CN104027294B - Eye cream containing fucoidin and Punica granatum L. extract and preparation method thereof - Google Patents
Eye cream containing fucoidin and Punica granatum L. extract and preparation method thereof Download PDFInfo
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- CN104027294B CN104027294B CN201410224642.XA CN201410224642A CN104027294B CN 104027294 B CN104027294 B CN 104027294B CN 201410224642 A CN201410224642 A CN 201410224642A CN 104027294 B CN104027294 B CN 104027294B
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Abstract
A kind of eye cream containing fucoidin and Punica granatum L. extract of the present invention, it is made up of the component of following weight percents: fucoidin 0.2%-2.0%, Punica granatum L. extract 0.1%-1.0%, glycerol 4.0%-7.0%, hyaluronate sodium 0.05%-0.1%, softener 1.5%-3.0%, cetostearyl alcohol 0.5%, IPM? 2.0%-3.0%, EUMULGIN? S2? 0.1%-1.0%, EUMULGIN? S21? 0.2%, thickening agent? 0.5%, polydimethylsiloxane 1.0%, skinfeel regulator? 1.0%-2.0%, Sensiva SC50 0.05%-0.5%, phenoxyethanol 0.5%-0.6%, essence 0.05%-0.08%, deionized water surplus. the preparation method that the invention also discloses above-mentioned eye cream. the eye cream of the present invention has desalination microgroove, the effect of anti-wrinkle.
Description
Technical field
The present invention relates to a kind of cosmetics and preparation method thereof, more particularly to a kind of eye cream containing fucoidin and Punica granatum L. extract and preparation method thereof.
Background technology
Along with growth in the living standard; the quickening of life speed; people stay up late for a long time, in the face of computer, see the mobile phone; the eyes making people are subject to injury in various degree; thus accelerating the aging of eye cell, seeking safe efficient protection, the eye cream of defying age becomes the pursuit of people, " advocating nature " is the Main Trends of The Development of countries in the world cosmetics; make every effort to use natural plant raw material in eye cream, especially pronounced.
Except simple protection eye part skin, the anti-senescence function of eye cream also makes people focus more on, and natural plant raw material fucose and Punica granatum L. extract can be resisted by H2O2Stimulate the cell ageing caused, improve the situation that cell circumference of eyes cell is constantly old and feeble, so can play effect of defying age from inside to outside.
Summary of the invention
The technical problem to be solved is to provide a kind of eye cream containing natural plants Thallus Laminariae (Thallus Eckloniae) extract (fucoidin), Punica granatum L. extract, the preparation method that another one technical problem to be solved by this invention is to provide a kind of above-mentioned eye cream.
Technical scheme: a kind of eye cream containing fucoidin and Punica granatum L. extract, is formed (percentage by weight) by following component:
Fucoidin 0.2%-2.0%
Punica granatum L. extract 0.1%-1.0%
Glycerol 4.0%-7.0%
Hyaluronate sodium 0.05%-0.1%
Softener 1.5%-3.0%
Cetostearyl alcohol 0.5%
IPM2.0%-3.0%
EUMULGINS20.1%-1.0%
EUMULGINS210.2%
Thickening agent 0.5%
Polydimethylsiloxane 1.0%
Skinfeel regulator 1.0%-2.0%
Sensiva SC50 0.05%-0.5%
Phenoxyethanol 0.5%-0.6%
Essence 0.05%-0.08%
Deionized water surplus.
Further, described thickening agent is SIMVLGELEG, gelatin, hydrolytic collagen, card ripple, cellulose, xanthan gum or alginic acid.
Further, described skinfeel regulator is GB1020, CM1000.
Further, described softener is CetioCC.
The above-mentioned preparation method containing fucoidin and the eye cream of Punica granatum L. extract, it is characterised in that the following step:
A. hyaluronate sodium is scattered in glycerol, then adds deionized water, be uniformly mixed post-heating temperature to 80-89 DEG C, as A phase;
B. by softener, cetostearyl alcohol, IPM, EUMULGINS2, EUMULGINS21 mix homogeneously post-heating temperature to 80-89 DEG C, as B phase;
C. by polydimethylsiloxane, skinfeel regulator mixing and stirring, as C phase;
D., A being added to B phase, starts emulsifying, be simultaneously introduced C phase and thickening agent, homogenizing stirs 3-10 minute;
E. treat that system homogenizing obtained for step d is complete, stir froth breaking, add fucoidin, Punica granatum L. extract, Sensiva SC50, phenoxyethanol and essence when being cooled to 30-50 DEG C, stir, regulation system PH to 5.5-7.0, discharging after room temperature.
Concrete, above-mentioned CetiolCC refers to dicaprylyl carbonate. IPM refers to isopropyl myristate; EUMULGINS2 refers to the stearic alcohol ether of polyoxyethylene-2. EUMULGINS21 refers to the stearic alcohol ether of polyoxyethylene-21. SIMVLGELEG refers to the mixture being made up of sodium acrylate/sodium acryloyldimethyl taurate copolymers, 2-Methylpentadecane, Polyoxyethylene Sorbitan Monooleate; it it is a kind of thickening agent (match BIC Corp of France; agent Shanghai hundred Hao Bo Chemical Co., Ltd., trade name SIMVLGELEG). GB1020 refers to the mixture (Wacker Chemie GmbH of Germany, agent Shanghai to soft Chemical Co., Ltd., trade name GB1020) being made up of polydimethylsiloxane, dimethiconol. CM1000S refers to the mixture (Wacker Chemie GmbH of Germany, agent Shanghai to soft Chemical Co., Ltd., trade name CM1000) being made up of ring five polydimethylsiloxane, dimethiconol. Skinfeel regulator is for regulating the lubricity of cosmetics, greasy feeling, rheological characteristic.
Aging is as the growth at age, and the physiological process of a series of degeneration change occurs body, and main cause has the accumulation of cell injury and the expression of SAG; Free-radical theory thinks that aging course is to carry out in the cell one by one of composition organism, and the aging of any organism is all the reflection of its composition cell ageing accumulation.
The eye cream of the present invention contains extract-fucoidin and the Punica granatum L. extract of natural plants Thallus Laminariae (Thallus Eckloniae), and it can significantly reduce H2O2Stimulate the cell injury caused, thus playing anti-aging effects; It it is one natural plants antiaging agent safely and efficiently. The preparation method of eye cream of the present invention make use of the conventional fabrication process of eye cream class cosmetics, and preparation method is simple, reliable.
The method have the advantages that
(1) worship the theory of natural environmental-protective, replace antiaging agent chemosynthesis, strong and stimulating, milder, more environmental protection with natural vegetable raw material.
(2) anti-aging effects of the present invention is clearly.
(3) present invention process is simple, workable.
Accompanying drawing explanation
Fig. 1 is the score value variation diagram of wrinkle near the eyes after the eye cream of the employing present invention.
Detailed description of the invention
Below in conjunction with example, the present invention is described in further detail:
Embodiment 1(eye cream formula)
Composition weight (%)
A kind of eye cream containing fucoidin and Punica granatum L. extract, is formed (percentage by weight) by following component:
Fucoidin 0.2
Punica granatum L. extract 0.2
Glycerol 7.0
Hyaluronate sodium 0.1
CetiolCC1.5
Cetostearyl alcohol 0.5
IPM2.0
EUMULGINS20.1
EUMULGINS210.2
SIMVLGELEG0.5
Polydimethylsiloxane 1.0
GB10202.0
Sensiva SC50 0.08
Phenoxyethanol 0.5
Essence 0.05
Deionized water surplus.
Described fucoidin is the polysaccharide material of extract from natural plants Thallus Laminariae (Thallus Eckloniae), and Punica granatum L. extract is the polyphenols extracted from natural plants Punica granatum L..
The preparation method of embodiment 2(eye cream)
A. hyaluronate sodium is scattered in glycerol, then adds deionized water, be uniformly mixed post-heating temperature to 85 DEG C, as A phase;
B. by CetiolCC, cetostearyl alcohol, IPM, EUMULGINS2, EUMULGINS21 mix homogeneously post-heating temperature to 85 DEG C, as B phase;
C. by polydimethylsiloxane, GB1020 mixing and stirring, as C phase;
D., A being added to B phase, starts emulsifying, be simultaneously introduced C phase and SIMVLGELEG, homogenizing stirs 4 minutes;
E. treat that system homogenizing obtained for step d is complete, stir froth breaking, add fucoidin, Punica granatum L. extract, Sensiva SC50, phenoxyethanol and essence when being cooled to 45 DEG C, stir, regulation system PH to 5.5-7.0, discharging after room temperature.
Above said content is only the basic explanation under present inventive concept, and according to any equivalent transformation that technical scheme is made, all should belong to protection scope of the present invention.
The efficacy test of embodiment 3(eye cream)
The crease-resistant function of compacting of eye cream prepared by embodiment 1 is carried out senile-resistant efficacy evaluation by the wrinkle parameter fed back by VISIA instrument.
Test instrunment and equipment: VISIA skinanalysis apparatus
Test method:
1., after experimenter's visiting, should confirm that experimenter correctly defers to experiment requirements;
2. tester informs the test concerns on the same day and time of later following up a case by regular visits to;
3. test process:
3.1 experimenters use cleansing milk to clean full face under tester instructs, and blot excessive moisture with napkin or dry towel with clear water after clean for flush with foam.
The eyes eye tail of experimenter is decided to be A point by 3.2, and eyes are decided to be B point now.
3.3 experimenters start test after waiting 15 minutes in constant temperature and humidity room.
3.4 with VISIA record experimenter left, just, right side photograph, and record wrinkle score value, picture saved as " 0 week ".
Namely 3.5 experimenters began to use defying age eye cream in test the same day, it is desirable to each use sooner or later once, uses 15 thoughtful tests to terminate continuously.
Result of the test
Wrinkle score value changes as shown in Figure 1 near the eyes, and after the defying age eye creams of 15 weeks use, wrinkle score value has bigger reduction amplitude near the eyes, it was demonstrated that this eye cream has significantly desalinates microgroove, anti-wrinkle effect, namely has anti-aging effects.
Claims (3)
1. the eye cream containing fucoidin and Punica granatum L. extract, it is characterised in that be made up of the component of following weight percents:
Fucoidin 0.2%-2.0%
Punica granatum L. extract 0.1%-1.0%
Glycerol 4.0%-7.0%
Hyaluronate sodium 0.05%-0.1%
Softener 1.5%-3.0%
Cetostearyl alcohol 0.5%
Isopropyl myristate 2.0%-3.0%
The stearic alcohol ether 0.1%-1.0% of polyoxyethylene-2
The stearic alcohol ether 0.2% of polyoxyethylene-21
Thickening agent 0.5%
Polydimethylsiloxane 1.0%
Skinfeel regulator 1.0%-2.0%
Sensiva SC50 0.05%-0.5%
Phenoxyethanol 0.5%-0.6%
Essence 0.05%-0.08%
Deionized water surplus;
Described softener is for referring to dicaprylyl carbonate, described skinfeel regulator is GB1020 or CM1000S, GB1020 refers to the mixture being made up of polydimethylsiloxane, dimethiconol, and CM1000S refers to the mixture being made up of ring five polydimethylsiloxane, dimethiconol.
2. a kind of eye cream containing fucoidin and Punica granatum L. extract as claimed in claim 1; it is characterized in that: described thickening agent is SIMVLGELEG, gelatin, hydrolytic collagen, card ripple, cellulose, xanthan gum or alginic acid, and described SIMVLGELEG refers to the mixture being made up of sodium acrylate/sodium acryloyldimethyl taurate copolymers, 2-Methylpentadecane, Polyoxyethylene Sorbitan Monooleate.
3. a kind of preparation method containing fucoidin and the eye cream of Punica granatum L. extract described in claim 1, it is characterised in that comprise the following steps:
A. hyaluronate sodium is scattered in glycerol, then adds deionized water, be uniformly mixed post-heating temperature to 80-89 DEG C, as A phase;
B. by softener, cetostearyl alcohol, isopropyl myristate, the stearic alcohol ether of polyoxyethylene-2, the stearic alcohol ether mix homogeneously post-heating temperature of polyoxyethylene-21 to 80-89 DEG C, as B phase;
C. by polydimethylsiloxane, skinfeel regulator mixing and stirring, as C phase;
D., A being added to B phase, starts emulsifying, be simultaneously introduced C phase and thickening agent, homogenizing stirs 3-10 minute;
E. treat that system homogenizing obtained for step d is complete, stir froth breaking, add fucoidin, Punica granatum L. extract, Sensiva SC50, phenoxyethanol and essence when being cooled to 30-50 DEG C, stir, regulation system PH to 5.5-7.0, discharging after room temperature.
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CN104622713B (en) * | 2015-01-26 | 2017-07-14 | 杭州易文赛生物技术有限公司 | A kind of cosmetic composition and preparation method thereof |
ITUB20152498A1 (en) * | 2015-07-24 | 2017-01-24 | Nati Srl | ANTI-AGING COSMETIC COMPOSITION AND METHOD FOR ITS PREPARATION |
CN106580826A (en) * | 2016-12-21 | 2017-04-26 | 宁波君瑞生物科技有限公司 | Cream with effects of increasing skin moisture and reducing wrinkles |
CN107397691A (en) * | 2017-09-11 | 2017-11-28 | 广州聚注通用技术研究院有限公司 | One kind dispels ocular edema additive and its application |
CN108685758A (en) * | 2018-07-05 | 2018-10-23 | 青岛明月爱熙化妆品有限公司 | Moisturizing emulsion and preparation method thereof containing fucoidin |
CN111991267A (en) * | 2020-08-04 | 2020-11-27 | 青岛明月海藻生物健康科技集团有限公司 | Moisturizing and anti-wrinkle eye cream containing rock algae polysaccharide and preparation method thereof |
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JPWO2006093175A1 (en) * | 2005-03-01 | 2008-08-07 | 宇部興産株式会社 | Fucoidan production method, fucoidan and fucoidan-containing composition |
AU2007267823A1 (en) * | 2006-06-01 | 2007-12-06 | Sakura Properties, Llc | Fucoidan compositions and methods |
CN203591454U (en) * | 2013-08-11 | 2014-05-14 | 长沙沁才生物科技有限公司 | Fucoidin superfine cellulose facial mask |
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