CN107737038A - Natural soda water rose self-emulsifying essential oil emulsion for Wudalianchi and preparation method thereof - Google Patents

Natural soda water rose self-emulsifying essential oil emulsion for Wudalianchi and preparation method thereof Download PDF

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Publication number
CN107737038A
CN107737038A CN201711092987.4A CN201711092987A CN107737038A CN 107737038 A CN107737038 A CN 107737038A CN 201711092987 A CN201711092987 A CN 201711092987A CN 107737038 A CN107737038 A CN 107737038A
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wudalianchi
essential oil
parts
oil emulsion
rose
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CN201711092987.4A
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CN107737038B (en
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方振兴
王希英
潘虹
曾颖
吴婧
谢振华
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INSTITUTE OF VOLCANO AND SPRING OF HEILONGJIANG ACADEMY OF SCIENCES
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INSTITUTE OF VOLCANO AND SPRING OF HEILONGJIANG ACADEMY OF SCIENCES
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Medicinal Preparation (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a natural soda water rose self-emulsifying essential oil emulsion in a Wudalianchi pool and a preparation method thereof, and relates to the field of skin care products. The invention aims to solve the technical problem that the skin is damaged by adding various additives into the existing rose essential oil emulsion. The emulsion is prepared from 60-80 parts by weight of natural soda water of a Wudalianchi, 10-20 parts by weight of rose petal micro powder and 10-20 parts by weight of rose essential oil. The method comprises the following steps: firstly, weighing raw materials; secondly, homogenizing under ultrahigh pressure; and thirdly, filling and sealing, and then performing cobalt-60 irradiation sterilization. The emulsion of the invention has the raw materials of the Wudalianchi natural soda water and the rose, is purely natural, nontoxic and harmless, avoids the potential safety hazard of adding other chemical substances, and is green and natural. The invention is used for preparing the natural soda water rose self-emulsifying essential oil emulsion of the Wudalianchi.

Description

A kind of self emulsifying essential oil emulsion of Wudalianchi salsoda water rose and its preparation Method
Technical field
The present invention relates to skin care field.
Background technology
The emulsion of Rosa Damascana adds adding for other materials of non-rose such as emulsifying agent, preservative, stabilizer itself at present Add agent, these materials have very big potential safety hazard to the skin of people, emulsifying agent just namely surfactant, verified table Face activating agent has very strong damaging action to skin, and injury of the preservative to people is bigger, and stabilizer is usually macromolecular substances, Mostly artificial synthesized, there is also certain potential safety hazard in skin care item.
The content of the invention
The invention solves the emulsion of current Rosa Damascana to add multiple additives, the technical problem for having damage to skin, And provide a kind of self emulsifying essential oil emulsion of Wudalianchi salsoda water rose and preparation method thereof.
A kind of self emulsifying essential oil emulsion of Wudalianchi salsoda water rose is in parts by weight by 60~80 part of five Dalian Chi Tianransudashui, 10~20 parts of roseleaf micro mists and 10~20 parts of Rosa Damascanas are prepared.
The preparation method of roseleaf micro mist is carried out according to the following steps：
Fresh roseleaf is gathered, it is -195 DEG C to control temperature, and it is low to carry out liquid nitrogen using Fluid nitrogen cryopreservation pulverizer Warm to crush at a high speed, crushing speed is 20000r/min, obtains the micro mist that granularity is 1~2 μm, is then freeze-dried, obtains rose Petal micro mist.
The preparation method of Wudalianchi salsoda water is carried out according to the following steps：
Wudalianchi Dong Jiao get Bu mountain springs are gathered, then by filtering with microporous membrane, obtain Wudalianchi salsoda water.
This method is specifically carried out according to the following steps；
First, 60~80 parts of Wudalianchi salsoda water, 10~20 parts of roseleaf micro mists and 10~20 are weighed by quality Part Rosa Damascana；
2nd, Wudalianchi salsoda water, roseleaf micro mist and the Rosa Damascana weighed step 1 carries out super-pressure Homogeneous, it is 300~310MPa to control homogenization pressure, and homogenizing temperature is 70~75 DEG C, and homogenizing time is 30~35min, is obtained pre- Emulsion processed；
3rd, the pre-emulsion that step 2 obtains is carried out filling and sealed, then carry out the irradiation sterilization of cobalt -60, complete system Preparation Method.
The water-quality test for the salsoda water that Wudalianchi Dong Jiao get Bu mountain springs obtain is analyzed as follows table in the present invention：
The beneficial effects of the invention are as follows：Wudalianchi salsoda water is the rarity of the Nature present mankind, and it contains day Right bicarbonate ion group, and the various trace elements such as potassium, sodium, strontium, lithium, Wudalianchi salsoda water is due to its hardness Low, water quality is soft, is natural skin care item water, and can be good at supplementing skin mineral matter, skin nutrition, and Rosa Damascana is Outstanding skin-care product base, there is good beauty, moisturizing, anti-aging, beauty treatment, anti-inflammatory and other effects, and rose micro mist not only makes rose Intracellular nutritional composition discharges completely, and can form stable emulsion with Rosa Damascana and Wudalianchi salsoda water and Other artificial chemical compositions need not be added.Therefore Rosa Damascana emulsion can not only give play to Rosa Damascana skin effect and Can there are more preferable absorbability and moistening effect.
The present invention is developed using rose Self substances and Wudalianchi salsoda water by appropriate formula and technique The no added self emulsifying essential oil emulsion of Wudalianchi salsoda water rose, the emulsion materials are entirely Wudalianchi salsoda Water and the material of rose itself, it is pure natural, it is nontoxic, avoid the potential safety hazard for adding other chemical substances, emulsion green Naturally.
The present invention is used to prepare a kind of self emulsifying essential oil emulsion of Wudalianchi salsoda water rose.
Embodiment
Technical solution of the present invention is not limited to the embodiment of act set forth below, in addition to each embodiment it Between any combination.
Embodiment one：A kind of self emulsifying essential oil emulsion of Wudalianchi salsoda water rose of present embodiment is pressed Parts by weight are by 60~80 parts of Wudalianchi salsoda water, 10~20 parts of roseleaf micro mists and 10~20 parts of Rosa Damascana systems It is standby to form.
Embodiment two：Present embodiment is unlike embodiment one：The roseleaf micro mist Preparation method is carried out according to the following steps：
Fresh roseleaf is gathered, it is -195 DEG C to control temperature, and it is low to carry out liquid nitrogen using Fluid nitrogen cryopreservation pulverizer Warm to crush at a high speed, crushing speed is 20000r/min, obtains the micro mist that granularity is 1~2 μm, is then freeze-dried, obtains rose Petal micro mist.It is other identical with embodiment one.
Embodiment three：Present embodiment is unlike embodiment one or two：The freeze-drying temperature Spend for -80 DEG C.It is other identical with embodiment one or two.
Embodiment four：Unlike one of present embodiment and embodiment one to three：Five Dalian Chi Tianransudashui preparation method is carried out according to the following steps：
Wudalianchi Dong Jiao get Bu mountain springs are gathered, then by filtering with microporous membrane, obtain Wudalianchi salsoda water. It is other identical with one of embodiment one to three.
Embodiment five：Unlike one of present embodiment and embodiment one to four：The micropore filter The aperture of film is 0.22 μm.It is other identical with one of embodiment one to four.
Embodiment six：A kind of Wudalianchi salsoda water rose described in embodiment one is self emulsifying The preparation method of essential oil emulsion, specifically carry out according to the following steps；
First, 60~80 parts of Wudalianchi salsoda water, 10~20 parts of roseleaf micro mists and 10~20 are weighed by quality Part Rosa Damascana；
2nd, Wudalianchi salsoda water, roseleaf micro mist and the Rosa Damascana weighed step 1 carries out super-pressure Homogeneous, it is 300~310MPa to control homogenization pressure, and homogenizing temperature is 70~75 DEG C, and homogenizing time is 30~35min, is obtained pre- Emulsion processed；
3rd, the pre-emulsion that step 2 obtains is carried out filling and sealed, then carry out the irradiation sterilization of cobalt -60, complete system Preparation Method.
Embodiment seven：Present embodiment is unlike embodiment six：In step 3 during irradiation sterilization, Sterilizing dose is 10kGy.It is other identical with embodiment six.
Beneficial effects of the present invention are verified using following examples：
Embodiment one：
A kind of self emulsifying essential oil emulsion of Wudalianchi salsoda water rose of the present embodiment is in parts by weight by 60 part five Dalian Chi Tianransudashui, 10 parts of roseleaf micro mists and 10 parts of Rosa Damascanas are prepared.
The preparation method of roseleaf micro mist is carried out according to the following steps：
Fresh roseleaf is gathered, it is -195 DEG C to control temperature, and it is low to carry out liquid nitrogen using Fluid nitrogen cryopreservation pulverizer Warm to crush at a high speed, crushing speed is 20000r/min, obtains the micro mist that granularity is 1~2 μm, and then temperature is that -80 DEG C of freezings are dry It is dry, obtain roseleaf micro mist.
The preparation method of Wudalianchi salsoda water is carried out according to the following steps：
Wudalianchi Dong Jiao get Bu mountain springs are gathered, then by filtering with microporous membrane, the aperture of miillpore filter is 0.22 μm, Obtain Wudalianchi salsoda water.
This method is specifically carried out according to the following steps；
First, 60 parts of Wudalianchi salsoda water, 10 parts of roseleaf micro mists and 10 parts of Rosa Damascanas are weighed by quality；
2nd, Wudalianchi salsoda water, roseleaf micro mist and the Rosa Damascana weighed step 1 carries out super-pressure Homogeneous, it is 300MPa to control homogenization pressure, and homogenizing temperature is 70 DEG C, homogenizing time 30min, obtains pre-emulsion；
3rd, the pre-emulsion that step 2 obtains is carried out filling and sealed, then carry out the irradiation sterilization of cobalt -60, bactericidal agent Measure as 10kGy, completion preparation method.
The present embodiment passes through appropriate formula and technique development using rose Self substances and Wudalianchi salsoda water Go out the no added self emulsifying essential oil emulsion of Wudalianchi salsoda water rose, rose micro mist not only make rose intracellular nutritional into Divide release completely, and stable emulsion can be formed without adding it with Rosa Damascana and Wudalianchi salsoda water His artificial chemical composition, the emulsion materials are entirely Wudalianchi salsoda water and the material of rose itself, pure natural, nontoxic It is harmless, avoid the potential safety hazard for adding other chemical substances, emulsion green natural.Rosa Damascana emulsion can not only give play to rose The skin effect of rare essential oil and can there are more preferable absorbability and moistening effect.

Claims (7)

  1. A kind of 1. self emulsifying essential oil emulsion of Wudalianchi salsoda water rose, it is characterised in that the emulsion in parts by weight by 60~80 parts of Wudalianchi salsoda water, 10~20 parts of roseleaf micro mists and 10~20 parts of Rosa Damascanas are prepared.
  2. 2. a kind of self emulsifying essential oil emulsion of Wudalianchi salsoda water rose according to claim 1, its feature exist Carried out according to the following steps in the preparation method of the roseleaf micro mist：
    Fresh roseleaf is gathered, it is -195 DEG C to control temperature, and it is high to carry out liquid nitrogen cryogenics using Fluid nitrogen cryopreservation pulverizer Speed crushes, and crushing speed is 20000r/min, obtains the micro mist that granularity is 1~2 μm, is then freeze-dried, obtains roseleaf Micro mist.
  3. 3. a kind of self emulsifying essential oil emulsion of Wudalianchi salsoda water rose according to claim 2, its feature exist In the temperature that is freeze-dried for -80 DEG C.
  4. 4. a kind of self emulsifying essential oil emulsion of Wudalianchi salsoda water rose according to claim 1, its feature exist Carried out according to the following steps in the preparation method of the Wudalianchi salsoda water：
    Wudalianchi Dong Jiao get Bu mountain springs are gathered, then by filtering with microporous membrane, obtain Wudalianchi salsoda water.
  5. 5. a kind of self emulsifying essential oil emulsion of Wudalianchi salsoda water rose according to claim 4, its feature exist In the aperture of the miillpore filter be 0.22 μm.
  6. 6. a kind of preparation method of the self emulsifying essential oil emulsion of Wudalianchi salsoda water rose as claimed in claim 1, It is characterized in that this method is specifically carried out according to the following steps；
    First, 60~80 parts of Wudalianchi salsoda water, 10~20 parts of roseleaf micro mists and 10~20 parts of roses are weighed by quality Rare essential oil；
    2nd, Wudalianchi salsoda water, roseleaf micro mist and the Rosa Damascana weighed step 1 carries out super-high-pressure homogenization, It is 300~310MPa to control homogenization pressure, and homogenizing temperature is 70~75 DEG C, and homogenizing time is 30~35min, obtains prefabricated breast Liquid；
    3rd, the pre-emulsion that step 2 obtains is carried out filling and sealed, then carry out the irradiation sterilization of cobalt -60, complete preparation side Method.
  7. A kind of 7. preparation side of self emulsifying essential oil emulsion of Wudalianchi salsoda water rose according to claim 6 Method, it is characterised in that in step 3 during irradiation sterilization, sterilizing dose 10kGy.
CN201711092987.4A 2017-11-08 2017-11-08 Natural soda water rose self-emulsifying essential oil emulsion for Wudalianchi and preparation method thereof Active CN107737038B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110973427A (en) * 2019-12-18 2020-04-10 黑龙江省科学院火山与矿泉研究所 Preparation method of gas-containing soda water based on Wudalianchi natural spring water
CN111011680A (en) * 2019-12-18 2020-04-17 黑龙江省科学院火山与矿泉研究所 Preparation method and application of micro-bubble water based on natural soda water of Wudalianchi
CN113520951A (en) * 2021-08-12 2021-10-22 黑龙江省科学院自然与生态研究所 Volcano cold spring green dragon's skin emulsion and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN105534846A (en) * 2015-12-30 2016-05-04 文有艺 Facial mask
CN106389175A (en) * 2016-09-07 2017-02-15 广州市澳键丰泽生物科技股份有限公司 Nourishing and moisturizing lotion containing rose essential oil
CN107006748A (en) * 2017-05-14 2017-08-04 云南淡定人生食品有限公司 A kind of rose soda water and its production method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105534846A (en) * 2015-12-30 2016-05-04 文有艺 Facial mask
CN106389175A (en) * 2016-09-07 2017-02-15 广州市澳键丰泽生物科技股份有限公司 Nourishing and moisturizing lotion containing rose essential oil
CN107006748A (en) * 2017-05-14 2017-08-04 云南淡定人生食品有限公司 A kind of rose soda water and its production method

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110973427A (en) * 2019-12-18 2020-04-10 黑龙江省科学院火山与矿泉研究所 Preparation method of gas-containing soda water based on Wudalianchi natural spring water
CN111011680A (en) * 2019-12-18 2020-04-17 黑龙江省科学院火山与矿泉研究所 Preparation method and application of micro-bubble water based on natural soda water of Wudalianchi
CN113520951A (en) * 2021-08-12 2021-10-22 黑龙江省科学院自然与生态研究所 Volcano cold spring green dragon's skin emulsion and preparation method thereof

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