN201711092987A CN107737038B CN 107737038 B CN107737038 B CN 107737038B CN 201711092987 A CN201711092987 A CN 201711092987A CN 107737038 B CN107737038 B CN 107737038B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses a natural soda water rose self-emulsifying essential oil emulsion in a Wudalianchi pool and a preparation method thereof, and relates to the field of skin care products. The invention aims to solve the technical problem that the skin is damaged by adding various additives into the existing rose essential oil emulsion. The emulsion is prepared from 60-80 parts by weight of natural soda water of a Wudalianchi, 10-20 parts by weight of rose petal micro powder and 10-20 parts by weight of rose essential oil. The method comprises the following steps: firstly, weighing raw materials; secondly, homogenizing under ultrahigh pressure; and thirdly, filling and sealing, and then performing cobalt-60 irradiation sterilization. The emulsion of the invention has the raw materials of the Wudalianchi natural soda water and the rose, is purely natural, nontoxic and harmless, avoids the potential safety hazard of adding other chemical substances, and is green and natural. The invention is used for preparing the natural soda water rose self-emulsifying essential oil emulsion of the Wudalianchi.
Description
Technical Field
The present invention relates to the field of skin care products.
Background
At present, the emulsion of the rose essential oil is added with additives of other non-rose substances such as an emulsifier, a preservative, a stabilizer and the like, the substances have great potential safety hazards to human skin, the emulsifier is a surfactant, the surfactant has been proved to have strong damage effect on the skin, the preservative has greater harm to human, the stabilizer is generally a macromolecular substance and is mostly synthesized artificially, and certain potential safety hazards also exist in skin care products.
Disclosure of Invention
The invention provides a natural soda water rose self-emulsifying essential oil emulsion of a Wudalianchi and a preparation method thereof, aiming at solving the technical problem that the skin is damaged by adding various additives into the existing emulsion of rose essential oil.
The natural soda water rose self-emulsifying essential oil emulsion for the Wudalianchi is prepared from, by weight, 60-80 parts of natural soda water for the Wudalianchi, 10-20 parts of rose petal micro powder and 10-20 parts of rose essential oil.
The preparation method of the rose petal micropowder comprises the following steps:
collecting fresh rose petals, controlling the temperature to be-195 ℃, performing liquid nitrogen low-temperature high-speed crushing by adopting a low-temperature liquid nitrogen freezing crusher at the crushing speed of 20000r/min to obtain micro powder with the particle size of 1-2 mu m, and then performing freeze drying to obtain the rose petal micro powder.
The preparation method of the natural soda water of the Wudalianchi comprises the following steps:
collecting Bozhou spring from east jiao of the Wudalianchi, and filtering with microporous membrane to obtain natural soda water of the Wudalianchi.
The method is specifically carried out according to the following steps;
firstly, weighing 60-80 parts of natural soda water of a Wudalianchi, 10-20 parts of rose petal micro powder and 10-20 parts of rose essential oil according to the mass;
secondly, homogenizing the natural soda water, the rose petal micro powder and the rose essential oil in the Wudalianchi pond weighed in the first step at the ultrahigh pressure of 300-310 MPa and the homogenization temperature of 70-75 ℃ for 30-35 min to obtain pre-emulsion;
and thirdly, filling and sealing the pre-emulsion obtained in the second step, and then performing cobalt-60 irradiation sterilization to finish the preparation method.
The water quality test analysis of the natural soda water obtained from the Wudalianchi Dongzhao Bobby spring is as follows:
the invention has the beneficial effects that: the natural soda water in the Wudalianchi pool is a treasure which is presented to human beings by nature, contains natural bicarbonate radical ion groups and various trace elements such as potassium, sodium, strontium, lithium and the like, is natural skin care product water due to low hardness and soft water quality, can well supplement skin mineral substances and nourish skin, is an excellent skin care product base material, has good effects of beautifying, moisturizing, resisting aging, beautifying, resisting inflammation and the like, and can completely release nutrient components in rose cells and form stable emulsion with the rose essential oil and the natural soda water in the Wudalianchi pool without adding other artificial chemical components. Therefore, the rose essential oil emulsion not only can exert the skin care effect of the rose essential oil, but also can have better absorbability and moisturizing effect.
The rose self-emulsifying essential oil emulsion is prepared by utilizing the rose self-substance and the natural soda water of the Wudalianchi through proper formula and process, the raw materials of the emulsion are completely the natural soda water of the Wudalianchi and the rose self-substance, and the emulsion is pure natural, non-toxic and harmless, avoids the potential safety hazard of adding other chemical substances, and is green and natural.
The invention is used for preparing the natural soda water rose self-emulsifying essential oil emulsion of the Wudalianchi.
Detailed Description
The technical solution of the present invention is not limited to the specific embodiments listed below, and includes any combination of the specific embodiments.
The first embodiment is as follows: the natural soda water rose self-emulsifying essential oil emulsion for the Wudalianchi is prepared from 60-80 parts by weight of natural soda water for the Wudalianchi, 10-20 parts by weight of rose petal micro powder and 10-20 parts by weight of rose essential oil.
The second embodiment is as follows: the first difference between the present embodiment and the specific embodiment is: the preparation method of the rose petal micropowder comprises the following steps:
collecting fresh rose petals, controlling the temperature to be-195 ℃, performing liquid nitrogen low-temperature high-speed crushing by adopting a low-temperature liquid nitrogen freezing crusher at the crushing speed of 20000r/min to obtain micro powder with the particle size of 1-2 mu m, and then performing freeze drying to obtain the rose petal micro powder. The rest is the same as the first embodiment.
The third concrete implementation mode: the present embodiment differs from the first or second embodiment in that: the freeze-drying temperature was-80 ℃. The other is the same as in the first or second embodiment.
The fourth concrete implementation mode: the difference between this embodiment mode and one of the first to third embodiment modes is: the preparation method of the natural soda water of the Wudalianchi comprises the following steps:
collecting Bozhou spring from east jiao of the Wudalianchi, and filtering with microporous membrane to obtain natural soda water of the Wudalianchi. The others are the same as in one of the first to third embodiments.
The fifth concrete implementation mode: the difference between this embodiment and one of the first to fourth embodiments is: the pore diameter of the microporous filter membrane is 0.22 mu m. The other is the same as one of the first to fourth embodiments.
The sixth specific implementation mode: the preparation method of the natural soda water rose self-emulsifying essential oil emulsion of the Wudalianchi concretely comprises the following steps of;
firstly, weighing 60-80 parts of natural soda water of a Wudalianchi, 10-20 parts of rose petal micro powder and 10-20 parts of rose essential oil according to the mass;
secondly, homogenizing the natural soda water, the rose petal micro powder and the rose essential oil in the Wudalianchi pond weighed in the first step at the ultrahigh pressure of 300-310 MPa and the homogenization temperature of 70-75 ℃ for 30-35 min to obtain pre-emulsion;
and thirdly, filling and sealing the pre-emulsion obtained in the second step, and then performing cobalt-60 irradiation sterilization to finish the preparation method.
The seventh embodiment: the sixth embodiment is different from the sixth embodiment in that: when the radiation sterilization is carried out in the third step, the sterilization dose is 10 kGy. The rest is the same as the sixth embodiment.
The following examples were used to demonstrate the beneficial effects of the present invention:
the first embodiment is as follows:
the natural soda water rose self-emulsifying essential oil emulsion for the Wudalianchi is prepared from 60 parts by weight of natural soda water for the Wudalianchi, 10 parts by weight of rose petal micro powder and 10 parts by weight of rose essential oil.
The preparation method of the rose petal micropowder comprises the following steps:
collecting fresh rose petals, controlling the temperature to be-195 ℃, performing liquid nitrogen low-temperature high-speed crushing by adopting a low-temperature liquid nitrogen freezing crusher at the crushing speed of 20000r/min to obtain micro powder with the particle size of 1-2 mu m, and then performing freeze drying at the temperature of-80 ℃ to obtain the rose petal micro powder.
The preparation method of the natural soda water of the Wudalianchi comprises the following steps:
collecting Bozhou spring of Dongjiao of WUDANCHA pond, and filtering with microporous membrane with pore diameter of 0.22 μm to obtain natural soda water of WUDANCHA pond.
The method is specifically carried out according to the following steps;
weighing 60 parts of natural soda water of a Wudalianchi, 10 parts of rose petal micro powder and 10 parts of rose essential oil according to the mass;
secondly, homogenizing the natural soda water, the rose petal micro powder and the rose essential oil in the Wudalianchi tank weighed in the first step at the ultrahigh pressure of 300MPa and the homogenization temperature of 70 ℃ for 30min to obtain pre-emulsion;
and thirdly, filling and sealing the pre-emulsion obtained in the second step, and then performing cobalt-60 radiation sterilization with the sterilization dose of 10kGy to finish the preparation method.
The natural soda water and the rose self-emulsifying essential oil emulsion without the additional natural soda water in the Wudalianchi are developed by utilizing the rose self substance and the natural soda water in the Wudalianchi through a proper formula and a proper process, the rose micro powder not only enables the nutrient components in rose cells to be completely released, but also can form stable emulsion with the rose essential oil and the natural soda water in the Wudalianchi without adding other artificial chemical components, the raw materials of the emulsion are completely the natural soda water in the Wudalianchi and the rose self substance, and the emulsion is pure natural, non-toxic and harmless, avoids the potential safety hazard of adding other chemical substances, and is green and natural. The rose essential oil emulsion not only can exert the skin care effect of rose essential oil, but also can have better absorbability and moisturizing effect.
Claims (3)
1. An essential oil emulsion of rose self-emulsified natural soda water in Wudalianchi is characterized in that the emulsion is prepared from 60-80 parts by weight of natural soda water in Wudalianchi, 10-20 parts by weight of rose petal micro powder and 10-20 parts by weight of rose essential oil;
the preparation method of the rose petal micropowder comprises the following steps:
collecting fresh rose petals, controlling the temperature to be-195 ℃, performing liquid nitrogen low-temperature high-speed crushing by adopting a low-temperature liquid nitrogen freezing crusher at the crushing speed of 20000r/min to obtain micro powder with the particle size of 1-2 mu m, and then performing freeze drying to obtain rose petal micro powder;
the preparation method of the natural soda water of the Wudalianchi comprises the following steps:
collecting Bozhou spring of the Wudalianchi, and filtering with microporous membrane to obtain natural soda water of the Wudalianchi;
the pore diameter of the microporous filter membrane is 0.22 mu m.
2. The natural suaeda salsa self-emulsifying essential oil emulsion as claimed in claim 1, wherein the freeze-drying temperature is-80 ℃.
3. The method for preparing the natural soda water rose self-emulsifying essential oil emulsion as claimed in claim 1, which is characterized in that the method comprises the following steps;
firstly, weighing 60-80 parts of natural soda water of a Wudalianchi, 10-20 parts of rose petal micro powder and 10-20 parts of rose essential oil according to the mass;
secondly, homogenizing the natural soda water, the rose petal micro powder and the rose essential oil in the Wudalianchi pond weighed in the first step at the ultrahigh pressure of 300-310 MPa and the homogenization temperature of 70-75 ℃ for 30-35 min to obtain pre-emulsion;
filling and sealing the pre-emulsion obtained in the step two, and then performing cobalt-60 irradiation sterilization to finish the preparation method; when the radiation sterilization is carried out in the third step, the sterilization dose is 10 kGy.
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| CN201711092987.4A CN107737038B (en) | 2017-11-08 | 2017-11-08 | Natural soda water rose self-emulsifying essential oil emulsion for Wudalianchi and preparation method thereof |
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| CN201711092987.4A CN107737038B (en) | 2017-11-08 | 2017-11-08 | Natural soda water rose self-emulsifying essential oil emulsion for Wudalianchi and preparation method thereof |
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| CN107737038B true CN107737038B (en) | 2020-11-06 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110973427A (en) * | 2019-12-18 | 2020-04-10 | 黑龙江省科学院火山与矿泉研究所 | Preparation method of gas-containing soda water based on Wudalianchi natural spring water |
| CN111011680A (en) * | 2019-12-18 | 2020-04-17 | 黑龙江省科学院火山与矿泉研究所 | Preparation method and application of micro-bubble water based on natural soda water of Wudalianchi |
| CN113520951B (en) * | 2021-08-12 | 2022-11-15 | 黑龙江省科学院自然与生态研究所 | Volcano cold spring green dragon's skin emulsion and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105534846A (en) * | 2015-12-30 | 2016-05-04 | 文有艺 | Facial mask |
| CN106389175A (en) * | 2016-09-07 | 2017-02-15 | 广州市澳键丰泽生物科技股份有限公司 | Nourishing and moisturizing lotion containing rose essential oil |
| CN107006748A (en) * | 2017-05-14 | 2017-08-04 | 云南淡定人生食品有限公司 | A kind of rose soda water and its production method |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105534846A (en) * | 2015-12-30 | 2016-05-04 | 文有艺 | Facial mask |
| CN106389175A (en) * | 2016-09-07 | 2017-02-15 | 广州市澳键丰泽生物科技股份有限公司 | Nourishing and moisturizing lotion containing rose essential oil |
| CN107006748A (en) * | 2017-05-14 | 2017-08-04 | 云南淡定人生食品有限公司 | A kind of rose soda water and its production method |
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