CN112716861A

CN112716861A - Comfortable degerming mask and preparation method thereof

Info

Publication number: CN112716861A
Application number: CN202110184239.9A
Authority: CN
Inventors: 王忠良
Original assignee: Individual
Current assignee: Individual
Priority date: 2021-02-10
Filing date: 2021-02-10
Publication date: 2021-04-30

Abstract

The invention discloses a comfortable and degerming mask liquid and a preparation method thereof, the comfortable and degerming mask liquid is a composite film liquid consisting of a faint scent leaf extract, a lacquer tree leaf extract, lacquer tree oil, an emulsifier, a phyllanthus emblica extract, baking soda and polyethylene glycol.

Description

Comfortable degerming mask and preparation method thereof

Technical Field

The invention relates to the technical field of cosmetics, in particular to a comfortable and degerming mask liquid and a preparation method thereof.

Background

The conventional cosmetics are designed according to the principle of cosmetic formula, and on the basis of functional raw materials, thickening agents, preservatives, essences and the like are added for keeping the stability of appearance state and the requirement of commercialization. In addition, in order to improve the effect of the functional cosmetics, various functional components are added, wherein the functional components comprise various functional extracts such as plant-derived extracts and the like and also comprise some auxiliary agents which are not plant-derived. For gestation, lactation and other people with sensitive skin, this increases the burden on the skin and even increases the risk of irritation and sensitivity.

As cosmetics pursue natural, whole plant ingredient market demands, more and more cosmetic formulations have reduced the use of non-plant derived materials. However, the existing cosmetic technology and invention only adopt the compounding and post-processing of plant cosmetic raw materials, and do not control and change from the source of the raw materials and the production technology, so as to meet the requirements of market consumers on all plant components of the facial mask liquid, nature and mild safety.

Patent CN111792134A discloses a facial mask containing traditional Chinese medicine components, a preparation process and a preparation system thereof, wherein essence used by the facial mask contains wormwood. The process comprises the following steps: firstly, placing facial mask paper on a positioning table and a folding table, and cutting by a cutting knife I and a cutting knife II; adjusting a folding table to fold the cut facial mask paper for the first time, and then packaging the facial mask paper into a packaging bag with essence while folding the facial mask paper for the second time by utilizing a thin-wall box; and step three, sealing the packaging bag by using the hot part I and the hot part II. The facial mask can be used for diminishing inflammation, inhibiting bacteria and removing mites on the face and the skin of the eyelid, and the facial mask at the eyelid is convenient to fold over or tear, so that intolerant eyelid skin allergy is avoided.

In patent CN111514044A, a zeolite energy mask and a preparation method thereof are disclosed, relating to the technical field of mask preparation; aiming at solving the problem that the mask can not be effectively sterilized and disinfected; a zeolite energy mask comprises the following components in parts by weight: 30% of zeolite; a preparation method of a zeolite energy mask comprises the following steps: preparing the raw materials according to the mass percentage; mixing squalane and carbomer sodium under stirring, and adding appropriate amount of deionized water, butanediol, and propylene glycol. The facial mask can adsorb a large amount of allergens, heavy metals, toxic and harmful substances and various waste toxins by adding zeolite, has very strong adsorption and removal effects, also has adsorption and removal effects on some toxic radioactive chemical substances and harmful toxins with serious pollution, obviously improves the bacterial adsorption capacity and the sterilization rate of the facial mask, can remove harmful garbage and impurities of various toxins on the face, and achieves the effects of sterilization, disinfection and bacteriostasis.

Patent publication No. CN111110615A discloses a tricholoma matsutake mask liquid, and a preparation method and application thereof. The invention adopts medicinal and edible plants as raw materials (natural ingredients such as oat, Chinese yam, tricholoma matsutake, dendrobium, pseudo-ginseng, tremella, vegetable oil and the like) and water as a medium, and directly prepares a safe and mild full-plant mask liquid with remarkable moisturizing effect by an extraction and impurity removal process, does not contain essence, preservative and bactericide, and does not generate irritation and side effect while nourishing skin; the facial mask liquid is absorbed by the facial mask carrier and applied on the facial skin, and the facial mask liquid has a skin care effect; the facial mask liquid disclosed by the invention has good moisturizing and whitening effects, the preparation method is simple in process, and the all-plant component tricholoma matsutake facial mask prepared by the preparation method has no irritation and high whitening effect, no potential safety hazard and improved efficacy.

In patent publication No. CN112107492A, a preparation method of a bacteriostatic emulsion essence mask is disclosed, which comprises the following steps: step one, preparing a soaking solution: mixing and stirring plant essence components with water, a thickening agent and an emulsifying agent to obtain a soaking solution; step two, filtering the soaking solution: filtering the soaking solution prepared in the first step to remove fine impurities in the soaking solution; step three, soaking the facial mask paper: soaking the facial mask paper in the soaking solution, and fully soaking to obtain the antibacterial emulsion essence facial mask; step four, folding and packing into bags: taking out the antibacterial emulsion essence mask from the soaking solution, folding, bagging and sealing; and the second step is completed by adopting a bacteriostatic emulsion essence mask preparation machine in a mechanical matching way.

In patent CN112043653A, an anti-allergy and soothing mask and a preparation method thereof are disclosed, comprising a mask liquid and a mask liquid carrier, wherein the mask liquid is prepared from the following raw materials: polyhydric alcohol, anti-allergy relieving composition, Hamamelis virginiana extract, aloe extract, sodium polyglutamate, Sparassis crispa extract, trehalose, allantoin, p-hydroxyacetophenone, lodestone, 1, 2-hexanediol, alpha-arbutin, ectoin, fullerene, hydrolyzed sclerotium rolfsii gum, dipotassium glycyrrhizinate, disodium ethylene diamine tetraacetate, sodium hyaluronate and deionized water.

The above patents all have the problems that the extracted components of the plant source are single, the plant source is not all plant components, and part of products have chemicals, irritant raw materials and the like.

Disclosure of Invention

The invention further improves the product effect and increases the bacteria removing property and the comfort property on the basis of the patents, so that the mask has the advantages of bacteriostasis, anti-inflammation, skin penetration and absorption in the using process, and the composite essence components are extracted by using plant sources, so that the problems of safety, irritant raw materials and the like do not exist.

The invention adopts the following scheme:

a refreshing antibacterial facial mask liquid comprises fragrant leaf extract, lacquer tree oil, emulsifier, fructus Phyllanthi extract, sodium bicarbonate, and polyethylene glycol.

2-3 parts of fragrant leaf extract, 2-3 parts of sumac oil, 1-2 parts of emulsifier, 4-8 parts of phyllanthus emblica extract, 1-2 parts of baking soda and 1-2 parts of polyethylene glycol.

The faint scent leaf extract is prepared by concentrating and drying an extracting solution of faint scent leaves subjected to microwave extraction by using ethanol with the volume fraction of 60-70%.

The preparation method of the sumac leaf extract comprises the following steps: (1) picking tender buds or leaves of the lacquer tree, cleaning the tender buds or leaves with clear water, drying the tender buds or leaves until the water content is 1-5%, and crushing the tender buds or leaves to 20-60 meshes; (2) according to the g-g solid-liquid ratio of 1: adding water and/or ethanol into the raw materials in the step (1) in a ratio of 20-100, uniformly mixing, treating for 1-48 h at 25-100 ℃, under a pressure of 0-0.3 MPa and at a stirring speed of 50-100 r/min for 1-2 times, and mixing for later use; (3) according to the mass ratio of the grease to the emulsifier of 1: 0.2-1, mixing the oil and the emulsifier, emulsifying for 0.5-2 hours at the temperature of 40-80 ℃ and at the stirring speed of 50-100 r/min, and uniformly and completely emulsifying for later use, wherein the mass ratio of the oil to the sumac leaves is 1-2: 1; (4) adding the extracting solution in the step (2) and lacquer tree leaves or buds into the emulsified oil in the step (3), stirring for 0.5-2 h, standing for 2-8 h, and then carrying out phase splitting; (5) and (4) separating the lower aqueous phase part of the layered liquid in the step (4) by using a separating funnel, and filtering to obtain the sumac leaf extract.

The grease in the step (3) is shea butter, walnut oil and prinsepia utilis royle oil.

The emulsifier in the step (3) is one or a mixture of lecithin, monoglyceride and sucrose fatty acid ester.

The lacquer tree oil is lacquer seed kernel oil of lacquer tree.

The preparation method of the phyllanthus emblica extract comprises the following steps: (1) sterilizing fructus Phyllanthi, and removing core; (2) freeze-drying the phyllanthus emblica fruits treated in the step (1) at the temperature of between 10 ℃ below zero and 30 ℃ below zero and under the vacuum degree of 30 to 100pa to obtain dried phyllanthus emblica fruits with the water content of 8 to 10 weight percent; (3) pulverizing the dried fructus phyllanthi product at-10 deg.C to-30 deg.C, and sieving with 20 mesh sieve; (4) and (3) mixing the crushed Yunnan olive in a solid-liquid ratio of 1: boiling and extracting for 1-2 h for 20-40 hours, and filtering to obtain filtrate; (5) and (3) concentrating the filtrate obtained in the step (4) at the temperature of 60-70 ℃ to enable the fruit juice to be concentrated to the mass percentage concentration of 25-35%, and then obtaining the phyllanthus emblica extract.

The preparation method of the comfortable and degerming mask liquid comprises the following steps:

(1) putting the fragrant leaf extract, the sumac leaf extract and the phyllanthus emblica extract into a stirring kettle, and uniformly stirring at the temperature of 50-60 ℃ for 15-30 min;

(2) uniformly stirring the lacquer tree oil and the emulsifier at the temperature of 60-70 ℃ for 10-20 min to obtain emulsified lacquer grease;

(3) integrally pumping the mixture prepared in the step (1) and the emulsified paint grease in the step (2) into a high-pressure homogenizer, adding 1.0-1.5 times of deionized water according to the mass ratio, adding baking soda and polyethylene glycol, and homogenizing for 15-30 min at the homogenizing pressure of 200-300 kg/cm 2;

(4) and standing the membrane liquid for 30-60 min at room temperature after vacuum degassing, and sterilizing and packaging to obtain the comfortable and degerming mask liquid.

Preferably, the emulsifier of the present invention is glyceryl monostearate or starch.

According to the comfortable and degerming mask liquid and the preparation method thereof, the prepared mask liquid can be used for women and other sensitive people.

By adopting the technical scheme, the invention has the beneficial effects that:

1. the folium myrtilli extract and the sumac leaf extract in the raw materials are mainly functional components such as enol, polyphenol, plant essential oil and the like, and the components are easy to overcome skin barriers, have certain transdermal property and are convenient for skin absorption, so that the transdermal property of the sumac oil and polyethylene glycol is improved, and the moisturizing performance is more durable;

2. the fructus phyllanthi extract in the raw materials of the invention has the functions of oxidation resistance, free radical removal, tumor resistance, aging resistance and the like, has very wide biological functions, such as oxidation resistance, cancer resistance, cardiovascular disease resistance and the like, and also has antibacterial function due to the property of the fructus phyllanthi extract;

3. the baking soda in the mask liquid is alkaline, and releases carbon dioxide gas when reacting with the acidic phyllanthus emblica extract in the mask essence, so that the mask base cloth still keeps a fine and loose microporous structure after soaking the mask liquid, thereby being beneficial to the introduction of nutrient components in the mask essence and being more beneficial to the absorption of skin;

4. the invention extracts the composite essence components by using the plant source, and has no problems of safety, irritant raw materials and the like.

Detailed Description

The invention will now be further illustrated with reference to specific examples. The described embodiments are only some embodiments of the invention, not all embodiments. All other embodiments, which can be obtained by a person skilled in the art without any inventive step based on the embodiments of the present invention, are within the scope of the present invention.

Example 1

A comfortable and refreshing degerming mask liquid comprises, by weight, 2 parts of a fragrant leaf extract, 2 parts of a sumac leaf extract, 2 parts of sumac oil, 1 part of an emulsifier (glyceryl monostearate), 4 parts of a phyllanthus emblica extract, 1 part of baking soda and 1 part of polyethylene glycol;

(1) placing the fragrant leaf extract, the lacquer tree leaf extract and the fructus phyllanthi extract in a stirring kettle, and stirring at 50 deg.C for 30 min;

(2) stirring lacquer tree oil and emulsifier at 60 deg.C for 20min to obtain emulsified lacquer oil;

(3) pumping the mixture prepared in the step (1) and the emulsified paint oil and fat in the step (2) into a high-pressure homogenizer, adding 1.0 time of deionized water according to the mass ratio, adding baking soda and polyethylene glycol, and homogenizing for 30min at the homogenizing pressure of 200kg/cm 2;

(4) and standing the membrane liquid for 30min at room temperature after vacuum degassing, and sterilizing and packaging to obtain the comfortable and degerming mask liquid.

Example 2

A comfortable and refreshing degerming mask liquid comprises, by weight, 3 parts of a fragrant leaf extract, 3 parts of a sumac leaf extract, 3 parts of sumac oil, 2 parts of an emulsifier (starch), 8 parts of a phyllanthus emblica extract, 2 parts of baking soda and 2 parts of polyethylene glycol;

(1) placing the fragrant leaf extract, lacquer tree leaf extract and fructus Phyllanthi extract in a stirring kettle, and stirring at 60 deg.C for 15 min;

(2) firstly, uniformly stirring the emulsifier at the temperature of 70 ℃ for 10min, and then adding lacquer tree oil to obtain emulsified lacquer grease;

(3) pumping the mixture prepared in the step (1) and the emulsified paint oil and fat in the step (2) into a high-pressure homogenizer, adding 1.5 times of deionized water according to the mass ratio, adding baking soda and polyethylene glycol, and homogenizing for 15min at the homogenizing pressure of 300kg/cm 2;

(4) and standing the membrane liquid for 60min at room temperature after vacuum degassing, and sterilizing and packaging to obtain the comfortable and degerming mask liquid.

Example 3

A comfortable and refreshing degerming mask liquid comprises, by weight, 2.5 parts of a fragrant leaf extract, 2.5 parts of a sumac leaf extract, 2.5 parts of sumac oil, 1.5 parts of an emulsifier (glyceryl monostearate), 6 parts of a phyllanthus emblica extract, 1.5 parts of baking soda and 1.5 parts of polyethylene glycol.

(1) placing the fragrant leaf extract, lacquer tree leaf extract and fructus Phyllanthi extract in a stirring kettle, and stirring at 55 deg.C for 25 min;

(2) stirring lacquer tree oil and emulsifier at 65 deg.C for 15min to obtain emulsified lacquer oil;

(3) pumping the mixture prepared in the step (1) and the emulsified paint oil and fat in the step (2) into a high-pressure homogenizer, adding 1.2 times of deionized water according to the mass ratio, adding baking soda and polyethylene glycol, and homogenizing for 25min at the homogenizing pressure of 250kg/cm 2;

(4) and standing the membrane liquid for 40min at room temperature after vacuum degassing, and sterilizing and packaging to obtain the comfortable and degerming mask liquid.

Example 4

A comfortable and refreshing degerming mask liquid comprises, by weight, 2 parts of a fragrant leaf extract, 3 parts of a sumac leaf extract, 2 parts of sumac oil, 1 part of an emulsifier (glyceryl monostearate), 5 parts of a phyllanthus emblica extract, 1 part of baking soda and 2 parts of polyethylene glycol.

(1) placing the fragrant leaf extract, lacquer tree leaf extract and fructus Phyllanthi extract in a stirring kettle, and stirring at 50 deg.C for 15 min;

(2) stirring lacquer tree oil and emulsifier at 60 deg.C for 10min to obtain emulsified lacquer oil;

(3) pumping the mixture prepared in the step (1) and the emulsified paint oil and fat in the step (2) into a high-pressure homogenizer, adding 1.5 times of deionized water according to the mass ratio, adding baking soda and polyethylene glycol, and homogenizing for 20min at the homogenizing pressure of 200kg/cm 2;

(4) and standing the membrane liquid for 50min at room temperature after vacuum degassing, and sterilizing and packaging to obtain the comfortable and degerming mask liquid.

Claims

1. A comfortable and degerming mask liquid and a preparation method thereof are characterized by comprising a fragrant leaf extract, a sumac leaf extract, sumac oil, an emulsifier, a phyllanthus emblica extract, baking soda and polyethylene glycol.

2. The comfortable and degerming mask liquid and the preparation method thereof according to claim 1, wherein the mask liquid comprises, by weight, 2-3 parts of fragrant leaf extract, 2-3 parts of sumac oil, 1-2 parts of emulsifier, 4-8 parts of fructus phyllanthi extract, 1-2 parts of baking soda and 1-2 parts of polyethylene glycol.

3. The refreshing and sterilizing mask liquid and the preparation method thereof according to claim 1, wherein the fragrant tree leaf extract is prepared by concentrating and drying an extracting solution of fragrant tree leaves which are subjected to microwave extraction by using ethanol with the volume fraction of 60-70%.

4. The comfortable and degerming mask liquid and the preparation method thereof according to claim 1, wherein the preparation method of the lacquer tree leaf extract comprises the following steps: (1) picking tender buds or leaves of the lacquer tree, cleaning the tender buds or leaves with clear water, drying the tender buds or leaves until the water content is 1-5%, and crushing the tender buds or leaves to 20-60 meshes; (2) according to the g-g solid-liquid ratio of 1: adding water and/or ethanol into the raw materials in the step (1) in a ratio of 20-100, uniformly mixing, treating for 1-48 h at 25-100 ℃, under a pressure of 0-0.3 MPa and at a stirring speed of 50-100 r/min for 1-2 times, and mixing for later use; (3) according to the mass ratio of the grease to the emulsifier of 1: 0.2-1, mixing the oil and the emulsifier, emulsifying for 0.5-2 hours at the temperature of 40-80 ℃ and at the stirring speed of 50-100 r/min, and uniformly and completely emulsifying for later use, wherein the mass ratio of the oil to the sumac leaves is 1-2: 1; (4) adding the extracting solution in the step (2) and lacquer tree leaves or buds into the emulsified oil in the step (3), stirring for 0.5-2 h, standing for 2-8 h, and then carrying out phase splitting; (5) and (4) separating the lower aqueous phase part of the layered liquid in the step (4) by using a separating funnel, and filtering to obtain the sumac leaf extract.

5. The method for preparing the sumac leaf extract according to claim 4, wherein the oil and fat in the step (3) is shea butter, pecan butter or prinsepia utilis royle oil.

6. The method for preparing the Rhus verniciflua Stokes leaf extract as claimed in claim 4, wherein said emulsifier in step (3) is one or mixture of lecithin, monoglyceride and sucrose fatty acid ester.

7. The comfortable and degerming mask liquid and the preparation method thereof as claimed in claim 1, wherein the sumac oil is lacquer seed kernel oil.

8. The comfortable and degerming mask liquid and the preparation method thereof according to claim 1, wherein the preparation of the fructus phyllanthi extract comprises the following steps: (1) sterilizing fructus Phyllanthi, and removing core; (2) freeze-drying the phyllanthus emblica fruits treated in the step (1) at the temperature of-10 to-30 ℃ and the vacuum degree of 30 to 100pa to obtain dried phyllanthus emblica fruits with the water content of 8 to 10 wt%; (3) crushing the dried fructus phyllanthi product at-10 to-30 ℃ and sieving the crushed fructus phyllanthi product by 20 meshes; (4) and (3) mixing the crushed Yunnan olive in a solid-liquid ratio of 1: boiling and extracting for 1-2 h for 20-40 hours, and filtering to obtain filtrate; (5) and (3) concentrating the filtrate obtained in the step (4) at the temperature of 60-70 ℃ to enable the fruit juice to be concentrated to the mass percentage concentration of 25-35%, and then obtaining the phyllanthus emblica extract.

9. The comfortable and degerming mask solution and the preparation method thereof according to claim 1, wherein the preparation method of the comfortable and degerming mask solution comprises the following steps:

(3) integrally pumping the mixture prepared in the step (1) and the emulsified paint grease in the step (2) into a high-pressure homogenizer, adding 1.0-1.5 times of deionized water according to the mass ratio, adding baking soda and polyethylene glycol, homogenizing for 15-30 min, wherein the homogenizing pressure is 200-300 kg/cm 2;